Operator Name: UFAM Report Date: 09/04/2018 16:11:00

Results File: C:\SOLAARM\DATA\TESTES forno.slr

General Parameters
Method : análise jessica Operator : UFAM Instrument Mode: Flame
Autosampler : None Dilution: None
Use SFI: No

Analysis Details
Analysis Name: Analysis 38 26/03/2018 Spectrometer: iCE 3000 C113500107 v1,30
Operator Name: UFAM

Current OQ Test Result: Fail Current PQ Test Result: Pass

Sample Details
Nominal Mass: 1,0000
No. Sample Id Sample Mass Dilution Ratio
1 sódio A 1,0000 1,0000
2 sódio B 1,0000 1,0000
3 sódio D 1,0000 1,0000
4 KA 1,0000 1,0000
5 KB 1,0000 1,0000
6 KD 1,0000 1,0000

Spectrometer Parameters - Na
Element: Na Measurement Mode: Absorbance
Wavelength: 589,0nm Bandpass: 0,2nm Lamp Current: 75%
Background Correction: Off High Resolution: Off Optimise Spectrometer Parameters: No
Signal Type: Continuous Resamples: Fast Number Of Resamples: 3
Measurement Time: 4,0secs Flier Mode: No
Use RSD Test: No

Flame Parameters - Na
Flame Type: Air-C2H2 Fuel Flow: 1,1L/min Auxilary Oxidant: Off
Nebuliser Uptake: 4secs Burner Stabilisation: 0mins Optimise Fuel Flow: No
Burner Height: 7,0mm Optimise Burner Height: No

Sampling Parameters - Na
Sampling: None
Calibration Parameters - Na
Calibration Mode: Off

Solution Results - Na
Sample ID Signal Rsd Auto Dilution
Abs %
Na sódio A 0,146 0,5 1,000
Na sódio B 0,112 2,1 1,000
Na sódio D 0,071 4,3 1,000

Spectrometer Parameters - K
Element: K Measurement Mode: Absorbance
Wavelength: 766,5nm Bandpass: 0,5nm Lamp Current: 100%
Background Correction: Off High Resolution: Off Optimise Spectrometer Parameters: No
Signal Type: Continuous Resamples: Fast Number Of Resamples: 3
Measurement Time: 4,0secs Flier Mode: No
Use RSD Test: No

Flame Parameters - K
Flame Type: Air-C2H2 Fuel Flow: 1,2L/min Auxilary Oxidant: Off
Nebuliser Uptake: 4secs Burner Stabilisation: 0mins Optimise Fuel Flow: No
Burner Height: 7,0mm Optimise Burner Height: No

Sampling Parameters - K
Sampling: None
Calibration Parameters - K
Calibration Mode: Off

Solution Results - K
Sample ID Signal Rsd Auto Dilution
Abs %
KKA 0,560 0,3 1,000
KKB 0,532 0,7 1,000
KKD 0,564 0,8 1,000

SOLAAR Data Station V11,03 Page 1 - Results