A-141, EPIP, RIICO Industrial Area, Neemrana, Rajasthan, India

CERTIFICATE OF ANALYSIS
Department : Quality Control
Title : Nicotinamide
Batch No. : 15-0541 AR.No. : XL/RM/15/077
Qty. Received : 50Kg Mfg. Date : 10/15
Date of Receipt : 19/01/2016 Exp.Date : 09/20
Manufactured By : LASONS INDIA PVT.LTD.
Supplied By : LASONS INDIA PVT.LTD.
Date of Report : 07/04/2016 Sample. Qty. : 30 g
GRN. No. : RM-063 Page : 1 of 2

S. No. Tests Specifications Results

A white or almost white, crystalline powder Complies
01 Description
or colourless crystals
02 Solubility Freely soluble in water and in ethanol. Complies

First identification: A, B Complies

03 Identification
Second identification: A, C, D
3A Melting point 128C to 131C. 130
The infra red absorption spectrum of the Complies
3B By IR sample should correspond to the similarly
obtained spectrum of standard.
Ammonia should evolve which should Complies
3C By Chemical
recognisable by its odour.
3D By Chemical A yellow colour should develop. Complies
6.9
04 pH 6.0 to 7.5
Any spot in the chromatogram obtained Complies
with the test solution, apart from the
05 Related Substances principal spot, should not more intense
than the spot in the chromatogram obtained
with the reference solution
< 30 ppm
06 Heavy metals* NMT 30 ppm
0.17
07 Loss on drying Not more than 0.5 %

Prepared By Checked By Approved By

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Date
Department Quality Control Quality control Head QC
Format No.QC37/F01-00
 A-141, EPIP, RIICO Industrial Area, Neemrana, Rajasthan, India
CERTIFICATE OF ANALYSIS
Department : Quality Control
Title : Nicotinamide
Batch No. : 15-0541 AR.No. : XL/RM/15/077
Qty. Received : 50Kg Mfg. Date : 10/15
Date of Receipt : 19/01/2016 Exp.Date : 09/20
Manufactured By : LASONS INDIA PVT.LTD.
Supplied By : LASONS INDIA PVT.LTD.
Date of Report : 07/04/2016 Sample. Qty. : 30 g
GRN. No. : RM-063 Page : 2 of 2

Results
S. No. Tests Specifications
0.07
08 Sulfated Ash NMT 0.1 %
Assay (Dry 99.41
09 99.0 to 101 %
Substance)

Remarks: Sample complies / Does not complies as per Specification No. SPC/RM/011-00
*Marked Tests results certified as per supplier COA.

Prepared By Checked By Approved By

Sign

Date
Department Quality Control Quality control Head QC
Format No.QC37/F01-00