OFOTO TIO2 0.3 Y REPLICA.

uqnd

Peak method No base (1 wavelength)

1.6
Peak wavelength 273 nm
1.5 Graph type Linear

Y=A*X +B
A = 0.0522649 +/- 0.00102821
B = -0.00999657 +/- 0.0175588
Correlation coefficient = 0.999806
Determination coefficient = 0.999612
Standard error = 0.229638
Min. detectable = 0.335959
1 Quantification limit = 5.13662

Abs.

0.5

0
0 10 20 30
Concentration [ppm]

Quantitation method Instrument name ESPECTROFOTOMETRO V-730

Description Model name V-730
Creator Serial No. A074261798
Division
Company UNIVERSIDAD DEL VALLE Accessory USE-753
Comment Accessory S/N 074261798
Cell
Creation date 08/02/2018 04:44 p.m. Ref. beam
Date modified 08/02/2018 04:47 p.m.

No. Sample Comment Conc. [ppm]Abs 273.0 nm

*Blank 0.0002
*1 3 ppm de Cafeina 3 0.140982 0.1410
*2 5 ppm de Cafeina 5 0.241483 0.2415
*3 15 ppm de Cafeina 15 0.768206 0.7682
*4 20 ppm de Cafeina 20 1.04453 1.0445
*5 25 ppm de Cafeina 25 1.30082 1.3008
*6 30 ppm de Cafeina 30 1.55006 1.5501
*7 10 ppm de Cafeina 10 0.509102 0.5091
*8 7 ppm de Cafeina 7 0.375315 0.3753
Name Instrument name ESPECTROFOTOMETRO V-730
User Model name V-730
Division Serial No. A074261798
Company UNIVERSIDAD DEL VALLE
Comment Accessory USE-753
Accessory S/N 074261798
Creation Date 15/02/2018 05:46 p.m. Cell
Ref. beam

Bandwidth 1.0 nm
Response 0.96 sec
Change source at 340 nm
Light source D2/WI
Dark correction Off

No. Mode Sample

Comment Conc. [ppm]Conc.(Lower)
Conc.(Upper)
Abs 273.0 nm
1 Blank-1 -0.0007
2 Blank-2 0.0002
3 Sample-1 0.319024-0.0172194 0.644383 0.0066772 0.0067
4 Sample-2 10.2727 10.0726 10.4697 0.526906 0.5269
5 Sample-3 50 min only O rpm 1200 1.93654 1.62704 2.2364 0.0912163 0.0912
6 Sample-4 35 min only O rpm 1200 2.29996 1.99633 2.59425 0.110211 0.1102
7 Sample-5 30 min only O rpm 1200 1.75336 1.44089 2.05606 0.0816427 0.0816
8 Sample-6 25 min only O rpm 1200 2.05904 1.75152 2.35702 0.097619 0.0976
9 Sample-7 20 min only O rpm 1200 2.17076 1.86504 2.46702 0.103458 0.1035
10 Sample-8 15 min only O rpm 1200 5.0878 4.82669 5.34171 0.255917 0.2559
11 Sample-9 5 min only O rpm 1200 21.8716 21.6407 22.1083 1.13312 1.1331
12Sample-10 10 min only O rpm 1200 12.5403 12.3546 12.7246 0.645422 0.6454
13 Sample-11 40 min only O rpm 1200 2.02663 1.71859 2.32511 0.0959251 0.0959
14Sample-12 0 min only O rpm 1200 30.7911 30.4269 31.168 1.5993 1.5993
15Sample-13 50 min only O rpm 900 7.09916 6.86524 7.32745 0.361041 0.3610
16Sample-14 40 min only O rpm 900 12.0062 11.818 12.1926 0.617506 0.6175
17Sample-15 35 min only O rpm 900 14.6463 14.465 14.8279 0.755493 0.7555
18Sample-16 30 min only O rpm 900 17.393 17.2033 17.5851 0.899049 0.8990
19Sample-17 25 min only O rpm 900 20.8012 20.5826 21.0249 1.07718 1.0772
20Sample-18 20 min only O rpm 900 23.1339 22.8871 23.3876 1.1991 1.1991
21Sample-19 15 min only O rpm 900 25.5334 25.2529 25.8225 1.3245 1.3245
22Sample-20 10 min only O rpm 900 28.3652 28.0409 28.7004 1.47251 1.4725
23Sample-21 5 min only O rpm 900 30.2914 29.9356 30.6595 1.57318 1.5732
24Sample-22 0 min only O rpm 900 31.4597 31.0842 31.8483 1.63424 1.6342
25 Blank-3 0.0394
26 Blank-4 0.0006
27Sample-23 50 min OCTIO2 0.3 gL 900 rpm 2.00189 1.69345 2.30075 0.094632 0.0946
28Sample-24 40 min OCTIO2 0.3 gL 900 rpm 1.73548 1.42272 2.03846 0.0807084 0.0807
29Sample-25 35 min OCTIO2 0.3 gL 900 rpm 1.31615 0.996518 1.62567 0.0587918 0.0588
30Sample-26 30 min OCTIO2 0.3 gL 900 rpm 1.33293 1.01358 1.64219 0.0596689 0.0597
31Sample-27 25 min OCTIO2 0.3 gL 900 rpm 1.61035 1.29555 1.91527 0.0741682 0.0742
32Sample-28 20 min OCTIO2 0.3 gL 900 rpm 2.66254 2.36468 2.95133 0.129161 0.1292
33Sample-29 15 min OCTIO2 0.3 gL 900 rpm 6.57563 6.33499 6.81024 0.333678 0.3337
34Sample-30 10 min OCTIO2 0.3 gL 900 rpm 13.1523 12.9689 13.3348 0.677408 0.6774
35Sample-31 5 min OCTIO2 0.3 gL 900 rpm 21.0942 20.8724 21.3213 1.09249 1.0925
36Sample-32 inicial min OCTIO2 0.3 gL 900 rpm 30.5153 30.1558 30.8874 1.58489 1.5849
37Sample-33 50 min OCTIO2 0.3 gL 1200 rpm 2.10377 1.79698 2.40106 0.0999569 0.1000
38Sample-34 40 min OCTIO2 0.3 gL 1200 rpm 1.78617 1.47423 2.08835 0.0833573 0.0834
39Sample-35 35 min OCTIO2 0.3 gL 1200 rpm -0.584365 -0.935963 -0.24435-0.0405383 -0.0405
No. Mode Sample
Comment Conc. [ppm]Conc.(Lower)
Conc.(Upper)
Abs 273.0 nm
40Sample-36 35R min OCTIO2 0.3 gL 1200 rpm 1.64866 1.33448 1.95298 0.0761705 0.0762
41Sample-37 30 min OCTIO2 0.3 gL 1200 rpm 1.5702 1.25474 1.87575 0.07207 0.0721
42Sample-38 25 min OCTIO2 0.3 gL 1200 rpm 2.00762 1.69927 2.30639 0.0949315 0.0949
43Sample-39 20 min OCTIO2 0.3 gL 1200 rpm 2.32255 2.01927 2.61649 0.111391 0.1114
44Sample-40 15 min OCTIO2 0.3 gL 1200 rpm 2.46525 2.16426 2.75703 0.11885 0.1188
45Sample-41 10 min OCTIO2 0.3 gL 1200 rpm 5.29725 5.03913 5.54833 0.266864 0.2669
46Sample-42 5 min OCTIO2 0.3 gL 1200 rpm 13.8444 13.6625 14.0259 0.713582 0.7136
47Sample-43 inicial min OCTIO2 0.3 gL 1200 rpm 32.0975 31.7112 32.4975 1.66758 1.6676
48Sample-44 50 min F 0.8 gL 1200 rpm replica 24.7428 24.4738 25.0199 1.28319 1.2832
49Sample-45 40min F 0.8 gL 1200 rpm replica 25.3192 25.0418 25.605 1.31331 1.3133
50Sample-46 35 min F 0.8 gL 1200 rpm replica 26.3538 26.061 26.6559 1.36738 1.3674
51Sample-47 30 min F 0.8 gL 1200 rpm replica 27.0747 26.7708 27.3885 1.40506 1.4051
52Sample-48 25 min F 0.8 gL 1200 rpm replica 27.5839 27.2721 27.906 1.43168 1.4317
53Sample-49 20 min F 0.8 gL 1200 rpm replica 28.6273 28.2988 28.9669 1.48621 1.4862
54Sample-50 15 min F 0.8 gL 1200 rpm replica 27.475 27.1648 27.7953 1.42598 1.4260
55Sample-51 10 min F 0.8 gL 1200 rpm replica 30.0626 29.7106 30.4268 1.56122 1.5612
56Sample-52 5 min F 0.8 gL 1200 rpm replica 30.6832 30.3208 31.0582 1.59366 1.5937
57Sample-53 inicial min F 0.8 gL 1200 rpm replica 32.2224 31.834 32.6247 1.67411 1.6741