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Consulted Distribution List

Date Name / Unit Company / Unit


July 2015 S.Monaco / PIEN eni/ITEM
July 2015 A.Marceglia / MECC eni/ITEM
July 2015 A.Di Lullo / TEFA eni/ITEM
July 2015 I.Hashi / COETA eni/ITEM
July 2015 A.Ghielmetti / PIPT eni/ITEM
July 2015 D.Welch / eee&p eni/eee&p

Informed Distribution List

Date Name / Unit Company / Unit


July 2015 M.Barbieri / ENTA eni/ITEM
July 2015 M.Caramuta / CIMS eni/CONSTR

REVISION TRACKING

Rev. 01: the revision includes 61 pages.


The document has been reviewed in the contents related to manufacture and supply of the
Clad and Lined Line Pipes.
Date: January 2015

Rev. 02: the revision includes 65 pages.


The document has been reviewed on the base of comments on Rev. 01 received from February
to May 2015. For each section the description of the type of amendment to API 5LD has been
added.
Date: 16 June 2015

Rev. 03: the revision includes 65 pages.


The document has been reviewed on the base of comments on Rev. 02 received from June to
July 2015.
Date: 27 July 2015
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INDEX
PART I - INTRODUCTION ............................................................................................ 6
1 Introduction ........................................................................................................... 6
1.1 Foreword ............................................................................................................ 6
1.2 Scope................................................................................................................. 6
1.3 References .......................................................................................................... 6
1.4 International Codes and Standards ........................................................................ 7
1.5 Definitions .......................................................................................................... 9
1.6 Symbols and Abbreviations ..................................................................................10
1.7 Quality Assurance and Company Inspection ...........................................................12
1.8 Special Requirements ..........................................................................................12
1.9 Linepipe Manufacturing Process ............................................................................12
1.10Purchase Order ..................................................................................................15
PART II - AMENDMENTS/SUPPLEMENTS TO API SPEC 5LD ....................................... 16
1 Scope.................................................................................................................... 16
1.1 Coverage ...........................................................................................................16
5 Manufacturing of Clad and Lined Steel Pipe .......................................................... 17
5.1 General .............................................................................................................17
5.2 Description of Clad and Lined Steel Pipe ................................................................17
5.4 Heat Treatment ..................................................................................................18
5.5 Welded Clad Pipe ................................................................................................19
5.6 CRA Liners .........................................................................................................21
6 Chemical Properties and Tests.............................................................................. 22
6.1 Composition .......................................................................................................22
6.6 Backing Material .................................................................................................23
6.7 Chemical Analysis of Weld Overlay ........................................................................27
7 Mechanical Properties and Tests .......................................................................... 27
7.1 Mechanical Properties (Backing Steel) ...................................................................27
7.2 Tensile Tests - General ........................................................................................28
7.3 Testing Frequency ..............................................................................................28
7.5 Transverse Tensile Tests......................................................................................28
7.6 Weld Tensile Tests ..............................................................................................28
7.10 Guided Bend Test ..............................................................................................28
7.11 Fracture Toughness Tests ...................................................................................29
7.12 Metallographic Examination ................................................................................29
8 Special Tests ........................................................................................................ 30
8.2 Corrosion Testing ...............................................................................................30
8.3 Tests for CRA Cladding Bond Strength and CRA Liner Tightness ................................30
8.5 Pitting and Intergranular Corrosion Test.................................................................31
8.6 HIC/SWC Testing ................................................................................................31
8.7 SSC Testing .......................................................................................................31
9 Hydrostatic Tests – Inspection Hydrostatic Test................................................... 32
10 Dimensions, Weights and Lengths ....................................................................... 32
10.1 Dimensions and weights.....................................................................................32
10.2 Diameter ..........................................................................................................32
10.5 Length .............................................................................................................32
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10.6 Straightness .....................................................................................................35


10.7 Jointers ............................................................................................................35
10.8 Pipe Ends .........................................................................................................35
11 Non-Destructive Inspection ................................................................................. 35
11.1 Inspection Methods for Welded Clad Pipe .............................................................36
11.2 Inspection Methods for Seamless Clad Pipe ..........................................................36
11.3 Inspection Methods for Lined Pipe .......................................................................36
11.4 Thickness of Cladding or Lining ...........................................................................38
11.5 Radiographic Inspection – Equipment ..................................................................38
11.6 Ultrasonic and Electromagnetic Inspection ............................................................39
11.7 Magnetic Particle Inspection ...............................................................................43
11.8 Dye Penetrant Inspection ...................................................................................43
12 Workmanship, Visual Inspection and Repair of Defects ....................................... 44
12.1 Workmanship ...................................................................................................44
12.2 Visual Inspection ...............................................................................................45
12.3 Defects and Disbonding......................................................................................45
13 Marking ............................................................................................................... 46
13.1 General ............................................................................................................46
13.2 Sequence of Markings ........................................................................................46
14 Documentation .................................................................................................... 47
14.1 Certification ......................................................................................................47
14.3 Manufacturing Data Book ...................................................................................47
14.4 Tally List ..........................................................................................................48
15 Packing and Handling .......................................................................................... 48
15.1 General ............................................................................................................48
15.2 Method of Packing and Storage ...........................................................................48
15.3 Transportation and Handling ...............................................................................48
15.4 Hot-Working Precautions ....................................................................................48
15.5 Documentation .................................................................................................49
Annex B - Manufacturing Procedure Specification .................................................... 50
Annex C - Welding Procedure Qualification Requirements ........................................ 52
Annex D - Manufacturing Procedure Qualification .................................................... 54
D.1 General .......................................................................................................54
D.2 Non-Destructive Testing ................................................................................54
D.3 Mechanical Testing ........................................................................................55
D.4 Macrographic, Micrographic and Hardness Examination .....................................55
D.5 Test for Bonding ...........................................................................................57
Annex H - Fracture Toughness Testing ..................................................................... 58
H.1 Fracture Toughness Testing (Charpy V-notch) ..................................................58
H.2 Drop Weight Tear Testing of Welded Pipe.........................................................60
H.3 Crack Tip Opening Displacement .....................................................................60
Annex I - Reference Standard Pipe/Plate for Inspection of Welds ........................... 61
Annex J - Summary of Testing and Inspection.......................................................... 62
Annex K - End Load Compensation for Hydrostatic Test Pressures ........................... 65
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PART I - INTRODUCTION

1 INTRODUCTION

1.1 FOREWORD
The present specification covers clad and lined pipes for onshore and offshore applications.
This specification is applicable to J-lay and S-lay offshore installation methods; in case of reel
laid pipelines, modifications to the present specification may be necessary.

As general guidelines, lined pipes (mechanically bonded) are preferred where the expected
mechanical stresses, e.g. during pipeline lying and/or normal operations, are reasonably low;
clad pipes (metallurgically bonded) provide a better bending resistance than lined pipes
allowing their utilization in a wider range of applications. The COMPANY recommends the
application of clad pipes for offshore risers and for all deep and ultra deep water applications.

1.2 SCOPE
This Specification forms an addendum to API Specification 5LD, Specification for CRA Clad or
Lined Steel Pipe - March 2015 and defines additional requirements covering the manufacture,
inspection, testing, marking, coding and supply of clad and lined pipes. This Specification must
be read in conjunction with API Specification 5LD, Specification for CRA Clad or Lined Steel
Pipe - March 2015.

All pipes shall be produced in accordance with a Manufacturing Procedure Specification that
has been approved by COMPANY and that has been qualified in accordance (Annex D).

For the use in sour service environment, the backing material shall be fully compliant with ISO
15156 / NACE MR0175, unless differently specified by the Company.

1.3 REFERENCES
The reference documents listed below form an integral part of this Specification. Unless
otherwise stipulated, the applicable version of these documents, including relevant appendices
and supplements, is the latest revision published at the elective date of the Contract.

The order of precedence of the applicable documents shall be:

- The Purchase Order (and TDS, if applicable);


- The present Specification;
- API 5LD:2015;
- The Codes and Standards referenced therein.

Applicable Codes and Standards which are to be used in conjunction with this specification are
stated in paragraphs hereafter.

Unless otherwise specifically indicated in writing by the Company, the Supplier shall work in
accordance with the requirements specified herein and the applicable requirements of the
latest editions at date of Contract award of the referenced Codes and Standards, whenever
requested in the present specification.

Standards equivalent to those referred to herein shall not be substituted without the written
approval of the Company. Approval of equivalent standards will not, in any way, remove
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responsibility from the Supplier to meet the requirements of the Standards referred to and
amended herein, in the event of conflict.

1.4 INTERNATIONAL CODES AND STANDARDS

1.4.1 American Petroleum Institute (API)

/1/ API Spec. 5LD Specification for CRA Clad or Lined Steel Pipe (4th Edition)
/2/ API RP 5L1 Railroad Transportation of Line pipe
/3/ API RP 5LW Recommended Practice for Transportation of Line Pipe on Barges and
Marine Vessels

1.4.2 American Society of Mechanical Engineers (ASME)

/4/ ASME II, Part Boiler and Pressure Vessel Code, Section II, Part C – Specifications for
C Welding Rods, Electrodes, and Filler Metals
/5/ ASME V Boiler and Pressure Vessel Code, Section V, Non-destructive
Examination
/6/ ASME VIII Boiler and Pressure Vessel Code, Section VIII Div. 2, Construction of
Pressure Vessels
/7/ ASME B46.1 Surface Texture, Surface Roughness, Waviness and Lay

1.4.3 American Society for Testing and Materials (ASTM)

/8/ ASTM A262 Standard Practices for Detecting Susceptibility to Intergranular Attack
in Austenitic Stainless Steels
/9/ ASTM A264 Standard Specification for Stainless Chromium-Nickel Steel-Clad Plate,
Sheet, and Strip
/10/ ASTM A265 Standard Specification for Nickel and Nickel-Base Alloy-Clad Steel
Plate
/11/ ASTM A312 Standard Specification for Seamless and Welded Austenitic Stainless
Steel Pipes
/12/ ASTM A358 Standard Specification for Electric-Fusion-Welded Austenitic
Chromium-Nickel Alloy Steel Pipe for High-Temperature Service
/13/ ASTM A370 Standard Test Methods and Definitions for Mechanical Testing of Steel
Products
/14/ ASTM A578 Standard Specification for Straight-Beam Ultrasonic Examination of
Plain and Clad Steel Plates for Special Applications
/15/ ASTM B423 Standard Specification for Nickel-Iron-Chromium-Molybdenum-Copper
Alloy (UNS N08825 and N08221) Seamless Pipe and Tube
/16/ ASTM B424 Standard Specification for Ni-Fe-Cr-Mo-Cu Alloy (UNS N08825 and
N08221) Plate, Sheet and Strip
/17/ ASTM B444 Standard Specification for Nickel-Chromium-Molybdenum-Columbium
Alloys (UNS N06625) and Nickel-Chromium-Molybdenum-Silicon Alloy
(UNS N06219) Pipe and Tube
/18/ ASTM B499 Standard Test Method for Measurement of Coating Thicknesses by the
Magnetic Method: Nonmagnetic Coatings on Magnetic Basis Metals
/19/ ASTM B705 Standard Specification for Nickel-Alloy (UNS N06625, N06219 and
N08825) Welded Pipe
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/20/ ASTM E112 Standard Test Method for Determining Average Grain Size
/21/ ASTM E165 Standard Test Method for Liquid Penetrant Examination
/22/ ASTM E709 Standard Guide for Magnetic Particle Examination
/23/ ASTM E571 Standard Practice for Electromagnetic (Eddy-Current) Examination of
Nickel and Nickel Alloy Tubular Products
/24/ ASTM G28 Standard Test Methods for Detecting Susceptibility to Intergranular
Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys
/25/ ASTM G48 Standard Test Method for Pitting and Crevice Corrosion Resistance of
Stainless Steels and Related Alloys by Use of Ferric Chloride Solution

1.4.4 International Standard Organization (ISO)

/26/ ISO 2178 Non-magnetic Coatings on Magnetic Substrates; Measurement of


Coating Thickness; Magnetic Method
/27/ ISO 2566-1 Steel – Conversion of Elongation Values – Part 1: Carbon and Low
Alloy Steels
/28/ ISO 9712 Non-destructive Testing; Qualification and Certification of Personnel
/29/ ISO 3183 Petroleum and Natural Gas Industries – Steel Pipe for Pipeline
Transportation Systems
/30/ ISO 10474 Steel and Steel Products, Inspection Document
/31/ ISO 15156-2 Petroleum, Petrochemical and Natural Gas Industries – Materials for
Use in H2S-containing Environments in Oil and Gas Production: Part 2:
Cracking-resistant Carbon and Low Alloy Steels, and the Use of Cast
Irons
/32/ ISO 15156-3 Petroleum, Petrochemical and Natural Gas Industries – Materials for
Use in H2S-containing Environments in Oil and Gas Production: Part 3:
Cracking-resistant CRAs (Corrosion-resistant Alloys) and Other Alloys
/33/ ISO 8501-1 Preparation of Steel Substrates Before Application of Paints and
Related Products – Visual Assessment of Surface Cleanliness – Part 1:
Rust Grades and Preparation Grades of Uncoated Steel Substrates and
of Steel Substrates after Overall Removal of Previous Coatings
/34/ ISO 19232-1 Non-destructive Testing – Image Quality of Radiographs – Part 1:
Determination of the Image Quality Value Using Wire-type Image
Quality Indicators

1.4.5 National Association of Corrosion Engineers (NACE)

/35/ NACE TM0177 Laboratory Testing of Materials for Resistance to Sulphide Stress
Cracking and Stress Corrosion Cracking in H2S Environments
/36/ NACE TM0284 Evaluation of Pipeline and Pressure Vessel Steels for Resistance to
Hydrogen-Induced Cracking

1.4.7 Company Standards

/37/ 23005.SLI.OFF.FUN Stacking of pipes.

This Functional Specification shall be used in conjunction with the relevant COMPANY data
sheets (Technical Data Sheet (TDS), Inspection Data Sheet (IDS) and Required Documentation
Data Sheet (DDS)) duly compiled with Project requirements.
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1.5 DEFINITIONS

1.5.1 General Definitions


COMPANY
Shall mean Eni E&P or its elected representatives.

CONTRACTOR
Shall mean the company appointed by COMPANY to perform the EPCI works of a package, and
its subcontractors, vendors, agents and authorised representatives.

MANUFACTURER
Shall mean the party that manufactures equipment and services to perform the duties
specified by COMPANY or CONTRACTOR.

May
Verbal form used to indicate a course of action permissible within the limits of the standard.

Shall
Indicates requirements strictly to be followed in order to conform to this standard and from
which no deviation is permitted.

Should
Indicates that among several possibilities, one is recommended as particularly suitable,
without mentioning or excluding others, or that a certain course of action is preferred but not
necessarily required. Other possibilities may be applied subject to agreement.

SUPPLIER
Shall mean the party that supplies equipment and services to perform the duties specified by
COMPANY or CONTRACTOR.

1.5.2 Specific Definitions


Backing Pipe: Shall mean the steel pipe forming the pressure envelope to which
the CRA layer is bonded;

Clad: Shall mean a metallurgically bonded CRA layer;

CRA Layer: Shall mean the internal corrosion resistant alloy layer;

Defect: Shall mean a discontinuity or group of discontinuities that produce


an indication during non-destructive testing, which does not meet
specified acceptance criteria;

Discontinuity: Shall mean an interruption in the physical structure or


configuration of a pipe that may be either intentional or
unintentional;

Flaw: Shall mean an interruption in the physical structure or


configuration of a pipe that is unintentional;

Indication: Shall mean evidence of a discontinuity observed during non-


destructive testing that requires interpretation to determine its
significance;

Jointer: Shall mean a pipe made from two smaller sections of pipe that are
welded together;
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Lined: Shall mean a mechanically bonded CRA layer;

Lot: Shall mean a group of pipes covered by a single test or analysis;

Mechanically bonded: Shall mean the technique used in the manufacture of lined pipe
relying upon the expansion of an internal CRA pipe into an outer
backing pipe;

Metallurgically bonded: Shall mean the technique used in the manufacture of clad pipe
where CRA layer is fused to the base material or backing pipe;

Pipe bevel: Shall mean the total weld preparation machined on the end of a
pipe;

Plate or coil: Shall mean the starting material from which a welded pipe is
formed;

Purchaser: The term used in API Spec 5LD that shall have the same meaning
as COMPANY;

Radiological: The term used in API Spec 5LD that has the same meaning as
radiographic, used in this Specification;

Seal weld: Shall mean the weld performed at the ends of a lined pipe to seal
the cavity between the CRA liner and the backing pipe;

Sour service: Exposure to oilfield environments that contains H2S and can cause
cracking of materials by the mechanisms addressed by ISO 15156
/ NACE MR0175.

1.6 SYMBOLS AND ABBREVIATIONS


Following abbreviations applies throughout this document.

API: American Petroleum Institute;


ASME: American Society of Mechanical Engineers;
ASTM: American Society for Testing and Materials;
AUT: Automatic Ultrasonic Thickness;
CE: Carbon Equivalent (based upon the International Institute of Welding
equation);
CLA: Centre Line Average;
CRA: Corrosion Resistant Alloy;
CS: Concession Request;
CTOD Crack Tip Opening Displacement
DN: Diameter Nominal;
DPI: Dye Penetrant Inspection;
DWT: Drop Weight Tear (Test);
ECT: Eddy Current Testing;
EMT: Electromagnetic Testing;
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ERW Electric Resistance Welding


ESW: Electro Slag Welding
FBH: Flat Bottomed Hole;
FCAW-MC: Flux Cored Arc Welding - Metal Cored;
GMAW Gas Metal Arc Welding;
GTAW Gas Tungsten Arc Welding;
HAZ: Heat Affected Zone;
HFI High Frequency Induction (Welding)
HIC: Hydrogen Induced Cracking;
HV: Vickers Hardness;
ID: Inside Diameter;
ISO: International Standard Organization;
ITP: Inspection Test Plan;
MFL: Magnetic Flux Leakage;
MPI: Magnetic Particle Inspection;
MPQ: Manufacturing Procedure Qualification;
MPS: Manufacturing Procedure Specification;
MT: Magnetic Particle Testing;
MUT: Manual Ultrasonic Thickness;
NACE: National Association of Corrosion Engineers;
NDT: Non-Destructive Testing;
OD: Outside Diameter;
PAW: Plasma Arc Welding;
Pcm: Carbon Equivalent (based upon the Ito-Bessyo equation);
PQR: Procedure Qualification Record;
PREN: Pitting Resistance Equivalent Number;
PT: Dye Penetrant Testing;
Ra: Roughness Average;
RDH: Radially Drilled Hole;
RT: Radiographic Testing;
SAW: Submerged-Arc Welding;
SMAW: Shielded Metal Arc Welding;
SMLS: Seamless;
SS: Stainless Steel;
SWC: Step-wise Cracking;
TDS Technical Data Sheet
TMCP: Thermo-mechanical Controlled Processing;
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TPI: Third Party Inspection;


TQ: Technical Query;
UNS: Unified Numbering System;
UT: Ultrasonic Testing;
WPQT: Welding Procedure Qualification Tests;
WPS: Welding Procedure Specification.

1.7 QUALITY ASSURANCE AND COMPANY INSPECTION


MANUFACTURER shall submit any manufacturing, testing and inspection procedures that
require approval by COMPANY prior to start of production. Production shall not start until
approval by COMPANY has been obtained.

MANUFACTURER shall have in place a quality assurance organization responsible for


formulating and implementing a quality system, which ensures that the requirements of this
specification are achieved.

Unless otherwise stated in a purchase order, the MANUFACTURER’s quality system shall be
based on ISO 9000 (or COMPANY approved equivalent) and shall be described in a quality
assurance manual.

The manual shall provide for the preparation of a Quality plan and Inspection Test plan that
shall include provisions for control of all raw materials, pipe manufacture and final inspections
including hold and witness point.

The Quality Manual and typical Quality Plan shall be submitted to COMPANY with the tender
documents. The Quality Plan shall be subject to COMPANY approval for incorporation of
COMPANY hold and witness points prior to the start of production. Evidence shall be included in
the plan that the inspection team is independent of production management.

1.8 SPECIAL REQUIREMENTS


All correspondence, reports, manuals, test reports, certificates shall be in the English language
or shall have authenticated translations accompanying them. Numeric data such as test results
shall be also provided in a format suitable for import in a spreadsheet approved by COMPANY.

If the requirements of this specification cannot be met, written notification of non-compliance,


including explanations and proposed change, shall be provided by the MANUFACTURER for
COMPANY approval.

Every request of change shall be submitted via Concession Request (CS) or Technical Query
(TQ).

All pipes supplied in accordance with this specification shall be suitable for application of
fusion-bonded coatings.

When specified in the purchase order, pipes shall be suitable for induction bending or hot
forming to produce tees; where this is the case the CRA layer shall be metallurgically bonded
to the backing pipe.

1.9 LINEPIPE MANUFACTURING PROCESS


The method to be used for cladding or lining the pipe has been intentionally left open in this
Specification. MANUFACTURER shall submit details of their facilities and their proposed
manufacturing process with their tender to COMPANY for approval prior to purchase order
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award. Production shall not start until the MPS is agreed between COMPANY and
MANUFACTURER. As a minimum, the following information shall be supplied:

1. A description of the production facilities.

2. The production capacity.

3. A reference list of similar pipe sizes and cladding materials produced using the proposed
manufacturing process including:

- full details of manufacturing process used;


- all dimensional tolerances achieved;
- product and heat analysis test results achieved;
- corrosion test results achieved;
- mechanical test results achieved;
- weldability test performed for girth welds and test acceptance criteria used.

4. The name of the steel-maker and CRA maker.

5. The steel-making process including rare earth additions, calcium treatment, de-
sulphurising, sulphide shape control, phosphorus removal and degassing techniques, if
used.

6. The nominal weight of each heat and the size and weight of ingots and billets.

7. The ingot or billet piercing method and forming techniques.

8. The manufacturing method proposed for each pipe size including where applicable:

- details of clad/lined pipe forming technique;


- forming temperatures;
- post-forming heat treatments;
- clad welding pre-heat temperatures and post weld heat treatment temperatures;
- longitudinal weld preparation and welding sequence;
- girth weld preparation and welding sequence, where applicable;
- clad interface activator compositions;
- maximum continuous joint length achievable (without butt welding two joints together);
- maximum and minimum tolerances (on pipe body and on pipe ends) achievable for pipe
wall thickness, out of roundness, straightness, internal and external diameter.

9. The method of controlling thickness of the CRA layer and backing pipe during forming.

10. Full details of all ultrasonic testing equipment used on pipe body and on pipe ends or on
plate for measuring the thickness of the CRA layer, the backing steel wall thickness, lack
of bond and laminations or defects, including:

- testing technique;
- extent of testing (100% coverage required);
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- acceptance criteria;
- sensitivity and calibration technique;
- calibration frequency;
- marking technique used to indicate loss of coupling.

11. Full details of proposed DPI and MPI techniques used for detection of surface defects in the
CRA layer and backing steel pipe including:

- testing technique;
- extent of testing;
- acceptance criteria;
- reference standards.

12. The proposed technique for confirming that surface indications do not extend through the
CRA layer to the underlying backing material, i.e. ferroxil method.

13. The proposed technique for checking iron dilution into the CRA layer for clad welding
technique.

14. The techniques proposed for measuring the straightness, length, diameter, wall thickness,
out-of-roundness and end squareness.

15. The percentage cold expansion used for sizing purposes (Note: This shall not change
desired mechanical, corrosion resistance or physical properties of pipe).

16. The hydrostatic testing procedures.

17. The method and number of heat treatments.

18. The technique for establishing the bond strength of the CRA layer.

19. The proposed thickness of the CRA layer if a different thickness is proposed to that
specified in this Specification.

20. The chemical composition of the backing pipe.

21. The chemical composition of CRA layer.

22. Full details of proposed Manufacturing Procedure Qualification testing including but not
limited to the following:

- product and heat analysis testing (clad and backing steel plates);
- tensile testing (pipe);
- impact testing (pipe);
- CTOD testing (pipe);
- hardness testing (pipe);
- bonding testing (pipe);
- SSC and HIC testing (pipe on backing steel);
- pitting testing; (pipe on clad material)
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- butt weld testing (pipe);


- bend testing (pipe);
- macro and metallurgical testing (pipe).

23. The NDT techniques to be used for the examination of the butt welds in welded and/or
jointed pipe.

24. Recommendations and precautions to be implemented when clad pipe is to be induction


bent or hot-form to produce tees, i.e.:

- maximum induction bending temperatures;


- post-forming heat treatments,
- the thickness of the CRA cladding at any point shall not be less than 3 mm, post
bending.

1.10 PURCHASE ORDER


In placing the order for Clad or Lined Pipe, reference should be made to the Section
“Information to be Supplied by the Purchaser” in API Specification 5LD, Specification for CRA
Clad or Lined Steel Pipe - March 2015, Page 4, and to the following table.

Issues to be specified in the Purchase Order Reference section in this Specification

PART I

Transported fluid (sour/not-sour) 1.1

Suitability for induction bending or hot forming 1.7

PART II

Quantity/Length -

Grade of backing pipe and CRA layer 1.1

Size (inside or outside diameter, wall thickness of backing pipe) 10.1

Further documentation and document submission dates 14.1 to 14.4, 15.5

Necessity for temporary corrosion protection requirements (coating) 15.1 and 15.2

Bevel configuration -

Minimum design temperature H.1

Absorbed energy requirements H.1


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PART II - AMENDMENTS/SUPPLEMENTS TO API SPEC 5LD

The technical requirements for clad or lined steel pipe materials are based on API 5LD - Fourth
Edition – March 2015.

The numbering of the following items corresponds to paragraph numbering in API 5LD, fourth
edition March 2015, on which this specification is based. Any additional clauses are numbered
sequentially. The text shown in each paragraph below is an addition or amendment to the
referenced API Specification.

Paragraphs not mentioned in this amendment shall be fully applicable.

In this specification amendments to API 5LD fall into the following categories:

ADD: Were addtions have been made to the API 5LD clause or
paragraph.

AMEND: Where the API 5LD clause has been modified.

DELETE: Where the complete clause or paragraph is to be regarded.

ADDITIONAL CLAUSE: Where new numbered clauses or paragraphs are added.

SUBSTITUTE: Where the text has been substituted for the complete clause or
paragraph in API 5LD.

All provisions of API 5LD that are not revised remain in force. Where a cross-reference is made
to another part of this Specification, the referenced section number is shown in brackets
“(section number)”.

1 SCOPE

1.1 COVERAGE

SUBSTITUTE

This specification covers seamless and welded clad steel line pipe and lined steel line pipe with
improved corrosion resistant properties.

The clad and lined steel line pipe specified herein shall be composed of a base metal out-side
and a corrosion-resistant alloy (CRA) layer inside the pipe. The base material shall conform to
API Spec 5L (ISO 3183) except as modified herein.

The primary product has square ends, but other special end preparation may be furnished by
agreement between the COMPANY and MANUFACTURER. Included are nominal pipe sizes
(NPS): 1 in. through 42 in.

Grades of base metal covered by this specification are X42, X52, X60, X65 and X70.

Grades of the CRA layer include UNS Grades S31603, N08825, and N06625. Other grades of
the CRA layer shall be subject to agreement by COMPANY.
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5 MANUFACTURING OF CLAD AND LINED STEEL PIPE

5.1 GENERAL

SUBSTITUTE

Clad or lined steel pipe furnished to this specification shall be seamless or welded pipe, clad or
lined, as defined below.

Clad or lined centrifugally-cast steel pipe shall not be furnished.

All welding consumables shall comply with the requirements ASME Section II, Part C. The
nominal thickness of the CRA layer shall be a minimum of 3 mm unless otherwise agreed with
COMPANY. The minimum 3 mm of nominal thickness of the CRA layer shall be guaranteed also
after bending.

Contamination of the CRA layer with carbon steel shall be avoided.

5.2 DESCRIPTION OF CLAD AND LINED STEEL PIPE

5.2.1 Clad Pipe

AMEND

a) Seamless. Seamless clad pipe shall be produced by hot working composite material to
form a tubular product that does not contain any welded seams.

b) Welded. Welded clad pipe shall be produced from clad plate or skelp, cold formed and
welded in accordance with (Annex C) of this Specification.

5.2.2 Lined Pipe

AMEND

a) Seamless. Seamless backing pipes and CRA liners shall be produced by hot working to
form a tubular product without a welded seam.

Seamless CRA liners shall be produced in accordance with the requirements of


(Section 5.6), as applicable.

b) Welded. Welded lined pipe consists of an outer welded pipe made to the requirements
of API 5L and (Section 6.6) of this Specification. The internal weld bead shall be
ground flush prior to lining. Welded CRA liners shall be produced in accordance with
the requirements of (Section 5.6), as applicable. The external weld bead shall be
ground flush prior to lining.

The offset between the longitudinal weld seams of the backing pipe and CRA liner shall
be 90°.

ADD

Before liner insertion and expansion, backing steel surfaces in contact with CRA shall be:

- blast cleaned to a surface cleanliness of ISO 8501 Sa 2 or better;


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- cleaned, dried and free from any dust or particles. It shall be demonstrated by the
MANUFACTURER that moisture at the interface between the liner and the carbon-
steel backing pipe is strictly controlled. Humidity shall be less than 80% and carbon
steel and CRA pipes temperatures shall be at least 5°C above the dew point.

Weld overlay shall be performed on minimum a 100 mm distance from pipe ends (see. sketch
below). An internal clamp shall be used during overlay welding to avoid any lifting-off of the
liner due to weld shrinkage.

Backing steel C-Mn


CRA liner Weld overlay

min 100 mm min 100 mm

Machining of the weld overlay shall be carried out to minimise step change between overlay
and liner.

Plastic straining > 0.5% of the C-Mn backing pipe during liner expansion process is not
allowed. In addition, the cumulated plastic straining resulting from the carbon steel pipe
manufacturing process (final cold expansion) and the liner expansion process shall not exceed
2.0%.

5.4 HEAT TREATMENT

SUBSTITUTE

The base material for backing pipes shall be produced by the electric furnace or basic oxygen
process and shall be fully killed. For sour service applications, vacuum degassing and ladle
refining shall be applied and the steel shall be calcium treated.

Slab or billet shall be produced by the continuous casting process. Ingot casting is accepted
provided that tight control of chemistry and segregation is in place and approved by COMPANY.

The material of the backing pipe shall have a grain size of ASTM 8 or finer, as defined in ASTM
E112.

Seamless backing pipes shall be furnished in the normalised, normalised and tempered or
quenched and tempered condition.

The plates for welded backing pipes shall be in the normalised, normalised and tempered,
TMCP, TMCP plus accelerated cooling, or the quenched and tempered condition.

Heat treatment shall be performed in accordance with a documented procedure. Heat


treatment parameters are to be included in the MPS. No heat treatment shall be performed
after pipe forming. MANUFACTURER shall establish and follow procedures for maintaining heat
and/or lot identity.

For lined pipe, heat treatment may be applied to the outer pipe and the inner pipe,
individually, before inserting the liner.

The CRA inner pipe of lined pipe shall be supplied in the solution annealed condition unless
otherwise agreed with COMPANY.
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Raw material for Alloy 625 CRA layer shall be delivered from sub-suppliers in the annealed
condition unless otherwise agreed with COMPANY.

5.5 WELDED CLAD PIPE

ADDITIONAL CLAUSE

5.5.1 Clad Steel Plate Inspection Prior to Pipe Manufacture


By agreement with COMPANY, NDT of the clad plate may be carried out prior to the plate being
formed into a pipe. NDT procedures shall be submitted to COMPANY and production shall not
start until the NDT procedures are agreed between COMPANY and MANUFACTURER.

a) Visual Inspection. Visual inspection of the clad plate shall be carried out over 100% of the
clad surface and shall take place after any pickling and passivation of it (or grinding, if
pickling and passivation is performed on pipe). The examination shall be performed in
accordance with ASME Section V Article 9.

An imperfection shall be considered unacceptable when any of the following limits are
exceeded.

Imperfection Limit

Scratches Maximum depth = 0.5 mm

Pits Maximum depth = 0.5 mm

Surface Roughness, Ra Maximum value = 12.5 µm

The surface roughness shall be defined by the Centre Line Average (CLA) method as per
ASME B46.1.

b) Ultrasonic Inspection. Ultrasonic scanning of the clad steel plate shall be carried out over
100% of the clad surface using a mechanised approach with automatic recording facilities.
In addition, an automatic scanning device designed to disclose edge defects shall be used
to examine the edges of the plate. An area extending a minimum width of 25 mm from the
plate edge shall be scanned. The use of manual UT for inspection of plate surface and/or
edges as an alternative to automatic UT shall be subject to approval by COMPANY.

The plate thickness shall be checked by scanning along a grid pattern such that at least
10% of the plate surface is covered. As an alternative subject to approval by COMPANY,
plate thickness may be checked taking at least 9 point wall thickness measurements
distributed around the plate circumference and in the mid section, according to a NDT
procedure agreed between COMPANY and MANUFACTURER. Any other procedure that may
be proposed by MANUFACTURER for plate thickness measurement by UT shall be subject
to agreement with COMPANY.

All ultrasonic examinations shall be carried in accordance with (Section 11.6).

c) Electromagnetic Thickness Measurements. The thickness of the clad layer shall be verified
by electromagnetic (inductive or adhesive force) methods or by other techniques agreed
with COMPANY. Measurements shall be made from the clad side over a grid pattern in such
a way that at least 25% of the surface is covered. As an alternative procedure subject to
approval by COMPANY, plate thickness may be checked taking at least 9 point wall
thickness measurements distributed around the plate circumference and in the mid section
according to a NDT procedure agreed between COMPANY and MANUFACTURER. Any other
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procedure that may be proposed by MANUFACTURER for plate thickness measurement by


electromagnetic method shall be subject to agreement with COMPANY.

The accuracy of the clad thickness measurement shall be better than 0.2 mm and shall be
carried out in accordance with ISO 2178 or ASTM B499.

d) Dye Penetrant Inspection. All plate edges shall be dye penetrant inspected for cracks,
laminations and disbondment in accordance with ASTM E165. The requirement for DPI
may be relaxed subject to agreement by COMPANY if CRA clad plate is delivered with
excess width and length 100% UT checked, and then cutting to final dimension and edge
preparation are performed at pipe mill.

No crack-like indications, laminations or disbondment shall be permitted at the plate


edges.

e) Repairs to the Clad Layer. All defects found during inspection of the clad plate shall be
documented by MANUFACTURER. If a defect has to be repaired by welding, approval shall
be obtained from COMPANY prior to the repair being made.

Defects on the surface of the cladding shall be removed by grinding and the defective area
examined by dye penetrant inspection. The remaining thickness shall be checked using an
electromagnetic method, as detailed in (Section 5.5.1c), and shall be within the limits
given in (Table 6).

If the remaining thickness of the cladding is below the limits given in (Table 6), the plate
shall be discarded.

The surface roughness of all repairs shall conform to the requirements of (Section 5.5.1a).

5.5.2 Process of Pipe Manufacture


a) Plate Forming into Pipe Processes. The plate shall be formed into pipe at room
temperature.

b) Welding Processes. All tack, longitudinal and girth welds shall be made with the addition of
filler metal using a qualified welding procedure in accordance with (Annex C).

Tack welds shall be made using GMAW, GTAW, gas shielded FCAW, or SMAW using low
hydrogen electrodes. The diffusible hydrogen content of the resulting weld metal shall not
exceed 10 ml / 100 g of deposited metal.

As part of the manufacturing procedure qualification test, the location of each tack weld
shall be marked adjacent to the weld. During subsequent sectioning of the weld for
mechanical testing, at least one macro specimen as detailed in (Annex D, Section D.4),
shall be removed from the location of a tack weld. Examination of the macro specimen
shall verify that complete fusion of the tack weld into the subsequent filler pass has been
achieved, without any cracking or voids.

Welds shall be full penetration and shall be made using one or more of the following
processes: SAW, GTAW and GMAW. Other welding processes, such as PAW or ESW, may
be used subject to approval by COMPANY. The use of electric resistance welding (ERW) or
high frequency induction (HFI) welding processes shall not be permitted.

All longitudinal seams shall be a double-sided butt weld and shall be weld overlaid on the
inside such that the depth of the overlay is at least equal to the thickness of the cladding
(See Section 7.12). Single-sided butt weld may be used subject to approval by COMPANY.
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Welding parameters controlling the consistency of overlay welding of the internal bead
shall be continuously recorded and records provided for subsequent verification.

Run-on and run-off tabs shall be used for all longitudinal seams. The tabs shall be
removed by cold cutting or grinding.

For gas shielded welding processes, hydrogen additions in the shielding and/or backing
gas shall not be permitted.

In case that PAW is approved by COMPANY, mixed gas shall have controlled hydrogen
content agreed with COMPANY and weld NDT shall be performed not earlier than 36 hours
after welding. Argon/hydrogen shielding gases shall only be used for PAW of austenitic
stainless steels and nickel alloys. Hydrogen additions shall not exceed 5% in the case of
manual welding and 10% in the case of mechanised welding.

c) AISI 316L Stainless Steel (UNS S31603) Clad Material. The longitudinal seam shall be weld
overlaid on the inside using either AISI 309Mo (ASME II Part C SFA-5.9 ER309Mo) or
309MoL (ASME II Part C SFA-5.9 ER309MoL) for the first layer and either 316L (ASME II
Part C SFA-5.9 ER316L) or 317L (ASME II Part C SFA-5.9 ER317L) for the subsequent
layers. The Mo content of the filler material shall be sufficient to ensure the Mo content of
the finished weld is equal to, or greater than, the Mo content of the clad material.

For girth welds made from two sides, the same requirements as those specified for the
longitudinal seam shall apply. For girth welds made from one side only, either AISI 309Mo
or 309MoL shall be used throughout.

d) Alloy 825 (UNS N08825) Clad Material. The longitudinal seam shall be weld overlaid on the
inside using an Alloy 625 filler material.

For girth welds made from two sides, the same requirements as those specified for the
longitudinal seam shall apply. For girth welds welded from one side only, Alloy 625 shall be
used throughout.

In the selection of the welding parameters, specific care shall be taken to avoid hot
cracking (see also Section 7.12).

e) Alloy 625 (UNS N06625) Clad Material. The longitudinal seam shall be weld overlaid on the
inside using an Alloy 625 filler material.

For girth welds made from two sides, the same requirements as those specified for the
longitudinal seam shall apply. For girth welds welded from one side only, Alloy 625 shall be
used throughout.

In the selection of the welding parameters, specific care shall be taken to avoid hot
cracking (see also Section 7.12).

5.6 CRA LINERS

ADDITIONAL CLAUSE

5.6.1 AISI 316L Stainless Steel (UNS S31603) Liners


a) Seamless. Seamless stainless steel liners shall be manufactured in accordance with ASTM
A312. Jointers shall not be permitted.
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b) Welded. Welded stainless steel liners shall be manufactured in accordance with ASTM A358
and shall comply with the requirements for Class 1 or Class 3 pipes specified therein. The
liner shall contain one longitudinal weld. Jointers shall not be permitted.

Welds shall be made using one or more of the following processes: SAW, GTAW and
GMAW. The use of other welding processes shall be subject to approval by COMPANY. The
use of welding to repair defects in the base material shall not be permitted.

5.6.2 Alloy 825 (UNS N08825) Liners


a) Seamless. Seamless Alloy 825 liners shall be manufactured in accordance with ASTM B423
in either the hot-finished, annealed and pickled condition or the cold-worked, annealed
and pickled condition. Jointers shall not be permitted.

b) Welded. Welded Alloy 825 liners shall be manufactured in accordance with ASTM B705 and
shall comply with the requirements for Class 2 pipes specified therein. The liner shall
contain one longitudinal weld. The use of jointers shall not be permitted.

Welds shall be made using one or more of the following processes: SAW, GTAW and
GMAW. The use of other welding processes shall be subject to approval by COMPANY. The
use of welding to repair of defects in the base material shall not be permitted.

5.6.3 Alloy 625 (UNS N06625) Liners


a) Seamless. Seamless Alloy 625 liners shall be manufactured in accordance with ASTM B444
and shall comply with the requirements for Class 1 or Class 2 pipes specified therein. The
outside and inside diameter shall have dull, matte (pickled) surfaces, i.e. pipes shall be
pickled and not ground. Jointers shall not be permitted.

b) Welded. Welded Alloy 625 liners shall be manufactured in accordance with ASTM B705 and
shall comply with the requirements for Class 2 pipes specified therein. The liner shall
contain one longitudinal weld. Jointers shall not be permitted.

Welds shall be made using one or more of the following processes: SAW, GTAW and
GMAW. The use of other welding processes shall be subject to approval by COMPANY. The
use of welding to repair of defects in the base material shall not be permitted.

6 CHEMICAL PROPERTIES AND TESTS

6.1 COMPOSITION

SUBSTITUTE

The composition of the CRA layer and limitations on heat and product analysis shall be
contained in the MPS as detailed in (Annex B). The composition of the CRA layer shall conform
to the applicable UNS number and shall be confirmed by product analysis as detailed in Section
6.3. The product analysis shall be reported on the material test certificate for the finished pipe.

In the case of pipes where the CRA layer is specified as UNS N08825 (LC 2242), the CRA layer
shall have a minimum Pitting Resistance Equivalent Number of 33 calculated using the
following formula:

PREN = Cr + 3.3 • Mo + 16 • N
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6.6 BACKING MATERIAL

SUBSTITUTE

MANUFACTURER shall propose a chemical composition for each type and grade of backing pipe
to be supplied. Each composition shall be contained in the MPS and, unless otherwise agreed
with COMPANY and specified in the TDS, shall be within the maximum allowable limits specified
in Table 6.6-1 or 6.6-2, as appropriate to the product type and grade.

For sour service application, the backing material shall be fully compliant with Annex H of API
5L / ISO 3183 and to ISO 15156 / NACE MR0175 Part 2, unless differently specified by the
Company.

Provided that the final alloy content does not exceed the maximum allowable limit, with
reference to the target chemistry proposed by the MANUFACTURER, the content of each of the
elements listed below may vary by up to the figure shown.

Element C Mn Si Cu Ni Mo Cr Nb V Ti
Maximum Allowable
± 0.03 ± 0.30 ± 0.25 ± 0.10 ± 0.10 ± 0.05 ± 0.05 ± 0.02 ± 0.02 ± 0.02
Variation, wt%

Any variation in excess of the figure shown above shall not be permitted.
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Table 6.6-1 - Chemical composition of welded steel pipe(1, 2, 3, 4)

Product analysis

Grade maximum weight %

X42 / L290 X52 / L360 X60 / L415 X65 / L450 X70 / L485

C (5) 0.12 0.12 0.12 0.12 0.12

Mn (5)
1.65 1.65 1.65 1.65 1.75

Si 0.40 0.45 0.45 0.45 0.45

P 0.020 0.020 0.020 0.020 0.020

S 0.010 0.010 0.010 0.010 0.010

Cu 0.35 0.50 0.50 0.50 0.50

Ni 0.30 0.50 0.50 0.50 0.50

Mo 0.10 0.50 0.50 0.50 0.50

Cr (6) 0.30 0.50 0.50 0.50 0.50

Al (total)
(7)
0.06 0.06 0.06 0.06 0.06

Nb (8, 9) 0.04 0.05 0.06 0.06 0.06

V (8) 0.04 0.05 0.08 0.10 0.10

Ti (8)
0.04 0.04 0.06 0.06 0.06

N (7) 0.010 0.010 0.010 0.010 0.010

B (10) 0.0005 0.0005 0.0005 0.0005 0.0005

CE (11)
0.34 0.37 0.38 0.39 0.41

Pcm (12) 0.19 0.20 0.21 0.22 0.23

Notes
1. Chemical composition applies for wall thicknesses up to 35 mm and shall be subject to agreement by COMPANY
for larger wall thicknesses.
2. When scrap material is being used in steel production, the amount of the following residual elements shall be
determined and reported, and the levels shall not exceed: 0.03% As, 0.01% Sb, 0.02% Sn, 0.01% Pb, 0.01% Bi
and 0.006% Ca.
3. When calcium is intentionally added, the Ca/S ratio shall be = 1.5 when S > 0.0015.
4. Except for deoxidation elements, other elements than those mentioned in this table shall not be intentionally
added if not specifically agreed with COMPANY.
5. For each reduction of 0.01% carbon below the maximum specified value, an increase of 0.05% manganese
above the specified maximum values is permitted with a maximum increase of 0.1%.
6. 0.5 - 1.0% Cr may be used subject to agreement by COMPANY.
7. Al : N ≥ 2:1 (not applicable for titanium killed steels).
8. (Nb + V + Ti)% maximum: 0.12%. This value may be increased to maximum 0.15% subject to agreement by
COMPANY.
9. The niobium content may be increased to 0.10% subject to agreement by COMPANY.
10. Intentional addition of Boron is not permitted unless otherwise agreed with COMPANY (30 ppm shall not be
exceeded in any case).

Mn Cr + Mo + V Cu + Ni
11. CE = C + + + .
6 5 15
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Si Mn + Cu + Cr Ni Mo V
Pcm = C + + + + + + 5 ⋅B
12. 30 20 60 15 10 .
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Table 6.6-2 - Chemical Composition of Seamless Steel Pipe(1, 2, 3)

Product analysis

Grade maximum weight %

X42 / L290 X52 / L360 X60 / L415 X65 / L450 X70 / L485

C (4) 0.14 0.14 0.14 0.15 0.16

Mn (4)
1.65 1.65 1.65 1.65 1.75

Si 0.40 0.45 0.45 0.45 0.45

P 0.020 0.020 0.020 0.020 0.020

S 0.010 0.010 0.010 0.010 0.010

Cu 0.35 0.50 0.50 0.50 0.50

Ni 0.30 0.50 0.50 0.50 0.50

Mo 0.10 0.50 0.50 0.50 0.50

Cr (5) 0.30 0.50 0.50 0.50 0.50

Al (total) (6)
0.06 0.06 0.06 0.06 0.06

Nb (7) 0.04 0.05 0.05 0.05 0.05

V (7) 0.04 0.07 0.08 0.09 0.10

Ti (7)
0.04 0.04 0.04 0.06 0.06

N (6) 0.010 0.010 0.010 0.010 0.010

B (8) 0.0005 0.0005 0.0005 0.0005 0.0005

t ≤ 15 0.34 0.37 0.39 0.41 0.40


CE (9)
15 < t < 26 0.35 0.38 0.40 0.42 0.41

t ≤ 15 0.20 0.21 0.22 0.24 0.23


Pcm (10)
15 < t < 26 0.21 0.22 0.23 0.25 0.24

Notes
1. The chemical composition shown applies for wall thicknesses up to 26 mm and shall be subject to agreement by
COMPANY for larger wall thicknesses.
2. When scrap material is being used in steel production, the amount of the following residual elements shall be
determined and reported, and the levels shall not exceed: 0.03% As, 0.01% Sb, 0.02% Sn, 0.01% Pb, 0.01% Bi
and 0.006% Ca.
3. Except for deoxidisation elements, other elements than those mentioned in this table shall not be intentionally
added if not specifically agreed with COMPANY.
4. For each reduction of 0.01% carbon below the maximum specified value, an increase of 0.05% manganese
above the specified maximum values is permitted with a maximum increase of 0.1%.
5. 0.5 - 1.0% Cr may be used subject to agreement by COMPANY.
6. Al : N ≥ 2:1 (not applicable for titanium killed steels).
7. (Nb + V + Ti)% maximum : 0.12%. This value may be increased to maximum 0.15% subject to agreement by
COMPANY.
8. Intentional addition of Boron is not permitted unless otherwise agreed with COMPANY (30 ppm shall not be
exceeded in any case).

Mn Cr + Mo + V Cu + Ni
9. CE = C + + + .
6 5 15
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Si Mn + Cu + Cr Ni Mo V
10. Pcm = C+ + + + + + 5 ⋅B
30 20 60 15 10 .

6.7 CHEMICAL ANALYSIS OF WELD OVERLAY

ADDITIONAL CLAUSE

A chemical analysis shall be made of the weld overlay on one of the specimens from (Section
7.12) or on another specimen prepared specially for this purpose.

The analysis shall be done by energy dispersive X-ray spectroscopy (or, alternatively, by light
optical emission spectroscopy, subject to approval by COMPANY) at a point located in the
middle of the overlay bead, approximately 1 mm below the surface. The analysis shall conform
with (Section 6.1). If overlay welding is done with more than one bead, each bead shall be
analysed separately.

As a minimum the analysis shall include Mn, Cr, Ni, Mo and Fe. The values measured shall be
consistent with a dilution of the filler metal composition by less than 25%. In the case of Alloy
625 overlay (UNS N06625), the iron content shall not exceed 5% at 2.5 mm from the base
metal interface unless otherwise agreed with COMPANY.

The dilution may be established either by a comparison of the alloy content of the weld deposit
against that shown on the welding consumable test certificate or by a direct measurement of
the combined thickness of the backing pipe and CRA layer.

Where a comparison of the alloy content is made, the values obtained from the deposit shall
not be less than 75% of the values shown on the welding consumable test certificate.

Where by a direct measurement of the combined thickness of the backing pipe and CRA layer,
the combined thickness of the backing pipe and CRA layer minus the original thickness of the
backing pipe (before the CRA layer was applied) shall be at least 75% of the total thickness of
the CRA layer (including the penetration into the backing pipe) as measured from a macro
specimen.

7 MECHANICAL PROPERTIES AND TESTS

7.1 MECHANICAL PROPERTIES (BACKING STEEL)

SUBSTITUTE

All mechanical tests shall be performed on specimens taken from backing pipe. The pipe shall
be in its final heat-treated condition and shall have been subjected to all hot or cold working
operations involved in the manufacture of the product of which it is representative (this shall
include any heat treatment required in the installation of a liner).

When tensile tests are made using flattened bar specimens, the ratio of body (base metal)
yield strength to tensile strength shall not exceed 0.90. When round bar or non-flattened
rectangular specimens are tested, the ratio of base metal yield strength to tensile strength
shall not exceed 0.93.

The measured yield strength shall not exceed the minimum specified value by more than 120
MPa, with a delta between maximum and minimum value not greater than 100 MPa.
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The minimum tensile elongation shall be not less than 20%.

Samples removed for the determination of tensile, toughness or microstructural properties


shall be prepared by machining. If thermal cutting is used to remove pipe coupons from which
test specimens are to be prepared, the full extent of the heat affected region shall be removed
during machining of the specimens.

7.2 TENSILE TESTS – GENERAL

SUBSTITUTE

The testing procedure shall be in accordance with ASTM A370.

7.3 TESTING FREQUENCY

SUBSTITUTE

Unless otherwise agreed with COMPANY and specified in the TDS, both longitudinal
andtransverse tensile tests shall be carried out.

Tests shall be performed on samples taken from two pipes per heat. Where a heat consists of
less than twenty pipes, tests shall only be required on samples taken from one pipe from the
heat.

7.5 TRANSVERSE TENSILE TESTS

SUBSTITUTE

Flattened rectangular specimens, from which the CRA layer has been removed, shall be used
to determine transverse tensile properties, unless otherwise agreed with COMPANY and
specified in the TDS. The ring expansion method shall not be used unless specific approval has
been obtained from COMPANY.

7.6 WELD TENSILE TESTS

SUBSTITUTE

Weld tensile specimens shall be taken from the same part of the pipe used for preparing
parent metal tensile specimens. The weld reinforcement shall be removed from both the inside
and outside surfaces of specimens before they are tested.

7.10 GUIDED BEND TEST

7.10.2 Guided Bend Test – Clad Pipe Only

SUBSTITUTE

Guided bend tests shall be performed on welded pipe in accordance with API Spec 5L. One side
bend test shall be made on the base material complete with the clad layer. In addition, in the
case of welded pipe, one transverse face and one transverse root bend test shall also be made
on the weld in accordance with ASTM A370.
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The minimum bending angle shall be 150° with a bend radius of 1.5•t, where t is the thickness
of the plate complete with the clad layer. Use of larger bend radius is subject to approval by
COMPANY.

A specimen shall have failed if it shows any disbondment or contains any open flaws exceeding
1.6 mm in length.

7.11 FRACTURE TOUGHNESS TESTS

SUBSTITUTE

In the case of both seamless and welded backing pipes, Charpy V-notch tests shall be
performed in accordance with (Annex H) on each test ring taken for tensile testing.

Where post weld heat treatment is to be carried out during installation of the pipe, a duplicate
set of Charpy V-notch tests shall be made on material in the simulated post weld heat treated
condition. Tests on pipe in the simulated post weld heat treated condition shall only be made if
instructed by COMPANY.

For gas transmission pipelines with a nominal outside diameter of 406.4 mm or greater, drop
weight tear tests shall also be carried out on one pipe from each heat. Tests shall be made in
accordance with (Annex H).

Crack tip opening displacement test of welded backing pipes shall be considered for MPQ if
specified in the purchase order.

7.12 METALLOGRAPHIC EXAMINATION

SUBSTITUTE

In the case of welded pipe, three metallographic test specimens shall be taken from each
longitudinal seam. The locations from which the specimens are removed shall be determined
by COMPANY. The testing frequency shall be that given in 7.3, unless otherwise agreed with
COMPANY and specified in the TDS.

Each specimen shall embrace the complete weld cross-section and shall include a minimum of
15 mm of unaffected parent material at each side of the weld. Specimens shall be polished and
etched to allow both macroscopic and microscopic examinations to be made.

Each specimen shall be assessed against the acceptance criteria in (Table 2).
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Table 2 - Acceptance Criteria

Feature Acceptance Criteria

Lack of fusion Not permitted(3)

Weld undercut on carbon steel and cladding 0.4 mm max.

Radial offset of plate edges at the longitudinal weld 1.5 mm max.

Maximum high-low across girth weld 1.5 mm max.

Weld bead centre-line alignment 0.15t, 3 mm max.

Weld bead height root penetration 2 mm max.


ID cap reinforcement permitted
Cap reinforcement
3.2 mm max.
Disruption in continuity in CRA layer Not permitted(3)

Minimum thickness of CRA layer(1) 2.8 mm

Cracking Not permitted(3)

Ferrite content of AISI 316L (UNS S31603) weld deposits(2) 5-13%

Ferrite content of duplex stainless steel weld metal(2) 35% to 65%

Sigma or other inter-metallic phases Not permitted(3)

Notes
1. The average thickness of the CRA layer shall be not less than 3.0 mm and the maximum thickness shall be not
greater than 4.0 mm.
2. The ferrite content shall be established by the point counting method (ASTM E562).
3. Not visible at micro-examination (minimum 200x magnification).

8 SPECIAL TESTS

8.2 CORROSION TESTING


a) Summary of test procedure.

ADD

In the case of Alloy 825 (LC 2242), intergranular testing shall be performed as per
ASTM A262 Practice C (Huey Test) on CRA layer and welds for both lined and clad
pipe. Specimens shall be tested without any preparation or cleaning to the internal
bore in order that coupons may be as representative as possible of the piece they
come from. Acceptance criteria for the CRA layer and welds shall be corrosion rate v
< 1 g/m²/h (= 40 mpy).

8.3 TESTS FOR CRA CLADDING BOND STRENGTH AND CRA LINER TIGHTNESS

AMEND

a) Clad steel pipe. Three transverse face bend tests shall be made in accordance with
ASTM A264 or ASTM A265 to verify the bond quality. In addition, three shear tests
shall be made in accordance with ASTM A264 or ASTM A265, except that the minimum
shear strength shall be 250 MPa. The test shall be carried out on one per 50 pipes
during the manufacturing process. Less than 50 pipes require one test, 50 plus one
pipes require 2 tests.
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Where tests are carried out on welded pipe, the location from which the test
specimens are taken shall be remote from the weld.

b) Lined steel pipe. The gripping force shall be measured using the residual compressive
stress test.

Four bi-axial strain gauges shall be placed on the inside surface of the CRA layer of a
250 mm long ring cut from the lined pipe. The CRA liner shall be taken out of the base
metal restriction by saw-cutting through the backing pipe. The change in hoop strains
and axial strains before and after take-out shall be measured and the bonding force
calculated as an average value. The test shall be carried out on one per 50 pipes
during the manufacturing process. Less than 50 pipes require one test, 50 plus one
pipes require 2 tests.

8.5 PITTING AND INTERGRANULAR CORROSION TEST

ADDITIONAL CLAUSE

During production, pitting corrosion test shall be carried out on CRA and SS weldments and
layer at a frequency of 1 per heat of CRA (or 1 per 100 pipes) in accordance with ASTM G48,
Method A. The complete specimen shall be pickled before being weighed and tested. Pickling
may be performed for 5 minutes at 60°C in a solution of 20% HNO3 + 5% HF. The test shall be
performed at a temperature of 50°C (for alloys 825 and 625), 25°C (for 316L stainless steel
layer) and 22°C (for 316L stainless steel weldments) for 24 hours. The acceptance criteria
shall be no pitting at 20X magnification and corrosion rate v < 4 g/m2/24 h (or 0.17 mm/y).

During production, intergranular corrosion test shall be carried out on weldments and CRA and
SS layer at a frequency of 1 per heat of CRA/SS (or 1 per 100 pipes) in accordance with ASTM
G28, Method A and ASTM A262 Practice C (for 316L stainless steel only). Specimens shall be
tested without any preparation or cleaning to the internal bore. The test shall be performed in
boiling solution for 120 hours. The acceptance criteria shall be corrosion rate v < 1.5 mm/y.

8.6 HIC/SWC TESTING

ADDITIONAL CLAUSE

HIC/SWC testing of backing material (and weld, for welded pipes) shall be considered as per
ISO 15156 / NACE MR0175 Part 2 clause 8 and Part 3 clause A.13.1. If the sulphur content of
backing material is within the maximum acceptable levels stated in ISO 15156 / NACE MR0175
Part 2 clause 8, the HIC/SWC test can be omitted if agreed with the COMPANY, otherwise
testing method and acceptance criteria are to be in accordance with Annex B of ISO 15156 /
NACE MR0175 Part 2.

8.7 SSC TESTING

ADDITIONAL CLAUSE

For the use in sour service environment, the backing material shall be fully compliant with ISO
15156 / NACE MR0175 after application of the cladding or overlay, unless differently specified
by the Company. In case SSC tests for the backing material are specified in the TDS, tests
shall be carried out as per ISO 15156 / NACE MR0175 Part 3 clause A.13.1 and Part 2 clause
7. Testing method and acceptance criteria are to be in accordance with Annex B of ISO 15156
/ NACE MR0175 Part 2. The test environment shall be Solution A as defined in NACE TM0177.
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9 HYDROSTATIC TESTS – INSPECTION HYDROSTATIC TEST

AMEND

9.1 Hydrostatic testing shall be in accordance with API 5L unless modified herein. Only fresh
water shall be used for the test and shall have a chloride ion content of less than 200
ppm (mg/kg) for Alloy 625 and less than 50 ppm (mg/kg) for other CRA materials. The
temperature of the water shall be not less than 5 °C.

AMEND

9.2 All pipes shall be hydrostatically tested after cladding or lining, and heat treatment and
shall be thoroughly cleaned to remove any contamination. The hydrostatic test shall be
carried out prior to the non-destructive testing required by (Section 11).

AMEND

9.4 The minimum holding time for all sizes shall be 15 seconds following stabilisation of the
pressure.

ADDITIONAL CLAUSE

9.6 After hydrostatic testing, pipes shall be dried and stored in such a way that they are kept
dry.

10 DIMENSIONS, WEIGHTS AND LENGTHS

10.1 DIMENSIONS AND WEIGHTS

SUBSTITUTE

Pipes shall be furnished in the outside diameters and wall thicknesses specified in the purchase
order. Where a specified nominal inside diameter is required, this will be indicated in the
purchase order and the outside diameter and/or wall thickness will be governed by this
requirement.

For the purpose of establishing compliance with dimensional tolerance requirements,


inspection shall be carried out on the pipe in its finished condition.

10.2 DIAMETER

SUBSTITUTE

The diameter shall be within the tolerances specified in (Table 6).

10.5 LENGTH

SUBSTITUTE

Unless otherwise agreed with COMPANY and specified in the purchase order, pipes shall be
supplied in lengths between 11.0 and 12.5 m and the minimum average length of each day’s
production shall be 11.9 m.
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Where the use of jointers has been approved by COMPANY, jointers shall be supplied in lengths
between 5.6 and 6.6 m. The minimum average length of the completed double joints of each
day’s production shall be 11.9 m.
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Table 6 − Tolerances on Dimensions

Outside / Inside Diameter Out-of-Roundness and Wall Thickness

Pipe Body - Outside Diameter Out-of-Roundness


Outside diameter measurements on the body of the pipe Each pipe on which diameter measurements have been
shall be at the mill using a diameter tape. Measurements made shall be checked for out-of-roundness.
shall be made on a random basis, but no less than three
measurements shall be made in every twenty pipes. The Pipe Body Out-of-Roundness
actual outside diameter shall not deviate from the The out-of-roundness of the pipe body shall be
specified nominal outside diameter by more than ±0.75 % determined by measuring the maximum and minimum
for seamless pipe; and +0.75 %, –0.25 % for welded pipe external diameter at a pipe cross-section.
with a maximum deviation from the nominal OD of ±3.0
mm or as specified in the purchase order. The maximum allowable out-of-roundness shall be given
by:
Pipe Ends - Inside Diameter
The inside diameter shall be checked on each of the pipes ODmax − ODmin and shall not exceed 1.5% of the nominal
on which outside diameter measurements have been outside diameter or 3.0 mm, whichever is the lesser or as
made. The inside diameter shall be checked at both ends specified in the purchase order.
of the pipe for a length of 100 mm from the pipe end and
shall not deviate from the nominal inside diameter by Measurements shall be made at three equidistant
more than ±1.0 %, except as noted below. locations along the pipe. In the case of welded pipe, non-
circularity at the position of the longitudinal weld shall be
In the case of seamless pipe, the maximum deviation from checked at the same three positions.
the nominal inside diameter shall not exceed ±2.0 mm
and, in the case of welded pipe, the maximum deviation Pipe Ends Out-of-Roundness
from the nominal inside diameter shall not exceed At the pipe ends the out-of-roundness shall be checked
±1.5mm or as specified in the purchase order. using an internal ring-gauge or as specified in the
purchase order. The outside diameter of the ring gauge
The nominal inside diameter shall be defined as the shall be 99% or 5.0 mm less than the nominal inside
nominal outside diameter, minus twice the nominal wall diameter of the pipe, whichever is the greater. The gauge
thickness of the backing pipe and CRA layer combined. shall be able to pass freely into each end of the pipe, for
a distance of at least 100 mm, when held normal to the
The inside diameter shall be measured using an internal pipe axis.
gauge or a measuring tape inside the pipe or as specified
in the purchase order. The method and equipment used Pipe Body and Ends
shall be subject to approval by COMPANY. For pipes with Any local irregularity of the inside surface shall be less
an outside diameter of 219.1 mm or smaller, the inside than 0.5 % of the outside diameter or 2 mm, whichever is
diameter may be calculated by taking the outside the lesser, and shall be measured using internal radius
diameter measurement and subtracting twice the actual gauge encompassing a 200mm length of arc or as
thickness of the pipe wall and CRA layer from this value. specified in the purchase order.

Pipe Wall Thickness:

Seamless Pipes - The actual pipe wall thickness shall


not vary from the nominal pipe wall thickness by more
than ±12.5% regardless of pipe size.

Welded Pipes - The actual pipe wall thickness shall be at


least 95% and not more than 110% of the nominal pipe
wall thickness or as specified in the purchase order.

Thickness of the CRA Layer


The thickness of the CRA layer shall be checked at four
equally spaced points around the circumference at each
end of the pipe or as specified in the purchase order.

The minimum thickness at any point shall be not less


than 2.8 mm and the average of the eight thickness
measurements shall be not less than 3.0 mm. The
maximum thickness at any point shall be not greater than
4.0 mm, unless agreed otherwise by COMPANY.
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10.6 STRAIGHTNESS

SUBSTITUTE

Every pipe shall be checked for straightness using a taut string or wire from end to end along
the side of the pipe. The maximum deviation from a straight line shall be 1.5 mm/m
(measured in any 1 m length of the pipe) and 12 mm total over a full length of pipe.

10.7 JOINTERS

ADD

Each finished pipe length shall be subject to a hydrotest as detailed in (Section 9). No
expansion shall be carried out after the circumferential weld has been completed.

10.8 PIPE ENDS

SUBSTITUTE

Unless specified otherwise by COMPANY, clad pipe shall be furnished with plain ends cut
perpendicular to the pipe axis. The ends of all lined pipe shall be seal-welded and shall be
prepared in accordance with a COMPANY approved procedure.

The maximum deviation from the perpendicular across the face at each end of the pipe shall
be 0.5% of the nominal outside diameter up to a maximum of 1.5 mm.

11 NON-DESTRUCTIVE INSPECTION

ADD

The Manufacturer shall demonstrate to COMPANY prior to the start of production that the NDT
techniques and procedures to be used are capable of identifying all of the surface and sub-
surface defects referred to in this Specification.

Measuring equipment for inspection and testing shall be selected such that it has a resolution
and accuracy at least five times better than the tolerance of the parameter being measured.
Similarly, the accuracy of standards against which a piece of equipment is calibrated shall be
at least five times better than the equipment being calibrated.Only measuring equipment
which can be demonstrated to have been previously calibrated satisfactorily and that is within
its documented calibration period shall be used for inspection and testing.

All NDT shall be performed by inspectors qualified to ISO 9712 level II or equivalent in the
relevant technique. Subject to approval by COMPANY, operators qualified to ISO 9712 level I
or equivalent may be used for certain activities provided that they are supervised by a level II
inspector. In the case of ultrasonic testing, an inspector qualified to ISO 9712 level III or
equivalent shall be responsible for the endorsement of relevant NDT procedures and
verification of the quality of NDT reports. The validity of equivalent qualifications shall be
determined by COMPANY.

If the documented calibration period will expire before the end of pipe production, then the
equipment shall be recalibrated at a suitable time, either before or during production, to
ensure that the calibration is valid throughout production.

All NDT shall be performed in accordance with written procedures approved by COMPANY.
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NDT for final acceptance shall be performed when the pipe is essentially complete, i.e. all heat
treatment and expansion operations shall have been done, and the pipe shall have been
hydrostatically tested. By agreement with COMPANY, NDT may be done on the pipe before it is
cut to length and bevelled.

By agreement with COMPANY, NDT of welded clad pipe body may be skipped if already carried
out on the clad plate prior to forming, in accordance with (Section 5.5.1). For pipe ends and
longitudinal weld, NDT is in any case required on the essentially complete pipe.

11.1 INSPECTION METHODS FOR WELDED CLAD PIPE

ADDITIONAL CLAUSE

11.1.4 The last 200 mm at both ends of the longitudinal weld seam shall be 100%
radiographed. Where the use of jointers has been approved by COMPANY, the
complete girth weld shall be 100% radiographed. Radiographic testing shall be
carried out in accordance with ASME Section V, Article 2 and (Section 11.5).

ADDITIONAL CLAUSE

11.1.5 The internal weld reinforcement shall be ground flush for a distance of 150 mm
from each end of the pipe and the resultant surface dye penetrant inspected in
accordance with ASTM E165. Any indications shall be removed by grinding and
the remaining thickness checked to verify that it is within the limits given in
(Section 10). If any indication of cracking is found, the pipe end shall be cut off
25 mm beyond the end of the crack and the longitudinal weld at the new pipe
end, ground and dye penetrant inspected as described above.

ADDITIONAL CLAUSE

11.1.6 The entire outside surface of the longitudinal seam in pipes used for the
manufacturing procedure qualification and pipes selected for production testing
shall be subject to 100% magnetic particle inspection in accordance with
(Section 11.7).

11.2 INSPECTION METHODS FOR SEAMLESS CLAD PIPE

ADD

The entire outside surface of the pipes used for the manufacturing procedure qualification and
pipes selected for production testing shall be subject to 100% magnetic particle inspection in
accordance with (Section 11.7).

11.3 INSPECTION METHODS FOR LINED PIPE

ADD

11.3.5 Each finished lined pipe shall be ultrasonically inspected along its entire length to
verify the continuity of the CRA liner. The pipe shall be scanned from the outside
and/or inside using a helical pattern which ensures that a minimum of 25% of
the outside/inside surface of the pipe is covered.

ADDITIONAL CLAUSE
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11.3.6 Where the liner is welded, the internal weld reinforcement shall be ground flush
for a distance of 100 mm from each end of the pipe and the resultant surface
together with the seal welds 100% dye penetrant inspected in accordance with
ASTM E165. Where the liner is seamless, the seal welds shall be 100% dye
penetrant inspected in accordance with ASTM E165. Any indications shall be
removed by grinding and the remaining thickness checked to verify that it is
within the limits given in Section 9.3.

In all cases where grinding is carried out to remove flaws that are disclosed by
NDT, the area of the weld that has been ground shall be subjected to additional
dye penetrant testing after the grinding operation.

11.3.7 Welded Backing Pipe

ADDITIONAL CLAUSE

a) Ultrasonic Testing. The entire length of the longitudinal seam in the backing pipe shall be
inspected for both longitudinal and transverse defects. Where automatic equipment is
used, inspection for longitudinal and transverse defects, including chevron cracking, shall
be carried out simultaneously. The end portions of the longitudinal weld seam that
cannot be tested automatically shall be tested manually.

All ultrasonic examinations shall be carried in accordance with (Section 11.6).

b) Radiographic Testing. The entire length of the longitudinal seam in the liner and the last
200 mm at both ends of the longitudinal weld seam in the backing pipe shall be 100%
radiographed.

Radiographic testing shall be carried out in accordance with ASME Section V, Article 2
and (Section 11.5).

c) Magnetic Particle Inspection. The entire outside surface of the longitudinal seam in pipes
used for the manufacturing procedure qualification and pipes selected for production
testing shall be subject to 100% magnetic particle inspection in accordance with (Section
11.7).

11.3.8 Seamless Backing Pipe

ADDITIONAL CLAUSE

a) Ultrasonic Testing. Each seamless backing pipe shall be 100% inspected along its entire
length for internal and external surface defects and for embedded longitudinal and
transverse defects. Where automatic equipment is used, inspection for longitudinal and
transverse defects shall be carried out simultaneously. The end portions of the pipe that
cannot be tested automatically shall be tested manually; the full circumference of pipe
ends shall be tested over the length of the untested portion plus a 25 mm overlap of the
automatically tested area.

In addition, each seamless backing pipe shall also be inspected for laminations. The pipe
shall be scanned from the outside surface using a helical pattern which ensures a
minimum of 25% of coverage.

b) Magnetic Particle Inspection. The entire outside surface of pipes used for the
manufacturing procedure qualification and pipes selected for production testing shall be
subject to 100% magnetic particle inspection in accordance with (Section 11.7).
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11.4 THICKNESS OF CLADDING OR LINING

ADD

a) Thickness of Cladding. Where possible, an ultrasonic inspection technique shall also


be used to determine the thickness of the CRA layer. The pipe shall be scanned using
a helical pattern which ensures that a minimum of 25% of the outside surface of the
pipe is covered.

Where it is not possible to determine the wall thickness of the CRA layer by ultrasonic
inspection, then an electromagnetic (inductive or adhesive force) method shall be
applied. Thickness measurements shall be from the inside pipe at 250 mm intervals
along its full length. The accuracy to which the thickness of the CRA layer can be
measured shall be 0.2 mm or better.

Alternative pattern of UT or electromagnetic thickness measurements may be adopted


subject to approval by COMPANY. If thickness of cladding has been already measured
on the plate, the measure on the finished pipe may be limited to both pipe ends only.
Testing procedure shall be subject to approval by COMPANY. For welded clad pipes,
the adopted procedure shall ensure that clad thickness close to both sides of the
longitudinal weld is also measured; the measurement shall be performed on at least 5
positions: 0 o’clock (left and right of the seam weld) and 3, 6 and 9 o’clock.

b) Thickness of Lining. Each finished lined pipe shall be ultrasonically inspected along
its entire length to verify the thickness of the backing pipe and the thickness of the
CRA liner. The pipe shall be scanned from the outside and/or inside using a helical
pattern which ensures that a minimum of 25% of the outside/inside surface of the
pipe is covered. The accuracy to which the thickness of the CRA layer is measured
shall be 0.2 mm or better.

ADDITIONAL CLAUSE

11.5 RADIOGRAPHIC INSPECTION – EQUIPMENT

ADDITIONAL CLAUSE

a) General. Each radiographic examination shall be made employing X-ray equipment and
using the film type indicated below:

- Speed: slow;
- Contrast: very high;
- Grain: very fine;
- Examples: Kodak Industrex M, Kodak Industrex TMX, Kodak Industrex T, Agfa D2,
Agfa D4, Fuji 50.

MANUFACTURER shall record on a review form accompanying the radiograph or within


the mill computer system, the interpretation of each radiograph and disposition of the
pipe inspected.

Radiographic examination shall not be used for pipe wall thicknesses in excess of 20 mm.
By agreement with COMPANY, higher threshold may be considered. Acceptance of pipes
with a wall thickness in excess of 20 mm (or agreed threshold) shall be based on
ultrasonic examination in accordance with (Section 11.6).
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b) Reference Standards. A wire type penetrameter in accordance with ISO 19232-1 shall be
used.

c) Acceptance Limits. The films shall be judged in accordance with ASME Section VIII,
Division 1, Paragraph UW 51 with the following additions:

- continuous or semi-continuous undercut on the inside or outside of the pipe may


not exceed a depth of 0.5 mm.
- any sharp or crack-like indication is unacceptable, regardless of depth.

d) Weld Repair. Defects detected during radiographic inspection of the weld shall be
rejected and shall be rectified in accordance with (Section 12.3.2).

11.6 ULTRASONIC AND ELECTROMAGNETIC INSPECTION

ADDITIONAL CLAUSE

a) General. MANUFACTURER shall demonstrate to COMPANY that the selected ultrasonic


techniques are capable of detecting the following defects in accordance with the
requirements of this Specification:

- disbondment between the CRA layer and the backing pipe;


- longitudinal and transverse defects in seamless pipe;
- longitudinal and transverse defects in the seam welds of welded clad pipe.
Project specific NDT procedure shall be submitted by MANUFACTURER and shall be
subject to approval by COMPANY. Production shall not start until NDT procedures are
agreed between COMPANY and MANUFACTURER.
b) Ultrasonic Equipment. Where ultrasonic inspection is feasible using an angle beam shear
wave technique, the entrance angles of shear wave probes shall be as follows:

SMLS pipe(1) 45°

SAW pipe - longitudinal defect detection(2) 50 - 70°

SAW pipe - transverse defect detection(1, 2) 45° on the weld bead. 50 - 70° for X or K transmission.

Notes
1. The probe angle may be between 40° and 48°.
2. Part of the completed weld will be austenitic and may have a relatively coarse grained microstructure
in comparison with the backing pipe. Consequently, the performance of conventional ultrasonic
examination using angle beam shear waves may be significantly reduced. Where a very poor signal to
noise ratio is obtained, the use of an angle beam compression wave or creep wave ultrasonic
examination technique should be considered.

The transducer arrangement shall be such that the sound intensity in both the
longitudinal and circumferential directions does not decrease by more than 3 dB at any
point in the pipe wall, when referred to the maximum sound intensity adjusted in the
static calibration.

Lamination testing may be performed in either the pulse echo or transmission mode.
Determination of the wall thickness shall only be made in the pulse echo mode. The
probe(s) used for lamination/wall thickness testing shall satisfy the following
requirements:
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- Twin crystal probes: the focal length shall be approximately 50% of the wall
thickness;
- Single crystal probes used in the pulse echo mode: the near surface resolution
shall be better than 25% of the wall thickness, measured at the primary reference
sensitivity level.

The detection of disbondment between the CRA layer and backing pipe may be
performed in the pulse echo or transmission mode. The probes used for detecting
disbondment in pulse echo shall satisfy the following requirements:

- Twin crystal probes: the focal length shall be equal to the position of the clad to
steel interface;
- Single crystal probes used in the pulse echo mode: the near surface resolution
shall be better than 25% of the wall thickness when testing from the outside
surface of the pipe or 50% of the thickness of the CRA layer when testing from the
inside surface of the pipe. All measurements shall be made at the primary
reference sensitivity level.

In order to demonstrate the effectiveness of the inspection procedures and to verify that
the equipment is functioning correctly, it shall be checked against an appropriate
reference standard as described in (Annex I) at least once every four hours and at the
beginning and end of a batch.

If a discrepancy of more than 3 dB is observed, then all of the pipes inspected since the
previous check shall be re-inspected. Proper functioning of the UT equipment and the
linearity of the electronic instrumentation shall be checked at least once every six months
and whenever an alteration is made to the equipment.

c) Automatic Ultrasonic Equipment. In addition to the requirements specified above,


automatic ultrasonic equipment shall incorporate the following:

i) A device that monitors the effectiveness of the coupling.

If a zero degrees compression wave probe is used to monitor coupling, or where a


through transmission technique is used for seamless pipe, it shall be assumed that
loss of coupling has occurred when the sensitivity (echo height) decreases by more
than 10 dB relative to the static calibration.

In the case of SAW pipe, where a through transmission technique is used, it shall be
assumed that loss of coupling has occurred when the signal drops below the
electronic noise plus 10 dB, at the position of the through transmission signal.

A clear acoustic warning system and an automatic paint spray system (or equivalent)
shall be activated when loss of coupling occurs.

ii) An automatic paint-spraying device, or equivalent system.

The system shall be activated when the received ultrasonic echo exceeds the preset
acceptance limit and shall operate without any interference from the operator.

If a defect is detected, a paint mark shall be applied to the pipe within 25 mm


advancement past the point at which the defect was detected. Alternative marking /
recording systems may also be acceptable subject to approval by COMPANY. The
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reset time for the system shall be less than the time required for the pipe to advance
25 mm in the scanning direction.

iii) In the case of welded pipe, an automatic seam tracking system, or equivalent
subject to approval by COMPANY, for correct positioning of the crystals/probes with
respect to the weld centre-line.

From each pipe under test, an automatic "on-line" record shall be made without operator
intervention. A summary record shall be made for each pipe. This shall include, as a
minimum, the pipe identification number, the time at which the test was carried out and
the examination results; where applicable it shall also include the results of any re-
examinations.

d) Electromagnetic Equipment. EMT methods such as eddy current testing (ECT) and
magnetic flux leakage (MFL) testing may be applied for surface defect and flaw detection
in seamless pipe.

Inspection of the backing pipe shall be carried out by MFL from the outside surface in
accordance with ASTM E570. The CRA layer shall be inspected by ECT from the inside
surface. In all cases, testing shall be performed using automatic equipment and shall
cover the entire surface of the pipe.

The end portions of the pipe that cannot be tested using an automatic EMT system shall
be tested manually using UT; the full circumference of pipe ends shall be tested over the
length of the untested portion plus a 25 mm overlap of the automatically tested area.
Manual UT shall be carried out in accordance with an approved procedure for manual
ultrasonic examination.

e) NDT Reference Standards. The reference calibration standard shall have the same
nominal diameter and wall thickness as the product being inspected and shall be of
sufficient length to permit calibration of ultrasonic inspection equipment at the speed to
be used in production. The reference standard shall also be of the same material type
and have the same surface finish and be in the same heat treatment condition as the
product to be inspected.

The reference standard shall be free from any discontinuities or other conditions that
could produce indications that might interfere with the detection of the reference
reflectors.

The reference standard shall contain the relevant notches and drilled holes shown in
(Annex I). MANUFACTURER may use a different type of reference reflector from that
shown in (Annex I), provided that he can demonstrate to COMPANY that the examination
is at least as sensitive as that prescribed in this Specification. In such cases,
MANUFACTURER shall obtain approval from COMPANY.

The primary reference sensitivity level shall be adjusted on the following reference
reflectors:
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Type of pipe
Type of examination
SMLS SAW

Lamination detection FBH 6.4 mm FBH 6.4 mm

Disbondment detection FBH 6.4 mm FBH 6.4 mm

Surface defect detection Notch N5 -

Defect detection - body and pipe ends Notch N5 -

RDH 3.2 mm
Defect detection - weld -
FBH 3.0 mm

Defect detection - plate end axial defect - Notch N5

All sensitivity adjustments shall be carried out dynamically.

Flat bottomed holes for detecting laminations shall be applied at the mid-wall position.
Flat bottomed holes for detecting disbondment shall be applied at the interface between
the CRA layer and the backing pipe.

f) Acceptance Limits. For all reference reflectors except for RDH 3.2 mm, the acceptance
sensitivity limit signal shall be equal to the primary reference sensitivity level, i.e. equal
to the height of the signal produced by the reference reflector. For the RDH 3.2 mm
reference reflector, the acceptance limit signal shall be 10 dB below the primary
reference sensitivity level.

Indications exceeding the acceptance limit signal are unacceptable, except for lamination
and disbonding examination, for which all indications exceeding the acceptance
sensitivity limit shall be evaluated in terms of dimensions.

When testing for laminations, any area where one or more discontinuities produce a
continuous total loss of back reflection, accompanied by continuous indications on the
same plane that cannot be encompassed within a 25 mm diameter circle, shall be
unacceptable. By agreement with COMPANY, evaluation of signal equal or exceeding the
above mentioned acceptance sensitivity limit can be based on API 5L / ISO 3183.

When testing for disbondment, both the frequency and extent of any indications shall be
considered. Any indication with an area greater than 30 mm2 shall be unacceptable;
alternative acceptance criteria based on indication dimensions and area may be agreed
with COMPANY. The acceptance limits for the number of indications in any given area of
the plate/pipe shall be in accordance with the Table below:

Location Maximum number of indications

Plate/Pipe Body:
locally per area of 1 m x 1 m 10
average per m2 5
Plate Edges/Pipe Ends None
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11.7 MAGNETIC PARTICLE INSPECTION

ADDITIONAL CLAUSE

a) Equipment. The equipment used for MT shall produce a magnetic field, transverse to the
defect orientation and shall be of sufficient intensity so as to indicate defects in the
external surfaces of the pipe.

MT shall be performed in accordance with the requirements of ASTM E709.

The surface to be examined and all adjacent areas within 25 mm shall be dry and free of
any dirt, grease or other extraneous matter that could interfere with the inspection.

b) Evaluation. An indication of an imperfection may be larger than the imperfection that


causes it; however, the size of the indication is the basis for acceptance evaluation.

Only indications with a dimension greater than 1.6 mm shall be considered relevant.

i) A linear indication is one having a length greater than three times the width.
ii) A rounded indication is one of circular or elliptical shape with a length equal to or less
than three times its width.
iii) Any questionable or doubtful indications shall be re-examined to determine whether
or not they are relevant.

MANUFACTURER shall mark each relevant indication and subsequently explore each
indication with respect to the depth of the imperfection.

c) Acceptance Limits. The pipe body and weld surfaces shall be free of:

i) Relevant linear indications;


ii) Relevant rounded indications greater than 4.8 mm;
iii) Four or more relevant rounded indications in a line separated by 1.6 mm or less,
edge to edge.

The surface of the weld bevel shall be free from any flaws that are visible to the naked
eye.

11.8 DYE PENETRANT INSPECTION

ADDITIONAL CLAUSE

a) General. PT shall be performed in accordance with the requirements of ASTM E165. The
surface to be examined and all adjacent areas within 25 mm shall be dry and free of any
dirt, grease or other extraneous matter that could interfere with the inspection.

b) Evaluation. An indication of an imperfection may be larger than the imperfection that


causes it; however, the size of the indication is the basis for acceptance evaluation.

Only indications with a dimension greater than 1.6 mm shall be considered relevant.

i) A linear indication is one having a length greater than three times the width.
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ii) A rounded indication is one of circular or elliptical shape with a length equal to or less
than three times its width.
iii) Any questionable or doubtful indications shall be re-examined to determine whether
or not they are relevant.

MANUFACTURER shall mark each relevant indication and subsequently explore each
indication with respect to the depth of the imperfection.

c) Acceptance Limits. The pipe body and weld surfaces shall be free of:

i) Relevant linear indications;


ii) Relevant rounded indications greater than 4.8 mm;
iii) Four or more relevant rounded indications in a line separated by 1.6 mm or less,
edge to edge.
The surface of the weld bevel shall be free from any flaws that are visible to the naked
eye.

12 WORKMANSHIP, VISUAL INSPECTION AND REPAIR OF DEFECTS

12.1 WORKMANSHIP

AMEND

The workmanship and defect requirements of API 5L, Section 9.10 and its subsections
(undercuts, arc burns, laminations, dents and other geometric deviations, hard spots and other
imperfections) shall apply where applicable.

ADD

Defects of the following types shall be considered poor workmanship. Pipes containing such
defects shall be rejected.

a) Dents. The pipe shall contain no dents greater than 6.35 mm measured as the gap
between the lowest point of the dent and a prolongation of the original contour of the
pipe. The length of the dent in any direction shall not exceed one half the diameter of the
pipe. All sharp gouges deeper than 1.0 mm and all cold formed dents with a sharp
bottom gouge shall be considered defects requiring rectification or rejection. Gouges may
be removed by grinding provided that the remaining wall thickness is within the limits
specified in (Table 6).

b) Offset of Plate Edges. The radial offset of plate edges (misalignment) for welded pipe
with a nominal wall thickness of 12.7 mm or less shall be no more than 1.6 mm. For pipe
with a nominal wall thickness greater than 12.7 mm, the maximum allowable radial
offset shall be 0.125•t or 2.4 mm, whichever is the smaller.

c) Out-of-Line Weld Bead. Out-of-line weld bead shall not be cause for rejection, provided
that complete penetration and complete fusion have been achieved as evidenced by non-
destructive examination.

d) Height of Outside and Inside Weld Beads. The maximum height of any weld bead shall be
3.2 mm regardless of wall thickness.
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The longitudinal weld reinforcement on the inside of the pipe shall be ground back to the
thickness of the cladding over a distance of minimum 100 mm from the pipe ends. The
weld reinforcement on the outside of the pipe shall be ground to the contour of the pipe
for a distance of minimum 300 mm from each end of the pipe. The pipe ends shall be
prepared as described above before hydrostatic testing is carried out.

Weld beads with a height in excess of 3.2 mm may be ground to within the acceptable
limit at the option of MANUFACTURER.

The height of the weld bead shall in no case come below a prolongation of the surface of
the pipe, except that contouring by grinding, otherwise covered in this Specification, shall
be permitted.

e) Grinding. Defects and flaws may be removed by grinding provided that the remaining
wall thickness is within the limits specified in (Table 6). The surface roughness, Ra, of the
pipe shall be a maximum of 12.5 µm (The surface roughness shall be defined by the
Centre Line Average (CLA) method as per ASME B46.1).

In all cases where grinding repairs are made as a result of defects or flaws that are
disclosed by NDT, the part of the pipe containing such repairs shall be subjected to
additional NDT using the same technique, and to MT and/or PT, after the grinding
operation.

f) CRA Layer. The CRA layer shall be inspected for continuity as described in (Sections 11.1,
11.2 and 11.3).

12.2 VISUAL INSPECTION

SUBSTITUTE

The complete surface of each finished pipe shall be examined both internally and externally in
accordance with ASME Section V Article 9 and shall be free of defects as defined in (Section
12.3). In the case of pipes with an inside diameter of 550 mm or larger, the inspector shall
pass through the bore of the pipe when performing his examination; if agreed with the
COMPANY, the pipe inside examination can be performed with an endoscope.

In the case of welded pipes, the ends of each pipe and two positions along its length shall be
checked for out-of-roundness at the position of the longitudinal weld using a template. For
pipes with an outside diameter of 406.4 mm or larger, the template shall have a minimum
chord length of 200 mm. For pipes with an outside diameter less than 406.4 mm, the template
shall have a chord length equal to at least 75% of the pipe diameter. The template profile shall
have a radius equal to the nominal outside radius of the pipe.

The template gauging surface shall have a cut-out to accommodate the weld bead of the pipe.
The cut-out shall be at the centre of the gauging surface and shall be no more than 5 mm
wider than the weld bead. Any local irregularity shall be measured by a calibrated taper gauge
inserted in any gap between the template and the pipe surface. The local irregularity shall not
exceed 1.6 mm, unless otherwise agreed with COMPANY and specified in the TDS.

12.3 DEFECTS AND DISBONDING

12.3.2 Repair of Defects

AMEND
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c) Weld Seam. There shall be no weld repairs in the longitudinal weld seam within 250
mm of the pipe ends.

ADD

The nature and extent of any NDT indication shall be established before a repair is performed
and, where necessary, complementary ultrasonic and/or radiographic inspections shall be
carried out to characterise the defect. Repair welding of seams containing cracks shall not be
permitted.

A maximum of three weld repairs may be carried out along a seam. No repair weld shall
exceed 5% of the total length of the seam and only one attempt at the repair shall be
permitted.

Weld repairs shall not be carried out after cold expansion or hydrostatic testing of a pipe,
unless repair welding is followed by re-hydrostatic test and re-final inspection.

Welding repair procedures shall be submitted to COMPANY for approval and shall be qualified.

12.3.3 Disbonded Areas

SUBSTITUTE

Disbondment is defined as a lack of bond between the base metal and CRA layer. Except in the
case of lined pipe, any disbondment shall be considered a defect. Disbonded areas are not
permitted within 50 mm of any of the edges to be longitudinally welded or within 100 mm of
any pipe end. In other areas of the clad plate the disbonded areas shall not exceed the limits
of (Section 11.6f).

13 MARKING

13.1 GENERAL

ADD

c) Paint markings shall be stencilled parallel with the main axis of the pipe and shall
begin within 400 - 600 mm from the pipe end.

d) Cold die stamping shall be carried out on the steel backing pipe only. There shall be no
cold die stamping on other parts of the pipe.

13.2 SEQUENCE OF MARKINGS

ADD i) In the case of pipes with a wall thickness of 10 mm or greater, the unique pipe
number shall be stamped on the end face/weld bevel at each end of the pipe using low
stress stamps. In the case of welded pipe, the pipe number shall be stamped
diametrically opposite the longitudinal weld seam.
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14 DOCUMENTATION

14.1 CERTIFICATION

AMEND

MANUFACTURER shall furnish COMPANY with a certificate of compliance containing the results
of all inspection and testing, as summarised in (Annex J).

Unless otherwise specified by COMPANY, the certificate shall comply with ISO 10474 Type 3.2.

TPI personnel engaged by COMPANY shall be allowed to access the manufacturing facilities and
to perform the inspections as per the agreed ITP. MANUFACTURER shall provide the necessary
assistance.

14.3 MANUFACTURING DATA BOOK

ADDITIONAL CLAUSE

MANUFACTURER shall prepare and maintain the data book throughout manufacturing,
comprising the following information:

- an index;
- the approved quality plan;
- the approved MPS;
- the manufacturing procedure qualification test results;
- approved WPS’s and their associated PQR’s;
- mill test certificates;
- pipe repair reports;
- welder and welding operator qualifications;
- NDT operator qualifications;
- deviation requests;
- tally lists (Section 13.6).

Only original or certified true copies of documents shall be included in the data book.

If COMPANY has been involved in monitoring production and/or inspection, then the
data book shall be completed by MANUFACTURER and approved by COMPANY before
the Inspection Release Note is issued. A copy of the Inspection Release Note shall be
included in the data book for later reference. The master copy of the data book shall
be retained by MANUFACTURER for at least 5 years after delivery. A copy of the signed
data book shall be submitted to COMPANY.
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14.4 TALLY LIST

ADDITIONAL CLAUSE

MANUFACTURER shall produce and maintain a tally list of all pipes. The list shall be available
both as a hard copy and in a spreadsheet format using standard commercial software
approved by COMPANY e.g. Dbase, Excel, etc.

The list shall identify against each pipe its unique pipe number, its individual length and
weight, its end dimensions and pipe body dimensions, its mill test certificate number, the heat
numbers of the backing pipe and CRA layer, the carbon equivalent of the backing pipe and
date of manufacture of the pipe.

15 PACKING AND HANDLING

ADDITIONAL CLAUSE

15.1 GENERAL
All pipes shall be cleaned, dried, packed, handled and transported so as to arrive at their
destination dry and without distortion or other damage.

All pipe surfaces shall be free of oil, grease, mill scale, dirt or any other substance that might
interfere with subsequent coating. Environmental contamination shall be avoided during
storage and shipping.

15.2 METHOD OF PACKING AND STORAGE


All pipes shall be packed and stored in accordance with a procedure approved by COMPANY.
MANUFACTURER shall fit caps over the ends of all pipes, such that damage to the weld bevel
and the ingress of moisture or dirt into the pipe is prevented. The use of plastic hookable end
caps with dessicant bags may be used upon agreement.

15.3 TRANSPORTATION AND HANDLING


During transportation, direct contact of the CRA layer with carbon steel (e.g. swarf, filings,
hooks etc.) shall be strictly prohibited.

The minimum requirements for transportation shall be as specified in the following


Recommended Practices:

- API RP 5LW for marine transportation;


- API RP 5L1 for railroad transportation.

Pipe handling by means of hooks in pipe ends shall not be permitted. Pipes transported by sea
shall not be shipped as deck cargo.

15.4 HOT-WORKING PRECAUTIONS


MANUFACTURER/CONTRACTOR shall advise COMPANY of any precautions that need to be
taken with regard to the maximum allowable temperature of the pipe during post weld heat
treatment or coating.

When specified in the purchase order that pipes are to be induction bent or hot-formed to
produce fittings, MANUFACTURER/CONTRACTOR shall advise COMPANY of any precautions that
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need to be taken with regard to the temperatures to be used during forming operations and/or
subsequent heat treatment.

15.5 DOCUMENTATION
Each shipment of pipe shall be accompanied by a packing list together with the relevant
documentation required by the purchase order.
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Annex B

Manufacturing Procedure Specification

SUBSTITUTE

MANUFACTURER shall provide a manufacturing procedure specification for review and approval
by COMPANY prior to the start of production. The MPS shall contain, as a minimum, the
following information:

a) Steel Supply. The MPS shall include the name of the steel maker and production plants
and shall provide details of the steel-making and casting techniques to be used, i.e.
- the steel making process; including rare earth additions, deoxidation and
desulphurisation practice, inclusion shape control method and the use of vacuum
degassing.
- the casting process, i.e. ingot or continuous casting, including casting speed,
tundish superheat, segregation and control measures.
- plate and strip manufacture; including slab reheating temperatures, start and
finish rolling temperatures and reduction ratios.

The MPS shall provide details of any heat treatments.

The MPS shall provide details chemical composition and shall include as a minimum:
- the target chemistry;
- the ranges for elements added intentionally;
- the maxima for each of the other elements specified in (Section 6).

b) CRA Supply. The MPS shall include the name of CRA maker and production plants and
shall provide details of the CRA-making and casting techniques to be used.

The MPS shall provide details of any heat treatments.

The MPS shall provide details chemical composition and shall include as a minimum:
- the target chemistry;
- the ranges for elements added intentionally;
- the maxima for each of the other elements specified in (Section 6).

c) Clad Steel Plate (if applicable). The MPS shall include the name of clad steel plate maker
and production plants, the method of plate production together with details of any
specialised cooling and/or heat treatment operations. It shall also include the NDT
methods and procedures to be used during manufacture and final inspection of the plate.

d) Pipe production. The MPS shall contain as a minimum details of the following:
- the material type and grade of the backing pipe and CRA layer;
- the principal operations involved in forming the pipe and applying or fitting the
CRA layer;
- any heat treatment operations and procedures involved in the manufacture of the
pipe and the final heat treatment condition of the backing pipe and CRA layer;
- the hydrostatic test procedure and acceptance criteria;
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- NDT procedures and acceptance criteria;


- repair procedures;
- pipe dimensions and tolerances;
- procedures used for packing, storage and shipment of the finished pipe,
- pickilng and passivation procedure.
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Annex C

Welding Procedure Qualification Requirements

SUBSTITUTE

a) Welding Procedure Specification. MANUFACTURER shall provide a separate WPS,


prepared in accordance with ASME Section IX, for each weld detail involved in the
manufacture of a pipe.

Each WPS shall include details of all the essential, supplementary essential and non-
essential variables listed in ASME Section IX for the relevant welding process(es).

Each WPS shall specify the brand name of each welding consumable and shall include a
sketch indicating the run sequence and state the heat input range in kJ/mm for each run
within the sequence.

In addition, in the case of a WPS involving the use of the SAW process, the WPS shall
also include the following information:

- the number of electrodes and polarity for each electrode;


- the welding current for each electrode;
- the welding voltage for each electrode;
- the electrode stick-out;
- the electrode separation;
- the number of weld passes;
- details of seam tracking system for both inside and outside welding and also the
method for checking the set up of the system;
- the limits on internal and external weld reinforcement.

In the case of repair welding procedures, a separate WPS shall be produced for each
repair method to be used. The WPS shall include as a minimum:

- the method by which the defect is to be removed;


- the method and extent of any NDT carried out to confirm that the defect has been
removed;
- sketches showing the profile of the excavation in both the transverse and
longitudinal directions.

b) Procedure Qualification Record. Each WPS shall be qualified in accordance with ASME
Section IX by a single PQR, i.e. a WPS shall not be qualified by two or more PQR’s to
cover the use of different welding processes or consumables. Repair welding procedures
shall be qualified by a PQR simulating the repair method.

Each welding procedure qualification shall be witnessed and endorsed by an independent


authority and/or COMPANY. Production welding shall not start until the relevant WPS and
associated PQR have been approved by COMPANY. WPQT may be run in parallel with
normal production only if agreed with COMPANY.

Unless otherwise agreed with COMPANY, each welding procedure qualification shall be
made using a full length test weld produced in accordance with the relevant
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manufacturing and welding procedure specifications. The welding procedure qualification


shall be tested, as detailed below, not less than 48 hours after the completion of the
weld:

1. Ultrasonic Examination. The complete weld shall be examined in accordance with


(Section 11.6).

2. Radiographic Examination. The complete weld shall be 100% radiographed in


accordance with (Section 11.5).

3. Dye Penetrant/Magnetic Particle Inspection. The complete weld shall be subject to


dye penetrant or magnetic particle inspection, as appropriate, from both the inside
and outside of the pipe in accordance with (Section 11.7 or 11.8), as applicable.

4. Tensile Tests. Two trans-weld tensile specimens shall be removed and tested in
accordance with ASME Section IX.

5. All-Weld Tensile Tests. One all-weld metal tensile specimen shall be removed and
tested in accordance with ASTM A370. The test results shall meet the minimum
specified requirements of the plate with regard to yield, tensile strength and
elongation.

6. Side Bends. Four side bend specimens shall be removed and tested in accordance
with ASME Section IX.

7. Fracture Toughness Testing. Four sets of Charpy V-notch impact specimens shall be
extracted and tested in accordance with (Annex H).

8. Macrographic, Micrographic and Hardness Testing. A specimen shall be removed from


the weld seam and subjected to a macro and micro examination (Section 7.12). A
hardness survey shall be carried out on a transverse weld macro-section as detailed
in (Section 7.13).

9. Chemical Analysis. Chemical analysis of the weld overlay shall be conducted in


accordance with (Section 6.7). The analysis shall meet the compositional
requirements of (Section 6).

c) Welder or Welding Operator Qualification. All welders and welding operators shall be
qualified in accordance with ASME Section IX or an equivalent internationally recognised
standard approved by COMPANY. Welder and welding operator qualifications shall be
witnessed and endorsed by an independent authority and/or COMPANY.
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Annex D

Manufacturing Procedure Qualification

SUBSTITUTE

D.1 GENERAL
Two of the completely finished pipes of each size from the first day's production shall be
selected at random for testing to verify that the submitted MPS results in fully acceptable pipe.
If more than one heat is used in the first day production pipes, at least two heats shall be
represented by the test pipes. At the discretion of COMPANY, COMPANY may make the
selection. For orders of less than 50 tonnes, first day production tests are not required.

MANUFACTURER shall provide COMPANY with a report giving the results of all of the tests
detailed below, together with photomacrographs of any weld cross-section, and
photomicrographs confirming the microstructure of the plate and seamless pipe. The report
shall be approved and countersigned by COMPANY.

If girth welding is used to produce double random length pipes, this girth weld shall be
included in the first day production test. The girth weld from one completed pipe shall be
tested.

In the event of a failure of any test during qualification, MANUFACTURER shall amend the MPS
as required and resubmit it to the COMPANY. Unless otherwise agreed with COMPANY,
MANUFACTURER shall repeat the full qualification testing.

MANUFACTURER shall make no changes to a successfully qualified MPS without prior approval
of COMPANY. Only after such approval has been obtained from COMPANY shall
MANUFACTURER re-qualify the MPS.

The pipes tested as above may be considered the test pipe(s) per heat or shift as required by
this Specification.

D.2 NON-DESTRUCTIVE TESTING


a) Visual Examination. All pipes shall be examined visually for dimensional tolerances and
for surface defects in accordance with (Sections 10 and 12) respectively.

b) Ultrasonic Examination. The weld seams of all pipes shall be examined by means of an
automatic ultrasonic scanning device in accordance with (Section 11.6) and shall meet
the requirements of therein.

c) Radiographic Examination. The weld seams of all pipes shall be radiographically


examined throughout their full length in accordance with (Section 11.5).

d) Dye Penetrant Check or Magnetic Particle Test. The weld seams of all clad pipes with an
outside diameter greater than or equal to 600 mm shall be subject to dye penetrant
inspection internally and magnetic particle inspection externally, along their full length.
For pipes with an outside diameter less than 600 mm, the full length of the weld seam
shall be subject to magnetic particle inspection externally and a length equivalent one
and a half times the outside diameter at each end of the pipe shall be subject to dye
penetrant inspection internally. Seamless pipes shall be subject to either dye penetrant
inspection or magnetic particle inspection over the entire outside surface of the pipe.

Dye penetrant checking shall be in accordance with ASTM E165 and magnetic particle
testing in accordance with ASTM E709.
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Any indications shall be evaluated against the relevant acceptance criteria specified in
(Sections 11.7 and 11.8), as appropriate. Any crack-like indications are unacceptable and
their cause shall be established and reported to COMPANY.

D.3 MECHANICAL TESTING


The mechanical properties of all pipes shall be tested as detailed below. The test results shall
meet the requirements for the specified grade and type of pipe.

a) Weld Seam. The weld seam of all selected welded pipes shall be physically tested as
specified in (Section 6). For SAW pipe, in addition, an all-weld metal tensile test shall be
made including the determination of tensile strength, yield strength and elongation. The
results of the all-weld metal tensile tests shall meet the minimum specified requirements
of the parent plate. For SAW pipe, in addition, weld impact tests shall be carried out in
accordance with (Annex H).

b) Pipe Material. Tensile tests shall be carried out on the two pipes made from each end of a
coiled skelp, or on two pipes made from different heats, except that for pipes with an
outside diameter greater than 219.1 mm, tensile tests shall be performed in both the
transverse and longitudinal directions.

c) Charpy Impact Tests. Tests shall be carried out on all selected pipes in accordance with
(Annex H). In addition, a full transition temperature curve shall be produced for each
pipe, showing the impact energy in Joules and percentage shear area plotted against
temperature over a temperature range that is sufficient to reproduce fracture appearance
from 10% to 100% fibrous shear.

d) Drop Weight Tear Test. For pipe to be used in gas transmission lines, drop weight tear
tests shall be carried out in accordance with (Annex H).

e) Crack Tip Opening Displacement. If the test is required in the purchase order, it shall be
carried out on all selected pipes in accordance with (Annex H).

D.4 MACROGRAPHIC, MICROGRAPHIC AND HARDNESS EXAMINATION


a) Longitudinally Welded Pipe. For SAW pipe, a specimen shall be extracted from one pipe
at three locations along the weld. Where tack welds are to be incorporated into the
finished weld, at least one specimen shall be removed from the location of a tack weld,
as specified in (Paragraph 4.4.b.2).

Each specimen shall be polished and etched to show the macro-structure of the weld
cross-section and shall include at least 25 mm of unaffected parent material adjacent to
each heat-affected zone.

Each specimen shall demonstrate that full fusion has been obtained throughout the
section thickness of the joint. Each specimen shall also show that the first and second
side welds are correctly aligned and there is adequate interpenetration.

A series of Vickers hardness tests using a 10 kg load shall be made on one of the etched
specimens selected by COMPANY. Each set of readings shall extend from unaffected base
metal on one side of the weld to unaffected base metal on the other side of the weld.
Three traverses shall be made, one 1 mm (-0/+0.5 mm) from the outer edge, the second
across the centre and the third 1 mm (-0/+0.5 mm) from the inner edge of the steel
pipe. The spacing between adjacent hardness indentations shall be a maximum of 0.75
mm. The location of hardness indentations are shown in (Figure D.1). The hardness
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indentations nearest the fusion line shall be within 0.5 mm of the fusion line. The
hardness indentations in the CRA liner shall be in accordance with API 5LD Figure 1.

Figure D1 − Location of indentations for longitudinal weld hardness survey

b) Seamless Pipe. Three specimens from one pipe shall be extracted from locations 120°
apart around the circumference from a position chosen by COMPANY. The specimens
shall be polished and etched to show the microstructure.

A hardness survey, as detailed in (Figure D.2), shall be made on one of the three
specimens selected by COMPANY. Three traverses shall be made, one 2 mm from the
outside surface of the pipe, one at the mid-section of the pipe wall and one in the
backing pipe 2 mm from the interface with the CRA layer. A minimum of twelve readings
shall be taken for each traverse. There shall be at least 5 mm between indentations. The
hardness indentations in the CRA liner shall be in accordance with API 5LD Figure 1.

Figure D2 − Location of indentations for hardness survey on seamless pipe

c) Acceptance Criteria. For sour service applications, the maximum hardness shall not
exceed the relevant limits specified within ISO 15156 / NACE MR0175 Part 2. For non
sour service applications, the hardness of the backing steel shall not exceed 325 HV10
and the hardness of the CRA shall not exceed the limits reported by API 5LD, Table 3.
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D.5 TEST FOR BONDING


The continuity of the bonding between the backing pipe and CRA layer shall be tested in
accordance with (Section 11.3.5).
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Annex H

Fracture Toughness Testing

ADDITIONAL CLAUSE

Fracture toughness testing shall be carried out in accordance with API 5L/ISO 3183 with the
following amendments:

H.1 FRACTURE TOUGHNESS TESTING (CHARPY V-NOTCH)


1. The fracture toughness of the pipes shall be determined by Charpy V-notch impact testing
in accordance with ASTM A370. The impact test temperature shall be lower than or equal to
that specified in the table below.

Nominal wall thickness Test temperature Maximum test temperature

mm °C °C

wt < 16.0 T 0

16.0 < wt < 25 T - 10 0

25 < wt ≤ 32 T - 20 0

wt > 32 T - 30 0

Note that T is the minimum design temperature, which should be specified in the purchase
order. If no minimum design temperature is indicated, then it shall be assumed to be 0°C.

2. Impact testing shall be carried out using 10 × 10, 10 × 7.5 or 10 × 5 mm cross-section


specimens. The largest possible specimen shall be used. Where the nominal pipe
dimensions are insufficient to extract a 10 × 5 mm specimen, impact testing is not required.

For pipes with an outside diameter of 273.1 mm or less, impact test specimens shall be
taken parallel to the axis of the pipe (i.e. longitudinal specimens shall be taken).

For pipes with an outside diameter greater than 273.1 mm, impact test specimens shall be
taken transverse to the axis of the pipe, except where the wall thickness prevents
extraction of a 10 × 5 mm specimen; where this is the case, longitudinal specimens shall be
taken.

For weld centre-line and HAZ impact tests, only transverse specimens shall be used.

3. One set of three specimens shall be taken from the mid-thickness location in the pipe wall
with the notch at the following positions (see Figure H.1):
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Seamless pipe -Pipe body


-Pipe body at 90° to the weld
-Weld centre-line

SAW pipe -Fusion line


-Fusion line + 2 mm
-Fusion line + 5 mm

Figure H1 − Location of Charpy V-notch specimens

4. The minimum absorbed energy requirements for full size (10 × 10 mm) specimens taken
transverse to the pipe axis are given in the table below.

Minimum average value Minimum Individual value


Grade
J J

X42 30 25

X46 32 27

X52 36 30

X56 39 32

X60 42 35

X65 45 38

For other specimen sizes and orientations, the values specified above shall be multiplied by
the following factors:

Size Orientation Factor

10 × 10 Longitudinal 1.5

10 × 7.5 Transverse 0.75

10 × 7.5 Longitudinal 1.125

10 × 5 Transverse 0.5

10 × 5 Longitudinal 7.5
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The percentage shear area at the fracture surface of the test specimens shall be recorded.
Each sample shall exhibit not less than 50% fibrous shear.

The Charpy test requirements specified are based on crack initiation principles. For gas
transmission and two-phase lines, different test temperature and higher absorbed energy
requirements may be specified to avoid the risk of running fractures. Where this is the case,
COMPANY shall specify the required values in the purchase order.

H.2 DROP WEIGHT TEAR TESTING OF WELDED PIPE


1. Drop weight tear tests shall be made on pipes with an outside diameter of 406.4 mm and
greater.

2. Two transverse DWTT specimens shall be taken from one length of pipe from each heat
supplied in the purchase order. The specimens shall be taken from a location 90° around
from the longitudinal seam. The specimens shall be taken from the backing steel with the
CRA layer machined off or removed.

Tests shall be carried out at the minimum design temperature unless otherwise agreed with
COMPANY and all specimens shall exhibit a minimum of 85% shear on the fracture surface.

3. In addition to the tests specified above, a full transition curve shall be produced for at least
one heat in every ten.

H.3 CRACK TIP OPENING DISPLACEMENT


1. Crack tip opening displacement test shall be performed on base metal, weld metal and heat
affected zone as required in the purchase order. The locations of the specimens shall be
indicated by COMPANY’s inspector.

2. The test temperature, the minimum acceptable values of CTOD and the specimen thickness
shall be as specified in the purchase order. The test should be performed at the minimum
design temperature on specimens having thickness equal to the maximum thickness that
can be obtained compatibly with pipe geometry.
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Annex I

Reference Standard Pipe/Plate for Inspection of Welds

ADDITIONAL CLAUSE

Transverse notch at outside, Type N5

Undercut notch at outside, Type N5 3 mm diameter flat bottom


hole (to simulate side wall lack of
fusion defects) (1)

Longitudinal weld seam Undercut notch at outside, Type N5


3 mm diameter flat bottom
hole (to simulate side wall lack of 3.2 mm diameter through thickness hole
fusion defects) (1)

Undercut notch at inside, Type N5

Transverse notch at inside, Type N5 Undercut notch at inside, Type N5

For all notches: Longitudinal notch at outside, Type N5


The length of the notch shall be at least
twice the width of the scanning head and
Longitudinal notch at inside, Type N5
the depth of the notch equal to 5% of the
scanning head

Additional 3.0 mm FBH references shall be considered if necessary to cover the complete weld configuration.
(1)

The location of each reference standard may be at MANUFACTURER’s discretion, provided that
no interference will occur.
Type of test Property Manufacturing procedure Production
and/or or qualification tests tests
inspection method component
eni spa

Frequency Remarks Frequency Remarks

100% coverage of external and 100% coverage of external


Surface defects All test pipes All pipes
Visual inspection internal surface. and internal surface.
(see Sections
5.5.1.a, 12.2 and Dimensions All test pipes As per (Section 10). All pipes
Annex D, Section Out-of-roundness All test pipes As per (Section 10). All pipes
D.2.a)
ADDITIONAL CLAUSE

2 pipes per
Pipe end squareness All test pipes As per (Section 10).
shift
Straightness All test pipes As per (Section 10). Random
100% coverage (there shall be 100% coverage (there shall be
no disbondment and/or no disbondment and/or
All
Clad plate All plates/skelp laminations within 50 mm laminations within 50 mm
plates/skelp
longitudinal and 100 mm longitudinal and 100 mm
transverse of the plate edges). transverse of the plate edges).
No disbondment and/or No disbondment and/or
Pipe ends All test pipes laminations allowed within 100 All pipes laminations allowed within
mm of the pipe ends. 100 mm of the pipe ends.

Welded pipe:
A 50 mm longitudinal and 100
Ultrasonic A 50 mm longitudinal and 100
mm transverse wide band
examination mm transverse wide band
All around the edge of the plate
(see Sections Plate/skelp All plates/skelp around the edge of the plate
plates/skelp shall be checked for
5.5.1.b, 11 and shall be checked for
disbondment and/or
Annex D, Section disbondment and/or laminations.
laminations.
D.2.b)
Weld seam All test pipes 100% of the weld. All pipes 100% of the weld.

100% coverage to check for


100% coverage to check for
disbondment and/or
Annex J - Summary of Testing and Inspection

disbondment and/or laminations.


laminations.
Seamless pipe All test pipes All pipes
25% coverage to check
25% coverage to check
thickness of the backing pipe
thickness of the backing pipe
and clad layer (if applicable).
and clad layer (if applicable).

The last 200 mm of the


Radiography Welded pipe - weld weld seam at each end of
(see Section 11, and All test pipes Full length. All pipes
seam the pipe shall be
Annex D, Section radiographed.
D.2.c)
Welded pipe - weld All weld
All weld repairs
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repair repairs
Type of test Property Manufacturing procedure Production
and/or or qualification tests tests
inspection method component
eni spa

Frequency Remarks Frequency Remarks

Only required (100%) Only required (100%)


MPI (1) and/or DPI Bevel faces All test pipes All pipes
when UT is impossible. when UT is impossible.
(see Sections 5.5.1.d,
11, and Annex D, (2) (2)
Weld seam All test pipes 100% of the weld . All selected pipes 100% of the weld .
Section D.2.d)
Seamless pipe body All test pipes 100% of the pipe. All selected pipes 100% of the pipe.
Electromagnetic
testing 250 mm intervals along 250 mm intervals along
Thickness of CRA layer All test pipes All pipes
(See Sections 5.5.1.c pipe full length (3). pipe full length (3).
and 11)
2 pipes per heat
Tensile test All test pipes Base metal only. (4) Base metal only.
2 pipes per heat
Cross-joint tensile test All test pipes (4)
All-weld metal tensile
All test pipes Not required
test
Charpy V-notch testing:
Backing pipe only - Backing pipe only -
2 pipes per heat
At test temperature All test pipes parent metal, weld (4) parent metal, weld
metal & HAZ. metal & HAZ.
Transition curve All test pipes Base metal only. Not required
Drop Weight Tear
Mechanical testing
Testing:
(See Sections 7, and At test temperature All test pipes Base metal only. All heats Base metal only.
Annex D, Section D.3) 1 pipe per 10
Transition curve 1 test pipe Base metal only. Base metal only.
heats
CTOD test of welded (5) Base metal, weld and
All test pipes Not required
pipes HAZ
2 pipes per heat
Guided bend test All test pipes (4)

Hardness test:
Backing pipe only - Backing pipe only -
Welded pipe All test pipes parent metal, weld All selected pipes parent metal, weld
metal & HAZ. metal & HAZ.
Seamless pipe All test pipes Backing pipe only. All selected pipes Backing pipe only.

Hydrostatic test
All test pipes All pipes
(see Section 9)

Ladle analysis All heats All heats


Chemical composition
(see Section 6) Backing pipe and CRA One pipe from Backing pipe and CRA
Product analysis All test pipes
layer. each lot layer.

Metallography Once per heat


(see Sections 7.12, and Welded pipe All test pipes (or as agreed
Annex D.4) with COMPANY)
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Rev. 3 July 2015
Type of test Property Manufacturing procedure Production
and/or or qualification tests tests
inspection method component
eni spa

Frequency Remarks Frequency Remarks


Base metal

3 transverse face bend 3 transverse face bend


CRA Cladding Bond
Clad pipe All test pipes and 3 shear tests (ASTM 1 every 50 pipes and 3 shear tests (ASTM
Strength and CRA
A264 or A265). A264 or A265).
Liner Tightness
(See Section 8.3)
Residual compressive Residual compressive
Lined pipe All test pipes 1 every 50 pipes
stress test. stress test.

1 per heat of CRA


Pitting corrosion test Base metal and, for
All test pipes ASTM G48, Method A or 1 per 100 ASTM G48, Method A
(See Section 8.5) welded pipes, weld.
pipes

Intergranular Base metal and, for All test pipes For Alloy 825, ASTM 1 per heat of CRA For Alloy 825, ASTM
corrosion test welded pipes, weld. A262 Practice C (Huey or 1 per 100 A262 Practice C (Huey
(See Section 8.2 and Test). pipes Test).
8.5)

ISO 15156 / NACE


HIC/SWC test Base metal and, for (6)
All test pipes MR0175 Part 2, Annex Not required
(See Section 8.6) welded pipes, weld.
B.

ISO 15156 / NACE


SSC test Base metal and, for (7)
All test pipes MR0175 Part 2, Annex Not required
(See Section 8.7) welded pipes, weld.
B.

(1)
Magnetic particle inspection is not applicable in relation to the CRA layer.
(2)
MPI for outside weld and DPI for inside weld.
(3)
May be limited to both ends of welded clad pipes if already performed on plates; procedure to be agreed with COMPANY; proximity of weld sides shall be
covered.
(4)
One pipe per heat if a heat consists of less than 20 pipes.
(5)
If required in the purchase order.
(6)
If S content of backing material is within the max. acceptable levels in clause 8 of ISO 15156 / NACE MR0175 Part 2, can be omitted if agreed with the
COMPANY.
(7)
Required in case SSC tests for the backing material are specified in the TDS.
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02949.MAT.COR.FUN
Rev. 3 July 2015
eni spa Sh. 65 of 65

Annex K

End Load Compensation for Hydrostatic Test Pressures

ADDITIONAL CLAUSE

(By agreement between COMPANY and MANUFACTURER the following method may be used to
determine the hydrostatic test pressure.)

K.1 As a measure to prevent distortion, MANUFACTURER may apply a calculation to


compensate for the forces applied to the pipe end that produce a compressive longitudinal
stress. The calculation in this annex is based on Barlow’s equation modified by a factor
based on the Maximum Shear Theory (see note). In no case shall the gauge pressure for
testing be less than that calculated using Barlow’s equation at 95% of specified minimum
yield strength.

Note: The calculation is an approximation of the effective hoop stress (SE), which is
practical for application under mill pipe testing conditions. Other calculations
provide closer approximations of the effective hoop stress but are complex and
therefore impractical for application.

K.2 The test pressure calculated shall be rounded to the nearest 100kPa.

K.3 The hydrostatic test pressure compensated for pipe end loading shall be calculated
according to the following equation:

SI Unit Equation:

PR ⋅ A R
SE −
AP
P1 = 1000 ⋅
D A
− 1
2 ⋅ t AP

where
A1 = internal cross-sectional area of pipe, mm2,
AP = cross-sectional area of pipe wall, mm2,
AR = cross-sectional area of ram, mm2,
P1 = hydrostatic test pressure in kPa,
PR = internal pressure on end-sealing ram in MPa,
SE = effective hoop stress in MPa equal to a percentage of the specified minimum yield
strength,
D = specified outside diameter, mm,
t = specified wall thickness, mm.

K.4 The above equation may be manipulated algebraically to provide calculation in other terms
appropriate to MANUFACTURER’s testing facility.

K.5 Appropriate techniques for the control of effective hoop stress based on measurements of
internal pipe and ram pressures vary according to hydrotester system design.
MANUFACTURER shall provide a control technique appropriate to his installation.

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