Manual Mobiledrop en

MobileDrop GH11
Contact Angle Measuring Instrument
User Manual
V3-19
© KRÜSS GmbH, Hamburg 2006-2016
KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

Contents page 3
Contents
1 General information .................................................................................. 5

1.1 General safety instructions ................................................................................................................................................. 5
1.2 Intended use and application restrictions .................................................................................................................... 6
1.3 Possible options with MobileDrop .................................................................................................................................. 6
1.4 Scope of documentation and reference to other documents ............................................................................. 6
1.5 Technical support ................................................................................................................................................................... 7
2 MobileDrop controls ................................................................................ 8
3 Handling the MobileDrop ...................................................................... 9

3.1 Safety information about dosing ..................................................................................................................................... 9
3.2 Filling the syringe ................................................................................................................................................................... 9
3.3 Inserting and removing the dosing unit .....................................................................................................................10
3.4 Depositing a drop ................................................................................................................................................................11
3.4.1 Handling the dosing unit ..........................................................................................................................................11

3.4.2 Lighting ............................................................................................................................................................................12
3.4.3 Surface properties........................................................................................................................................................13
3.4.4 Using the laser positioning guide .........................................................................................................................13
3.5 Exchanging the syringe ......................................................................................................................................................15

3.6 Cleaning ...................................................................................................................................................................................16
3.6.1 Syringe guide .................................................................................................................................................................17

3.6.2 Prisms and bottom ......................................................................................................................................................17
4 Working with the MobileDrop HT (optional) ............................... 18
5 Using the optional DS3601 fine dosing unit ................................ 19

5.1 Design of the fine dosing unit ........................................................................................................................................19
5.2 Assembling and filling the fine dosing unit...............................................................................................................19
5.3 Adjusting the dosing volume ..........................................................................................................................................21
6 Calibration using the Drop Shape Standard Set CP3621/22 . 22

6.1 Properties of the standards ..............................................................................................................................................22
6.1.1 Versions............................................................................................................................................................................22
6.1.2 Geometry of the shapes ............................................................................................................................................22
6.1.3 Accuracy...........................................................................................................................................................................23

page 4 Contents
6.2 Handling...................................................................................................................................................................................23
6.3 Only for MobileDrop HT: Exchanging the foot ........................................................................................................23
6.4 Carrying out the calibration measurements..............................................................................................................24
6.5 Comparison with the tolerances given for the standards ...................................................................................25
6.6 Cleaning ...................................................................................................................................................................................25
Appendix ......................................................................................................... 26

I Computer requirements ....................................................................................................................................................26
II Procedure if repairs should be necessary...................................................................................................................27
III Material resistance ...............................................................................................................................................................28
IV CP3621/22: drop shapes by the Young-Laplace equation ..................................................................................29
V Warranty and caveat emptor ...........................................................................................................................................29
VI Copyright and right to make alterations ....................................................................................................................30

General information page 5
1 General information
Dear KRÜSS GmbH Customer,
Thank you for having chosen our MobileDrop – GH11. This manual will help you with the
commissioning, operation and maintenance of the MobileDrop.
 This manual is subject to continuous quality control. You can download the latest version of
the manual from the customer download area on our website www.kruss.de.
1.1 General safety instructions

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As well as this general safety information, please follow the safety instructions in the
remainder of the manual text.
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The MobileDrop may only be used by trained personnel.

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The MobileDrop is not designed for working with liquids that are classified as toxic,
corrosive, explosive and/or radioactive.
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When carrying out measurements with hazardous substances the safety regulations and, if
available, information in the appropriate safety data sheets must be taken into account when
handling such substances.
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The controls of the MobileDrop and a connected computer must not be operated when
wearing protective gloves, which have already been used for handling hazardous materials.
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MobileDrop is equipped with a laser pointer as a positioning guide. Long-term exposure of

the retina to the laser pointer can adversely affect your vision. Before using the pointer it is
essential that you read the safety information on p. 13 and p. 14 of the User’s Manual.
Do not use the MobileDrop in explosion-proof areas.

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Do not use the MobileDrop if the instrument is obviously damaged.

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page 6 General information
1.2 Intended use and application restrictions

 MobileDrop is only intended for measuring the contact angle of liquids on solid surfaces and
for determining the surface free energy of solids.
 The intended use includes the exclusive use of accessories supplied by KRÜSS or substitutes
with an identical design if disposable accessories are being used.
 The optical components of MobileDrop and parts of its housing are not resistant to several
liquids – the Annex contains a list of liquids/classes of liquids which could primarily damage
the optics. Please make sure that such liquids do not come into contact with the instrument.
 Do not use the instrument in atmospheres containing dust, smoke or aerosols; these affect
the optical components of the instrument and could damage them.
 Do not expose the MobileDrop to temperatures above 50°C or below 0°C.
 Avoid contacting the optical components with sharp objects.
1.3 Possible options with MobileDrop

MobileDrop offers you:
 mobile measurement of the contact angle of liquids on a solid sample
 determination of the surface free energy from contact angle measurements
 quick change of test liquids
 precise drop positioning using a laser pointer
 programmable measuring procedures
 extendable database for test liquids
1.4 Scope of documentation and reference to other

documents
This handbook describes the manual operating steps for the MobileDrop. The measurement and
all other functions of ADVANCE are described in the software help.
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General information page 7
1.5 Technical support

If your KRÜSS product should not word as expected, please consult our technical support. You
can contact them at:
KRÜSS GmbH
Technical support
Tel: +49 040/514401-55
Fax: +49 040/514401-98
E-mail: service@kruss.de
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page 8 MobileDrop controls
2 MobileDrop controls
General view
Syringe plunger
Laser pointer
button
Clamping
spring Hand grip
Dosing head
with dosing
USB cable
wheel
Brightness
control
Sample rest
From below
Prisms
Dosing needle

Handling the MobileDrop page 9
3 Handling the MobileDrop

This section describes handling of the instrument and its components:
 Safety information about depositing  this page
 Filling a syringe  p. 9
 Inserting the depositing system  p. 10
 Depositing drops  p. 11
 Using the positioning guide  p. 13
 Replacing a syringe  p. 15
 Chapters 3.2 to 3.5 describe the procedure with a standard dosing head DS3600. Additional
information for the procedure with a fine dosing unit DS3601 can be found in ch. 4.
3.1 Safety information about dosing

Do not use MobileDrop for depositing toxic, corrosive, infectious, explosive and/or
radioactive liquids.
Work with other hazardous substances should only be carried out by trained personnel and
under observance of the safety information contained in the relevant safety data sheets.
Never fill the syringe with more liquid than is necessary for the planned measurement. Do
not keep hazardous substance residues in the syringe, but empty them out and dispose of
them and the syringe in accordance with local regulations.
After the measurement take up the deposited hazardous substances on suitable tissues.
Samples that are to be used again after the measurement must be cleaned with a suitable
solvent.
Keep highly flammable liquids away from sources of ignition.
3.2 Filling the syringe

1. Place the vessel with the sample liquid on a solid surface.
2. Turn the dosing/adjusting wheel to bring the syringe plunger right to the bottom.
3. Immerse the syringe needle in the liquid.

page 10 Handling the MobileDrop
4. Draw up the liquid into the syringe by turning the dosing wheel.
Plunger bridge
5. Remove the air from the syringe by inverting the dosing unit so that the needle faces up and
tap the syringe walls so that any adherent air bubbles detach and rise up. Turn the syringe
plunger up to force out the air.
! When the air is forced out some liquid will also escape from the syringe. Take this up
with a suitable tissue.
3.3 Inserting and removing the dosing unit
Insertion
 Let the syringe slip into the opening with the plunger bridge pointing to the clamping
spring.

 Press down the dosing head until the clamping spring clicks into position and is located
above the dosing head.
Removal
 Pull back the clamping spring and lift the dosing head out of the guide.
3.4 Depositing a drop
! If drops have already been deposited on a sample then avoid contacting these drops with
the bottom of the MobileDrop, as this could contaminate the prisms and – with unsuitable
liquids – even damage them.
3.4.1 Handling the dosing unit
1. Connect MobileDrop to a USB connection of the computer. Start the ADVANCE software.
2. Hold the MobileDrop as shown in the illustration so that your hand grips the curved hand
grip and your index and middle fingers lie on the two dosing wheels.

page 12
2 Hanndling the Mo
obileDrop
3. Press the
t dosing wheels down to
o lower the needle.
n
 Ke
eep the need
dle tip in the approximate
e center of th
he image. If the needle is too low
du
uring drop de
eposition theen the drops are frequenttly pushed ouut slightly an
nd appear
lesss sharp.
4. Rotate
e the dosing/a
adjustment w
wheel towardss the palm of your hand to
o generate a drop.
d
2 1
3
 If the dosing unit has beeen set correctly then click

k-points shouuld be felt during the
otation. A goo
ro od drop size can be achie
eved with a rotation throuugh 3 click-points (see
illu
ustration). If the drops aree always app
proximately th
he same sizee the reprodu
ucibility of
the contact ang
gle will be bettter.
3.4.2 Lighting
g
Set the image brightness so that thee grey area in the drop bac only weakly visible.
ckground is o
 he backgroun d is produced by the sma

The grrey area in th all light gap b
between the prism
p and
the surface and doe
es not interfeere with the measurement
m if the brightnness is adequa
ate.
KRÜSS GmbH | Borrsteler Chausseee 85 | 22453 Ha

amburg | Germ
many | www.kruuss.de
3.4.3 Surface properties
! The contact angle measurement reacts very sensitively to contamination on the surface. Do
not touch the sample with your fingers.
! Surface irregularities will result in poor contact angle reproducibility. Avoid drop deposition
at sample positions with increased inhomogeneity. Increase the total number of drops for
inhomogeneous samples.
3.4.4 Using the laser positioning guide
A laser pointer is built in as a positioning guide in order to deposit a drop exactly at a particular
position.
Laser pointer
button

WARNING
Risk of vision impairment by laser beam
If the laser beam is pointed directly at your eye the retina could be damaged in that eye with
resulting blindness.
 Use the pointer only as an aid to drop positioning.
 Do not use the laser pointer on reflecting surfaces.
 Never look directly into the laser beam. If the beam accidentally contacts your eye do not
suppress the eyelid reflex, but close the eye.
 Never remove the instrument from the surface while the laser is still lit up. The instrument
must always have at least one edge on the surface.
Procedure
1. Tilt the instrument so that it lies on the front edge of the handle (deposition side) and the
rear edge of the sample rest.
Target position
2. Press the laser pointer button.
3. Move the instrument about without lifting it up until the point of light is on the required
drop deposition position.
Light point

4. Tilt the instrument back over the edge until the sample rest lies flat on the sample. Do not
rotate or displace the instrument during this procedure.
 For safety reasons the laser pointer switches off automatically after some time. It can be
switched on again by pressing the button again.
 The light point cannot be seen on reflecting surfaces. For this reason, and for safety reasons,
the positioning guide must not be used on reflecting surfaces.
3.5 Exchanging the syringe

1. Use the 2.5 mm allen wrench to loosen the two screws that attach the plunger bridge to the
dosing head.
Plunger
bridge
 Loosen the screws alternately as otherwise the plunger bridge could be tilted.
2. Pull the plunger out of the syringe (the last piece requires a little force) and remove the
syringe from the dosing head.
 As an alternative, the plunger bridge can be removed completely so that the syringe can
be removed with the plunger still inserted.
3. Take the new syringe out of the packaging and pull out the plunger.

4. Insert the bottom edge of the syringe sleeve in the slit of the dosing head.
Slit
5. Insert the plunger and rotate it so that the profile engages in the groove of the plunger
bridge.
6. Tighten up the two screws alternately. Do not tighten them up too much; the bridge should
only press the plunger down lightly. Check that the plunger moves when the
dosing/adjustment wheel is rotated. At the same time click-points should be felt as slight
resistances during rotation. If the dosing/adjustment wheel is too hard-going then loosen
the plunger bridge screws slightly.
7. Attach a needle to the syringe. Press it on firmly as otherwise it could easily fall off and
remain in the guide of the MobileDrop.
3.6 Cleaning
! Do not use ketones (e.g. acetone), alcohols (e.g. ethanol), esters (e.g. acetic acid ethyl ester)
or aromatic solvents (e.g. toluene) for cleaning purposes. We recommend the use of clean
cleanser’s solvent for removing fatty residues.
! Only use cleaning liquids that evaporate without leaving residues.
 A list showing the resistance of the prisms to various classes of substances can be found in
the Annex on p. 28.

3.6.1 Syringe guide
The syringe guide channel could be contaminated by drops of liquid.
 With water-soluble contaminants rinse the guide channel thoroughly with distilled water and
let it dry in the air.
 With organic contaminants that are insoluble in water rinse the guide channel with a suitable
solvent (e.g. cleanser’s solvent) and let it dry in the air.
3.6.2 Prisms and bottom
! The prisms are very sensitive. Do not touch them with hard objects. For cleaning use soft,
lint-free cotton swabs.
 Clean the bottom with cotton swabs moistened with cleaner’s solvent.
 Also clean the prisms with cotton swabs moistened with cleaner’s solvent without applying
pressure.
 Allow the cleaned components to dry.

page 18 Working with the MobileDrop HT (optional)
4 Working with the MobileDrop HT (optional)

The MobileDrop HT is equipped with a heat-resistant foot and with glass prisms in order to carry
out measurements on hot surfaces.
HT foot
! Do not place the MobileDrop HT on surfaces hotter than 250°C.
! The time of contact between the hot surface and the foot must not exceed five seconds.
Observe a waiting period of at least ten seconds between measurements.
 The boiling point of test liquids used must exceed the temperature of the surface.

Using the optional DS3601 fine dosing unit page 19
5 Using the optional DS3601 fine dosing unit

The DS3601 is used for dispensing an exactly reproducible dosing volume onto the sample.
5.1 Design of the fine dosing unit
Thimble
Barrel
Spindle
Syringe piston with

spring
Bottom edge seated

in recess
5.2 Assembling and filling the fine dosing unit

1. Withdraw the syringe piston. Fit the spring to the syringe piston. Insert the piston with the
spring into the syringe.
2. Push the piston down as far as possible. Hold the needle in a container with the test liquid.
Allow the piston to slide back so that the liquid is drawn into the syringe.

page 20 Using the optional DS3601 fine dosing unit
3. Screw the spindle of the micrometer screw up until it no longer protrudes.
4. Hold the syringe with the needle upwards and tap the wall of the syringe so that any air
bubbles sticking to it detach and rise to the top.
5. Insert the bottom edge of the syringe about half way into the recess in the fine dosing unit.
6. Push the syringe piston slowly up until it fits into the piston guide. Push the bottom edge
into the recess as far as the stop.
! If the test liquid is a hazardous substance, catch any fluid escaping in this and in the
following step with a cloth.

Using the optional DS3601 fine dosing unit page 21
7. Turn the thimble until its edge is in line with the top graduation of the barrel (13 mm) and
the 0 scale mark forms an extension of the long middle line.
13 mm
8. Insert the fine dosing unit into the MobileDrop.
 The procedure is described in Chapter 3.3.
5.3 Adjusting the dosing volume

The dosing volume is adjusted by turning the thimble.
Rotation (thimble graduations) Volume
1 graduation 0.175 l
5 graduations 0.875 l
10 graduations 1.75 l
11 graduations ≈2 l

page 22 Calibration using the Drop Shape Standard Set CP3621/22
6 Calibration using the Drop Shape Standard

Set CP3621/22
The Drop Shape Standard Set CP3621/22 is available from KRÜSS for calibrating the MobileDrop
and image evaluation with ADVANCE.
The set consists of three holders with inserted glass plates on which drop shapes with contact
angles of 30°, 60° und 120° have been applied lithographically.
 During the calibration the optical components of the MobileDrop and the image evaluation
of the software are checked to see with which accuracy the contact angle of a calculated
drop shape is measured.
6.1 Properties of the standards
6.1.1 Versions
Drop shape standards are available in two versions:
 CP3621: Uncalibrated standards
 CP3622: Standards with calibration certificates
6.1.2 Geometry of the shapes
The shapes have been calculated by using the Young-Laplace equation, which provides the most
accurate geometrical description of real drop shapes (further information Appendix p.29). This
is why the test measurement must also made using the Young-Laplace method.

Calibration using the Drop Shape Standard Set CP3621/22 page 23
6.1.3 Accuracy
 The following information describes the optical precision of the standards themselves, not
the accuracy of the drop shape analysis carried out by using KRÜSS measuring tools.
Standard Accuracy
30° ±0,09°
60° ±0,07°
120 ±0,04°
6.2 Handling
! Only touch the stands of the standards; never touch the glass surface.
! The standards must not come into contact with sharp-edged objects.
! Never heat the standards above 40°C, as otherwise the drop shapes themselves could be
distorted.
 After use return the standards to their storage box.
 Check the standards from time to time (depending on how frequently they are used) for
scratches or other damage.
6.3 Only for MobileDrop HT: Exchanging the foot

For MobileDrop HT the heat resistant foot must be exchanged with the standard foot.
standard foot
HT foot

page 24 Calibration using the Drop Shape Standard Set CP3621/22
1. Use the wrench supplied with the MobileDrop to unscrew the four screws that fasten the HT
foot to the MobileDrop.
2. Remove the HT foot and exchange it with the standard foot.
3. Fix the standard foot using the previously removed screws.
6.4 Carrying out the calibration measurements
 The calibration is made using ten single measurements on each standard. In order to ensure
that the measurements are meaningful, the complete measuring sequence is repeated for
each individual value:
Set up and align instrument (focus)Adjust brightnessCarry out measurement.
1. Connect up MobileDrop and start the ADVANCE software.
2. Create a sessile drop measurement. Select Young Laplace as fitting method.
3. Place the MobileDrop in the holder for the standard used.
4. Move the instrument in the holder so that:
 The longer side of the MobileDrop base is touching the left or right-hand edge of the
holder.
 The whole drop shape is shown as sharply as possible.

Calibration using the Drop Shape Standard Set CP3621/22 page 25
5. Adjust the brightness so that the drop image has a high contrast and the grey area in the
background is only weakly visible.
 The grey area in the background is produced by the small light gap between the prism
and the surface and does not interfere with the measurement if the brightness is
adequate.
6. Carry out a measurement.
7. Repeat steps 3 to 5 until the procedure is finished and 10 measured values have been
obtained.
6.5 Comparison with the tolerances given for the standards

The mean value of the 10 individual measurements is shown in the results list of ADVANCE.
 Check that the results are within the tolerance range given for the standard.
Tolerance
Standard
Max. variation of mean value
from nominal value
30° ±1°
60° ±1°
120° ±1°
 If the tolerance has been exceeded for one of the standards you should check the quality of
the video image (sharpness, illumination) and correct it if necessary. If the result is still
outside the tolerance limits please contact us.
6.6 Cleaning
! Do not clean the standards with rough or linting cloths or with hard brushes.
 If the glass surface is contaminated (e.g. by fingerprints) clean it with a cotton-wool tip
soaked with a solvent (e.g. isopropanol) and let the solvent vaporize.
 Remove any dust with a cold air blower or a soft brush.

page 26 Appendix
Appendix
I Computer requirements
The following is a list of the minimum requirements to enable the ADVANCE software to run
without any problems:
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General
Current version 1.41
Supported operating systems Windows 7

Windows 8
Windows 8.1
Architecture For DFA100: 64 bit required

For other instruments: 64 bit strongly recommended; 32 bit possible
User privileges Administrator privileges required only for installation
Processor Minimum Intel Core i5 or i7 with DualCore (QuadCore or higher

recommended) and 2 GHz (4 GHz or higher recommended)
Main memory ≥ 4 GB
Hard disc ≥1 GB free memory + space for stored data; SSD recommended
Resolution Minimum 1366 x 768 pixel

Optimal 1680 x 1050 or 1920 x 1080 pixel
Required ports for individual instruments
Mobile Surface Analyzer – MSA 1 × USB 3.0 port or 2 × USB 2.0 port
MobileDrop – GH11 1× USB 2.0 port (or higher)
Drop Shape Analyzer – DSA25 For IEEE1394 camera: 1 × PCIe slot for IEEE1394b board (PC) or
Drop Shape Analyzer – DSA30 1 × PC card slot for IEEE1394b interface (Notebook)
Drop Shape Analyzer – DSA100 For USB camera: 1 × USB 3.0 port
For instrument: 1 × RS232 or 1 × USB 2.0 port (or higher) with

RS232 USB adapter
Dynamic Foam Analyzer – DFA100 1× USB 2.0 port (or higher)
+ Foam Structure Module – FSM One additional USB 2.0 port (or higher)
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Appendix page 27
II Procedure if repairs should be necessary

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Contact KRÜSS
 Contact KRÜSS customer support.
 If you did not obtain the measuring instrument directly from KRÜSS but from a dealer,
please contact your dealer first. He may be able to rectify the damage. If not, contact
KRÜSS customer support directly.
 You will be given a repair number. Please quote this number in your covering letter when
you dispatch the instrument.
Send us the measuring instrument or accessories
! Do not dispatch the measuring instrument or accessories without consulting KRÜSS

customer support.
 Components which are not directly affected by the damage may also have to be sent
with the instrument. KRÜSS customer support will advise you on the necessary scope of
the shipment.
! Remove liquids (e.g. samples, temperature control liquid) completely from the instrument
and the accessories.
! Clean the instrument or accessories before dispatch. This applies particularly if there is
contamination due to hazardous substances.
! Use the original packaging to pack the instrument or accessories. If you no longer have the
original packaging, it must be ordered from KRÜSS at the customer’s expense.
! Pack all components separately which were packed separately when the instrument was
supplied. Do not dispatch the unit in the assembled state.
! If the instrument or accessories were provided with transportation locks, refit these before
shipping.
! Use box-in-box packaging.
 Our customer support department will be pleased to advise you regarding the proper
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packaging.

page 28 Appendix
III Material resistance

The observation prism consists of an optical plastic that is not resistant to some liquids. Make
sure that the prism does not come into contact with such substances. If you wish to use a liquid
that does not appear in the following list please contact us first.
Substance class resistant not resistant
Acids •
Alicyclic hydrocarbons •
Aliphatic hydrocarbons •
Aromatic hydrocarbons •
Bases •
Chlorinated hydrocarbons •
Diiodomethane (standard test

•
liquid)
Esters •
Ketones •
Mineral oils •
Monovalent alcohols •
Polyvalent alcohols •
Vegetable fats, oils •

Appendix page 29
IV CP3621/22: drop shapes by the Young-Laplace equation

The Young-Laplace equation is the most accurate mathematical description of the shape of real
drops. It describes the curve of a drop shape by using the differential pressure between the
inside and outside of the drop. As their own weight means that sessile drops are asymmetrical,
two radii of curvature exist for each point on the drop shape:
1 1
p     
 r1 r2 
(p = Differential pressure between inside and outside of drop;
 = surface tension;
r1 and r2 = radii of curvature.)
As not only the surface tension, but also the weight of a drop determines its shape, predefined
values for the density of the liquid and the acceleration due to gravity are used for calculating
the shapes of the standards.
The resulting shape of the curve obtained from the Young-Laplace equation is intersected by a
horizontal line. The contact angle is the angle between the horizontal line and the drop shape at
both points of intersection.
The following parameters are used for the drop shape:
Parameter Value
Surface tension 50 mN/m
Density 1.000 g/cm3
Acceleration due to gravity 9.80665 m/s2
5 mm (4.33 mm for
Diameter
120° standard)
 Although these parameters are used for calculating the shapes of the standards, they need
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not be taken into account in the test measurement of the contact angle.
V Warranty and caveat emptor

The warranty terms and deadlines are described in the general terms and conditions of KRÜSS
GmbH.
There is no warranty claim if the product was damaged due to careless usage or improper
treatment or if it was not used according to purpose, and if the instructions and danger warnings
in the manual were not observed.
The warranty claim is void if changes on the product are performed by the customer or a third
party without prior consultation of KRÜSS GmbH, which go beyond the activities described in
the manual. This also applies to repair work, which was independently performed or carried out
by a third party.
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page 30 Appendix
VI Copyright and right to make alterations

The information contained in this document may be altered without notice and does not
represent any obligation by KRÜSS GmbH.
Neither this manual nor any part of it may be reproduced or transmitted for any purpose
whatsoever in any form and by any means, electronic or mechanical, by photocopy or drawing
without the express approval of KRÜSS GmbH in writing.
2006-2016 , KRÜSS GmbH, Hamburg, all rights reserved.

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MobileDrop GH11

Contact Angle Measuring Instrument

© KRÜSS GmbH, Hamburg 2006-2016

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

1 General information .................................................................................. 5

2 MobileDrop controls ................................................................................ 8

3 Handling the MobileDrop ...................................................................... 9

3.4.1 Handling the dosing unit ..........................................................................................................................................11

3.5 Exchanging the syringe ......................................................................................................................................................15

3.6.1 Syringe guide .................................................................................................................................................................17

4 Working with the MobileDrop HT (optional) ............................... 18

5 Using the optional DS3601 fine dosing unit ................................ 19

6 Calibration using the Drop Shape Standard Set CP3621/22 . 22

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

Appendix ......................................................................................................... 26

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

1.1 General safety instructions

The MobileDrop may only be used by trained personnel.

MobileDrop is equipped with a laser pointer as a positioning guide. Long-term exposure of

Do not use the MobileDrop in explosion-proof areas.

Do not use the MobileDrop if the instrument is obviously damaged.

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

1.2 Intended use and application restrictions

 Do not expose the MobileDrop to temperatures above 50°C or below 0°C.

 Avoid contacting the optical components with sharp objects.

1.3 Possible options with MobileDrop

 mobile measurement of the contact angle of liquids on a solid sample

 determination of the surface free energy from contact angle measurements

 quick change of test liquids

 precise drop positioning using a laser pointer

 programmable measuring procedures

 extendable database for test liquids

1.4 Scope of documentation and reference to other

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

1.5 Technical support

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

3 Handling the MobileDrop

 Safety information about depositing  this page

 Inserting the depositing system  p. 10

 Using the positioning guide  p. 13

3.1 Safety information about dosing

Keep highly flammable liquids away from sources of ignition.

3.2 Filling the syringe

3. Immerse the syringe needle in the liquid.

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

3.3 Inserting and removing the dosing unit

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

3.4 Depositing a drop

3.4.1 Handling the dosing unit

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

 If the dosing unit has beeen set correctly then click

 he backgroun d is produced by the sma

KRÜSS GmbH | Borrsteler Chausseee 85 | 22453 Ha

3.4.3 Surface properties

3.4.4 Using the laser positioning guide

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

 Use the pointer only as an aid to drop positioning.

 Do not use the laser pointer on reflecting surfaces.

2. Press the laser pointer button.

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de

3.5 Exchanging the syringe

KRÜSS GmbH | Borsteler Chaussee 85 | 22453 Hamburg | Germany | www.kruss.de