Documenti di Didattica
Documenti di Professioni
Documenti di Cultura
Analysis
Guidelines for Estimating the
High- and Low-Temperature
Properties of Metals
J. Gilbert Kaufman
ASM International
Materials Park, Ohio 44073-0002
www.asminternational.org
Copyright 2011
by
ASM International
All rights reserved
No part of this book may be reproduced, stored in a retrieval system, or transmitted, in any form or by any
means, electronic, mechanical, photocopying, recording, or otherwise, without the written permission of the
copyright owner.
Great care is taken in the compilation and production of this book, but it should be made clear that NO
WARRANTIES, EXPRESS OR IMPLIED, INCLUDING, WITHOUT LIMITATION, WARRANTIES OF
MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE, ARE GIVEN IN CONNECTION
WITH THIS PUBLICATION. Although this information is believed to be accurate by ASM, ASM cannot
guarantee that favorable results will be obtained from the use of this publication alone. This publication is
intended for use by persons having technical skill, at their sole discretion and risk. Since the conditions of
product or material use are outside of ASMs control, ASM assumes no liability or obligation in connection with
any use of this information. No claim of any kind, whether as to products or information in this publication, and
whether or not based on negligence, shall be greater in amount than the purchase price of this product or
publication in respect of which damages are claimed. THE REMEDY HEREBY PROVIDED SHALL BE THE
EXCLUSIVE AND SOLE REMEDY OF BUYER, AND IN NO EVENT SHALL EITHER PARTY BE
LIABLE FOR SPECIAL, INDIRECT OR CONSEQUENTIAL DAMAGES WHETHER OR NOT CAUSED
BY OR RESULTING FROM THE NEGLIGENCE OF SUCH PARTY. As with any material, evaluation of the
material under end-use conditions prior to specification is essential. Therefore, specific testing under actual
conditions is recommended.
Nothing contained in this book shall be construed as a grant of any right of manufacture, sale, use, or
reproduction, in connection with any method, process, apparatus, product, composition, or system, whether or
not covered by letters patent, copyright, or trademark, and nothing contained in this book shall be construed as a
defense against any alleged infringement of letters patent, copyright, or trademark, or as a defense against
liability for such infringement.
Comments, criticisms, and suggestions are invited, and should be forwarded to ASM International.
Prepared under the direction of the ASM International Technical Book Committee (20102011), Michael J.
Pfeifer, Chair.
ASM International staff who worked on this project include Scott Henry, Senior Manager, Content Development
and Publishing; Steven R. Lampman, Content Developer; Sue Sellers, Editorial Assistant; Bonnie Sanders,
Manager of Production; Madrid Tramble, Senior Production Coordinator; and Diane Whitelaw, Production
Coordinator.
ISBN-13: 978-1-61503-824-4
ISBN-10: 1-61503-824-8
SAN: 204-7586
ASM International
Materials Park, OH 44073-0002
www.asminternational.org
Printed in the United States of America
Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals Copyright 2011 ASM International
J.G. Kaufman All rights reserved.
www.asminternational.org
Contents
Preface and Acknowledgments...............................................................v 5.3 Analysis of Data for the Sand Cast 300.0 Alloy Series62
About the Author....................................................................................vi 5.4 Analysis of Data for the Permanent Mold Cast 300.0 Alloy
Series66
5.5 Analysis of Data for the Die Cast 300.0 Alloy Series69
Chapter 1Introduction and Background 1
5.6 Summary of Baseline Relationships for All 300.0 Casting
1.1Relational Analysis of Temperature Effects1
Alloys72
1.2 Interrelation of Relational Analysis and Parametric Analysis2
5.7 Cast Aluminum Alloys of the 400.0, 500.0, and 700.0
Series 76
Chapter 2Relational Analysis Procedures5 5.8 Baseline Relationships for Cast Aluminum Alloys77
2.1 Procedure for Relational Analysis of Tensile Properties 5.9 Analysis of Subzero Temperature Data for Cast Aluminum
with Temperature6 Alloys78
2.2 Other Examples of Relational Analysis6 5.10Analysis of Elastic Moduli of Cast Aluminum Alloys80
2.3 Cautions in Using Relational Analysis 10
Chapter 6Application of Relational Analysis to New or
Chapter 3Accuracy of Relational Analysis for Several Wrought Untested Wrought and Cast Aluminum Alloys81
Aluminum Alloys 15 6.1 Alloy 1060-H14 and -H18 (Table 6.1)81
3.1 Alloy Alc 2014-T6 and -T651 (Table 3.1)15 6.2 Alloy 1350-O and -H18 (Table 6.2)84
3.2 Alloy 2021-T81 (Table 3.2)19 6.3 Alclad 2024-T3 and -T81 (Table 6.3) 86
3.3 Alloy 5005-O (Table 3.3)22 6.4 Propeller Alloys 2025-T6 (Table 6.4) 88
3.4 Alloy 6151-T6 (Table 3.4)25 6.5 Alloy 2324-T351 (Table 6.5)89
3.5 Alloy 7079-T6 (Table 3.5)26 6.6 Alloy 3105-O and -H22 (Table 6.6)90
3.6 Alloy 7080-T7 (Table 3.6)27 6.7 Alloy 5457-O and -H25 (Table 6.7)92
3.7 Conclusions about Accuracy and Precision28 6.8 Alloy 6005A-T5 and -T61 (Table 6.8)94
6.9 Alloys 6066-T6 and 6070-T6 (Table 6.9) 96
6.10Alloy 6082-T6 and -T651X (Table 6.10)98
Chapter 4Application of Relational Analysis to Archival 6.11Alloy 6351-T6 (Table 6.11)99
High- and Low-Temperature Tensile Property Data 6.12Alloy 7049-T73 and -T7352 (Table 6.12)100
for Wrought Aluminum Alloys29 6.13Alloy 7076-T6 (Table 6.13)102
4.1 Relational Analyses of Various Tempers of 1xxx and 3xxx 6.14 Permanent Mold (PM) Cast 357.0-T6 and A357.0-T6
Alloys29 (Table 6.14) 103
4.2 Relational Analyses of Various Tempers of 2x24 and Other
2xxx Alloys34
4.3 Relational Analyses of 4032-T643 Chapter 7Application of Relational Analysis to the High-
4.4 Relational Analyses of Various Tempers of 5xxx Aluminum Temperature Tensile Properties of Steel,
Alloys44 Magnesium Alloys, and Titanium Alloys105
4.5 Relational Analyses of Various Tempers of 6xxx Aluminum 7.1 AISI 200 Steels 105
Alloys47 7.2 AISI 300 Steels 107
4.6 Relational Analyses of Various Tempers of 7xxx Aluminum 7.3 AISI 400 Steels 109
Alloys48 7.4 AISI 600 Steels 110
4.7 Comparisons of Relational Analyses for Annealed Non-Heat- 7.5 Representative Examples of Other Steels 113
Treatable Alloys49 7.6 Baseline Relationships and Summary for Steels 115
4.8 Comparisons of Relational Analyses of Some 2xxx, 5xxx, 7.7 Relational Analyses of High-Temperature Moduli for Steels 117
6xxx, and 7xxx Alloys50 7.8 Magnesium Alloys 119
4.9 Application of Relational Analyses to Cryogenic Tensile 7.9 Titanium Alloys125
Properties54
4.10Application of Relational Analyses to Elastic Moduli56 Chapter 8Other Potential Applications of Relational
Analysis127
Chapter 5Application of Relational Analysis to Archival 8.1 Compressive, Shear, and Bearing Design Properties at High
High- and Low-Temperature Tensile Property Data and Low Temperatures127
for Cast Aluminum Alloys59 8.2 Alloy Selection for Equatorial Environments127
5.1 Analysis of Data for the Sand Cast 200.0 Alloy Series59 8.3 Alloy Selection for Enhanced Recycling Rates129
5.2 Analysis of Data for the Permanent Mold Cast 200.0 Alloy
Series61 Chapter 9References 131
iii
iv/Contents
Appendix AResource Data Utilized for Relational Analyses133 Appendix C Terminology and Nomenclature267
A1Compositions and Resource Data for Aluminum Alloys133 Selected Abbreviations267
A2Compositions and Resource Data for Steels 232 Glossary of Selected Terms267
A3Compositions and Resource Data for Magnesium Alloys248
A4Compositions and Resource Data for Titanium Alloys260 Appendix DAluminum Alloy and Temper Designation
Systems271
Alloy Designations271
Appendix B SI/Metric Unit Conversions265 Temper Designations272
Tensile and Tensile Yield Strengths265
Temperature265 Index273
Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals Copyright 2011 ASM International
J.G. Kaufman All rights reserved.
www.asminternational.org
It is the objective of this book to define and describe the potential usefulness of rela-
tional analysis in analyzing and extrapolating the properties of metallic alloys at high tem-
peratures and also for estimating the properties of those alloys for which little or no data
are available.
The use of relational analysis is illustrated by presenting a broad spectrum of high-tem-
perature tensile property data for aluminum alloys, using data generated from a single
source and developed using consistent testing procedures and practices. Data for a number
of steels, magnesium alloys, and titanium alloys from the literature are also presented and
analyzed.
Attention is called to the fact that the estimated high- and low-temperature properties of
metal alloys presented in this book based on the application of relational analysis are just
that, estimates, and have no statistical basis. Therefore, they are not to be considered as the
basis for design. Their usefulness lies primarily in filling in gaps in material property data
and for making preliminary judgments on materials selection and performance.
Attention is also called to the empirical and, to some degree, subjective nature of rela-
tional analysis. For this reason, relational analysis should be used with caution, carefully
considering the guidelines and limitations described in the text of this book.
The author gratefully acknowledges the past support of Alcoa, Inc. in providing the au-
thor and ASM International with access to many previously unpublished data for alu-
minum alloys. The author also acknowledges ASM International for access to a number of
its material property data archives.
v
Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals Copyright 2011 ASM International
J.G. Kaufman All rights reserved.
www.asminternational.org
John Gilbert (Gil) Kaufman has a background of over 50 years in the aluminum and
materials information industries and remains an active consultant in both areas. In 1997,
he retired as Vice President of Technology of the Aluminum Association, Inc., then head-
quartered in Washington, D.C. (now in Arlington, VA), and is currently president of his
own consultancy, Kaufman Associates.
Earlier in his career, he spent 26 years with the Aluminum Company of America, where
he managed engineering properties and fabricating metallurgical research at Alcoa Labo-
ratories. Many of the data presented in this book were generated during the period when
the author was active in and/or managing Alcoa Laboratories engineering properties re-
search.
Kaufman subsequently spent five years with ARCO Metals, where he was Director of
Research and Development and, later, Vice President of Research and Engineering.
Kaufman also served for nine years as President and Chief Executive Officer of the Na-
tional Materials Property Data Network where, working with STN International and
Chemical Abstracts Service, he established a worldwide online network of more than 25
numeric materials properties databases.
Gil is a Fellow and Honorary Member of ASTM International and a Fellow and Life
Member of ASM International. He is a licensed professional engineer in Ohio and Dela-
ware. Gil has published more than 140 articles and 5 books on aluminum alloys and mate-
rials data systems.
vi
Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals Copyright 2011 ASM International
J.G. Kaufman All rights reserved.
www.asminternational.org
Chapter 1
RELATIONAL ANALYSIS is the quantitative analysis of the been shown to be very useful for the analysis of creep and stress-
relationships among the known mechanical properties of metals rupture data for various metals (Ref 47). The greatest value de-
and alloys at various temperatures to their room-temperature ten- rived from parametric analysis is for interpolation and extrapola-
sile properties, with the object of using the calculated relation- tion of high-temperature creep and stress-rupture data in instances
ships to either interpolate or extrapolate the properties of those when there is already sufficient data for the alloy in question to
same alloys or to estimate the properties of related or similar al- permit derivation of a useful parametric equation, including the
loys. The use of relational analysis as defined, that is, by compar- value of a constant that satisfactorily collapses test data taken at
ing the relationships of the properties at various temperatures to various times at various temperatures into a single relationship, as
those at room temperature, has been found to be useful at temper- in Fig. 1.1. Parametric evaluation has some theoretical basis for its
atures both above and below room temperature. use (Ref 46).
While not always recognized by the term relational analysis, However, parametric analysis has serious limitations in the
there have been and still are a number of applications of the rela- analysis of the tensile properties of these same alloys (Ref 7), as
tionships among various properties of metal alloys to their room- illustrated in Section 1.2 of this chapter, and by itself is of little
temperature tensile properties in use today. For example, for many value for this purpose without a reasonable amount of test data for
years, the room-temperature compression, shear, and bearing de- the specific alloy in question.
sign properties of metal alloys have been generated using the In contrast, relational analysis is a purely empirical approach
measured relationships among these properties and the tensile that provides useful estimates of the high- and low-temperature
strengths and tensile yield strengths of those metals. Illustrations tensile properties of alloys for which little or no data are available,
of this may be found in The Aluminum Design Manual (Ref 1), the provided that tensile property data for some alloys of similar com-
American Institute of Steel Constructions Code of Standard
Practice for Steel Buildings and Bridges (Ref 2), and the Metallic
Materials Properties Development and Standardization (MMPDS)
Handbook (previously known as MIL-HDBK-5), the aerospace
design bible (Ref 3). These examples are examined more closely
in Section 2.2, Other Examples of Relational Analysis, in Chap-
ter 2 of this book.
position are available. Relational analysis is based solely on the level, because it stems primarily from empirical observations that
quantitative analysis of the relationships among the properties of the material properties of groups of alloys in many metallic sys-
metals at different time-temperature exposures to their original tems follow patterns that prove useful in predicting those same
room-temperature values, as described in more detail in Chapter 2 properties in similar alloys.
of this book. Parametric analysis, on the other hand, uses some of the princi-
Specifically, relational analysis has great value for analyzing the ples of rate-process theory (Ref 1, 8, 9) to analyze creep and
high-temperature tensile properties of metals, particularly alu- stress-rupture properties of metals, leading to time-temperature
minum alloys because of their complex dependence on both time parameters useful for the interpolation and extrapolation of those
and temperature of exposure. As illustrated herein, it also seems properties to conditions beyond the range of recorded test data.
to be of use in analyzing data for steels, magnesium alloys, and Parametric analysis is most useful for creep and stress-rupture
titanium alloys, and potentially for other metal alloy systems as properties, with very limited or no value for tensile properties or
well. other mechanical properties for which both time and temperature
Recommendations for the use of relational analysis are not are not involved, as was illustrated in Ref 7.
meant to exclude the use of any other techniques for analyzing In Ref 7, high-temperature tensile strength and tensile yield
high-temperature data. Relational analysis is simply another com- strength data for 5456-H321 were analyzed using the Larson-
plement to the usual means, notably graphical analysis. In fact, il- Miller parameter. Figures 1.2 and 1.3 present the resultant plots
lustrations are provided of the usefulness of graphical analysis in of tensile and yield strength, respectively, as a function of the Lar-
combination with relational analysis. son-Miller parameter. Larson-Miller equation constants of 54 and
46 were used for tensile strength and yield strength, respectively.
As illustrated in Fig. 1.2 and 1.3, the parametric approach does
1.2Interrelation of Relational Analysis and not work very well at relatively high and relatively low tempera-
Parametric Analysis tures within the range of interest. It was not possible to identify a
Larson-Miller constant that would bring data across the entire
It is understandable that there may be some confusion in under- range of interest into a single relationship. At intermediate tem-
standing the differences between relational analysis and paramet- peratures, say 300 to 400 F, some success in interpolating or ex-
ric analysis of the properties of metals (Ref 47). While both serve trapolating may be possible, but the overall parametric relation-
to aid in interpolating and extrapolating properties to conditions ship is of little value, especially at temperatures of 450 F and
for which test data do not exist, they are quite different. higher.
As noted previously, relational analysis is a purely empirical ap- This is in contrast to the case for stress-rupture data for 5456-
proach based on quantitative analysis of the relationships among H321. As illustrated in Fig. 1.1, a relatively smooth and consistent
the measured properties of metal alloys to their room-temperature Larson-Miller parametric relationship was developed for the
tensile properties. There is little theoretical basis for this at any stress-rupture strengths of welded 5456-H321. That relationship
Fig. 1.2 Larson-Miller parametric master curve for tensile strengths of 5456-H321 plate. Source: Ref 7
Chapter 1:Introduction and Background/3
Fig. 1.3 Larson-Miller parametric master curve for tensile yield strengths of 5456-H321 plate. Source Ref 7
would be quite useful for either interpolation or extrapolation over alloy in question to permit derivation of a single time-temperature
the entire temperature range. parameter (Fig. 1.1). In contrast, relational analysis is a purely
In summary, it appears that these two types of analysispara- empirical approach that provides useful estimates of the high-tem-
metric and relationalstand alone in their value in achieving perature tensile properties of alloys for which little or no data are
specific objectives. As noted, parametric analysis is useful for available, provided that tensile property data for some alloys of
interpolation and extrapolation of high-temperature creep and
similar composition are available
stress-rupture data when there is already sufficient data for the
Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals Copyright 2011 ASM International
J.G. Kaufman All rights reserved.
www.asminternational.org
Chapter 2
RELATIONAL ANALYSIS, defined as quantitative analysis of tem rather than the International System of Units (SI) or metric
the relationships of high- and low-temperature properties in rela- units. This was done because all of the tabular and graphical data
tion to their room-temperature values, provides a useful technique presented herein were generated using the English/engineering
for estimating the properties of similar metals and alloys for which system, and conversions would have added potential confusion
limited or no data are available. This results from the fact that and unnecessarily odd numbers for temperatures and properties.
within specific alloy compositions and/or temper/production prac- For those interested in SI/metric units and methods for the conver-
tices, some relative uniformity in the relationships is often ob- sion of data herein to SI/metric equivalents, attention is called to
served and can be used in estimating the properties of other mate- the conversions listed in Appendix B.
rials of the same or similar type(s). There are several terms and abbreviations used regularly in the
The method of relational analysis is described in this chapter, text, tables, and figures that are noted as follows:
along with some specific guidelines and caveats in its use. Subse-
quent chapters illustrate the application of relational analysis of
Baseline relationship: The relationship calculated by rela-
tional analysis with data from one or more source alloys to
wrought and cast aluminum alloys, including its application in
be used to estimate the high- and/or low-temperature proper-
Chapter 6 to estimate the properties of wrought and cast aluminum
ties of a target alloy
alloys for which few or no test data exist. Chapter 7 illustrates the
application of relational analysis to data for steels, magnesium al-
Source data or source alloy(s): Data for an alloy or alloys for
which high- and/or low-temperature data are used for rela-
loys, and titanium alloys. Chapter 8 includes speculation about
tional analyses
some additional applications of relational analysis in judging
properties and performance of metals.
Target alloy: An alloy for which estimates of high- and/or low-
temperature properties are desired using relational analysis
As noted in Chapter 1, the use of relational analysis is not meant
to exclude the use of other techniques, such as parametric analysis
TS: Tensile strength, ultimate tensile strength
of time-temperature conditions for creep deformation and stress
TYS or YS: Tensile yield strength, at 0.2% offset unless other-
wise noted
rupture. Relational analysis is simply a quantitative method of an-
alyzing the relationships among the known mechanical properties
El or Elong: Elongation in 2 in. or 4D, where D is the speci-
men diameter
of metals and alloys at various temperatures relative to their room-
temperature tensile properties. The objective of using the calcu-
T: Test temperature
lated relationships is either to interpolate or extrapolate the prop-
t: Time at test temperature
erties of those same alloys or to estimate the properties of related
Avg: Average relationship for the property and/or baseline
group being analyzed
or similar alloys that have not previously been tested. The use of
relational analysis also has been found to be useful at tempera- A broader list of definitions of terms is provided in Appendix C,
tures both above and below room temperature. Terminology and Nomenclature, and the alloy and temper des-
The source data for the relational analyses discussed herein are ignations used herein for aluminum alloys are described in Ap-
from Ref 8 to 12. Because relational analysis may be relatively pendix D.
subjective by nature, depending on the breadth of available source One important caveat concerning the use of relational analysis
data, all of the source data used in analyses discussed herein are involves the character of the resources, that is, the test data, used
presented in Appendix A, along with their relational analyses. in the analysis. For optimum results, it is highly desirable that the
Readers are encouraged to carry out their own analyses of the collections of actual test data used as the starting point have been
available information, and reach their own conclusions. obtained, analyzed, and reported using the same test procedures,
It is appropriate to note at this point that throughout most of this including, ideally from the same laboratory. This ideal is met
book, the principal focus is placed on the calculation and presen- nicely for the aluminum alloys in this study by using the substan-
tation of mechanical properties in the English or engineering sys- tial archive of high- and low-temperature data obtained for alu-
6 /Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals
minum alloys at various temperatures at Alcoa Laboratories and alloy led to the relationship shown for the T9 temper, it still
made available previously for publication by ASM International represents the best information available for use as a baseline.
(Ref 10). Illustrations of the use of these principles for other me-
tallic alloys, including steels (Ref 11), magnesium alloys (Ref 8, To illustrate how this information would be applied in estimat-
12), and titanium alloys (Ref 9), are also provided herein, although ing the tensile properties of another alloy for which little or no
such a consistent comparable archive of reliable data for these al- data are available, estimates were derived in Table 2.4 of the high-
loys was not available to the author. and low-temperature tensile properties of 6151-T6. This is an
alloy not included in the original analysis described in Tables 2.1
and 2.2 but for which some high-temperature tensile property data
2.1Procedure for Relational Analysis of Tensile were available. The following are tabulated in Table 2.4:
Properties with Temperature Source relationships for 6xxx alloys in the T5 or T6 tempers
from Table 2.2
From the original tensile property data, relational analyses are
made of the data for the individual alloys and tempers, leading to
Estimated properties of 6151-T6 based on relational analysis
(i.e., multiplying the percentages in the previous column times
tabulations of baseline percentages of room-temperature tensile
the room-temperature typical tensile properties of 6151-T6)
strength, tensile yield strength, and elongation as a function of
temperature. These are the relationships that may be used in inter-
Previously independently measured properties for that alloy
and temper for comparison
polating and extrapolating from existing data or estimating the
properties of similar alloys for which no data are available. Typi- The agreement between the properties estimated using relational
cally, most attention is paid to the relationships for tensile strength analysis (columns 2, 5, and 8) and the measured tensile properties
and tensile yield strength rather than to those for elongations, be- (columns 3, 6, and 9) is reasonably good over the entire range.
cause the latter are not typically used in quantitative assessments There are differences of as much as 2 or 3 ksi, but such differences
of alloy performance. are normal for different lots of the same alloy and temper. Overall,
To illustrate the usual procedures for the application of rela- the relational analysis has provided reasonable estimates of the
tional analysis, the tensile properties of several Al-Mg-Si (6xxx- high- and low-temperature tensile properties of 6151-T6.
series) aluminum alloys at high and low temperatures are consid-
ered first. The original resource data are shown in Tables A1.19
through A1.23 in Appendix A1; they describe the effects of time at 2.2 Other Examples of Relational Analysis
temperature on the tensile properties of several 6xxx-series alloys:
6061, 6063, 6101, 6262, and 6351. As noted in Chapter 1, estimated design properties have been
Continuing the illustration, these baseline relationships are de- derived for many years using a form of relational analysis, that is,
veloped in the following manner: by using the relationships between the properties in question and
the room-temperature tensile properties. Some specific illustra-
1.The tensile properties of each of the alloy(s) in question for tions are given here.
which data are available are input to Excel (or other numerical) Structural Design Properties in Metallic Materials Proper-
spreadsheets of the type in Table 2.1, using 6061-T6 as the ex- ties Development and Standardization (MMPDS) Handbook
ample. Similar analyses are made for each of the alloys in the (Ref 3). The generation of expected minimum (design) values of
group being studied, in this case, the other four 6xxx alloys metallic alloys for use in aircraft structures, as defined in Chapter
mentioned earlier. 9 of MMPDS (formerly known as MIL-HDBK-5), the structural
2.The relationships generated for the several alloys being studied design bible for the aircraft industry, is carried out by:
are combined into a table of the type shown in Table 2.2, in
three parts, for tensile strength, tensile yield strength, and elon- 1.Measuring the properties of interest, typically the tensile, com-
gation. This places the alloys where the relationships for the pression, shear, and bearing properties, for a representative
alloys in question can be readily compared and, where appro- sampling (usually at least ten lots) of the alloy and temper in
priate, averaged. question
3.Using the data tabulated in Table 2.2, comparisons are made to 2.Calculating the average ratios of the compression, shear, and
establish the similarities and divergences of the alloys in ques- bearing properties to the tensile properties of the same lots, and
tion, to see which may be averaged to determine baseline rela- noting specifically the average ratios of shear strength and
tionships for some or all of the alloys and tempers. In this case, bearing ultimate strength to the tensile strength and the ratios
it appears that data for all of these alloys in the T5 and T6 tem- of compressive yield strength and bearing yield strength to the
pers follow relatively similar patterns, while the pattern for the tensile yield strength.
one T9 temper alloy differs a bit and should not be averaged in 3.Using those relationships to generate the expected minimum or
with the others. design compression, shear, and bearing properties by multiply-
4.Based on the analysis of data of the type in Table 2.2, the base- ing those ratios times the guaranteed minimum tensile strength
line values are calculated for tensile strength, tensile yield and tensile yield strength of that same alloy and temper. The
strength, and elongation; they are presented in Table 2.3 as the guaranteed tensile properties are those expected to be met by
baseline relationships for 6xxx alloys. While data for only one 99% of lots with 95% confidence.
Chapter 2:Relational Analysis Procedures/7
Table 2.1Example of relational analysis of high- and low-temperature tensile properties of 6061-T6
Tensile
yield Elongation
Tensile strength, Tensile strength, in 2 in. or 4D,
Test Holding Tensile % of room- yield % of room- Elongation % of room-
Alloy temperature, temperature, Holding strength, temperature strength, temperature in 2 in. temperature
name UNS No. Temper F F time, h ksi value ksi value or 4D, % value
6061 A96061 T6, T651 452 . . 74 164 53 133 27 159
6061 A96061 T6, T651 423 . . 73 162 53 133 27 159
6061 A96061 T6, T651 320 . . 58 129 46 115 23 135
6061 A96061 T6, T651 112 . . 49 109 42 105 19 112
6061 A96061 T6, T651 18 . . 47 104 41 103 18 106
6061 A96061 T6, T651 75 . . 45 100 40 100 17 100
6061 A96061 T6, T651 75 212 10 45 100 40 100 17 100
6061 A96061 T6, T651 75 212 1000 46 102 41 103 17 100
6061 A96061 T6, T651 75 212 10,000 46 102 42 105 17 100
6061 A96061 T6, T651 75 300 10 46 102 41 103 16 94
6061 A96061 T6, T651 75 300 1000 43 96 40 100 16 94
6061 A96061 T6, T651 75 300 10,000 39 87 35 88 17 100
6061 A96061 T6, T651 75 350 10 44 98 40 100 16 94
6061 A96061 T6, T651 75 350 1000 38 84 34 85 16 94
6061 A96061 T6, T651 75 350 10,000 33 73 27 68 18 106
6061 A96061 T6, T651 75 400 10 40 89 36 90 16 94
6061 A96061 T6, T651 75 400 1000 31 69 24 60 17 100
6061 A96061 T6, T651 75 400 10,000 26 58 18 45 19 112
6061 A96061 T6, T651 75 450 10 34 76 28 70 17 100
6061 A96061 T6, T651 75 450 1000 25 56 15 38 19 112
6061 A96061 T6, T651 75 450 10,000 20 44 11 28 24 114
6061 A96061 T6, T651 75 500 10 29 64 20 50 18 106
6061 A96061 T6, T651 75 500 1000 21 47 10 25 24 141
6061 A96061 T6, T651 75 500 10,000 18 40 8 20 30 176
6061 A96061 T6, T651 75 600 10 23 51 12 30 22 129
6061 A96061 T6, T651 75 600 1000 18 40 8 20 30 176
6061 A96061 T6, T651 75 600 10,000 18 40 8 20 30 176
6061 A96061 T6, T651 75 700 10 18 40 8 20 30 176
6061 A96061 T6, T651 75 700 1000 18 40 8 20 30 176
6061 A96061 T6, T651 75 700 10,000 18 40 8 20 30 176
6061 A96061 T6, T651 212 212 10 41 91 38 95 18 106
6061 A96061 T6, T651 212 212 1000 42 93 39 98 18 106
6061 A96061 T6, T651 212 212 10,000 42 93 39 98 18 106
6061 A96061 T6, T651 300 300 10 38 84 36 90 19 112
6061 A96061 T6, T651 300 300 1000 38 84 36 90 18 106
6061 A96061 T6, T651 300 300 10,000 33 73 31 78 19 112
6061 A96061 T6, T651 350 350 10 36 80 35 88 18 106
6061 A96061 T6, T651 350 350 1000 30 67 28 70 19 112
6061 A96061 T6, T651 350 350 10,000 24 53 22 55 22 129
6061 A96061 T6, T651 400 400 10 30 67 29 73 18 106
6061 A96061 T6, T651 400 400 1000 22 49 20 50 23 135
6061 A96061 T6, T651 400 400 10,000 17 38 14 35 28 165
6061 A96061 T6, T651 450 450 10 24 53 23 58 18 106
6061 A96061 T6, T651 450 450 1000 15 33 13 33 30 176
6061 A96061 T6, T651 450 450 10,000 12 27 8.5 21 40 235
6061 A96061 T6, T651 500 500 10 18 40 16 40 20 118
6061 A96061 T6, T651 500 500 1000 10 22 8 20 45 265
6061 A96061 T6, T651 500 500 10,000 8 18 6 15 65 382
6061 A96061 T6, T651 600 600 10 9 20 8 20 30 176
6061 A96061 T6, T651 600 600 1000 5 11 4.2 11 80 471
6061 A96061 T6, T651 600 600 10,000 5 11 4.2 11 80 471
6061 A96061 T6, T651 700 700 10 3.6 8 3 8 80 471
6061 A96061 T6, T651 700 700 1000 3.6 8 3 8 80 471
6061 A96061 T6, T651 700 700 10,000 3.6 8 3 8 80 471
This application of the average relationships represents an exam- an unacceptable deformation at a bolt or rivet hole, in the ADM
ple of relational analysis as it is defined in this book. (Ref 1). It has been determined from years of testing in accord-
Bearing Design Properties of Aluminum Alloys in The Alu- ance with ASTM E 238 and confirmed more recently in a study
minum Design Manual (ADM) (Ref 1). Another example of the conducted by Dr. Craig Mensemer at the University of Akron (Ref
application of relational analysis in the aluminum industry is the 13) that the bearing ultimate stress for aluminum is approximately
treatment of bearing design strength, the stress that will produce equal to twice the tensile ultimate strength, or Fbru = 2Ftu. This is
8 /Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals
Table 2.2Relational analysis of high- and low-temperature tensile properties of 6xxx-series aluminum alloys
Testing Holding Holding Tensile strength, % of room-temperature value
temperature, temperature, time,
F F h 6061-T6 6063-T5 6063-T6 6101-T6 6262-T9 6351-T5 6351-T6 Avg T5 Avg T6 Avg 6xxx
452 . . 164 175 . . . . . 175 164 170
423 . . 162 . . . . . . . 162 162
320 . . 129 134 134 134 128 131 131 133 132 132
112 . . 109 109 109 113 107 113 113 111 111 110
18 . . 104 103 103 106 103 107 106 105 105 105
75 . . 100 100 100 100 100 100 100 100 100 100
75 212 10 100 100 100 100 100 100 100 100 100 100
75 212 1000 102 103 106 100 102 102 104 103 103 103
75 212 10,000 102 103 109 100 98 100 100 102 103 102
75 300 10 102 103 106 100 98 100 102 102 103 102
75 300 1000 96 100 97 94 86 87 85 94 93 92
75 300 10,000 87 81 80 84 72 73 73 77 81 79
75 350 10 98 103 103 97 91 98 98 101 99 98
75 350 1000 84 78 77 81 66 67 73 73 79 75
75 350 10,000 73 69 60 63 52 51 58 60 64 61
75 400 10 89 91 83 91 78 80 83 86 87 85
75 400 1000 69 66 57 63 50 51 58 59 62 59
75 400 10,000 58 53 46 47 40 38 42 46 48 46
75 450 10 76 78 71 78 62 69 71 74 74 72
75 450 1000 56 56 46 47 41 42 42 49 48 47
75 450 10,000 44 41 37 41 36 33 31 37 38 38
75 500 10 64 66 57 63 52 53 58 60 61 59
75 500 1000 47 41 40 41 38 38 35 40 41 40
75 500 10,000 40 38 34 41 34 38 . 38 38 38
75 600 10 51 50 40 44 40 38 40 44 44 43
75 600 1000 40 38 31 38 34 36 . 37 36 36
75 600 10,000 40 38 31 38 31 . . 38 36 36
75 700 10 40 44 37 41 38 . . 38 39 40
75 700 1000 40 34 31 38 . . . 31 36 36
75 700 10,000 40 34 29 38 . . . 31 36 35
212 212 10 91 91 89 88 95 89 90 90 90 90
212 212 1000 93 91 91 88 95 91 90 91 91 91
212 212 10,000 93 94 94 88 91 91 90 93 91 92
300 300 10 84 84 80 78 86 80 81 82 81 82
300 300 1000 84 81 80 75 74 67 67 74 77 75
300 300 10,000 73 66 63 66 60 56 56 61 65 63
350 350 10 80 84 71 72 72 73 73 79 74 75
350 350 1000 67 56 57 59 50 49 52 53 59 56
350 350 10,000 53 50 40 47 38 38 46 44 47 45
400 400 10 67 63 57 59 55 56 54 60 59 59
400 400 1000 49 44 37 41 33 33 35 39 41 39
400 400 10,000 38 34 26 31 24 21 25 28 30 28
450 450 10 53 50 43 47 40 42 44 46 47 46
450 450 1000 33 34 23 27 22 20 19 27 26 25
450 450 10,000 27 23 17 22 19 16 13 20 20 20
500 500 10 40 38 29 34 26 27 33 33 34 32
500 500 1000 22 20 14 17 16 12 . 16 18 17
500 500 10,000 18 16 13 15 15 . . 16 15 15
600 600 10 20 20 11 15 12 . . 20 15 16
600 600 1000 11 11 9 10 9 . . 11 10 10
600 600 10,000 11 10 9 9 9 . . 10 10 10
700 700 10 8 8 7 8 7 . . 8 8 8
700 700 1000 8 7 7 8 6 . . 7 8 7
700 700 10,000 8 6 7 8 6 . . 3 8 7
addressed in the 2010 ADM, Part I, Section J.3.7 and J.4.7, and the available. Several such cautions are noted here, particularly with
corresponding commentary in Part II, wherein the bearing design respect to the selection of so-called resource alloys in establish-
strength is calculated using this ratio. ing reliable baseline relationships. Resource alloys should be as
The steel industry uses the same approach, citing in the Ameri- similar as possible in terms of alloy composition and fabrication
can Institute of Steel Constructions structural steel design code methods.
(Ref 2) that the ultimate bearing strength for steels is 2.4 times the The most reliable baseline relationships are those developed
ultimate tensile strength for steels. using multiple source alloys for the type of alloy and temper rep-
resented by the target alloy for which properties are to be esti-
mated. A greater number of source alloys used to develop baseline
2.3 Cautions in Using Relational Analysis relationships improves the level of confidence. It is also beneficial
to have consistent data for the multiple source alloys (i.e., data for
The usefulness of relational analysis is detailed in subsequent the same combinations of time and temperature for each of the
chapters for aluminum, steel, magnesium, and titanium alloys, source alloys). For those temperatures or exposure times at tem-
with the greatest emphasis on aluminum because of the more perature for which data for one or more of the source alloys are
complex dependence of its strength on both time and temperature missing, the remaining data may skew the average relationships.
of exposure, and the availability of a wealth of archival data (Ref The most reliable relationships are those for which actual test data
10). Relationships have been shown to be fairly consistent within for all source alloys are represented at all time-temperature test
individual alloy series for each metal, sometimes with some con- conditions being analyzed.
sistency also with fabrication practice. For all of these reasons, each discussed below in more detail, it
It is appropriate to note several very important cautions when is important to consider all high- or low-temperature data derived
preparing to use relational analysis to estimate the properties of an with relational analysis to be estimated values, not to be used in
alloy for which high- and/or low-temperature properties are not design without verification testing.
Chapter 2:Relational Analysis Procedures/11
Table 2.3 Summary of relationships among tensile properties for various tempers of 6xxx aluminum alloys at various
temperatures
Average relationships, % of room-temperature value
Composition Variables. As already noted in the latter part of the target alloy as possible. An illustration of the challenges that
Section 2.1 of this chapter, relationships of high- and low-temper- may be encountered when relational analysis is carried out using
ature properties to room-temperature properties vary with compo- source alloys with different alloying elements from those in the
sition, especially with significant differences in major alloying el- target alloy is shown in the example for 2021-T8 in Section 3.2 in
ements. Therefore, it is important to select a resource alloy or Chapter 3 of this book.
alloys (i.e., those whose relationships will be used as the pattern Fabrication Variables. In some cases, relationships also vary
for estimating properties) with a composition as close to that of with fabrication practice or temper. Therefore, it is important to
12 /Relational AnalysisGuidelines for Estimating the High- and Low-Temperature Properties of Metals
Table 2.4Relational analysis prediction accuracy for high- and low-temperature tensile properties of aluminum alloy 6151-
T6
Tensile strength (TS) Tensile yield strength (TYS) Elongation (El) in 4D
select the resource alloy with production history as close as practi- alloy 2024 in Table 4.3, discussed in Section 4.2 in Chapter 4 of
cal to that of the target material, most notably, distinctions be- this book.
tween heat treated and non-heat-treated alloys. An illustration of Advantage of Having Multiple Source Alloys. The most reli-
the degree to which relationships may vary with different fabrica- able baseline relationships are those developed using multiple
tion histories is included in the data for five tempers of aluminum source alloys for the type of alloy and temper represented by the
Chapter 2:Relational Analysis Procedures/13
target alloy for which properties are to be estimated. The greater ever, because the principal purpose of relational analysis is to note
the number of source alloys, the greater the dependability of the changes with temperature, some variations in test procedures can
relationships derived. There are times when only one source alloy be tolerated.
of suitable composition and temper/fabrication history is availa- Subjective Analysis. It is appropriate to note that some aspects
ble, and it may well be useful to make estimates for a comparable of the use of relational analysis rely on subjective analysis, for
target alloy based on the one source. However, in such circum- example, whether data for specific alloys should or should nor be
stances, the resulting estimate will not be as reliable as if multiple averaged, or judging how best to deal with missing data points.
source alloys had been available. This means that different investigators may come to different con-
Consistency of Source Data Patterns. In developing baseline clusions using the same data for relational analyses. It is for this
relationships, it is most useful to have consistent data for the mul- reason that all of the raw data used in the analyses presented
tiple source alloys, that is, data for the same combinations of time herein are provided in the appendixes, with encouragement for
and temperature for each of the source alloys. For those tempera- those interested to perform their own independent analyses.
tures or exposure times at temperature for which data for one or Variability of Elongation Values. Because elongation values
more of the source alloys are missing, the remaining data may tend to be much more variable than tensile strengths and yield
skew some points in the average relationships. The most reliable strengths, relational analysis is not as helpful in interpolating or
relationships are those for which all source alloys are represented extrapolating those values to other alloys and tempers. For that
by actual measured test data at all time-temperature conditions reason, the value of relational analysis for estimating elongation is
being considered. For those time-temperature combinations for more limited than for estimates of tensile strength and tensile
which no data are available for one or more source alloys, some yield strength. This does not minimize the value of relational anal-
adjustment may need to be made in the calculated percentage to ysis very significantly, because elongations are usually less impor-
minimize the bias of the remaining source alloys. Graphical plot- tant in quantitative analyses of material performances. In cases
ting of the results of relational analysis assists in minimizing the where elongation values were available for the alloys discussed
effects of missing data points. herein, they were included in the analysis, but little use is made of
Consistency of Test Procedures. In cases where the source al- the average relationships.
loys were tested in different laboratories, care must be taken to be Lack of Adequate Resource. In some cases, there simply are
sure that other variables in the data have not been introduced by no suitable resource alloys that will enable the useful estimate of
differing test procedures used at the different labs. Ideally, all of the properties of a particular alloy. In those cases, there may be no
the source alloys will have been tested using the same practices, alternative but to begin testing. An illustration of such a problem
those represented by ASTM E 139 (Ref 14), especially for varia- for an aluminum alloy is described in Section 3.2 in Chapter 3 of
bles such as yield strength offset and specimen gage length. How- this book.