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AIAA-2001-1418

SOME MICROMECHANICS CONSIDERATIONS OF THE FOLDING OF


RIGIDIZABLE COMPOSITE MATERIALS
Thomas W. Murphey*, Troy Meink†, and Martin M. Mikulas‡
Air Force Research Lab, Kirtland Air Force Base, New Mexico

launch vehicle shroud. In the early 60’s, NASA flew


Abstract
the 125 ft. diameter inflatable ECHO spherical
There is considerable interest in the use of satellite.1 To maintain shape after initial pressurization,
composites with a softened matrix to improve the the thin walled sphere was constructed of multiple
compact packaging of structures for space applications. layers of Mylar and aluminum. During pressurization,
It has been surmised that a soft matrix will enable a the aluminum in the wall was intentionally over
composite to be bent to a much tighter bend radius than stressed to the point of yielding such that after the
is achievable with a normal stiff matrix. Over the past pressure was gone, the “rigidized” sphere would
30 years, numerous empirical attempts have been made maintain its shape. In the years since that initial
at developing what is commonly referred to as success, NASA and the DOD have conducted
rigidizable composites. These are composites for which considerable research on the development of structures
the matrix is in a softened state during packaging and made of filamentary composite with polymer resins.
deployment, and then rigidized for use once deployed Although numerous developmental structures have
in space. Although some success has been achieved been built from such rigidizable material systems, the
with various rigidizable processes, there does not exist technology remains unused. One reason for the
a basic understanding of the complex mechanisms material remaining unused is the lack of an underlying
associated with the required tight folding or the limits fundamental technology database. An important aspect
to which the folding can be achieved. of this technology database is a basic micromechanics
This paper explores the basic micromechanics kinematics analysis of the large rotations and
deformation mechanisms associated with the folding of deformations that are associated with compact
softened matrix composites. It is assumed that the packaging of rigidizable composites.
primary mechanism that enables the large deformations The ratio of fold radius to material thickness
associated with tight folding is micro-buckling of the (hence forward called the bend ratio, β ) provides a
fibers in the softened matrix. The basic kinematic
first order estimate of the packageability of a
relations that govern folds with micro-buckled fibers
construction system. Material failure strain directly
are developed and used to quantify the associated
limits minimum bend ratio. Figure 1 shows two typical
internal fiber motion and matrix strains. Experimental
fiber materials, there assumed failure strains, and their
results are presented that verify the assumed
subsequent minimum bend ratios. To be comparable to
micromechanics model and provide insight into the
traditional technology, rigidizable packaging schemes
level of folding that can be achieved with rigidizable
must better the bend ratio possible with graphite-epoxy
composites. laminates, approximately 50. Rigidizable and
Introduction traditional graphite-epoxy laminates employ similar
fibers limited to the same failure strains; simply
Since early in the space program inflatable
switching to a rigidizable resin system does not enable
structures have been considered as a means for
a smaller bend ratio. Rigidizable composites have the
achieving a spacecraft on orbit that is larger than the
potential to enable deployable structure packaging

*
Research Engineer, AIAA member

Senior Aerospace Engineer, Senior AIAA Member

Professor Emeritus, University of Colorado, Boulder, Colorado, AIAA Fellow
This paper is declared a work of the U.S. Government and is not subject to copyright protection in the United States.

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American Institute of Aeronautics and Astronautics
configurations that are denser and more versatile As shown in Figure 2, the inside fold surface is of
(smaller bend ratios) because a soft matrix facilitates length li = π ( r − t 2 ) while the mid-plane length
more diverse fiber deformations modes. These new
remains l = π r . The resulting difference in length
deformation modes kinematically allow fibers to
achieve effective strains much greater than that of the between the mid-plane ( l ) and the inside surface ( li )
constituent fiber. This paper presents a is,
micromechanics analysis of the kinematics of folding π
soft matrix composites. A deformation mode allowed δ = l − li = π r − π ( r − t 2 ) =t. (1)
2
by soft resins, micro-buckling, is shown to
Strains on the inside (compressive) and outside (tensile)
kinematically allow much greater effective strains and
surfaces are given by,
hence, smaller bend ratios than non-rigidizable
materials. Experimental results supporting the analysis δ πt 2 t
ε= = = . (2)
and demonstrating the method are also presented. l πr 2r
The four major classes of resin systems being Casting Equation (2) in terms of the bend ratio ( β )
considered for rigidizable structures are, thermosets, gives,
UV cured, thermoplastics, and elastic memory r 1
polymers.2 The thermosets and UV cured resins require β= = . (3)
curing in space while the thermoplastic and elastic t 2ε
memory resins are cured on the ground and only Equation (3) is graphed in Figure 1, illustrating the
involve reheating in space to allow deployment and limits of typical fiber materials. To achieve a
rigidization. This paper is concerned with the folding foldability significantly better than these materials, an
of fiber composites while the resin is softened because effective extensional strain on the order of 5% is
either it is not cured (thermoset and UV cured resins) or required.
the resin it heated (thermoplastic and elastic memory To fully appreciate the magnitude of deformations
resins). In order to make a rational design selection required for small bend ratio folding, it is revealing to
among these resin systems, it is necessary to be able to modify the previous assumptions from that of pure
understand and predict the basic mechanics of fiber and extensional deformation to that of pure shear
resin deformation of these systems during the deformations. Again, material thickness does not
packaging and deployment process. This paper change, however, extensional strain components
develops the basic micromechanics of folding softened parallel to the surfaces are assumed zero and shear
composite systems, and provides a basis for comparing strains are non-zero. As shown in Figure 2, the bending
different resin systems. is accommodated through shear deformations. Shear
strain is greatest at the ends of the fold where it is given
Kinematic Fold Models by,
The micromechanics of folding are well described !δ " !π "
by the kinematics of deformations, regardless of the γ = tan −1 # $ = tan −1 # $ ≈ 1 . (4)
t
% & % & 2
forces responsible for them. To provide a first order
understanding of the severe deformations associated δ is evaluated using Equation (1). Regardless of fold
with folding, a two-dimensional plane-strain kinematic radius or material thickness, a shear strain of 100% is
model is considered. required to accommodate folding. Lines initially
An infinite homogenous plate of thickness t is perpendicular to the plane of the lamina shear at an
assumed initially flat. It is then folded, back upon angle of γ = 1 rad = 57.5° .
itself, about a mid-plane radius r to form a 180 deg. Two factors combine to prevent realization of pure
fold. Plate thickness is assumed to remain constant and extensional and shear folds in soft matrix composites.
mid-plane strain zero throughout the process; bending First, soft resins violate the assumption of zero shear
is accommodated purely through extensional strains stiffness. As described in the extensional fold model, a
proportional to the distance from mid-plane. Further, shear stiffness generates surface normal stresses that
shear strain components parallel to plate surfaces are resist shear deformations. These stresses have a
assumed zero so that strains only occur within the tendency to return the shear strain to zero far from the
region of bending. This idealized, extensional fold is fold region. Assume the limiting case of a shear fold
illustrated in Figure 2. With the above assumptions, the with all extensional strain occurring outside of the fold
maximum strain required to construct the fold is a region in the form of a 1% fiber strain. Normalization
function only of the material thickness and the bend of the shear strains requires extensional strains to be
radius. distributed along 80 times the material thickness or 0.8
in. along a 10 mil thick plate.

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American Institute of Aeronautics and Astronautics
Second, continuous fibers are extremely slender Combining Equations (5) and (6) gives the maximum
structures that individually buckle under near zero effective strain a fiber can achieve through micro-
compressive loads. Only the matrix shear stiffness buckling,
prevents fibers from buckling.3 Fibers in soft matrix 1
composites have been observed to buckle under small ε effective = 2
(7)
2!
compressive stresses, indicating the lack of significant Rf "
1 + 4π # $
shear stiffness in soft resins. Once buckled, % λ &
considerable matrix strain compliancy is required to Equation (7) is graphed in Figure 6 for a range of
prevent matrix failure by separation. Soft resins also micro-buckle wavelengths. The plot reveals that with a
lack this compliancy and matrix separation generates a micro-buckle wavelength of 1.0 mm, an effective strain
crack-like geometry that can propagate into catastrophic
of 19% is possible for graphite fibers ( R f = 0.33 mm).
delamination of fold inner surface fibers. The severity
of delaminations required to accommodate a shear fold Laminate Folding with Micro-buckling
are illustrated in Figure 3.
In a micro-buckle fold, compressed fibers micro-
Micro-buckling buckle and exhibit a drastically reduced effective axial
Soft matrix composites are potentially highly stiffness. The effective axial stiffness of a sinusoid is
foldable because they allow fibers to accommodate a given by,5
bending deformation mode not allowed by stiff resins. σ Euler 2 EI ' π 2 1 1 (
Specifically, a soft matrix allows fibers to Eeffective = = ) + 2*, (8)
2ε effective A )+ 4 λ 2
ao *,
synchronously micro-buckle and take the shape of a
sinusoid (Figure 4). Local axial fiber strains are where EI is the fiber bending stiffness and A is the fiber
relatively small due to the minuscule loads required to cross-sectional area. Assuming a solid circular cross-
buckle fibers. Thus, the primary deformation mode of a section and λ >> ao , Equation (8) reduces to,
micro-buckled fiber is bending and axial strains need 2
not be considered. Eeffective 2I r fiber
= = . (9)
Due purely to bending, a sinusoid has an effective E Aao2 2ao2
extensional strain that depends on the ratio of the On the fold outside surface, fibers are in tension and
micro-buckle wavelength ( λ ) to amplitude (ao), given remain straight and axially stiff. In effect, the outside
by,4 fibers are axially rigid. As explained below, this large
1 discrepancy in stiffness forces the fold neutral axis
ε effective = 2
. (5)
(plane of zero extensional strain) very close to the
4 !λ "
1+ 2 # $ outside fold surface.
π % ao &
The reduced effective axial stiffness of buckled
Equation (5) is graphed in Figure 5 where it is apparent fibers allows them to be highly compliant without
that a micro-buckle amplitude to wavelength ratio of generating significant compressive stresses. The tensile
0.15 is required for an effective strain of 5%. There is fibers are opposite to this because their large axial
potential to achieve larger effective strains as the ratio stiffness results in large stresses for small strains. As
is increased. shown in Figure 7, to maintain moment equilibrium on
Micro-buckling could result in fiber breakage if the each side of the fold neutral axis, the neutral axis moves
sinusoid shape causes a bend radius smaller than the to the outside fold surface. In a fold accommodated
fiber is capable of. Table 1 lists typical composite through micro-buckling, the deformations occur
fibers, their assumed diameters, their assumed failure primarily through effective axial compression of micro-
strain, and the corresponding minimum radius around buckled fibers. This deformation mode is illustrated in
which they could be folded by Equation (2), Figure 7 and the corresponding bend ratio as a function
rmin = d fiber ( 2ε failure ) . The minimum fold radius is a of strain (assuming the neutral axis is the outside fold
surface) is now two times greater than the previous
fiber property that determines the limit of micro- case,
buckling and likely has a strong influence on the
r 1
foldability of a fiber/resin system. β microbuckled = = . (10)
t ε effective
The maximum curvature of a micro-buckled fiber
occurs at the sinusoid peak (or trough) and is given by, Equation (10) is graphed in Figure 1 as the region
λ 2 applicable to rigidizables. Combining Equations (7)
Rf = . (6) and (10) gives the minimum laminate fold ratio as a
π 2 ao

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American Institute of Aeronautics and Astronautics
function of minimum fiber bend radius and micro- The first and most commonly observed mode is out of
buckle wavelength, plane buckling, as shown in Figure 7. While a large
2 effective strain is achieved, this mode can lead to early
!R "
β microbuckled = 1 + 4π # f $ .
2
(11) lamina failure as the micro-buckles grow and eventually
% λ & result in matrix failure in the form of delaminations.
Equation (11) is graphed in Figure 8 for a range of Another stability mode is in-plane buckling. In this
micro-buckle wavelengths. Assuming a wavelength of mode, the fibers deform sideways, remaining in the
1.0 mm and graphite fibers ( R f = 0.33 mm), a plane of the material. Because the fibers remain in-
plane, delamination is inhibited and larger effective
theoretical minimum fold ratio of 5.3 is possible. The strains may result.
validity of the analysis for a fold this tight is
Experiment observation has shown the lowest
questionable because the analysis assumes a bend
mode to be out-of-plane. However, by applying a
radius several times larger than the material thickness.
compressive pressure to the inside fold surface, it is
However, the results demonstrate that tight folds,
theoretically possible to force the in-plane buckling
β <<50, are theoretically feasible with fiber micro- mode. An apparatus was designed and built to bend
buckling. laminates around a mandrel while applying a
Micro-buckling Inter-Fiber Shear compressive pressure (Figure 10). The pressure is
generated through an axial force (P) on the sample and
The failure mode of interest may not be fiber the compressive pressure σz is given by,
bending. A micromechanics analysis shows that
extreme inter-fiber shear strains are required to P
σz = , (14)
accommodate fiber micro-buckling. As the fibers rw
micro-buckle, large interlaminar matrix shear strains where r is the bend radius and w is the width of the
occur as shown in Figure 9. By assuming a sinusoidal sample. Experiments using this technique have had
micro-buckling deformation, an expression for the moderate success at inducing in-plane buckling.
maximum interlaminar shear strain can be obtained as,3
Experiment
'π a ! h "( π a ! h "
γ xy max = tan ) o # 1 + $ * ≈ o #1 + $ , (12)
−1
A series of folding experiments were performed on
+ λ % 2c & , λ % 2c & elastic memory resin laminates with graphite fibers
where h is the effective micromechanics thickness of using the described apparatus. Tensile tests were used
the fibers and 2c is the effective thickness of the matrix. to evaluate fiber breakage, with the assumption that
Using Equations (5) and (12), a quantitative assessment large numbers of broken fibers show up as a reduction
of the interlaminar shear strains required to obtain a in sample tensile strength. Matrix integrity was
given amount of effective compression strain is, evaluated with fixed-fixed end condition buckling tests.
Because it is predominantly the matrix that prevents
' ! h" ε ( ! h" ε
γ xy max = tan−1 )2 #1 + * ≈ 2 #1 + $ . (13) local fiber buckling, a degraded matrix should show as
+) % 2c $& 1 − ε ,* % 2c & 1− ε a decrease in buckling strength.
Equation (13) indicates that the shear strain increases as The test protocol was to first elastically buckle a
the matrix thickness (2c) decreases. Thus, as fibers are sample before it was folded. Then fold the sample
packed more densely (larger fiber volume fraction) the using the bending apparatus. After full cooling, the
shear strain required to accommodate a fold increases. samples were reheated to return them to a flat
Assuming an effective matrix thickness of 1/10 the (deployed) state and cooled again. The buckling test
fiber thickness, h 2c = 10 , Equation (13) indicates a was repeated and finally, the samples were pulled to
determine ultimate tensile strength. For comparison of
large shear strain of 144% is required to accommodate
the tensile test results, a control group was pulled
a compressive strain of 10% ( β = 10 ). Lowering the
without going through the folding process.
fiber volume fraction to an effective h 2c = 1 requires Typical buckling test results are shown in Figure
significantly lower shear strains of 92% to 11. For the test shown, the folding process (bend ratio
accommodate the same fold. Laminates with lower of 10) degraded the load carrying capacity of the
fiber volume fractions may accommodate a micro- sample by 21%. The tensile testing of ten samples (5
buckle fold with a lower chance of matrix failure due to pristine and 5 folded to a bend ratio of 20) showed a
inter-fiber shear. 15.7% reduction in strength. In all tests, combinations
Micro-buckling Modes of in-plane and out-of-plane micro-buckle modes were
observed.
The folding of soft matrix laminates shows two
characteristically different fiber micro-buckling modes.

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American Institute of Aeronautics and Astronautics
Concluding Remarks References
1
This paper explores the basic micromechanics of Elder, E. C., "Out from Behind the Eight-Ball: A
deformation mechanisms associated with the folding of History of Project Echo," AAS History Series, Volume
composites with a softened matrix. It is assumed that 16, 1995 by American Astronautical Society.
the primary mechanism that enables the large 2
Tupper, M., Munshi, N., Beavers, F., Gall, K.,
deformations associated with tight folding is micro- Mikulas, M., and Meink, T., “New Developments in
buckling of the fibers in the softened matrix. The basic
Elastic Memory Composite Materials for Spacecraft
kinematic relations that govern the large deformations
Deployable Structures and Components,”
associated with tight folding are developed and used to
Proceedings of the 42th AIAA/ASME/ASCE/AHS/ASC
quantify the associated internal fiber motion and matrix
strains. Experimental results are presented that verify Structures, Structural Dynamics, and Materials
the assumed micromechanics model and provide insight Conference and Exhibit, April 16-19, 2001, Seattle,
into the level of folding that can be achieved with WA.
3
rigidizable composites. Jones, R. M., "Mechanics of Composite Materials,"
It is shown that compressive strains associated with Hemisphere Publishing Co., Taylor and Francis,
laminate bending on the order of 5% are required to 1975.
achieve compact packaging. This very high 4
Murphey, T. W., "A Nonlinear Elastic Constitutive
compressive strain is enabled by micro-buckling of the Model for Wrinkled Thin Films" Ph. D. Dissertation,
fibers in a soft matrix. It is also shown that matrix University of Colorado at Boulder, 2000.
shear strains in excess of 100% are induced as a 5
consequence of these large compressive strains. Murphey, T. W. and Mikulas, M. M., Jr., "Nonlinear
Experimental studies indicate that the mechanism of Effects of Material Wrinkles on the Stiffness of Thin
micro-buckling allows softened matrix composites to be Polymer Films," Proceedings of the 40th
folded to very small bend ratios. Experiment also AIAA/ASME/ASCE/AHS/ASC Structures, Structural
revealed that the folding process can degrade tensile Dynamics, and Materials Conference and Exhibit,
strength and buckling strength. April 12-15, 1999, St. Louis, MO., AIAA 99-1341.

Table 1: Minimum bend radius and maximum effective axial strain due to micro-buckling.
Assumed Assumed Calculate Maximum Axial Minimum Micro-
Fiber Failure Fiber Minimum Fiber Micro-buckle Strain buckled Bend
Strain Diameter Bend Radius, Rf ( λ = 1.0 mm) Ratio
Graphite 1.0% 6.5 µm 0.33 mm 19% 5.3
Fiberglass 1.5% 3.0 µm 0.10 mm 72% 1.4

100

50 Gr/Ep
Fiberglass
r
t
Bend Ratio, β =

20 r 1
=
t ε
10
r 1 Rig
= idi
zab
5 t 2ε les

0.01 0.02 0.05 0.1 0.2 0.5


Strain, ε
Figure 1: Achievable bend ratio as a function of strain.

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l =πr

li = π (r − t 2 ) Extensional
Fold

Flat
Plate

57.5°
Shear
δ Fold
t

δ  π 
tan −1   = tan −1   = 57.5°
t 2
Figure 2: Shear and extensional folds and their assumed deformations.

Figure 3: Simulation of fiber buckling and the ensuing delamination observed in soft resins under
compression.

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American Institute of Aeronautics and Astronautics
l

df ao Rf

Figure 4: The sinusoid profile of micro-buckled fibers.

0.4

0.35
1
0.3 ε= 2
4 λ
1+ 2  
ao 0.25 π  ao 
λ 0.2

0.15
λ
0.1
ao
0.05

0.05 0.1 0.15 0.2 0.25


Strain, e
Figure 5: Effective strain due to bending in a micro-buckled fiber.

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0.4

0.35 1
ε effective = 2
R 
0.3 1 + 4π  f 
2

 λ 
0.25 Gr/Ep
ε effective

0.2
l = 10 mm
0.15
5.0
0.1
2.0
0.05 1.0
0.5
0.2
0.5 1 1.5 2 2.5 3 3.5 4
R f (mm)
Figure 6: Theoretical maximum effective strain due to micro-buckling as a function of minimum fiber
bending radius for various micro-buckle wavelengths.

Stress Profile

lo = π (r + t 2 ) Tensile
Stresses
l − l π (r + t 2 ) − π (r − t 2 ) t s t
ε= o i = = l =πr
l πr r
Compressive Neutral
Stresses Axis
li = π (r − t 2 )

Figure 7: Out-of-plane micro-buckle fold deformation mode and stress profile.

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40
l = 0.2 l = 0.5 l = 1.0
35 l = 2.0
30
r
t
Bend Ratio, β =

25

20

15 Graphite
10
l = 5.0
5
l = 10

0.25 0.5 0.75 1 1.25 1.5 1.75 2


Rf
Figure 8: Bend ratio as a function of minimum fiber bend radius and micro-buckle wavelength.

Figure 9: Inter-fiber shear strains.

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Mandrel

Test Specimen

Constant Force Spring

Figure 10: Experimental apparatus for folding soft matrix composite laminates while inducing the in-plane
micro-buckling mode.

2000
Before Folding
1800 (6 Trials)
1887 Psi

1600
Axial Compressive Stress (Psi)

1400
1490 Psi
Folded Once
1200
(6 Trials)

1000
Buckling Test Specifications
All tests performed on same specimen
800
0,0,0 layup
Jog attributed to unidirectional IM7 graphite fabric
600
removal of test 40% fiber volume fraction
apparatus play when Cross section 0.70 x 0.050 in
400 Active Length 5.75 in
fixed-pinned buckle
mode occurs. Fixed-fixed end conditions
200

0
0.000 0.001 0.002 0.003 0.004
Axial Strain

Figure 11: Buckling tests results before and after folding demonstrate a 21% reduction in load carrying
capacity.

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