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Correlating Aggregate Properties and Concrete Rheology

to Dynamic Segregation of Self-Consolidating Concrete


Lin Shen 1; Hamed Bahrami Jovein 2; and Qian Wang 3

Abstract: Segregation is a common problem in self-consolidating concrete (SCC), which is sensitive to mix proportions such as super-
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plasticizer dosage, as well as the size, volume, and gradation of the aggregate. Dynamic segregation, when coarse aggregate lags behind
during the flowing process, is distinguishable from static segregation, when coarse aggregate settles in concrete at rest. In the research
reported in this paper, a flow trough and a concrete rheometer were used to study the effects of various aggregate properties and concrete
rheology on dynamic segregation of SCC. An equation for the drag force was found useful to understand how various mix proportions and
concrete rheology affecting dynamic segregation. Higher paste volume, lower superplasticizer percent by weight of cement, lower slump
flow, smaller coarse aggregate, and better gradation may increase dynamic stability. Smaller aggregate size has more significant effect than
other aggregate properties. Mixtures with dynamic yield stress less than 50 Pa exhibited severe segregation from both flow trough and visual
stability index (VSI) tests. Mixtures with static yield stress of 250 Pa or higher had satisfactory dynamic stability, while mixtures with static
yield stress of 100 Pa or lower showed severe dynamic segregation. No clear correlation was observed between concrete plastic viscosity and
dynamic segregation. DOI: 10.1061/(ASCE)MT.1943-5533.0001325. © 2015 American Society of Civil Engineers.
Author keywords: Segregation; Dynamic segregation; Stability; Self-consolidating concrete (SCC); Flow trough; Rheology.

Introduction as silica fume, fly ash, or limestone filler (Khayat 1999; Daczko
2002; Khatib 2008). A viscosity-modifying admixture (VMA)
Segregation refers to movement of the coarse aggregate relative to may also be utilized to reduce segregation by enhancing the mix-
the mortar and segregation resistance is a critical functional require- ture’s capacity to retain free water and increasing the viscosity of
ment for self-consolidating concrete (SCC; Khayat 1999). Exces- the suspended liquid phase (Khayat et al. 2004; Lachemi et al.
sive segregation may cause lower flowability, aggregate blocking, 2004; Leeman and Winnefeld 2007). Decreasing slump flow (in-
higher drying shrinkage, and nonuniform compressive strength. creasing concrete yield stress), water:cement (W:C) ratio, paste
Two distinguishable types of segregation may exist in a mixture, as volume, aggregate size, increasing plastic viscosity, as well as using
follows: (1) static segregation, and (2) dynamic segregation. Static well-graded coarse aggregate may reduce dynamic segregation
segregation is the separation of mortar and coarse aggregate when (Esmaeikhanian et al. 2014). Regardless of these strategies, segre-
the concrete is at rest, typically in a vertical direction after place- gation problems are still commonly observed in SCC mixtures.
ment. And dynamic segregation occurs when coarse aggregate lags And there is still a lack of understanding of the mechanism of how
behind mortar while the concrete is flowing, generally in a near various aggregate properties and the rheology of cement paste and
horizontal direction while being cast into the formwork. concrete affecting dynamic segregation.
Compared with ordinary concrete, the composition and rheo- The main objective of the research reported in this paper is
logical properties of SCC should be closely controlled in order to to study the effects of aggregate properties and concrete rheology
satisfy the requirements of flowability, passing ability, and segre- on dynamic segregation of SCC mixtures based on experimental
gation resistance simultaneously. Small fluctuations of the plastic tests and rheological models. The test methods to assess dynamic
viscosity and yield stress of paste (as a result of changes in w=cm segregation included the VSI [ASTM C1611 (ASTM 2007)] and
and other properties of cement such as fineness), and the size, flow trough test (Shen et al. 2008).
volume, gradation, as well as moisture content of the fine and
coarse aggregates could adversely affect workability, composition,
and durability (Bonen and Shah 2005). Experimental Program
Researches have shown that segregation can be controlled by
limiting free-water content and incorporating fine powders such
Details of Materials
1
Assistant Professor, Dept. of Civil and Environmental Engineering, Type I portland cement complying with ASTM C150/C150M-12
Univ. of Hawaii, Manoa, HI 96822 (corresponding author). E-mail: (ASTM 2012b) and Type C fly ash complying with ASTM
linshen@hawaii.edu C618-12a (ASTM 2012a) were used. Coarse Aggregate (CA) 1,
2
Graduate Student, Dept. of Civil and Environmental Engineering, i.e., CA1, is crushed basalt rock, has maximum size of 19 mm,
Univ. of Hawaii, Manoa, HI 96822. E-mail: hamedbj@hawaii.edu and Coarse Aggregate CA2 is crushed basalt rock, has maximum
3
Assistant Professor, Dept. of Civil and Environmental Engineering,
size of 9.5 mm. The properties and the gradation curve of coarse and
Manhattan College, Riverdale, NY 10471.
Note. This manuscript was submitted on August 9, 2014; approved on fine aggregate (FA) are shown in Table 1 and Fig. 1, respectively.
March 6, 2015; published online on May 18, 2015. Discussion period open A polycarboxylate-based superplasticizer (SP) was used. It was
until October 18, 2015; separate discussions must be submitted for indivi- a solution with a specific gravity of 1.06 and a solid content of
dual papers. This paper is part of the Journal of Materials in Civil Engi- 35%. The VMA (methylhydroxyethylcellulose) used had a specific
neering, © ASCE, ISSN 0899-1561/04015067(9)/$25.00. gravity of 1.00 and a solid content of 35%.

© ASCE 04015067-1 J. Mater. Civ. Eng.

J. Mater. Civ. Eng.


Table 1. Aggregate Properties
Aggregate Bulk density Bulk specific gravity, Fineness modulus, Absorption Packing density
name [kg=m3 (lb=ft3 )] dimensionless dimensionless capacity (%) dimensionless
CA1 1,473 (93.07) 2.74 3.97 2.66 0.54
CA2 1,491 (90.53) 2.7 2.95 3.61 0.54
FA1 1,460 (91.13) 2.71 1.55 2.3 0.54
FA2 1,675 (104.67) 2.64 3.5 5.16 0.63

100 • Mixer was restarted, and SP and/or VMA were slowly poured
CA2
90 and mixed for 2 min before the slump flow, flow trough, and
CA1
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Cumulative Passing (%)

80 rheology tests.
FA1
70 The fresh concrete performance data right after mixing is not
FA2
60 inevitably representative for the concrete performance after a while
50 and over the course of time
40
30
20
Dynamic Segregation Test
10 To study dynamic segregation of SCC, it is important to be able to
0 quantify dynamic segregation accurately and effectively. For static
0.01 0.1 1 10
segregation, commonly used methods include column segrega-
Sieve Size (mm)
tion [ASTM C1610/C1610M-10 (ASTM 2010)], penetration test
Fig. 1. Gradation curves of coarse and fine aggregates [ASTM C1712-09 (ASTM 2009)], V-funnel test (JSCE 1999),
electrical conductivity (Jolicoeur et al. 2000), sieve segregation re-
sistance test (EFNARC 2005), hardened visual stability index [VSI;
AASHTO PP58-08 (AASHTO 2008)], image analysis of hardened
Mix Proportions cylinder (Shen et al. 2005), and segregation probe (Shen et al. 2007;
Shen and Bahrami 2013), among others. The V-funnel, L-box,
As shown in Table 2, a total of 29 mixtures were tested to study the
U-box, and J-ring tests (Khayat et al. 2004; Assaad et al. 2004)
effects of aggregate volume, size, gradation, and packing density,
do not predict segregation directly, but are related to both static
mineral and chemical admixtures, and concrete viscosity and yield and dynamic segregation by considering the rheological properties
stress on dynamic segregation. measured by these tests (Tregger et al. 2012). The only specific
Four basic types of mixtures were designed, as follows: standarderized method directly measuring dynamic segregation is
(1) graded aggregate (GA), (2) mineral admixture (MA), (3) VMA, the visual stability index determined by observation of the periph-
and (4) well-balanced (WB). Graded aggregate mixtures had three ery of concrete during the slump flow test [ASTM C1611 (ASTM
types of aggregate, relatively high packing density, and a FA:CA 2007)]. A VSI value from 0 and 1 (stable) to 2 and 3 (unstable) can
ratio of 1. Mineral admixture mixtures used fly ash to increase paste be given based on criteria in ASTM C1611 (ASTM 2007). Since
volume, had two types of aggregates, and a FA:CA ratio of 1. The the VSI value was based on observation of a very small flow length,
VMA mixtures used VMA to improve the viscosity, had two types it was found to only provide a rough estimation of dynamic seg-
of aggregate, and a FA:CA ratio of 0.87. Well-balanced mixtures regation and some researchers question whether it identifies static
combined the benefits of VMA and graded aggregate mixtures. or dynamic segregation (Tregger et al. 2010). Other methods such
Within each basic mixture type, the volume, gradation, packing as the V-funnel (JSCE 1999), LCPC method (Roussel 2007), and
density, maximum size of aggregate, as well as slump flow may sieve segregation resistance test (EFNARC 2005) can also give use-
also be modified to explore the effects of these properties on dy- ful information on predicting dynamic segregation, although these
namic segregation. Labels þ5% P, −5% P, LS, HP, and SA indicate tests do not provide direct measurements of dynamic segregation.
that compared with the basic mixture, a modified mixture has 5% A reliable dynamic segregation test is urgently needed in order to
more paste volume, 5% less paste volume, lower slump flow, higher better quantify dynamic segregation and understand the mecha-
aggregate packing density, and smaller coarse aggregate size, re- nisms responsible.
spectively. For example, GA þ5% P mixture has 5% higher paste A satisfactory laboratory test for dynamic segregation should
volume than the basic GA mixture, and VMA-HP mixture has meet the following requirements: (1) flowing distance should be
higher aggregate packing density than the basic VMA mixture. long enough to give useful information about dynamic segregation
in typical field conditions, (2) test should be sensitive enough to
detect meaningful differences in dynamic segregation, (3) apparatus
Mixing Procedure
should be portable and the amount of sample concrete should be
Each batch of concrete has a volume of about 43 L (1.5 ft3 ) and was small enough for both laboratory and field applications, and (4) test
prepared in a drum mixer with a capacity of 58 L (2 ft3 ). The fol- results must be sufficiently precise and accurate that results can be
lowing procedure was used: used with confidence.
• Sand, coarse aggregate, and one-third of water were put in a To meet these requirements, the flow trough shown in Fig. 2 was
drum mixer and mixed for 30 s; developed (Shen et al. 2008). It was made by assembling 25-mm
• Cement and mineral admixture, if any, were put in the mixer and (1-in.) thick wood boards to form a 0.15 × 0.15 × 1.80 m (6 in: ×
mixed for 3 min and remaining water was slowly added during 6 in: × 6 ft:) trough. The 0.23-m (9-in.) height difference between
the first minute of mixing process; two ends gives a 7° angle of inclination, which was found to be
• Mixer was stopped for 3 min; and the smallest slope that allowed the SCC to flow to the lower

© ASCE 04015067-2 J. Mater. Civ. Eng.

J. Mater. Civ. Eng.


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Table 2. Proportions of SCC Mixtures


Material (kg=m3 ) Aggregate propertiesa Admixture (mL=m3 )

© ASCE
Mix Cement, Fly ash, Aggregate CA1 Viscosity-modifying
Mix Mix type identifier Water:cement Type 1 Class C CA1 CA2 FA1 FA2 Water (%) FA:CA (%) ϕm Superplasticizer admixture
1 Graded aggregate GA 0.35 450 107 198 579 756 0 195 59 1.00 0.13 0.67 9,707 0
2 GA-LS 0.35 450 107 198 579 756 195 59 1.00 0.13 0.67 3,269 0
3 GA-HS 0.35 450 107 198 579 756 195 59 1.00 0.13 0.67 10,576 0
4 GA þ 5% P 0.35 506 120 181 530 692 219 54 1.00 0.13 0.67 7,908 0
5 GA − 5% P 0.35 394 94 214 629 821 171 64 1.00 0.13 0.67 11,696 0
6 GA-A 0.38 405 96 193 989 557 190 64 0.47 0.11 0.70 8,974 0
7 GA-A 0.38 486 93 178 688 739 219 59 0.85 0.11 0.68 3,481 0
8 GA-A 0.46 372 88 208 650 844 213 63 1.00 0.12 0.73 5,175 0
9 Mineral admixture MA 0.31 442 239 693 0 678 211 53 1.01 0.50 0.65 9,299 0
10 MA-LS 0.31 442 239 693 678 211 53 1.01 0.50 0.65 5,000 0
11 MA-HS 0.31 442 239 693 678 211 53 1.01 0.50 0.65 10,692 0
12 MA þ 5% P 0.31 487 263 627 621 233 48 1.01 0.50 0.65 8,804 0
13 MA − 5% P 0.31 398 215 749 743 190 58 1.01 0.50 0.65 10,501 0
14 MA-A 0.39 393 212 168 647 683 234 56 0.85 0.11 0.71 9,018 0
15 MA-A 0.39 393 212 168 647 683 234 56 0.85 0.11 0.71 5,881 1,567
16 MA-A 0.39 358 194 196 612 794 213 60 1.00 0.12 0.73 7,906 0
17 Viscosity-modifying VMA 0.41 515 0 854 0 729 209 62 0.87 0.53 0.66 3,051 1,371
18 admixture VMA-LS1 0.41 515 854 729 209 62 0.87 0.53 0.66 2,370 1,371
19 VMA-LS2 0.41 515 854 729 209 62 0.87 0.53 0.66 2,716 1,371
20 VMA-HS 0.41 515 854 729 209 62 0.87 0.53 0.66 4,807 1,371
21 VMA þ 5% P 0.41 582 783 670 236 57 0.87 0.53 0.66 2,823 809
22 VMA − 5% P 0.41 447 923 789 181 67 0.87 0.53 0.66 3,497 881
23 HP 0.41 585 468 593 585 238 59 0.56 0.28 0.71 8,044 1,360

04015067-3
24 VMA-A 0.51 467 469 593 586 238 61 0.56 0.28 0.71 4,651 1,683

J. Mater. Civ. Eng.


25 VMA-A 0.51 457 186 718 759 234 62 0.85 0.11 0.71 5,813 4,809
26 Well-balanced WB-SA 0.42 474 0 712 188 748 199 63 1.34 0.00 0.66 4,090 1,424
27 WB1 0.42 502 533 115 222 743 211 61 1.53 0.33 0.74 3,383 1,131
28 WB2 0.42 502 509 136 445 522 211 61 1.53 0.31 0.71 5,007 1,131
29 WB3 0.36 502 534 142 467 547 181 64 1.53 0.31 0.71 6,495 646
a
CA = course aggregate; and FC = fine aggregate.

J. Mater. Civ. Eng.


Fig. 2. Flow trough for dynamic segregation; trough dimensions are
0.15 × 0.15 × 1.80 m (6 in: × 6 in: × 6 ft; image by Hamed Bahrami
Jovein)
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end. The surface of the trough was painted to make it water-


resistant and easy to wash.
The test was performed based on the following procedure:
• Before the test, the surface of trough was slightly wetted with
water and superficial water was wiped off;
• Fresh concrete was measured using a single lift into one
100 × 200 mm (4 × 8 in:) cylinder mold, one 150 × 300 mm
Fig. 3. Vane-type concrete rheometer (image by Hamed Bahrami
(6 × 12 in:) cylinder mold, and a water-tight container having
Jovein)
a volume of around 13.5 L (∼3.5 gal.);
• The concrete in the 150 × 300 m mold was poured onto the
trough from the higher end as a priming step;
• After the concrete stopped flowing, the trough was straightened
up vertically for 30 s to let the priming concrete flow off and
leave a mortar layer on the trough surface;
• The trough was then put back into initial inclined position and
the concrete in 13.5-L container was poured gradually and con-
tinuously on the trough from the higher end;
• An empty 100 × 200 mm (4 × 8 in:) mold was filled with the
leading portion of concrete flowing through the trough;
• Coarse aggregates were collected from the concrete samples
in the two 100 × 200 mm molds, one collected at the beginning
of the flow test and the other collected at the end of the test, Fig. 4. Rheological protocol to determine yield stress and viscosity of
by washing the concrete samples over a 4.8-mm (0.19-in.) concrete for the vane-type rheometer
No. 4 sieve;
• Each coarse aggregate sample was weighed; and
• The dynamic segregation index (DSI) was then calculated as perpendicular directions. A visual stability index ranges from 0
(stable) and 1 (stable), to 2 (unstable) and 3 (unstable) was assigned
DSI ¼ ðwCA1 − wCA2 Þ=wCA1 ð1Þ
to the mixture by observation of the separation of mortar and coarse
where wCA1 = weight of coarse aggregate in the first mold, col- aggregate of the slump flow patty.
lected at the beginning of the test; and wCA2 = weight of coarse
aggregate in the second mold, collected at the end of the test. Concrete Rheology Test
The purposes of the priming step are to eliminate variations in
surface friction when different materials are used to construct the Rheological properties were measured using a portable rheometer
flow trough, and to better simulate the actual situation in the field, with vane geometry (Fig. 3). After the mixture was prepared in
where SCC typically flows over previously poured concrete. accordance with the steps in the section of mixing procedure
The flow trough can be used in the laboratory or in the field and transferred into the rheometer, a stress growth test was per-
and dynamic segregation measured using this test was shown to formed immediately to determine the static (at-rest) yield stress.
correlate well with dynamic segregation observed in the field (Shen A stress growth test involves rotating the vane at a low, constant
et al. 2008). speed of 0.025 revolutions=s while monitoring the buildup in
torque and the maximum measured torque used to calculate yield
stress. Then a flow curve test was performed immediately. The test
Slump Flow Test
protocol consisted of a 20-s preshear period at a constant speed of
The slump flow test followed the procedure in ASTM C1611 0.50 revolutions=s and then seven flow curve points in descending
(ASTM 2007) and was performed on a flat, smooth, and level steel order from 0.50 to 0.05 revolutions=s (Fig. 4). The purpose of the
plate with a size of 1 × 1 m. After raw materials were thoroughly preshear period is to minimize the effects of thixotropy and to pro-
mixed in a drum mixer according to steps listed in the Mixing vide a consistent shear history. The dynamic yield stress and plastic
Procedure section, fresh concrete was transferred to a bucket viscosity were calculated from the flow curve. The calculation of
and filled into an inversed slump cone with one lift without tamp- the Bingham model parameters of yield stress and plastic viscosity
ing. The top surface of the concrete was then trowelled flat and the is based on the Reiner–Riwlin equation. Different concrete rheom-
slump cone was lifted carefully and vertically to allow the concrete eters apply different geometries; therefore, significant difference
to flow under its own weight. The slump flow was measured after could exist between rheological parameters obtained from different
concrete stopped as the average diameter of the concrete pie in two rheometers.

© ASCE 04015067-4 J. Mater. Civ. Eng.

J. Mater. Civ. Eng.


Table 3. Experimental Results of SCC mixtures
Visual Dynamic Plastic
Mix Slump stability segregation Static yield Dynamic yield viscosity
Mix Mix type identifier Water:cement mm index index (%) stress (Pa) stress (Pa) (Pa · s)
1 Graded aggregate GA 0.35 710 1 5 164.1 113.9 6.1
2 GA-LS 0.35 610 0 15 —
3 GA-HS 0.35 762 2 22 5.8 0.1 21.9
4 GA þ 5% P 0.35 710 1 11 134.7 125.0 1.2
5 GA − 5% P 0.35 710 1 14 304.0 234.0 5.5
6 GA-A 0.38 660 3 10 —
7 GA-A 0.38 686 1 8
8 GA-A 0.46 710 0 7
9 Mineral admixture MA 0.31 710 0 3 188.8 64.8 14.6
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10 MF-LS 0.31 635 0 3 —


11 MA-HS 0.31 762 3 10
12 MA þ 5% P 0.31 710 0 4 230.9 135.9 13.8
13 MA − 5% P 0.31 710 2 21 173.2 8.6 31.2
14 MA-A 0.39 737 3 21 —
15 MA-A 0.39 737 1 7
16 MA-A 0.39 710 2 26 204.0 40.7 12.3
17 Viscosity-modifying VMA 0.41 710 1 15 433.3 107.4 26.7
18 admixture VMA-LS1 0.41 585 0 — —
19 VMA-LS2 0.41 635 0 6
20 VMA-HS 0.41 762 1 12 313.5 129.2 10.4
21 VMA þ 5% P 0.41 710 1 13 219.0 116.3 2.0
22 VMA − 5% P 0.41 660 1 2 338.0 31.8 43.7
23 HP 0.41 660 1 12 185.0 95.5 5.9
24 VMA-A 0.51 686 1 10 145.0 76.1 2.3
25 VMA-A 0.51 686 1 16 159.0 104.0 3.1
26 Well-balanced WB-SA 0.42 660 0 6 380.4 305.6 7.0
27 WB1 0.42 660 2 31 82.7 26.7 8.4
28 WB2 0.42 660 1 23 197.9 30.0 32.5
29 WB3 0.36 660 2 22 184.0 43.0 32.9

Results and Discussions and MA − 5% P mixture had 5% less paste volume compared with
the MA mixture. Other mix proportions were virtually identical
The experimental results of the 29 SCC mixtures are summarized within the same series of mixtures. The slump flow was controlled
in Table 3. The effects of aggregate volume, size, gradation, slump at 710 mm for all six mixtures (by varying SP dosage).
flow, SP dosage, and concrete viscosity and yield stress on dynamic The DSI for GA, GA þ 5% P, and GA − 5% P mixture were
segregation will be discussed in detail as described next. 5, 11, and 14%, respectively. And the DSI for MA, MA þ 5% P,
and MA − 5% P mixture were 3, 4, and 21%, respectively. It seems
that reducing paste volume may increase dynamic segregation, as
Effects of Aggregate Volume on Dynamic Segregation the highest DSI occurred in the mixture with the least paste volume
Fig. 5 shows the DSI of the GA series mixtures and the MA series for each series (GA − 5% P and MA − 5% P mixture).
mixtures. Compared with the GA mixture, GA þ 5% P mixture had One factor that may help to explain the higher dynamic segre-
5% more paste volume, and GA − 5% P mixture had 5% less paste gation for mixtures with less paste volume is paste rheology con-
volume. Similarly, MA þ 5% P mixture had 5% more paste volume trolled by the dosage of SP. The SP dosages (solid percent by
weight of cementitious materials) of GA type of mixturewere
0.58% (GA þ 5% P), 0.80% (GA), and 1.10% (GA − 5% P). And
25 the SP dosages of MA type of mixtures were 0.67% (MA þ 5% P),
0.78% (MA), and 0.98% (MA − 5% P). For each type of mixtures,
Dynamic Stability Index (%)

20
21 the mixture with highest SP dosage coincided with highest dynamic
segregation.
15 To further understand how SP dosage affecting dynamic segre-
14 gation, it may be helpful to examine the drag force acting on the
11 GA aggregate by the paste during the flowing process of a SCC mixture
10
MA (Shen et al. 2009). The drag force acting by the paste on the ag-
gregate, FA , can be expressed as
5 5
3
4     
ϕ ϕ ϕ 21 ϕ1 ϕ2 ϕ3
FA ¼ abc 9ηpl ΔV 21 þ 22 þ 23 þ π2 τ 0 þ þ
0 r1 r2 r3 4 r1 r2 r3
(-)5% 0 (+)5%
ð2Þ
Paste Content (%)
where a, b, and c = dimensions (height, width, and length) of the
Fig. 5. Effects of aggregate volume on dynamic segregation
concrete sample; ϕ1 , ϕ2 , and ϕ3 = volume fractions of different

© ASCE 04015067-5 J. Mater. Civ. Eng.

J. Mater. Civ. Eng.


types of aggregates; ηpl = paste plastic viscosity; r1 , r2 , and r3 = The reason why lower slump flow coincided to better resistance
radii of the aggregates; ΔV = velocity difference between aggregate to dynamic segregation may also be justified by higher paste yield
and paste, calculated from the initial conditions and forces; and stress and viscosity. The SP dosages of the GA type of mix-
τ 0 = paste yield stress. tures were 0.27% (610-mm slump flow, 15% DSI) and 0.87%
According to Eq. (2), higher paste plastic viscosity and yield (762-mm slump flow, 22% DSI). The SP dosages of the MA type
stress correspond to higher drag force by the paste to carry the of mixtures were 0.42% (635-mm slump flow, 3% DSI) and 0.90%
aggregate forward, and thus reduce the chance and extent of (762-mm slump flow, 10% DSI). And the SP dosages of the VMA
dynamic segregation. Because the slump flow was kept constant type of mixtures were 0.20% (635-mm slump flow, 6% DSI) and
for the mixtures under comparison, mixtures with higher paste 0.35% (762-mm slump flow, 12% DSI). Again, according to
content (lower aggregate volume) had less interparticle friction and Eq. (2), less SP percent means higher paste yield stress, higher drag
required less SP to achieve the same slump flow. Less SP percent force to carry the coarse aggregate forward, and thus less dynamic
by weight of cementitious materials increases paste yield stress segregation.
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and viscosity, raises the drag force, and thus reduces dynamic
segregation.
From Eq. (2), it seems that a mixture with higher aggregate Effects of Aggregate Size and Gradation on Dynamic
volume (ϕ1 , ϕ2 , and ϕ3 ) should have higher drag force and thus Segregation
less dynamic segregation. However, higher aggregate volume also Fig. 7 illustrates how dynamic segregation was influenced by ag-
corresponds to higher aggregate mass and the acceleration due
gregate size and gradation. The WB-SA mixture had only medium-
to drag force, FA =mass, will not change significantly because of
size (9.5 mm) coarse aggregate and packing density of 0.66, while
higher aggregate volume and mass.
the WB1 and WB2 mixtures had both large-size (19 mm) and
As discussed in a subsequent section, this relationship between
medium-size (9.5 mm) coarse aggregate and higher packing density
SP dosage and dynamic segregation is not obvious when different
(0.74 for WB1 and 0.71 for WB2). Compared with the WB1 mix-
series of mixtures with various average aggregate size and grada-
ture, WB2 mixture has smaller average aggregate size (less 19-mm
tion are compared, which could also be expected from Eq. (2).
All the observations discussed previously were performed right coarse). There is no other major difference in mix proportions
after the mixing procedure was stopped. The effects of factors such between these mixtures. The DSI of WB-SA, WB1, and WB2 mix-
as hydration, admixture adsorption, and thixotropy on dynamic tures were 6, 31, and 23%, respectively. It seems that reducing the
segregation will be studied in future tests. aggregate size had a more significant effect on improving dynamic
segregation resistance compared with better gradation and higher
aggregate packing density.
Effects of Slump Flow on Dynamic Segregation The improved dynamic segregation resistance with smaller
Fig. 6 shows how the slump flow is related to dynamic segregation aggregate can still be explained by Eq. (2). The reduction in DSI
of the GA, MA, and VMA series of mixtures. Within the same is mainly attributed to increased drag force provided by cement
series of mixtures, the slump flow was varied by changing dosage paste on smaller aggregates (smaller radii r1 , r2 , and r3 ), which
of superplasticizer while other mix proportions were virtually have higher surface area/mass ratios. Another possible factor is
identical. static segregation; concrete with larger aggregates is more likely to
For the GA series, the DSI of mixtures with slump flow of experience static segregation, and when more aggregates settle to
610, 710, and 762 mm were 15, 5, and 22%, respectively. For the the bottom and the frictional force provided to the aggregate by the
MA series, the DSI of mixtures with slump flow of 635, 710, and underlying surface increases, dynamic segregation increases (Shen
762 mm were 3, 3, and 10%, respectively. And for the VMA series, et al. 2009).
the DSI of mixtures with slump flow of 635, 710, and 762 mm were One may also analyze dynamic stability using other analytical
6, 15, and 12%, respectively. For each series, the mixture with low- methods such as the LCPC box test. For example, the LCPC box
est slump (610 or 635 mm) always showed less dynamic segrega- test (Roussel 2007) can use spread length and shape to calculate
tion than the mixture with highest slump (762 mm), which indicates concrete yield stress, which in turn affects dynamic segregation.
reducing slump flow could reduce dynamic segregation. The trend
of higher DSI with higher slump flow was also observed when
superplasticizer was added in a single mixture and slump flow and 35
DSI were monitored (Shen et al. 2015).
30
25
Dynamic Stability Index (%)

25
Dynamic Stability Index (%)

20
20

15
GA 15

10 MA
VMA 10

5
5

0
600 620 640 660 680 700 720 740 760 780 0
Slump Flow (mm) WB-SA WB1 WB2

Fig. 6. Effects of slump flow on dynamic segregation Fig. 7. Effects of aggregate size and gradation on dynamic segregation

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J. Mater. Civ. Eng.


350

300

Dynamic Yield Stress (Pa)


250

200

150

100

50

0
0 0.5 1 1.5 2 2.5
Visual Stability Index
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Fig. 10. Effect of concrete dynamic yield stress on visual stability


index
Fig. 8. Effects of superplasticizer percent by weight of cement on
dynamic segregation; all mixture had water:cement of around 0.41

500
450

Static Yield Stress (Pa)


350 400
350
300
Dynamic Yield Stress (Pa)

300
250
250
200
200 150
100
150
50
100 0
0 5 10 15 20 25 30 35
50
Dynamic Stability Index (%)
0
0 5 10 15 20 25 30 35 Fig. 11. Effect of concrete static yield stress on dynamic segregation
Dynamic Stability Index (%) index
Fig. 9. Effect of concrete dynamic yield stress on dynamic segregation
index
500
450
Static Yield Stress (Pa)

400
Effects of SP Dosage on Dynamic Segregation 350
300
Previous sections indicate that higher SP dosage increases dynamic 250
segregation within the same type of mixture (GA, MA, VMA, and 200
so on). The reason is because less SP dosage means higher paste 150
yield stress, and thus higher drag force is available for the paste to 100
50
carry the coarse aggregate forward, which in turn results in less
0
dynamic segregation. 0 0.5 1 1.5 2 2.5
Fig. 8 shows how dynamic segregation index was influenced by Visual Stability Index
SP percent by weight of cement when different series of mixtures
were compared together. The W:C ratio was controlled at around Fig. 12. Effect of concrete static yield stress on visual stability index
0.41 for all mixtures. No clear correlation between SP dosage and
dynamic segregation was observed when mixtures with various
aggregate properties are compared. Based on Eq. (2), the drag force (six of seven, or 86%) were higher than 20%, indicating severe
is a function of not only yield stress and viscosity of paste, but also dynamic segregation.
aggregate size, volume, and gradation. Furthermore, rheological Fig. 10 illustrates how VSI was influenced by dynamic yield
properties of paste also depend upon early hydration phases and stress. For mixtures with VSI of 0 and 1, there is a wide range of
anions, which varies between difference series of mixtures. The ef- dynamic yield stress values and no clear correlation was found. For
fect of paste rheology (via SP dosage) became less obvious when mixtures with VSI of 2, all dynamic yield stress values (five of five,
more variables were introduced. The paste rheology is going to be or 100%) are less than 50 Pa.
measured in future test to further validate the theory. Fig. 11 plots the relationship between concrete static yield stress
and DSI. All mixtures (five of five, or 100%) with static yield stress
of 250 Pa or higher had DSI values of 15% or less, while all mix-
Effects of Concrete Rheology on Dynamic Segregation
tures (two of two, or 100%) with static yield stress of 100 Pa or
Fig. 9 shows how DSI was affected by dynamic yield stress of lower had DSI value of 20% or higher. For mixtures with static yield
mixtures. When the dynamic yield stress was higher than 50 Pa, stress between 100 and 250 Pa, the DSI values are highly variable.
most DSI values (11 of 12, or 92%) were less than 15%, whereas Fig. 12 shows the correlation between static yield stress and
when the dynamic yield stress was less than 50 Pa, most DSI values VSI. All mixtures (five of five, or 100%) with static yield stress

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J. Mater. Civ. Eng.


50
45 aggregate size seem to have more significant effect compared
Plastic Viscosity (Pa.s)
40 with better gradation.
35 • No clear reverse relationship between SP percent by weight of
30
cement and dynamic segregation was observed when mixtures
25
20
with various aggregate properties are compared. This is because
15 the drag force is a function of not only yield stress and viscosity
10 of paste, but also aggregate size and volume. The effect of paste
5 rheology (via SP dosage) became less obvious when more vari-
0
0 5 10 15 20 25 30 35 ables were introduced.
Dynamic Stability Index (%) • Most mixtures with dynamic yield stress higher than 50 Pa had
DSI less than 15%, and mixtures with the dynamic yield stress
Fig. 13. Results of concrete plastic viscosity and flow trough test less than 50 Pa typically had DSI higher than 20%.

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Most mixtures with VSI of 2 or higher had dynamic yield stress


less than 50 Pa, while mixtures with VSI of 0 and 1 exhibited a
wide range of dynamic yield stress values.
50 • Most mixtures with static yield stress of 250 Pa or higher had
45
DSI values of 15% or less and VSI of 0 or 1 (stable), and most
Plastic Viscosity (Pa.s)

40
mixtures with static yield stress of 100 Pa or lower had DSI
35
30
value of 20% or higher and VSI of 2 (unstable) or 3 (unstable).
25 For mixtures with static yield stress between 100 and 250 Pa, the
20 DSI and VSI values are highly variable.
15 • No direct relationship was observed between concrete plastic
10 viscosity and dynamic segregation (DSI and VSI).
5 • The paste rheology of the mixtures will be measured and the
0
0 0.5 1 1.5 2 2.5 effects of hydration, time-dependent adsorption of admixtures
Visual Stability Index (%) (Flatt et al. 1998; Plank and Hirsch 2007), and thixotropy on
dynamic segregation will be studied in future tests of dynamic
Fig. 14. Results of concrete plastic viscosity and visual stability index segregation.

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J. Mater. Civ. Eng.

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