Complete Technology Of Lubricating

Oils, Synthesis Of Lubricants Additives,

Re Refining Of Used Lubricating Oil,
Base Oil And Greases Manufacturing
With Formulations

Author: Dr. Himadri Panda

ISBN: 9788193563748
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COMPLETE TECHNOLOGY OF LUBRICATING OILS, SYNTHESIS OF LUBRICANTS ADDITIVES,

RE-REFINING
REFINING OF USED LUBRICATING OIL, BASE OIL AND GREASES MANUFACTURING
MANUFACT WITH
FORMULATIONS

The book Complete Technology of Lubricating Oils, Synthesis of Lubricants Additives, Re-Refining of
used Lubricating Oil, Base Oil and Greases Manufacturing with Formulations covers Manufacture of
Products, Extra Temperature Lubricating Grease, Synthesis of Lubricant’s Additives, Calcium Base
Grease, Re Refining of used lubricating oil , Food Grade Grease or Lubricant, Lubricant Base Oil
Hydrotreatment Process, Lubrication in wire drawing, Wire Drawing Lubricants, Copper Wire Drawing
Lubricant, Applications of Lubricants, Production of Various Greases, Production of Lithium and Sodium
Lubricating Greases, Bio alkali Grease Manufacture, Grease Manufacturing with formulae, Production of
grease from used lubricant, Molybdenum Based Lubricant Formulations/Paterns of Molybdenum Based
Lubricant Molybdenum Compounds, Manufacture of High Temperature Grease from Waste Lubricant
sludge and Silicone Oil , Multipurpose Lubricating Grease from Vegetable Residual Oils, Rust Prevention
Lubricating Oils, Long Life Grease manufacture, Lithium complex Grease, Silicon Grease, Teflon Grease,
Grease Chemistry

MANUFACTURE OF PRODUCTS

 Raw materials
 Steps in the prodution process of Lube oil
 Atmospheric distillation
 Vacuum distillation
 Deasphalting
 Solvent extraction
 Dewaxing
 Hydrogenation

EXTRA TEMPERATURE LUBRICATING GREASE

 Manufacturing Process for extra high tempt.

 Grease (25000-3000oC)
 As per Formulation No.1

SYNTHESIS OF LUBRICANT'S ADDITIVES

 Lubricants
 Additives
 Overbased detergent
 Antioxidants
 Pyrazole
 Pyranopyrazoles
 Chromene
 2-Amino-3-cycano-4 aryl-7.7-dimethyl
 5,6,7,8 tetrahydro chromene
 Materials
 Instrumentation
 Test methods
 Experimental Methods
 Formulation of oil blends

CALCIUM BASE GREASE

 Formulations of Calcium Base Grease

RE REFINING OF USED LUBRICATING OIL

 Combustion products
 Abrasives
 Chemical products

FOOD GRADE GREASE OR LUBRICANT

 Formulations of Food Grade Grease

 Manufacturing Process

LUBRICANT BASE OIL HYDROTREATMENT PROCESS

 Introduction
 HDT-lub is Approached on three levels
 The Hdt-lub Process
 Compositional Model And Reaction Network
 Hdt lub Modeling
 Economic Objective

LUBRICATION IN WIRE DRAWING

 Mechanical properties
 Drawing dies

WIRE DRAWING LUBRICANTS

 Technology
 Process of Manufacture

COPPER WIRE DRAWING LUBRICANT

 Introduction
 Experimental Procedures
 Mixture Analysis and Results

APPLICATIONS OF LUBRICANTS

PRODUCTION OF VARIOUS GREASES

 Introduction
 Batch process Continuous process
 Base Oil
 Effect of Base Oil on Grease Properties
 Soap Based Grease
 Lithium Grease
 Calcium Grease
 Sodium Grease
 Aluminium Grease
 Non-soap Based Grease
 Polyurea Grease
  Organo clay
 Function
 Functions of Lubricating Grease
 High temperature Effects
 Low temperature Effects
 Properties of Grease
 Physical Properties
 Manufacturing Process
 Steps Involved During Batch Process
 Continuous Process
 Process Selection
 Advantages of Batch Process
 Lithium Based Grease
 Factors Affecting Quality of Grease

PRODUCTION OF LITHIUM AND SODIUM

 Lubricating Greases
 Introduction
 Sodium and lithium greases properties
 Lithium and sodium greases
 Production Process

BIO ALKALI GREASE MANUFACTURE

 Background of the study

 Consistency
 Grease Manufacturing Methods
 Prospect of Using Plantain Peel Ash as the Source of Alkali
 The plantain
 Potassium Hydroxide
 Bio-Alkali
 Materials and Methods
 Lubricating Grease Formulation
 Testing
 Design of Experiment
 Production of NLGI grease from Bio alkali and Sodium hydroxide
 Consistency Test (Un-Worked and Worked Penetration)
 Dropping Point Test

GREASE MANUFACTURING WITH FORMULAE

 Manufacturing Process (For Grease (Petroleum Base)

 Formulation of Greases
 Lithium Based Grease
 Sodium Based Grease
 Silicone Based Grease

PRODUCTION OF GREASE FROM USED LUBRICANT

 Manufacturing Process
 Introduction
  Problem Statement
 Grease Background
 Function
 Grease Characteristics
 Fluid Lubricants
 Soap Thickeners
 Additives
 Grease Application Guide
 Introduction
 Overall Methodology
 Experimental Methodology

MOLYBODENUM BASED LUBRICANT FORMULATIONS/PATERNS OF MOLYBDENUM BASED

UBRICANT
MOLYBDENUM COMPOUNDS

 Over based complexes

 Manufacturing Process for Lubricants
 Manufacture of High Temperature Grease from Waste Lubricant Sludge and Silicone Oil
 Introduction
 Materials and Methods
 Results and Discussion
 Effect of mixing time on grease characteristics

MULTIPURPOSE LUBRICATING GREASES FROM VEGETABLE RESIDUAL OILS

 Introduction
 Experimental
 Preparation of Lithium Stearate/Oleate Soaps
 Additives
 Apparatus
 Synthesis of Greases
 Mechanical and Physico Chemical Characterization
 Toxicity
 Results and Discussion
 Formulations with Jatropha Residual Oil

RUST PREVENTION LUBRICATING OILS

 Formulation of Rust Prevntion Lubricating Oil

 Manufacturing Process of Rust Prevenjation Lubricating Oil

LONG LIFE GREASE MANUFACTURE

 Introduction
 Mechanism of oxidative deterioration
 Natural antioxides
 Weight decrease of greases at higher temperature
 Application of natural antioxidants to lubricating grease
 High temperature grease life
 Difference in effect with varied amount of addition
 Noise reduction characteristics
  Running torque
 Decreased bearing running torque by reduction in amount of grease prefill

LITHIUM COMPLEX GREASE

 Experimental
 Materials
 Grease preparation-open kettle process
 Grease manufacturing comparison
 Performance testing
 Grease characteristics
 High temperature testing
 Oxidation resistance
 Low temperaure testing
 ASTM D4693
 Grease mobility
 Lincoin Ventmeter
 Finished grease performance
 Evaluation by ASTM D4950

SILICON GREASE

 Manufacturing Process of Silicone Grease Using (1A) Thickener

 Preparation of Chromium Methyl Phenyl
 Phosphinate Dioxtyl Phosphinat Thickener

TEFLON GREASE

 Formulations of Teflon Grease

 Manufacturing Process

GREASE CHEMISTRY

 The Fundamental Grease Formulation

 Mineral Oils
 Synthetic Fluids
 Polyalphaolefin (PAO)
 Esters
 Polyglycols
 Polyethers
 The Thickener
 Metal Soaps
 Advanced Soaps
 Development of Technology

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