sample ID mass carbonate (g) volume of acid (cm3)

1-----A 1.18 22
1-----B 0.64 20
1-----C 0.44 20
2-----A 1.46 23
2-----B 1.33 22
2-----C 1.49 21
3-----A 0.93 21
3-----B 0.68 21
3-----C 1.02 22
4-----A 0.69 21
4-----B 0.98 21
4-----B 1.36 22

C+G G C
3.36 2.18 1.18
1.65 1.01 0.64
1.28 0.84 0.44
3.56 2.1 1.46
3.85 2.52 1.33
3.03 1.54 1.49
2.72 1.79 0.93
2.14 1.46 0.68
3.02 2 1.02
2.24 1.55 0.69
2.74 1.76 0.98
3.51 2.15 1.36
mole of carbonate (mol) mass of Nickel (mg/L) mole of Nickel
0.6006 0
0.3583 0
0.2464 0
0.7108 0
0.6770 0
0.7945 0
0.4959 0
0.3626 0
0.5192 0
0.3679 0
0.5226 0
0.6922 0
mole ratio Ni solubility in ppm
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
sample ID mass carbonate (g) volume of acid (cm3) mole of carbonate (mol)
1-----A 1.02 21.5 0.5312
1-----B 1.15 21.5 0.5990
1-----C 1.17 21.5 0.6094
2-----A 1.31 21.5 0.6823
2-----B 1.08 21.5 0.5625
2-----C 0.82 21.5 0.4271
3-----A 0.87 21.5 0.4531
3-----B 1.18 21.5 0.6146
3-----C 1.4 21.5 0.7292
4-----A 1.29 21.5 0.6719
4-----B 1.24 21.5 0.6458
4-----B 1.28 21.5 0.6667
mass of Nickel (mg/L) mole of Nickel mole ratio Ni solubility in ppm
0.23 3.9188958937E-06 7.376801E-06 7
0.31 0.000005282 8.818694E-06 9
0.21 3.5781223377E-06 5.871835E-06 6
0.24 4.0892826717E-06 5.993498E-06 6
0.22 3.7485091157E-06 6.664067E-06 7
0.2 3.4077355597E-06 7.979148E-06 8
0.14 2.3854148918E-06 5.264404E-06 5
0.21 3.5781223377E-06 5.822074E-06 6
0.14 2.3854148918E-06 3.271451E-06 3
0.3 5.1116033396E-06 0.000007608 8
0.14 2.3854148918E-06 3.693574E-06 4
0.16 2.7261884478E-06 4.089314E-06 4

mass NiO = 3g
mass of LiNa carbonate = 80g
carbon dioxide = 60 cm3
air = 140 cm3

1--- AFTER 1 HR
2--- AFTER 24HRS
3--- AFTER 48HRS
3--- AFTER 72HRS
 sample ID mass carbonate (g) volume of acid (cm3) mole of carbonate (mol)
2-----1 1.04 21 0.5546
2-----2 0.92 21 0.4906
2-----3 0.64 21 0.3413
3-----1 0.7 21 0.3733
3-----2 0.95 21 0.5066
3-----3 1.13 21 0.6026
4-----1 1.04 21 0.5546
4-----2 0.25 20 0.1400
4-----3 0.08 20 0.0448
5-----1 0.7 20 0.3919
5-----2 0.8 21 0.4266
5-----3 0.37 20 0.2072

TEMP = 650
carbon dioxide = 60 cm3
air = 140 cm3
SAMPLE ID A B
A-----B 2&3 === LiNaCO3 1--- AFTER 1 HR
4&5 ===LiNaCO3 + ADDIT 2--- AFTER 24HRS
3--- AFTER 48HRS
mass of Nickel (mg/L) mole of Nickel mole ratio Ni solubility in ppm
0.48 8.17856534333E-06 1.47478642673E-05 15
0.29 4.94121656159E-06 1.00723638202E-05 10
0.14 2.3854148918E-06 6.98987316834E-06 7
0.32 5.45237689555E-06 1.46074084171E-05 15
0.18 0.000003067 6.05438638341E-06 6
0.23 3.91889589368E-06 6.50385164589E-06 7
1.11 1.89129323564E-05 3.41044361181E-05 34
0.54 9.20088601125E-06 6.5733337877E-05 66
0.43 7.3266314534E-06 0.0001635725 164
0.88 0.000014994 3.82574982353E-05 38
5.33 9.08161526666E-05 0.0002128916 213
3.26 5.55460896234E-05 0.0002681315 268
sample ID mass carbonate (g) volume of acid (cm3) mole of carbonate (mol)
2-----1 0.41 21 0.2186
2-----2 0.64 21 0.3413
2-----3 0.47 20 0.2631
2-----4 0.46 20 0.2576
3-----1 0.29 10 0.3247
3-----2 0.61 21 0.3253
3-----3 0.69 21 0.3679
3-----4 0.63 21 0.3359
4-----1 0.23 10 0.2576
4-----2 1.17 21 0.6239
4-----3 0.67 21 0.3573
4-----4 0.1 10 0.1120
5-----1 0.23 10 0.2576
5-----2 0.97 20 0.5431
5-----3 0.55 20 0.3079
5-----4 0.48 21 0.2560

SAMPLE ID
A-----B
 mass of Nickel (mg/L) mole of Nickel mole ratio Ni solubility in ppm
0.48 8.1785653433294E-06 3.7409216678E-05 37
0.51 8.6897256772875E-06 2.5463109399E-05 25
0.45 7.6674050093713E-06 2.91371178533E-05 29
0.51 8.6897256772875E-06 3.37399379199E-05 34
0.77 1.3119781904924E-05 4.04012373605E-05 40
0.3 5.11160333958085E-06 1.5714937334E-05 16
0.49 0.000008349 2.26917621697E-05 23
0.65 1.1075140569092E-05 3.29681092747E-05 33
1.33 2.2661441472142E-05 8.79884655559E-05 88
10.8 0.0001840177 0.0002949573 295
3.8 0.000064747 0.00018123 181
7.96 0.0001356279 0.0012111976 1211
0.85 1.4482876128812E-05 5.62332298666E-05 56
0.82 1.3971715794854E-05 2.57261058892E-05 26
0.75 0.000012779 4.14983193668E-05 41
0.9 1.5334810018743E-05 5.99131985858E-05 60

TEMP = 650
carbon dioxide = 60 cm3
air = 140 cm3
A B
2&3 === LiNaCO3 1--- AFTER 1 HR
4&5 ===LiNaCO3 + ADDIT 2--- AFTER 24HRS
3----AFTER 60HRS
4----AFTER 84HRS
sample ID mass carbonate (g) volume of acid (cm3) mole of carbonate (mol)
1-----1 0.061 10 0.0683
1-----2 0.122 10 0.1366
1-----3 0.125 10 0.1400
2-----1 0.085 10 0.0952
2-----2 0.138 10 0.1545
2-----3 0.059 10 0.0661
4-----1 0.057 10 0.0638
4-----2 1.059 30 0.3953
4-----3 0.109 10 0.1221
5-----1 0.191 10 0.2139
5-----2 1.754 31 0.6336
5-----3 1.197 30 0.4468

SAMPLE ID A
A-----B 1&2 === LiNaCO3
4&5 ===LiNaCO3 + ADDIT
mass of Nickel (mg/L) mole of Nickel mole ratio Ni solubility in ppm
0.14 2.3854148918044E-06 3.492208296439E-05 35
0.32 5.4523768955529E-06 0.000039911 40
1.94 0.000033055 0.0002361531 236
0.27 4.6004430056228E-06 4.833333667425E-05 48
2.72 4.63452036122E-05 0.0002999106 300
0.76 1.2949395126938E-05 0.0001960034 196
0.52 8.8601124552735E-06 0.0001388131 139
2.18 3.7144317600954E-05 9.396881004867E-05 94
1.79 3.0499233259499E-05 0.0002498783 250
0.21 3.5781223377066E-06 1.672968895938E-05 17
0.36 6.133924007497E-06 9.681363902444E-06 10
0.4 6.8154711194411E-06 1.525418589923E-05 15

TEMP = 650
carbon dioxide = 60 cm3
air = 140 cm3
B
1--- AFTER 1 HR
2--- AFTER 24HRS
3--- AFTER 48HRS
sample ID mass carbonate (g) volume of acid (cm3) mole of carbonate (mol)
1-----1 0.015 10 0.0168
1-----2 0.032 10 0.0358
1-----3 0.098 10 0.1097
1-----4 1.015 30 0.3789
3-----1 0.024 10 0.0269
3-----2 0.03 10 0.0336
3-----3 0.099 10 0.1109
3-----4 0.791 20 0.4429
4-----1 0.019 10 0.0213
4-----2 0.019 10 0.0213
4-----3 0.077 10 0.0862
4-----4 0.031 10 0.0347

SAMPLE ID A
A-----B 1 === LiNaCO3
3&4 ===LiNaCO3 + ADDIT
 mass of Nickel (mg/L) mole of Nickel mole ratio Ni solubility in ppm
0.09 1.5334810019E-06 9.129630261E-05 91
0.05 8.5193388993E-07 2.37750788E-05 24
0.03 5.1116033396E-07 0.000004658 5
0.15 2.5558016698E-06 0.000006746 7
0.08 1.3630942239E-06 5.072016811E-05 51
0.07 1.1927074459E-06 3.550411768E-05 36
0.05 8.5193388993E-07 7.684873957E-06 8
0.05 8.5193388993E-07 1.923647337E-06 2
0.06 1.0223206679E-06 4.805068558E-05 48
0.04 6.8154711194E-07 3.203379039E-05 32
0.08 1.3630942239E-06 1.580888357E-05 16
0.04 6.8154711194E-07 1.963361346E-05 20

TEMP = 650
carbon dioxide = 60 cm3
air = 140 cm3
B
1--- AFTER 1 HR
2--- AFTER 24HRS
3--- AFTER 48HRS
4----AFTER 72HRS
 LiNa carbonate solubilty REMARKS
1 91.2963026069
2 23.7750788039
3 4.6579746228
4 6.7460322123
5 35
6 40
7 236
8 48
9 300
10 196
11 37.409216678
12 25.463109399
13 29.1371178533
14 33.7399379199
15 40.4012373605
16 15.714937334
17 22.6917621697
18 32.9681092747
19 14.7478642673
20 10.0723638202
21 6.9898731683
22 14.6074084171
23 6.0543863834
24 6.5038516459
25 7.3768009214
26 8.8186935779
27 5.8718348472
28 5.9934977284
29 6.6640665329
30 7.9791483986
31 5.2644036561
32 5.8220735349
33 3.2714508434
34 7.6080252172
35 3.6935735329
36 4.0893135543

EXPT 1
EXPT 2
EXPT 3
EXPT 4
EXPT 5
LiNa cabonate + Addi
50.720168115
35.5041176805
7.6848739568
1.9236473369
48.0506855826
32.0337903884
15.8088835683
19.6336134639
138.813091683
93.9688100487
249.8782594287
16.7296889594
9.6813639024
15.2541858992
87.9884655559
294.9572853454
181.2299738316
1211.1976145851
56.2332298666
25.7261058892
41.4983193668
59.9131985858
34.1044361181
65.733337877
163.5725421707
38.2574982353
212.8915656415
268.131483332