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a
Julius Kruttschnitt Mineral Research Centre (JKMRC), University of Queensland, Isles Road, Indooroopilly, Qld, Australia
b
The CSIRO Thermal and Fluids Engineering Laboratory at Highett, Vic., Australia
Abstract
This paper presents and interprets results of experimental measurements of the spatial gas hold-up distribution in a 3 m3 glass rect-
angular otation cell at the JKMRC using two dierent techniques. The gas hold-up device with the capturing technique was developed
at the JKMRC and has been used widely in the P9 project1 while the one with conductivity technique was developed at the CSIRO Ther-
mal and Fluids Engineering laboratory at Highett, Victoria, Australia. Measurements were conducted at more than 64 locations in the
cell to determine the local gas hold-up distribution in the cell. Since the measurements using the two techniques were conducted at the
same locations, the results may be compared with each other.
The results indicate that the gas hold-up varies widely inside the otation cell. The gas hold-up distributions measured by the two
techniques are relatively similar except in some locations which can be reasonably explained.
2006 Elsevier Ltd. All rights reserved.
0892-6875/$ - see front matter 2006 Elsevier Ltd. All rights reserved.
doi:10.1016/j.mineng.2006.01.006
E. Sanwani et al. / Minerals Engineering 19 (2006) 13621372 1363
AC oscillator
capturing
probe
compressed conductivity
air probe
laptop
computer
froth (thin)
air layer
flows
rectangular
glass tank
impeller
shaft
stator
impeller
support arm
for the cell
Fig. 1. Schematic drawing of the experimental rig for the measurement of gas hold-up (eg).
stainless steel
three-way valve support arm
compressed air
the atmosphere
plastic
wire insulation
air
line
cylindrical pinch
rubber valve stainless steel
needle
=1.09 mm
silver plated
cylindrical copper wire
plastic tube
= 0.25 mm
pinch
cylindrical valve Fig. 3. Conductivity probe head assembly (not to scale).
rubber
Fig. 2. The gas hold-up device: capturing probe (JK sensor). laboratory at Highett, Victoria, and was modied at the
JKMRC during the experimental measurement. It con-
sisted of a needle and support arm. The needle had two
3.2.2. Conductivity probe (CSIRO sensor) electrodes at the tip. The probe was connected to an in-
The conductivity (or resistivity) probe, shown in Fig. 3, house AC oscillator developed at CSIRO that powers the
was developed at CSIRO Thermal and Fluids Engineering probe and supplies an output signal.
E. Sanwani et al. / Minerals Engineering 19 (2006) 13621372 1365
age was read due to the high resistance (Fig. 4). Over a per-
iod of sampling, the ratio of the total time when voltage 4
9 16.5
was high to the total sampling duration was interpreted 18
as the gas hold-up, i.e., B
14 11 0.0
8 17 20 23
X
in
Ti
eg 2 -16.5
7 3 16
i1
T total
During the measurements in the 3 m3 cell, the signal -40.5
10 2 19
from the probe was logged into a PC via a National Instru-
ment data acquisition board. Labview-based software was
used to count the bubble numbers and calculate the gas 13 1
22
-71.5
hold-up value.
-71.5 -40.5 -16.5 0.0 16.5 40.5 71.5
C (cm)
3.3. Experimental program A
Gas hold-up (eg) was measured using both the capturing Fig. 5. Points of measurement at each horizontal level.
and conductivity probes in a two-phase system of waterair
with Dowfroth 250 as a frother. The measurements of eg
were taken at many dierent points in the cell at the follow-
ing operating conditions:
95
frother dosage: 10 ppm
impeller speed: 255 rpm
air ow rate: 950 l/min
70
Table 1
Reproducibility of gas hold-up measurement at some dierent locations in the cell by capturing probe
Measurement location Gas hold-up (%) Standard deviation
Run 1 Run 2 Run 3 Run 4 Run 5 Average
Level 20, position 19 6.15 5.87 6.42 6.42 5.87 6.15 0.28
Level 45, position 14 7.82 7.54 6.42 6.98 6.42 7.04 0.64
Level 70, position 3 8.38 8.38 7.82 8.10 8.66 8.27 0.32
Table 2
Reproducibility of gas hold-up measurement at some dierent locations in the cell by conductivity probe
Measurement location Gas hold-up (%) Standard deviation
Run 1 Run 2 Run 3 Run 4 Run 5 Average
Level 20, position 19 5.70 6.31 6.26 6.94 5.93 6.23 0.47
Level 30, position 6 10.29 10.95 10.06 10.65 10.70 10.53 0.35
Level 45, position 14 6.55 7.90 7.11 7.57 7.47 7.32 0.51
Level 70, position 3 7.94 8.23 7.92 8.04 8.45 8.12 0.22
Level 95, position 1 9.33 9.31 9.71 9.27 8.90 9.30 0.29
average was considered as the gas hold-up value at that is composed of three principal regions, viz. the circulation
location. region above the impeller (quiescent zone), the circulation
region below it (turbulent zone-1), and the impeller dis-
3.4. Reproducibility charge stream (turbulent zone-2). This ow pattern was
observed visually from top, side, and bottom views of the
An important measure of any experiments is the repro- glass cell when the cell was running (under gas sparging
ducibility of the results. Tables 1 and 2 show the results of or with liquid only). Measurement of ow pattern in a
the reproducibility tests carried out with capturing and 0.95 m3 cylindrical Outokumpu otation cell in a single-
conductivity techniques respectively, for some locations phase of liquid system using a TSI 2D optical bre LDV
of measurement. Five measurements were made at each system by Zhu et al. (2004) conrmed this observation.
of measurement locations in the cell, and the average and In the circulation region above the impeller (above the
standard deviation of each location were calculated. The level of 35 cm), it can be seen that the gas hold-up values
standard deviation at each location of measurement is an resulting from the two measurement techniques are rela-
indication of how widely the value of gas hold-up spread tively similar except at some points e.g. at the level of
over the mean value at that location. The reproducibility 45 cm and about half-way between the impeller shaft and
of the eg measurements by capturing and conductivity tech- the wall, and at some points in the corners of the cell.
niques was found to be very good for both of them. At all In the corner region, it is harder to circulate the bub-
measurement locations, the standard deviations were bles, and consequently there is a sharp decrease of gas
mostly around the overall average of 0.51 and 0.46 for cap- hold-up as the corner is neared. In this region, the point
turing and conductivity techniques respectively, which are measurement from the conductivity probe will be dierent
very good. from that obtained using the capturing technique since the
latter technique has a capturing area diameter of 50 mm,
much larger than the conductivity probe tip, and is there-
4. Results and discussions fore less sensitive to changes occurring over a small
distance, i.e. the gas hold-up value is averaged over the
4.1. Comparison of the two techniques whole area.
In the impeller discharge stream (about at the level of
The results of measurements using capturing and con- 30 cm), the gas hold-up measured by conductivity probe
ductivity probes are presented in Figs. 7 and 8 as local gas are greater than in any other regions in the otation cell.
hold-up maps. At the level of 95 cm from the bottom of In this region, the radial velocity of the liquid is very high
the cell (near the surface), measurements were only taken resulting in a very high bubble passages frequency and,
using conductivity probe due to the size of capturing probe. consequently, a very high gas hold-up. The gas hold-up
Measurement using capturing probe were only able to be reduces considerably away from the impeller, as reected
taken up to the level of 70 cm from the bottom of the cell. in the conductivity probe data at z = 30 cm and both mea-
The gas hold-up maps of Figs. 7 and 8 show that eg var- surements at z = 20 cm. This decrease is not surprising, as
ies widely inside the otation cell. The ow eld in the cell (ignoring jet stream dispersion and recirculation of gas
E. Sanwani et al. / Minerals Engineering 19 (2006) 13621372 1367
(a) (b)
___-___ __-___
7.07 6.09 6.03
11.32 8.64
4.94 6.03 7.71 5.05 ___-___ ___-___
(c) (d)
(e)
Fig. 7. eg (%) values at dierent horizontal level of measurements from the bottom of the cell (italicsmeasured by capturing probe; normalmeasured
by conductivity probe): (a) level of z = 70 cm; (b) level of z = 45 cm; (c) level of z = 20 cm; (d) level of z = 30 cm; (e) level of z = 95 cm.
bubbles into the jet stream) mass conservation requires that from shaft axis). The magnitude of the gas hold-up data is
the gas hold-up should be the function of 1/r (r is the radius in reasonably agreement with the trend.
1368 E. Sanwani et al. / Minerals Engineering 19 (2006) 13621372
_-__ _-__ _-__ _-__ _-__ _-__ _-__ _-__ _-__ _-__ __-__ _-__
8.71 9.67 8.57 9.54 9.13 9.30 7.43 9.10 9.01 8.70 10.29 6.72
8.49 8.44 8.88 8.27 8.49 8.49 7.32 8.10 8.10 8.55 8.38 7.88
8.91 8.30 7.47 8.12 7.83 7.43 6.38 6.74 7.14 8.34 7.17 7.85
6.31 7.99 8.21 7.82 7.82 6.70 7.07 7.88 7.99 8.66 7.77 7.04
10.23 3.59 8.43 6.83 3.26 8.25 7.04 3.48 6.96 5.61 2.95 7.32
(a) (b)
_-__ _-__ _-__ _-__ __-__ __-__ __-__ __-__ _-__ _-__ _-__ _-__
7.01 9.18 7.66 8.70 10.37 10.34 10.87 10.29 9.43 8.77 9.22 6.89
5.81 8.60 8.66 8.77 7.82 5.59 5.70 8.66 8.44 8.38 7.77 5.98
6.21 8.79 6.64 7.48 8.44 10.00 11.28 8.44 8.24 7.96 7.67 5.92
5.75 8.04 7.71 8.60 7.71 _5.53 5.70 7.65 7.65 7.60 7.82 5.87
8.84 5.10 5.06 5.61 3.50 10.00 11.11 3.32 8.50 6.13 4.36 7.11
(c) (d)
Fig. 8. Distribution of eg (%) values at vertical plane of measurements (italicsmeasured by capturing probe; normalmeasured by conductivity probe):
(a) vertical plane A; (b) vertical plane B; (c) vertical plane C; (d) vertical plane D.
Near the wall, the gas ows upwards with the circulating the capturing probe due to the relative size of the probes.
liquid at high velocities, whereas near the impeller shaft the The detector of the conductivity probe is very small, with
buoyancy of the gas acts in an opposite direction to the diameter of 0.25 mm, whereas the diameter of capturing
downward owing uid. At the level of 45 cm and about tube is about 50 mm and 200 mm in high. Therefore, the
half-way between the wall and the impeller shaft, gas conductivity probe can detect a rapid change of gas hold-
hold-up measured by capturing probe is always bigger than up over a very small distance or, in other words, conductiv-
that measured by conductivity by about 23 fold, and this ity probe is more sensitive than capturing probe. Where the
phenomenon is consistent at every quadrant of the otation gas hold-up is uniform over a large volume, the results of
cell. This location is believed to be the location of a vortex the two techniques are comparable.
where liquid and gas velocities are very low resulting in very The conductivity probe is easier to handle than the cap-
low gas hold-up. This vortex is not able to be detected using turing probe, and to move from one point to another than
the capturing probe due to the size of the probe, since the capturing probe. It can also be operated on line. In addi-
vortex occupy only a small volume inside the cell. tion, it can measure gas hold-up in more locations of mea-
In the circulating region in the lower part of the otation surement in a otation cell, even in the locations which are
cell, the hold-up measured by conductivity probe decreases very close to the pulp-froth interface.
consistently towards the wall, with very low values near the Gas hold-up measurements using the two techniques
wall, in general, especially at the corners of the cell. These were only made in a two phase airwater system. While
locations are probably the locations of a second vortex of the capturing probe has been used widely in the real
the circulating loop. three phase system on industrial otation plants (Zheng,
In general, it can be said that the measurement of gas 2000; Power et al., 2000; Sanwani, 2003), the conductivity
hold-up using conductivity probe is more localized than probe needs to be tested in these systems. Because the con-
E. Sanwani et al. / Minerals Engineering 19 (2006) 13621372 1369
100 100
Diagonal #1
90 90 Diagonal #2
Corner #1
40 40
#1 #2
#3 #4
30 30
20 #1 #2
20
10 10
0 0
0 2 4 6 8 10 12 14 16 0 2 4 6 8 10 12 14 16
Gas Hold up (%) Gas Hold up (%)
(a) (b)
100
90 Diagonal #1
Diagonal #2
Vertical Position (Cm)
80 Diagonal #3
Diagonal #4
70
60
50
40
30
#3 #4
20 #1 #2
10
0
0 2 4 6 8 10 12 14 16
Gas Hold up (%)
(c)
Fig. 9. Vertical proles of gas hold-up at the diagonal positions: (a) outer or corner, (b) middle, and (c) inner (see inset).
100 100
90 90 Side #1
Side #1
Side #2
Vertical Position (Cm)
80 Side #2 80
Vertical Position (Cm)
Side #3
Side #3
70 Side #4
70 Side #4
60 60
50 #3 50
#4 #2 40
40
30 #1 30
#3
20 20 #4 #2
#1
10 10
0 0
0 2 4 6 8 10 12 14 16
0 2 4 6 8 10 12 14 16
Gas Hold up (%) Gas Hold up (%)
(a) (b)
100
90
Vertical Position (Cm)
80
70 Side #1
Side #2
60
Side #3
50 Side #4
40
30 #3
#4 #2
20 #1
10
0
0 2 4 6 8 10 12 14 16
Gas Hold up (%)
(c)
Fig. 10. Vertical proles of gas hold-up at the side positions: (a) outer, (b) middle, and (c) inner (see inset).
ductivity probe is principally based on bubble passed fre- itself, the eect of solid particles on the tip of the probe
quency, and does not directly measure the gas hold-up during the measurement needs to be investigated.
1370 E. Sanwani et al. / Minerals Engineering 19 (2006) 13621372
4.2. Proles of gas hold-up where left side shows bigger values of gas hold-up than
right side, and at the side near the wall (Fig. 9b) where
In order to make easier in reading and understanding the proles at each quadrant are slightly dierent. These
the proles of gas hold-up in a mechanical otation cell, anomalies are dicult to explain. Maybe the condition or
the data that have been shown in Figs. 7 and 8 are pre- position of the probe tip against the impeller during the
sented in the form of graphics as will be shown below. measurement at the corner and near the wall can cause
The proles shown here are the data of gas hold-up mea- the dierent, especially at the corner.
surement carried out using conductivity probe. This is The gas hold-up at the location near the bottom (at
because the measurement was carried out in the more loca- 20 cm from the bottom of the otation cell) is very low.
tions in the cell than using capturing techniques. This shows that only little gas exist in this region. At
30 cm from the bottom, the gas hold-up increases rapidly.
4.2.1. Vertical proles In this region, the gas hold-up reaches highest values. As
The vertical proles of gas hold-up are presented graph- explained earlier in the previous section, the radial velocity
ically as shown in Figs. 9 and 10. Fig. 9 shows the vertical of the liquid is very high resulting in a very high bubble
proles of gas hold-up at the diagonal positions, while passages frequency, and, consequently, a very high gas
Fig. 10 shows the proles at the side positions. As can be hold-up. It is expected that maybe attachment between par-
seen from Figs. 9 and 10, the proles at each quadrant ticles and bubbles take place more intense in this region
are generally comparable except at the corner (Fig. 9a) than others.
16 16
Diagonal #1
#1 #3
14 Diagonal #2 #4
14
Gas Hold up (%)
Side #3 #2
Gas Hold up (%)
12 12
Side #4
10 10
8 8
6 6 Diagonal #1 #1 #3
Diagonal #2 #4
4 4 Side #3 #2
Side #4
2 2
0 0
-1 -0.5 0 0.5 1 -1 -0.5 0 0.5 1
Radial Position Radial Position
(a) (b)
16 16
Diagonal #1 Diagonal #1
14 #1 #3 14 #1 #3
Diagonal #2 Diagonal #2 #4
Gas Hold up (%)
#4
Gas Hold up (%)
Side #3 12 Side #3 #2
12 #2
Side #4 Side #4
10 10
8 8
6 6
4 4
2 2
0 0
-1 -0.5 0 0.5 1 -1 -0.5 0 0.5 1
Radial Position Radial Position
(c) (d)
16
14
12
Gas Hold up (%)
10
6 Diagonal #1 #1 #3
Diagonal #2 #4
4 Side #3 #2
Side #4
2
0
-1 -0.5 0 0.5 1
Radial Position
(e)
Fig. 11. Horizontal proles of gas hold-up: (a) 20 cm, (b) 30 cm, (c) 45 cm, (d) 70 cm, and (e) 95 cm from the bottom of the otation cell (see inset).
E. Sanwani et al. / Minerals Engineering 19 (2006) 13621372 1371
At the location of 45 cm from the bottom (right above regions in the otation cell. The values decrease with dis-
the impeller) and about halfway between the impeller and tance away from the impeller.
the wall, the gas hold-up shows a very low in value. It is The conductivity probe has a number of advantages
very clear that this location is believed to be the location compared to the capturing probe as follows:
of a vortex. The possibility of attachment between particles
and bubbles is expected to be very low in this location. As it can be operated on line
the surface of the otation cell is neared, the gas hold-up it is easier to handle
increases gradually toward the surface. it can detect a rapid change of local gas hold-up over a
very small distance (more sensitive)
4.2.2. Horizontal proles it can be used to measure the gas hold-up in more loca-
The horizontal proles of gas hold-up at various dis- tion in the otation cell, even those close to the pulp-
tance (20 cm, 30 cm, 45 cm, 70 cm, and 95 cm) from the froth interface
bottom of the otation cell are presented graphically in
Fig. 11. As can be seen from this gure, the proles at each However, the conductivity probe has been used only in a
level are dierent. At the levels 20 cm and 30 cm, the pro- two-phase system of airwater and still needs to be tested
les are similar but the magnitudes are very dierent. At in real three-phase otation systems.
the level 20 cm, the gas hold-up is quite low and this is The proles of gas hold-up both vertically and horizon-
an indication that only little gas exist in this region. On tally are also presented graphically. In general, the proles
the other hand, the highest values of gas hold-up are show similar trend at each quadrant, except at some loca-
reached at the level of 30 cm (impeller discharge region). tion where anomalies found. Vertically, the proles show
This region is rich in air and is expected to have highest similar trends from the bottom of the otation cell toward
possibility of attachment between particles and bubbles. the surface but with dierent magnitudes depending on the
At the level 45 cm from the bottom of the otation cell distance from the impeller. On the other hand, the horizon-
(right above the impeller), the proles are not the same hor- tal proles show a dierent trend at each level from the
izontally. It can be seen from Fig. 11c, the lowest gas hold- bottom of the cell.
up is at the location about the halfway of distance between
the impeller and the wall. Once again, this location is the
Acknowledgements
location of vortex where liquid and gas velocities are very
low resulting in very low gas hold-up.
The authors would like to thank the JKMRC pilot plant
At the level 70 cm and 95 cm from the bottom of the o-
sta, especially Bob Marshall, Mick Kilmartin, Leo
tation cell (above the impeller and close to the surface), the
Koeleman, and Jon Worth for their help during the con-
proles of gas hold-up are similar. The gas hold-up at these
struction of the 3 m3 cell and during the test work, and
levels are relatively uniform, except at some locations in the
the JKMRC instrumentation laboratory sta, Graham
corners. The magnitudes are also not too dierent between
Sheridan and Kurt Russel, and Bon Nguyen of CSIRO
these two levels with the values increase slightly toward the
for their help in commissioning the conductivity probe.
surface of the otation cell.
Edy Sanwani would like to thank PT Freeport Indonesia
for nancial support of his doctoral studies, and the spon-
5. Conclusions sors of the AMIRA P9M project, without whom this work
would not has been possible.
Maps of local gas hold-up in a two phase airwater sys-
tem in a 3 m3 rectangular glass otation cell, measured by
capturing and conductivity probes, have been presented. References
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