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Article history: Intermittent microwave convective (IMCD) drying is an advanced drying technology that improves both
Received 2 August 2015 energy efciency and food quality during the drying of food materials. Despite numerous experimental
Received in revised form studies available for IMCD, there is no complete multiphase porous media model available to describe the
19 January 2016
process. A multiphase porous media model considering liquid water, gases and the solid matrix inside
Accepted 20 January 2016
Available online 19 April 2016
the food during drying can provide in depth understanding of IMCD. In this article, rstly a multiphase
porous media model was developed for IMCD. Then the model is validated against experimental data by
comparing moisture content and temperature distributions after each heating and tempering periods.
Keywords:
Intermittent microwave
The prole of vapour pressures and evaporation during IMCD are presented and discussed. The relative
Drying contribution of water and vapour uxes due to gas pressure and diffusion demonstrated that the uxes
Mathematical model due are relatively higher in IMCD compared to convection drying and this makes the IMCD faster.
Lambert's law 2016 Elsevier Masson SAS. All rights reserved.
Moisture ux
Vapour pressure
COMSOL multiphysics
Multiphase porous media
http://dx.doi.org/10.1016/j.ijthermalsci.2016.01.018
1290-0729/ 2016 Elsevier Masson SAS. All rights reserved.
C. Kumar et al. / International Journal of Thermal Sciences 104 (2016) 304e314 305
ow and evaporation. Describing all the water transport as diffu- observable phenomenon, it was not taken into consideration in this
sion cannot be justied under all situations [57]. Therefore, multi- study. IMCD itself is a complex model and inclusion of shrinkage
phase models considering transport of liquid water, water vapour would further complicate the simulation of the model. As it is the
and air insider the food materials are more realistic. Although the rst multiphase IMCD model, it is logical that we start with a
nal equations of multiphase models seem to be simple conser- simplied model. It is our assumption that although consideration
vation equations it still provides the more fundamental and of shrinkage may provide better prediction, the trends of transport
convincing basis of transport than single-phase models [13,55]. phenomena would be the same. Therefore, we neglected the
Multiphase models can be categorised into two groups viz. equi- shrinkage in our study to focus more on transport phenomena.
librium and non-equilibrium approach of vapour pressure. In
equilibrium formulations, the vapour pressure, pv, is assumed to be
equal with equilibrium vapour pressure, pv,eq, and vice versa [57]. 2.2. Governing equations
There are some multiphase models considering the equilibrium
approach applied in vacuum drying of wood [51] and convection In this section the mathematical formulation, initial condition,
drying of wood and clay [49,10], microwave spouted bed drying of boundary conditions, and input parameters are presented. It also
apple [18] and large bagasse stockpiles [17]. discusses the heat generation term due to microwave, Qmic (W/m3).
However, equilibrium conditions may not be achieved due to
lower moisture content at the surface during drying. Therefore,
non-equilibrium multiphase models are computationally effective 2.2.1. Mass and momentum balance equations
and applied to a wide range of food processing such as frying [4,38], The representative elementary volume DV (m3) is the sum of the
microwave heating [11,45], pufng [43], baking [58], meat cooking volume of three phases, namely, gas, water, and solid, thus,
[14] etc. However, application of these non-equilibrium models in
drying of food materials is very limited. To the authors' best DV DVg DVw DVs ; (1)
knowledge, not only is there no satisfactory multiphase model,
there is not even a comprehensive single-phase model for IMCD. where DVg is the volume of gas (m3), DVw is the volume of water
The objectives of this study are to: 1) develop a multiphase (m3), and DVs is the volume of solid (m3).
porous media model for IMCD drying of food materials considering The apparent porosity, 4, is dened as the volume fraction
transport of liquid water, vapour and air, 2) validate the model for occupied by gas and water, thus,
the IMCD of an apple slice with experimental moisture and tem-
perature proles, 3) investigate the temperature distribution and DVg DVw
4 : (2)
redistribution due to the intermittency of microwave application, DV
and 4) investigate the transport mechanisms, such as, pressure
driven, binary diffusion and capillary driven ow in IMCD. The water, Sw, and gas, Sg, saturation are dened as the fraction of
pore volume occupied by that particular phase, namely,
2. Mathematical model
DVw DVw
Sw ; (3)
In this section, the equations for multiphase porous media are DVw Vg 4DV
developed describing heat, mass and momentum transfer for IMCD.
and
We also present the transport mechanism involved in drying, as-
sumptions and input parameters for the model. Apple has been
DVg DVg
considered as the sample food material for this study. Sg 1 Sw ; (4)
DVw DVg 4DV
The model developed in this research considers transport of
liquid water, vapour and air inside food materials. The mass and
respectively.
energy conservation equations include convection, diffusion and
The mass concentrations of water, cw (kg/m3), vapour, cv (kg/
evaporation of water and vapour. The energy equation also includes
m3), and air, ca (kg/m3), are given by,
a microwave heat generation term using Lambert's Law. Mo-
mentum conservation is developed from Darcy's equations. Evap- cw rw 4Sw ; (5)
oration is considered as distributed throughout the domain and a
non-equilibrium evaporation formulation is used for evaporation
pv Mv
condensationecondensation phenomena. cv 4Sg ; (6)
RT
2.1. Problem description and assumptions and
Fig. 1. Schematic showing 3D sample, 2D axisymmetric domain and representative elementary volume (REV) with the transport mechanism of different phases.
! kg kr;g
2.2.2. Mass balance equations for gas phase n g rg uv VP 4Sg rg Deff;g Vuv ; (14)
mv
The total gas pressure, P, is calculated by solving the overcall
mass balance for the gas phase, namely, ! kw kr;w
n w rw VP Dc Vcw : (15)
v kg kr;g mw
rg 4Sg V$ rg VP Revap ; (11)
vt mi The thermo-physical properties change due to the change in
mass and volume fraction in each phase. Therefore, the following
C. Kumar et al. / International Journal of Thermal Sciences 104 (2016) 304e314 307
and and
keff 4 Sg kth;g Sw kth;w 1 4kth;s : (18) Tt0 303 K; (28)
Here rs is the solid density (kg/m3); cpg, cpw and cps are the specic respectively.
heat capacities of gas, water and solid (J/kg/K), respectively; kth,g,
kth,w and kth,s are the thermal conductivities of gas, water and solid, 2.5. Boundary conditions
(W/m/K) respectively; mg, mw and ms are the mass fraction of gas,
water and solid, (W/m/K) respectively. The heat and mass transfer takes place at the transport
boundaries as shown in Fig. 1. The boundary conditions for Equa-
2.3. Evaporation rate tions (8) and (9) can be written as,
Mv
! pv pv air
Revap Kevap pv;eq pv : (19) n v;s hmv 4Sg ; (30)
RT RT
Here Mv is the molecular weight of vapour (kg/mol), pv,eq is the respectively, where pv,air vapour pressure of ambient air (Pa) and
equilibrium vapour pressure (Pa), pv is the vapour pressure (Pa), hmv is the mass transfer coefcient (m/s).
and Kevap is evaporation constant (1/s). The boundary condition for continuity equation (11) can be
The equilibrium vapour pressure, pv,eq, is obtained via the expressed as,
sorption isotherm of apple given by Ratti et al. [46] as,
P Pamb ; (31)
0:696
pv;eq Pv;sat Texp 0:182Mdb
where Pamb is the ambient pressure (Pa).
0:232e43:949M Mdb
0:0411
lnPsat T ; (20) For Equation (13), the boundary condition is given by,
pv pv air
and the saturated vapour pressure of water, Pv,sat (Pa), is a function qsurf hT T Tair hmv 4Sw hfg
of temperature and is given by Vega-Mercado et al. [53] as, RT
pv pv air
h hmv 4Sg Cp;v T; (32)
Pv;sat exp 5800:2206=T 1:3915 0:0486T 0:4176 RT
i
where hT is the heat transfer coefcient (W/m2/K) and Tair is the
104 T 2 0:01445 107 T 3 6:656 lnT :
drying air temperature (K), and Cp,v is the specic heat of vapour at
(21) constant volume (J/kg/K).
The heat and mass transfer coefcients were calculated from
The vapour pressure, pv, is obtained from partial pressure re-
well established empirical relationship as discussed in authors'
lations given by,
previous publications [27,30,34,41].
pv cv P; (22)
2.6. Input parameters
where cv is the mole fraction of vapour given by,
The input parameters of the model are listed in Table 1 and some
uv Ma of them are derived and discussed in the latter of this section.
cv : (23)
uv Ma ua Mv
Here Ma is the molecular mass of air (kg/mol). 2.6.1. Calculation of ambient vapour pressure
The moisture content (dry basis), Mdb can be calculated from, The partial pressure of vapour in ambient condition can be
calculated by pv,amb RH psat. In our experiment the ambient air
cw cv of RH 70% and 30 C was heated up to 60 C with specic hu-
Mdb : (24)
1 4rs midity of 0.0188 kg/kg db. This condition yields a relative humidity
of 15% using the psychometric chart. Therefore, ambient vapour
pressure for drying air, pv,amb 0.15 19,947 2992 Pa.
Table 1 and
Input properties for the model.
0:65
Parameter Value Reference T
mg 0:017 103 ; (38)
Sample diameter, Dias 40 mm This work 273
Sample thickness, Ths 10 mm This work
Equivalent porosity, initial, 40 0.922 [37,42] respectively.
Water saturation, initial, Sw0 0.794 [37,42]
Initial saturation of vapour, Sv0 0.15 [37,42]
Gas saturation, initial, Sg0 0.206 [37,42]
Initial temperature, T0 303 K 2.6.4. Effective gas diffusivity
Vapour mass fraction, wv 0.026 Calculated The effective gas diffusivity can be calculated as a function of gas
saturation and porosity according to the Bruggeman correction
Constants
[37], namely,
Evaporation constant, Kevap 1000 This work
Drying air temperature, Tair 333 K This work 4=3
Universal gas constant, Rg 8.314 J mol1 K1 [9] Deff;g Dva Sg 4 ; (39)
Molecular weight of water, Mw 18.016 g mol1 [9]
Molecular weight of vapour, Mv 18.016 g mol1 [9]
where Dva is the binary diffusivity between air and water vapour
Molecular weight of gas (air), Ma 28.966 g mol1 [9]
Latent heat of evaporation, hfg 2.26e6 J kg1 [9]
(m2/s).
Ambient pressure, Pamb 101,325 Pa [9]
Gas intrinsic permeability, kg 4.0 1012 m2 [19]
Binary diffusivity, Dva 2.6 106 m2/s [13]
2.6.5. Capillary diffusivity of liquid water
Ambient vapour pressure, pv,air 2992 Pa Calculated
Heat transfer coefcient, hT 16.746 W/(m2 K) Calculated Capillary diffusivity of liquid water used in the model is a
Mass transfer coefcient, hm 0.017904 m/s Calculated function of moisture content is given by [29],
Density
Apple solid, rs 1419 kg m3 This study 2.7. Microwave power absorption
Vapour, rv Ideal gas law, kg m3
Air, ra Ideal gas law, kg m3
Water, rw 1000 kg m3 Lamberts Law has been widely used for developing microwave
heating models in literature [1,3,25,28,36,47,60]. In this study, we
also used Lambert's Law to calculate the microwave energy ab-
43 sorption inside the food samples. This law considers exponential
kw 5:578 1012 ; 0:39 < 4 < 0:77: (33) attenuation of microwave absorption within the product, given by,
1 42
The gas intrinsic permeability is considered to be constant and is Pmic P0 exp2ahz : (42)
given by [19],
Here P0 the incident power at the surface (W), a is the attenuation
kg 4:0 1012 m2 : (34) constant, h is the thickness of the material, and (h z) is the dis-
tance from top surface (towards centre). The measurement of P0 via
In this study, the relative permeabilities were considered as a experiments is presented in authors' previous publication [30].
function of water saturation given by [19], The attenuation constant, a is given by,
v
kr;w S3w ; (35) u 2s
2
3
u
u 00
u 6 1 33 0 17
2p u 0 6 7
and a u3 6 7; (43)
u
l t 4 6 2 7
5
kr;g 1:01e10:86Sw ; (36)
2.8. Dielectric constant and tempering period by placing the camera 10 cm above the
sample.
The dielectric constant, 3 0 and dielectric loss, 3 00 , are the most
important parameters that control the microwave power absorp- 3.4. Numerical solution
tion of the materials. Here we use the data of Martn-Esparza et al.
[35] in a quadratic regression analysis in which the intercept of the Engineering simulation software COMSOL Multiphysics 4.4 was
0 00
3 and 3 versus Mwb graph was set to 0.1 in order to avoid numerical used to solve the equations. COMSOL is an advanced software tool
singularity in 3 0 and 3 00 when Mwb is zero. The resulting quadratic used for modelling and simulating any physical process described
expression is found to be, by partial derivative equations.
Combinations of a rectangular function and an analytic function
0 2
3 36:638Mwb 30:289Mwb 0:1 (45) in COMSOL Multiphysics were used to develop an intermittency
function as shown in Fig. 2. Then it was multiplied with the heat
and generation term in the energy equations to implement intermit-
00
2
tency of the microwave heat source.
3 13:543Mwb 26:8150Mwb 0:1: (46) Since heat and mass transport phenomena is happening at the
transport boundaries as shown in Fig. 1, a ner mesh (maximum
element size 0.1 mm) was chosen at those boundaries to capture
this phenomena more accurately. The ner mesh at the boundary
3. Materials and methods
help to converge the solution and investigate the physics more
accurately. On the other hand, rest of the region of the domain left
In this section, we discuss the experimental IMCD procedures,
with normal mesh (coarser than boundary) because ner mesh
sample preparation, and data acquisition method.
throughout the domain will increase the computational cost and
time. To ensure that the results are grid-independent, several grid
3.1. IMCD
sensitivity tests were conducted. Finer mesh than the chosen one
shown in Fig. 3, showed similar results. Therefore, the mesh size
The IMCD was achieved using a microwave oven and a con-
0.1 mm at the boundary was chosen to capture the transport
vection dryer. The sample was placed in the microwave oven for
phenomena while minimizing the computational time and cost.
20 s followed by convection drying, for 80 s, in the convection dryer.
The time stepping was set to be 1 s. The simulation was per-
The experiments were conducted with a Panasonic Microwave
formed using a Windows 7 computer with Intel Core i7 CPU,
Oven (Model NNST663W) having inverter technology with internal
3.4 GHz processor and 24 GB of RAM. Direct solver PARDISO was
cavity dimension 352 mm (W) 230 mm (H) 347 mm (D) and a
used in order to obtain faster solution and solve complex coupling
convection dryer. The inverter technology enables accurate and
of the model.
continuous power supply at lower power settings [40]. The mi-
crowave oven is able to supply 10 accurate power levels with a
4. Results and discussion
maximum of 1100 W at 2.45 GHz frequency. The apple slices were
placed in the centre of the microwave cavity, in order to achieve an
In this section, the results of the theoretical and experimental
even absorption of microwave energy.
In order to get the intermittency of the microwave power investigations are given. Experimental data was also used to vali-
date the model developed. Specically, moisture content and
application, the sample was placed in MW for 20 s after the con-
vection drying for 80 s. The moisture loss was recorded at regular temperature obtained from experiments were compared with that
of the model. Moreover, spatial and temporal proles of moisture,
intervals at the end of each tempering period with a digital balance
(specication: 0.001 g accuracy). temperature, evaporation rate, pressure and, uxes are also
discussed.
3.2. Sample preparation
4.1. Moisture content and temperature
Fresh Granny Smith apples obtained from the local Australian
supermarkets were used for the intermittent microwave drying The prole of average moisture content obtained from simula-
experiments. The samples were stored at 5 1 C to keep them as tion and experiments is presented in Fig. 4. The model provided a
fresh as possible before they were used in the experiments. The
apples taken from the storage unit were washed and put aside for
1 h to allow their temperature to equilibrate to room temperature
prior to each drying experiment. The samples were cut into disks
with a thickness of 10 mm and diameter of approximately 40 mm.
The initial moisture content of the apple slices was approximately
0.868 kg/kg (wet basis.) or 6.61 kg/kg (dry basis).
Table 2
Comparison of experimental and model temperature at centre of top surface at different times.
Time (s) 320 400 420 500 520 600 620 700 720 800
pressure obtained from simulation is compared with literature [9] Fig. 7. Comparison of surface temperature between experimental and model.
and found to be consistent with available data. The equilibrium
vapour pressure is calculated from the sorption isotherm of apple
and, as expected, it was found to be lower than the saturation 4.6. Evaporation
vapour pressure. Fig. 9 shows that the difference between vapour
pressure and equilibrium vapour pressure is higher during the Evaporation is zero in the inner part of the sample (as shown
initial stage of drying resulting higher evaporation. Unlike the in Fig. 10), as the equilibrium nature of vapour pressure, due to
convection drying [29,31], the vapour pressure uctuates due to the higher moisture content, exists in the inner part of the sample. In
uctuation in temperature resulting from the intermittent micro- contrast to this, higher evaporation near the surface indicates
wave heat source. Moreover, Fig. 9 shows that the equilibrium that a non-equilibrium condition exists on the surface (as shown
vapour pressure in IMCD is much higher (14 kPa) compared to that in Fig. 10). It is found that the evaporation starts about 1 mm
of the convection drying (3 kPa) after drying time of 10 min [29,31]. beneath the surface and the evaporation rate increases as it
This is because of the higher temperature due to microwave heat moves towards the surface. This is because the difference be-
generation. However, after some time, the vapour pressure and tween equilibrium vapour pressure and vapour pressure starts
equilibrium vapour pressure coincide because the surface becomes about 1 mm beneath the surface and that increases with the
dried and equilibrium vapour pressure becomes lower. move towards the surface.
Fig. 8. Spatial distribution of total pressure across the half thickness the sample in
Fig. 6. Spatial distribution of vapour with different times. different times.
312 C. Kumar et al. / International Journal of Thermal Sciences 104 (2016) 304e314
Fig. 10. Spatial distribution of evaporation rate at different drying times. Fig. 12. Water ux due to capillary at different drying times.
C. Kumar et al. / International Journal of Thermal Sciences 104 (2016) 304e314 313
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