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Article history: In the current research, nano-composites of commercial casting aluminum alloy reinforced with nano-silicon
Received 27 August 2011 carbide were produced. Experimental and modeling investigations were carried out on the porosity, wear,
Received in revised form 15 November 2011 hardness, elongation, yield strength and ultimate tensile strength (UTS) of these nano-composites. The
Accepted 17 November 2011
density measurements showed that the amount of porosity in the composites increased with increasing
Available online 26 November 2011
the volume fraction of nano-particles. The wear sliding test revealed that composites offer superior wear
Keywords:
resistance as compared to the alloy irrespective of nano-particles volume fraction. The tensile strength
Nano-composite results show that the yield strength and ultimate tensile strength of the composites increased with
Silicon carbide increasing volume fraction of nano-particles. The incorporation of nano-particles deteriorates the ductility
FEM of A356 alloy. However, the elongation remains rather constant with increasing the volume fraction of
nano-particles. In the other word, increasing the nano-sized ceramic particles content helps to strengthen
the composites, while the ductility is retained. In this paper, a technique based on articial neural network
(ANN) and nite element method (FEM) was proposed to investigate on nano-silicon carbide reinforced
commercial casting aluminum alloy matrix. It was observed that prediction of this study is consistent with
experimental measurements for aluminum matrix composites.
2011 Elsevier B.V. All rights reserved.
0032-5910/$ see front matter 2011 Elsevier B.V. All rights reserved.
doi:10.1016/j.powtec.2011.11.020
A. Mazahery, M.O. Shabani / Powder Technology 217 (2012) 558565 559
Fig. 1. Schematic representation of the neural network architecture. Fig. 3. Effect of applied load on wear resistance.
560 A. Mazahery, M.O. Shabani / Powder Technology 217 (2012) 558565
The tension tests were used to assess the mechanical behavior of into some output values as follows:
the composites. The tensile specimens were machined from compos-
ite rods according to ASTM.B 557 standard. For each volume fraction y : y f x 6
of SiC particles, three samples were tested. To study the hardness,
the Brinell hardness values of the samples were measured on the MLP tries to nd the best possible approximation of the function
polished samples using a ball with 2.5 mm diameter at a load of f as a complex combination of elementary nonlinear functions. This
31.25 kg. approximation is coded in the neurons of the network using weights
Sliding wear tests were conducted in pin-on-disk wear testing that are associated with each neuron. The weights of MLP are learned
apparatus under varying applied loads against case hardened steel using an iterative procedure in which examples of correct input
disk of hardness 63 HRC. Test specimens were cut and shaped in the output associations are shown to the network. The weights are mod-
form of pins having 6 mm in diameter and 25 mm in height. Before ied when the network starts to mimic the desirable inputoutput
the abrasion tests, each specimen was polished to 0.5 m. The pin behavior. This ability to learn from examples and the ability for gen-
samples were solution treated at 540 C for 4 h, quenched into eralization to new situations are the most attractive features of the
warm water (40 C) and then peak aged to T6 condition (155 C for ANN paradigm.
9 h). Fig. 2 shows Schematic diagram of the abrasion wear test. The The LevenbergMarquardt algorithm (LM) is an approximation to
experiment was carried out at room temperature (21 C, relative the Newton method used also for training ANNs. The Newton method
humidity 55%) with water as the lubricant. The samples were approximates the error of the network with a second order expres-
cleaned with acetone and weighed (up to an accuracy of 0.01 mg sion, which contrasts to the back-propagation algorithm that does it
using microbalance) prior to and after each test. The temperature with a rst order expression [2532]. LM is popular in the ANN do-
rise was recorded from the digital display interfaced with the wear main (even if it is considered the rst approach for an unseen MLP
test machine. A set of three samples was tested in every training task), although it is not that popular in the metaheuristics
experimental condition, and the average along with standard eld. LM updates the ANN weights as follows:
deviation for each set of three tests is measured. The wear tests h i1
p p T p
were conducted up to the total sliding distance of 2000 m. w I p1 J w J w Ew 7
3. FEM where J p (w) is the Jacobian matrix of the error vector E p (w) evalu-
ated in w, and I is the identity matrix. The vector error E p (w) is the
The nite element method is a powerful technique for solving dif- error of the network for pattern p:
ferential or partial differential equations as well as integral equations.
p p p
For each triangular element, a linear relationship between nodes tem- E w T O w: 8
peratures is used in the solution to the heat transfer problem. Eq. (1)
is the general heat conduction equation, including unsteady heat The parameter is increased or decreased at each step. If the error
storage and variable conductivity [2330]: is reduced, then is divided by a factor , while it is multiplied by in
other case.
T x; y; z; t 2 It calculates the network output, the error vectors, and the Jacobi-
Cp k T x; y; z; t 1
t an matrix for each pattern. Then, it computes w using Eq. (7) and
recalculates the error with w + w as network weights. If the error
C p C PS T b TS
2 has decreased, is divided by , the new weights are maintained,
C p C PL T > TL
and the process starts again; otherwise, is multiplied by , w is cal-
culated with a new value, and it iterates again [3134].
L
C P f s C ps 1f s C pL f T b T b TL 3 LevenbergMarquardt algorithm steps:
TT s s S
Randomly select the initial value of the weight vectors w.
The evolution of fraction solid (fs) is given by the Scheil equation: Calculates E p for each pattern p.
8 1
< TT m k0 1
fs 1 T e TT L 4
: T L T m p p T p
1 T Te E1 p1 E w E w 9
where q is heat generation, density, C heat capacity, L latent heat, k Calculates J p (w) for each pattern p
heat diffusion coefcient and k0 solute partition coefcient. In this re-
Calculates w; E2
search, mechanical properties are considered to be related to cooling
rate, temperature gradient and volume percentage of nano-SiC. The
FEM method is used for discretization and to calculate the transient
N p T p
temperature eld of quenching. E2 p1 E w w E w w 10
Fig. 5. Weight loss as a function of sliding distance. Fig. 6. Hardness as a function of nano-SiC particles volume fraction.
562 A. Mazahery, M.O. Shabani / Powder Technology 217 (2012) 558565
Sliding wear is related to asperity-to-asperity contact of the two phenomena, frictional heating remains almost constant as observed
counter surfaces, which are in relative motion against each other. in Fig. 7. It is also mentioned earlier that surface and subsurface defor-
Fig. 5 shows the weight loss as a function of sliding distance at an mation took place during sliding which also causes heating of the
applied load of 15 N. It is noted that the weight loss of the compos- contact surfaces.
ites is less than that of unreinforced alloy, increases with increase Because of combined action of load, sliding speed and sliding dis-
in sliding distance, and has a declining trend with increasing the tance, subsurface micro cracks are generated which nally leads to re-
particles volume fraction. moval of wear debris, especially from asperity contacts. In addition
In general, composites offer superior wear as compared to the higher temperature rise also leads to greater owability of surface
alloy irrespective of applied load and sliding speed [36]. This result materials and thus increases greatly the possibility of compaction of
is consistent with the rule that in general, materials with higher hard- wear debris on the specimen surface. In this case, valleys between
ness have better wear and abrasive resistance (Fig. 6). The higher the asperities of the counter surface gets partially occupied with the
hardness of the composites could be attributed to the fact that SiC material of the specimen, which results in the reduction of surface
particles act as obstacles to the motion of dislocation [37,38]. abrasive action effectiveness of the counter surface asperities. With
At the initial stage of sliding, the wear is mainly due to fragmenta- further increase in sliding distance, the temperature increases to a
tion of asperities and removal of material due to cutting and owing critical value at which specimen surface gets oxidized. This oxidized
actions of penetrated hard asperities into the softer surface. Higher surface either gets fragmented or becomes stable to some extent.
amount of stress is expected to act on the asperities, due to the great- The fragmented oxide particles sometimes act as lubricating agent
er degree of their hardness and sharpness. Because of the higher and thus these oxide layers reduce the effective wear rate. Further-
stress concentration on these points, they get plastically deformed more, the fragmentation and compaction of wear debris, counter sur-
and some of the sharpest asperities get fractured due to combined ac- face material and thin oxide layers leads to formation of mechanically
tion of normal and shear stress. During the sliding, in fact a consider- mixed layer which protects the specimen surface from wear [36].
able fraction of energy is spent on overcoming the frictional force, However, further increasing sliding distance leads to increasing tem-
which leads to heating of the contact surfaces. Thus, it is expected perature which leads to subsurface softening and because of plastic
that initially the temperature of the contact surface is less and incompatibility, and thermal mismatch, the MML gets fractured and
hence the asperities are expected to be stronger and more rigid. As subsequently removed from the specimen surface. Thus at higher
time progresses, the frictional heating increases, which leads to sliding distance it is expected that the formation and removal of
higher temperature and softening of the surface materials. MML are taking place simultaneously and the rate of removal and
Fig. 7 represents the variation of temperature with sliding distance the rate of growth of MML might be same and thus the wear rate re-
at an applied load of 20 N. It is noted that temperature rise is greater mains unchanged with sliding distance. It is reported that as the slid-
in the case of unreinforced alloy as compared to that in the composite ing distance reaches to the point of seizure, the MML becomes
irrespective of the applied load and surface conditions. In general, it is unstable because of greater degree of temperature rise in the subsur-
observed that the temperature initially increases at a sharp rate and face resulting in higher degree of thermal as well as plastic incompat-
then gradually reaches to a stable value. The rise in surfaces temper- ibility between MML and subsurface [36,39].
ature is an outcome of a couple of facts that cause heating of the con- Normally micron-sized particles are used to improve the ultimate
tact surfaces. During sliding, frictional force acts between the counter tensile and the yield strengths of the metal. However, the ductility of
surfaces, which caused frictional heating of them. While the counter the MMCs deteriorates signicantly with high ceramic particle con-
surfaces are in relative motion, the frictional heating is continuous be- centration [4043]. It is of interest to use nano-sized ceramic particles
cause of insufcient time for heat dissipation. Initially, the asperities to strengthen the metal matrix, while maintaining good ductility [44].
are stronger and sharper, and that is why frictional force and as a re- Fig. 8 displays the tensile ow curves of the composites. It is noted
sult frictional heating takes place at higher rate. After a certain period, that the addition of nano-particles deteriorate the ductility of A356
because of the increase in owability of the material on the specimen alloy. The stir casting method that is used in the present work to pro-
surface, slipping action is higher which results in reduction of fric- duce the nano-composites can most probably create different inter-
tional heating. The more possibility of adhesion between the counter faces between nano-particles and matrices and thus, encourage
surfaces leads to higher degree of friction. Because of these counter crack initiation and propagation [9]. It is also noted that the
Fig. 7. Temperature as a function of sliding distance. Fig. 8. Flow curves in tensile deformation of the composites.
A. Mazahery, M.O. Shabani / Powder Technology 217 (2012) 558565 563
Fig. 10. MAPE values for various neuron in the hidden layer.
564 A. Mazahery, M.O. Shabani / Powder Technology 217 (2012) 558565
As shown in Fig. 1, the general structure of the implemented ANN UTS of the composites. Different strengthening mechanisms contrib-
models consists of an input layer, a hidden layer and an output layer. uted in the obtained strength improvements including Orowan
The problem of choosing a suitable architecture for MLPs lies in strengthening, grain renement, accommodation of CTE mismatch
specifying the activation function and the number of neurons in the between the matrix and the particles, and the load bearing effects.
hidden layer. Trial-and-error analysis resulted in the selection of a Unlike the experimental approach, which is time consuming, com-
suitable activation function for each model. The selection of the bination of FEM with ANN method is capable of generalizing the com-
number of hidden nodes in MLPs is both the most difcult and plex relationships and provide approximate solutions. Mechanical
important step. Since the use of these training algorithms is indeed properties are related to cooling rate, temperature gradient and vol-
very time consuming process, it is important to be convinced that ume percentage of SiC. Information obtained from the model predic-
the obtained solutions are the optimum ones. Therefore, the error tions and simulations can be used as guidelines during the conceptual
behavior of the neural network has to be observed to nd the design and optimization of manufacturing processes thus reducing
results with minimum errors. There is no known concept about the time and costs that would otherwise be incurred by experimental
selection of the number of neurons in the hidden layer. The neuron methods.
number in the hidden layer can be found experimentally. In Fig. 10,
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