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3 FEB03
Method of Determining and Expressing Fineness of Feed
Materials by Sieving
S
T ASABE is a professional and technical organization, of members worldwide, who are dedicated to advancement of
engineering applicable to agricultural, food, and biological systems. ASABE Standards are consensus documents
developed and adopted by the American Society of Agricultural and Biological Engineers to meet standardization
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and water resource management, turf and landscape equipment, forest engineering, food and process engineering,
electric power applications, plant and animal environment, and waste management.
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ASABE, 2950 Niles Road, St. Joseph, MI 49085-9659, USA ph. 269-429-0300, fax 269-429-3852, hq@asabe.org
ANSI/ASAE S319.3 FEB03
Approved JUL 1997; reaffirmed FEB 2003 by American National Standards Institute
Proposed initially by a subcommittee of the American Feed 3.1 aperture size: Dimension defining an opening.
Manufacturers Association; approved by the ASAE Electric Power and 3.2 blinding: Obstruction of the apertures of a sieving medium by
Processing Division Technical Committee; adopted by ASAE December particles of material being sieved.
1968; reconfirmed December 1973, December 1978, December 1983;
revised March 1985; revised by the ASAE Food and Grain Processing 3.3 charge: A test sample, or part of a test sample, placed on a test
and Storage Committee; approved by the Food and Process Engineering sieve or a nest of test sieves.
Institute Standards Committee December 1989; revised editorially 3.4 cumulative oversize distribution curve: A curve obtained by
November 1990; reaffirmed December 1994, December 1995; revised plotting the total percentages by mass retained on each of a set of sieves
October 1996; approved as an American National Standard July 1997; of descending aperture size against the corresponding aperture sizes.
reaffirmed December 2001, February 2003; reaffirmed by ANSI February 3.5 cumulative undersize distribution curve: A curve obtained by
2003. Editorially revised March 2003. plotting the total percentages by mass passing each of a set of sieves of
descending aperture size against the corresponding aperture sizes.
1 Purpose and scope 3.6 dispersion agent: Non-toxic chemicals that help break up
agglomerates.
1.1 The purpose of this Standard is to define a test procedure to
determine the fineness of feed ingredients and to define a method of 3.7 end-point: The point in time after which further sieving fails to pass
expressing the particle size of the material. Surface area and number of an amount sufficient to change the result significantly.
particles per unit mass can be calculated from the determined particle 3.8 frame: A rigid framework that supports the sieving medium and limits
size. the spread of the material being sieved.
1.2 This Standard should be used to determine the fineness of feed 3.9 log-normal standard deviation: The standard deviation of the
ingredients where the reduction process yields particles which are logarithm of particle diameters in a log-normal size distribution curve
primarily spherical or cubical. It is not adequate to define the particle size (refer to equation 2).
of materials such as steamed and rolled grains, which are a flaked 3.10 median size: Particle diameter at 50% probability of a size
product, or products such as chopped hay where a substantial fraction distribution curve. Equivalent to geometric mean diameter (see equation
consists of elongated particles. 1).
1.3 This Standard is compatible with ISO 565, ISO 2395, ISO 2591-1, 3.11 nest of test sieves: A set of test sieves assembled together with
ISO 3310-1, and ISO 9276-1. a lid (cover) and a receiver (pan).
3.12 oversize: That portion of the charge that has not passed through
2 Normative references the apertures of a stated sieve.
The following standards contain provisions which, through references in 3.13 sample: A representative part taken from a quantity of material.
this text, constitute provisions of this Standard. At the time of publication,
3.14 sieving: The process of separating a mixture of particles according
the editions indicated were valid. All standards are subject to revision,
to their size by means of one or more sieves.
and parties to agreements based on this Standard are encouraged to
investigate the possibility of applying the most recent editions of the 3.15 size distribution curve: A graphical representation of the results of
standards indicated below. Standards organizations maintain registers of a size analysis.
currently valid standards. 3.16 test sieve: A sieve, intended for the particle size analysis of the
ASTM E11-95 Specification for Wire-Cloth Sieves for Testing Purposes material to be sieved, that conforms to a test sieve standard
ASTM D1921-89 Test Methods for Particle Size (Sieve Analysis) of specification.
Plastic Materials 3.17 undersize: That portion of the charge that has passed through the
ASTM D4749-87 Test Method for Performing the Sieve Analysis of Coal apertures of a stated sieve.
and Designating Coal Size 3.18 woven wire cloth: A sieving medium of wires that cross each other
ASTM D4570-86 Test Methods for Rubber Chemicals—Determination of to form the apertures.
Particle Size of Sulfur by Sieving (Dry)
ISO 565:1990 Test sieves—Metal wire cloth, perforated metal plate and 4 Test equipment
electroformed sheet—Nominal sizes of openings
4.1 A set of woven wire-cloth sieves having a frame diameter of either
ISO 2395:1990 Test sieves and test sieving—Vocabulary
200 mm (ISO 565) or 203 mm (8 in.) (ASTM Standard E11) are used.
ISO 2591-1:1988 Test sieving—Part 1: Methods using test sieves of
With the most common shaking equipment, sieves having a height of 25
woven wire cloth and perforated metal plate
mm (1 in.) or half-height sieves are most suitable to avoid the necessity
ISO 3310-1:1990 Test sieves—Technical requirements and testing—Part
of resieving the finer fraction. These sieves should consist of the aperture
1: Test sieves of metal wire cloth
sizes shown in table 1.
ISO 9276-1:1990 Representation of results of particle size analysis—Part
1: Graphical representation 4.2 A sieve shaker, such as a Tyler Ro-Tap1) or equivalent unit, is
required.
4.3 A balance that can weigh to an accuracy better than 0.1% of the
3 Definitions charge mass should be used.
The following is a list of the definitions for the terms related to this
Standard. Refer to ISO 2395 for more general terminology of test sieving. 1)
Registered trade name
冋 册
150 100 149 0.0059 100 Headley (1976) and Sokhansanj and Yang (1996), are as follows:
106 140 105 0.0041 150 n
兺
75 200 74 0.0029 200
53 270 53 0.0021 270 共 W i log d i 兲
i⫽1
Pan ⫺1
d gw ⫽log n (1)
兺 Wi
冋 册
i⫽1
n 1/2
4.4 Sieve agitators such as plastic or leather rings, or small rubber balls
may be required to break up agglomerates on finer sieves, usually those 兺
i⫽1
W i 共 log d i ⫺log d gw 兲 2
S ln
smaller than 300 mm in opening (ISO 3310-1) or US sieve No. 50. S log⫽ n ⫽ (2)
2.3
4.5 A dispersion agent2) should be used to facilitate sieving of high-fat or
similar materials.
兺
i⫽1
Wi
4.6 Sieve openings must be kept free of feed particles so that normal
sieving can be accomplished. A stiff bristle sieve cleaning brush, or 1
S gw ⬇ d gw 关 log⫺1 S log−(log⫺1 S log)−1] (3)
compressed air, is useful for cleaning sieves clogged due to blinding. 2
Sieves must be cleaned periodically to remove oil. Oil can be removed by where:
washing with water containing a detergent. Sieves must be dried before
use. di is nominal sieve aperture size of the i th sieve, mm
d i⫹1 is nominal sieve aperture size in next larger than ithsieve
(just above in a set), mm
5 Method of sieving d gw is geometric mean diameter or median size of particles
5.1 A charge of 100 g should be used, although larger or smaller by mass, mm, or
charges may be used if necessary. Extra care shall be taken to recover is geometric mean diameter or median size of particles
all material from the sieves when smaller charges are used. on ith sieve, mm, or
5.2 Place the charge on one sieve or the top sieve of the nest of test is (d i ⫻d i⫹1 ) 1/2
sieves and shake until the mass of material on any one sieve reaches S log is geometric standard deviation of log-normal distribution
end-point. End-point is decided by determining the mass on each sieve by mass in ten-based logarithm, dimensionless
at 1-min intervals after an initial sieving time of 10 min. If the mass on the
S ln is geometric standard deviation of log-normal distribution
smallest sieve containing any material changes by 0.1% or less of the
charge mass during a 1-min period, the sieving is considered complete. by mass in natural logarithm, dimensionless
For industrial applications, the end-point determination process can be S gw is geometric standard deviation of particle diameter by mass,
omitted, and the end-point is set to be the sieving time of 15 min. mm
Wi is mass on ith sieve, g
5.3 For hand-sieving, take the test sieve or nest of test sieves in one
hand, or cradle it in the crook of the arm if too heavy. Incline the sieve n is number of sieves +1 (pan)
(or the nest) at an angle of about 20° with the point at which the sieve S log can, in addition to equation 2, also be determined by graphical
is held in the lower position, and tap the sieve (or nest) approximately method as:
冉 冊 冉 冊
120 times a minute with the other hand. After tappings, return the test
sieve to a horizontal position, turn 90° and give a hard tap by hand d 84 d 50
S log⫽log ⫽log (4)
against the sieve frame. From time to time the sieve may also be shaken d 50 d 16
vertically.
5.4 Mass of material on all sieves should be determined and recorded. 1
S gw ⬇ 共 d 84 ⫺d 16 兲 (5)
5.5 If a dispersing agent is required, it should be added at a level of 2
0.5% relative to total charge mass, and its effect on particle size need not where:
be considered.
d 84 is particle diameter at 84% probability
2)
Dispersion agents include Cab-O-Sil MS available from the Cabot Corp., Boston; d 50 is particle diameter at 50% probability
Ziolex 23A and Zeofree 80 available from the J. M. Huber Corp., New York; and
Flo-Gard available from the Pittsburgh Plate Glass Co., St. Louis. d 16 is particle diameter at 16% probability
 sW t
冋 册 冉 冊
1/2 1/2
A st ⫽ exp共 4.5 ln2−ln gw 兲 (6) 兺 W i 共 log d i ⫺log d gw 兲 2 11.256
 v S log⫽ ⫽ ⫽0.341
兺 Wi 96.3
where:
A st is estimated total surface area of a charge, cm2 1 0.591 共 2.19⫺2.19 ⫺1 兲
S gw ⫽ d gw 关 log⫺1 S ln⫺ 共 log⫺1 S ln兲 ⫺1 兴 ⫽
 s is shape factor for calculating surface area of particles. Cubical, 2 2
 s ⫽ 6; Spherical,  s ⫽ ⫽0.512 mm
 v is shape factor for calculating volume of particles. Cubical,
 v ⫽ 1; Spherical,  v ⫽ /6 The geometric mean diameter (or median size) (d gw ) and log-normal
geometric standard deviation (S log) may also be obtained graphically by
is particle density of the material, g/cm3
plotting the summed percentages in table 2 (兺 P i , %<) on logarithmic
ln is log-normal geometric standard deviation of parent population probability paper in relation to particle diameter (figure 1). From figure 1,
by mass in natural logarithm, use S ln as an estimate
d gw ⫽d 50 ⫽0.59 mm
gw is geometric mean particle diameter of parent population by
mass, cm, use d gw as an estimate
(Note: gw is expressed in cm and d gw in mm)
S log⫽log 冉 冊 冉 冊 冉 冊 冉 冊
d 84
d 50
⫽log
1.3
0.59
⫽log
d 50
d 16
⫽log
0.59
0.26
⫽0.34
Table 2 – Typical data sheet used for tabulation of sieving data and calculation of log-normal particle size distribution parameters by mass
6.70 3 6.73
4.75 4 4.76 0.751
3.35 6 3.36 100.00 0.602
2.36 8 2.28 4.0 4.15 95.86 0.451 1.806 0.680 1.848
1.70 12 1.68 5.1 5.30 90.56 0.301 1.535 0.529 1.429
1.18 16 1.19 9.6 9.97 80.59 0.150 1.444 0.379 1.377
0.850 20 0.841 13.5 14.02 66.57 −0.000 −0.001 0.228 0.703
0.600 30 0.595 18.8 19.52 47.05 −0.152 −2.866 0.076 0.108
0.425 40 0.420 13.0 13.50 33.55 −0.303 −3.938 −0.075 0.072
0.300 50 0.297 11.6 12.05 21.50 −0.452 −5.243 −0.224 0.580
0.212 70 0.210 10.1 10.49 11.01 −0.603 −6.085 −0.374 1.414
0.150 100 0.149 6.6 6.85 4.16 −0.752 −4.965 −0.524 1.812
0.106 140 0.105 3.6 3.74 0.42 −0.903 −3.250 −0.675 1.638
0.075 200 0.074 0.4 0.42 0.00 −1.055 −0.422 −0.826 0.273
0.053 270 0.053 −1.203 0.000
0.045 pan 0.044 −1.356 0.000
1)
P i is equal to the mass of the particles on the i th sieve divided by the total charge mass.
Annex A
(informative)
Bibliography
The following documents are cited as reference sources used in
development of this Standard.
Pfost, H. and V. Headley. Methods of determining and expressing
particle size, in: Feed Manufacturing Technology. American Feed
Industry Council, Arlington, VA, pp. 512-517;1976.
Sokhansanj, S., and W. Yang. Revision of ASAE standard: ASAE
S319.2. Method of determining and expressing fineness of feed materials
by sieving. ASAE Paper No. 966002, St Joseph, MI 49085-9659; 1996.