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Journal of the University ofC.Chemical Technology I.

Atic, S. Immamoglu, and Metallurgy, 40, 3, 2005, 199-204


Valchev

DETERMINATION OF SPECIFIC BEATING ENERGY - APPLIED


ON CERTAIN PULPS IN A VALLEY BEATER
C. Atic1, S. Immamoglu2, I. Valchev3

1
Istanbul University, Faculty of Forestry, Received 14 June 2005
Istanbul - Turkey Accepted 21 July 2005
2
Kafkas University, Artvin Faculty of Forestry,
Artvin - Turkey
3
University of Chemical Technology and Metallurgy,
8 Kl. Ohridski, 1756 Sofia, Bulgaria

ABSTRACT

Beating performance of certain kraft pulps were accurately investigated in a laboratory valley beater device. To
determine beating response of the pulps, empirical specific edge load (SEL) or beating intensity, specific surface load
(SSL) and specific beating energy consumption (SBE) were experimentally found for each kraft pulp. Industrial applica-
tion of refining or beating theory usually refers to the specification of three parameters: SEL, SSL and SBE, because of the
fact that, beating performance is controlled by these parameters. In order to simulate laboratory beating performance,
where beating is controlled by the time elapsed, and industrial beating performance, it is really necessary to investigate and
control the beating performance of the pulp using the aforementioned parameters. These laboratory results give us firstly,
significant information about the amount of energy and beating intensity necessary to put to the pulp samples to reach
required properties and secondly, information about comparable values for laboratory and industrial application.
Keywords: Beating performance, valley beater, kraft pulp, specific edge load, specific surface load, specific beating
energy.

INTRODUCTION Refining plays an important role in stock prepa-


ration as well as throughout the complete paper making
It would be desirable to make fundamental mea- process. Next to the raw material selection, it has the
surements to obtain basic information about the paper greatest influence on the final product quality [2]. There-
that could then be used to predict the utility of the pa- fore, one of the important pulp tests tries to determine
per for any purpose [1]. With the development of in- the beating response of the pulps. ISO 5264 standard
dustrial paper making during the last century, exigency method describes bench top beating devices used for
for fine determination of properties of utilized materi- beating of small amount of pulp samples. The Valley
als became unavoidable. Therefore, a number of ana- beater (ISO 5264-1), the PFI mill (ISO 5264-2) and
lytical tests were developed and can be performed on the Jokro mill (ISO 5264-3) are most widely used stan-
pulp samples for quality assessment. dard devices. These devices have different nature of fi-

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Journal of the University of Chemical Technology and Metallurgy, 40, 3, 2005

bre treatment compared to each other and to industrial into the Valley beater tube and the beater motor was
refining applications. driven for approximately 10 min prior to the addition
The valley beater is widely used in paper research of pulp. Over a period of 3 to 5 minutes all the pulp
laboratories to investigate beating performance of pulp. and the water used for soaking were slowly added into
In terms of the beating process, this device seems to be the tube. The total volume of water and pulp in the
most similar to the industrial applications. In the paper beater was set to be 23 ± 0.21 L. Pulp was circulated in
industry presently beating is controlled by the power the beater with the bedplate in its lowered (no load)
applied to the unit of pulp. Modern refiner control theory position until it was completely disintegrated. Beating
is introduced with the specific refining energy as the was initiated with the weight of 5500 ± 50 g by releas-
important measure of refining power put into the stock. ing the lever, and the timer was started when the bed-
The average magnitude of fibre deformation is plate bars move up against the bar roll.
directly related to the applied power divided by the prod- As recommended in standard beating schedules,
uct of rotating speed and edge length. This is the basis bleached pine (softwood) and eucalypt kraft pulp (hard-
of the Specific Edge Load Theory, which was first in- wood) samples were taken from the beater and tested at
troduced back in the 1960’s. The calculated variable is 5, 15, 30, 45 and 60 min intervals and unbleached pine
referred to as “refining intensity” or “specific edge load” kraft pulp samples were taken from the beater at 5, 15,
(SEL), and is typically expressed in units of watt-sec- 30, 60 and 90 min intervals.
onds per meter (Ws/m) or joule per meter (J m-1) [3, 4]. The total motor power (TMP) and no load power
It is possible to determine refining response of (NLP) in Watts, were measured with an Emta GP22
pulps with measuring of the refining power put in to model wattmeter and the rotational speed of the beater
the stock in pilot scale refiners [2, 5]. But this is a labour (RPM) was 509-513 rpm measured with a Line Seiki
intensive way that needs expensive and sophisticated TM-4000 model tachometer.
equipments. On the other hand in laboratory cooking In order to calculate the refining intensity or spe-
and bleaching research activities, a relatively small cific edge load, it is necessary to first determine the
amount of pulp is used, therefore using of laboratory true load or effective power applied (EPA) to the fi-
beating devices is necessary for evaluation and com- bers. Because of that, measured no load power was sub-
parison of the results. tracted from the total motor power. The cutting edge
The aim of this study is to determine the appli- length (CEL) of used the Valley beater is 34.16 m.r-1,
cability of the Valley Beater, one of the most widespread and the beating surface (BS) is 0.135 m² r-1. The spe-
laboratory beating devices, for measuring the power cific edge load (SEL) or refining intensity was calcu-
applied to the pulp. For this purposes beating responses lated by the effective power applied (TMP-NLP) di-
of some kraft pulp were used. vided by the rotating speed and cutting edge length.

EXPERIMENTAL SEL = [TMP − NLP] /[CEL × RPM] (1)

Bleached and unbleached calabrian pine kraft SSL = [TMP − NLP] /[BS × RPM] (2)
pulps and bleached eucalypt kraft pulp with air-dried
were suplied by Mopak Pulp and Paper Mill, Dalaman, SEL - Specific edge load (J m-1) or (W s m-1)
Turkey. The kraft pulps were reslushed by tearing the SSL - Specific surface load (J m-2) or (W s m-2)
lap pulp samples into thin pieces of less than 10 cm² The net specific beating energy consumption of
and soaking overnight in distilled water. All beating treat- a refiner or refining system determines the amount of
ments of pulps were performed with a Valley beater refining that is applied to a pulp in industry. In this
equipped and calibrated as described in the standard laboratory study, the specific beating energy for each
ISO 5264/1. The initial pulp amount was 360 g of oven step was calculated by dividing the effective beating
dry pulp and the consistency of the stock in the beater power by the oven dry fiber mass. It has been indicated
15.70 ±0.03 g/L. 18 L of water at 20 ±5°C was poured above that, over a beating period, pulp samples were

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C. Atic, S. Immamoglu, I. Valchev

Table 1. No load and total motor power applied to the certain pulps.

Beating Amount of Bleached Bleached Unbleached


Stage oven dry pulp eucalypt pine pine
NLP TMP NLP TMP NLP TMP
(g) (W) (W) (W) (W) (W) (W)
1 360.0 845 1005 870 1030 860 1110
2 341.2 815 967 845 1007 845 1075
3 322.4 795 941 815 995 820 1040
4 303.6 777 925 790 979 780 1010
5 284.8 755 910 772 962 750 995

taken from the tube at scheduled five intervals and ana- This energy produces no measurable change in the prop-
lyzed. Therefore at each step the 18.8 g oven-dry pulp erties of the pulp being beaten. No-load power is mostly
sample was decreased in the Valley beater tube. The dependent on the diameter and rotational speed of the
amount of decrease was taken into consideration when rotor, stock consistency and amount of pulp being circu-
the specific beating energy (SBE) was calculated for each lated. During the laboratory study all circumstances were
step. The total specific beating energy (TSBE) was beat- keep constant except pulp amount. As seen in Table 1,
ing energy that was applied from the beginning of the no load and total motor power decreased throughout the
beating to a particular beating step expressed as Wh kg-1. steps due to removal of sample from the tube. In addi-
Finally, the beating response (BRp) of a certain pulp was tion, fiber length and bleaching operation notably affected
calculated using Eq. 4 the no load and total motor power.
To better illustrate the influence of TSBE on
SBEn = [EPA n × BTn ] / FMn (3) Schopper Riegler values, the results are plotted in
Fig. 1. This figure shows clearly that Schopper Riegler
[ ]
BRp = SR o n − SR o n−1 / SBE n (4) values increas dramatically at higher TSBE levels. In
order to reach the same SR°, the unbleached pine needs
SBEn - Specific beating energy in the step, Wh kg-1 at least twice hiaher beating energy than that for the
EPA - Effective power applied (TMP-NLP), W bleached pine. The bleached eucalypt hardwood pulp,
n - Sample removal step having shorter fibre and fines, behavior is more sen-
BTn - Beating time in the step, h sible than that of the softwood pulp. Hence it is reached
FMn - Oven-dry fibres mass in the step, kg 50 SR° easily whenjust applying 500 Wh kg-1 SBE.
BRp - Beating response, DSR°/Wh kg-1
Freeness was measured using a Schopper Riegler
devices according to ISO 5267-1 standard method and the
preparation of laboratory sheets for physical tests were
based on ISO 5269-2 standard method. Mass, tensile prop-
erties, tearing resistance (Elmendorf method) and burst
strength were measured according to ISO 536, ISO 1924,
ISO 1974 and ISO 2758 standard methods respectively.

RESULTS AND DISCUSSION

In a valley beater application, a certain amount of


Fig. 1. Increase of Schopper-Riegler values with increasing beating
applied power is consumed for the circulation of the pulp. energy.

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Journal of the University of Chemical Technology and Metallurgy, 40, 3, 2005

Fig. 2 illustrates beating responses of pulp with beat-


ing time. Delta SR° values, for applied Wh per kg pulp of
bleached and unbleached pine pulps, increase gradually up
to some point. Maximum level was attained at stage 3 then
dropped at final stage. Eucalypt pulp indicates the similar
trend throughout the stages with slight increases.
In industry, beating or refining is controlled by
the beating intensity and randomly by SSL. The nature
of the fiber treatment in a valley beater device for labo-
ratory studies is very different compared to industrial
refining, and in admitted standard, beating is controlled
by the time elapsed. Hence, it is not possible to directly
compare the results of a laboratory test to the results of
on industrial one. In order to simulate a valley beater
Fig. 4. Tensile strength conversions according to applied SBE.
to the industrial application, SEL or beating intensity
and SSL plotted against beating time is shown in fig-
ure 3. In industrial applications, the net specific en- ergy of kraft pulp for 1 pass is about 40-80 Wh kg -1
for hardwood and 60-600 Wh kg-1 for soft-
wood, and SEL of kraft pulp is 0.4-1.5 J m-1
for hardwood and 2.0-6.0 J m-1 for softwood,
and SSL of kraft pulp is 200-500 J m-² for
hardwood and 500-1000 J m-² for softwood
[6].
With increasing beating time, the spe-
cific edge load of unbleached pine pulp de-
creases up to stage 3, then gradually increases
at the final stage. There is notably a distinc-
tion between unbleached and bleached pine
specific edge load. In the light of these re-
sults, control of beating in the valley beater
Fig. 2. Beating responses of pulps according beating time. can be easily made by specific edge load or
specific surface load.
Fig. 4 shows the results of tensile in-
dex as a function of the total specific beat-
ing energy. The tensile strength development
of softwood fibres increases rapidly from the
first to stage 3 where the applied energy is
about 250-350 Wh.kg-1 and becomes steady
after that. The tensile strength properties of
the eucalypt pulp increases slowly in every
stage.
Fig. 5 exhibits burst strength versus to-
tal specific energy. Burst strength develop-
ment is almost similar to tensile strength de-
velopment. Tearing resistance (Fig. 6) of soft-
Fig. 3. Beating intensity changes during beating. wood pulps decreases with beating while eu-

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C. Atic, S. Immamoglu, I. Valchev

ratories, is based on the time used for beating of fibers.


On the contrary, industrial application of the beating
theory usually refers to the specification of three pa-
rameters: SEL, SSL and SBE. Because of the fact that
the laboratory studies should be simulated with indus-
trial application.
Beating performance of three pulps (bleached and
unbleached calabrian pine kraft and bleached eucalypt kraft)
were investigated in a laboratory valley beater device.
Empirical SEL or beating intensity, SSL and SBE con-
Fig. 5. Burst index conversions according to applied SBE. sumption were experimentally found for each kraft pulp.

Fig. 5. Burst index conversions according to applied SBE.


Based on this laboratory study with certain kraft
pulps beaten in a valley beater instrument, it can be
concluded that:
• Beating intensity depends on the type of the
pulps and the amount of pulp which is decreased after
sample withdraw during treatment.
• Significant information about the amount of
energy and beating intensity must be necessary to put to
the certain pulp samples to reach required properties.
• Valley beater can be used for beating response
determination of pulp samples, and the influence of the
applied energy on development of strength properties
of pulps.
• Finally, these laboratory results will give sig-
nificant information about pulp properties and infor-
mation about that can be compared with other pulp and
Fig. 6. Tear index conversions according to applied SBE.
industrial applications.

REFERENCES

calypt pulp resistance increases. Changes of the tearing 1. C.E. Brandon, Properties of paper in Pulp and Paper;
index become more steady after applying of 300 Wh/kg Chemistry and Chemical Technology, Third Edition,
beating energy. J.P. Casey, A Wiley-Interscience Publication,
Toronto, v. 3, 1981, p.1715 -1956.
CONCLUSIONS 2. R. Sigl, , D. Bergfeld, Low intensity refining of hard
wood and deinked pulps with a new type of filling in
It has been agreed that simulation of industrial with a double disc refiner, TAPPSA J, July, 2001, p. 24- 29.
laboratory beating performance is really necessary to investi- 3. www.finebar.com., Introduction to stock prep refin-
gate and control beating performance of pulp and the labora- ing, Finebar Refining Technology, 2004, p.63.
tory beating method should be internationally acceptable, adopt- 4. D.H. Robinson, R.J. Defoe, Low Intensity Refining
able in industry, applicable for all fibre types and if possible of Mechanical Pulps, A New Approach to Quality
energy consumption during beating has to be measured. Control, Tappi Pulping Conf. Proc., 1984,p. 255 - 263.
The present version of the laboratory beating stan- 5. J. Blechscmidt, M. Strunz, New demands on labora
dard in a Valley beater which is widely used in labo- tory refining in quality assessment of paper pulps

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Journal of the University of Chemical Technology and Metallurgy, 40, 3, 2005

Proceedings of the European Conference on Pulp 6. J. Lumiainen, Selection of fillings and other refining
and Paper Research October 9-11, Stockholm, 1996, conditions for various pulps, PITA Mini-conference,
p. 226-230. Inverkeithing, Nov 1993.

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