Filtration: Filter the solution's a. b. c.

purified substance may contain differ

ent types of impurities: colorless soluble impurity in the solvent cold and hot
hot Impurity Impurity insoluble colorless soluble colored
In case (a) the technique is performed without filtering hot as impurities remai
n in the mother liquor. In case (b) and (c) is necessary hot filtration to remov
e impurities from the compound found in solution. In particular the case (c) is
necessary filtration with activated carbon. Filter media There are various types
of filter media, the most common of which is the filter paper can be found in t
rade with different degrees of porosity depending on the type of precipitate to
be filtered. You can also use glass wool that is useful in the case of large cry
stals suspended in a liquid that could attack the filter paper (eg. NaOH (c) or
acids (c)). Can be used in a similar way to asbestos or asbestos fiber that has
a smaller pore size and the ability to filter smaller crystals. Gooch crucibles
are used (crucible) and filter by suction. Both methods are used when what is de
sired is the filtrate it is difficult to separate the crystals. Another filter m
edia is porous sintered glass plate or porcelain that is adjusted using a specia
l funnel. They come with varying degrees of porosity and are inert to chemical r
eagents. Unfortunately not suitable for ppdos. gelatinous as they are used with
suction and clog pores. A further disadvantage is its difficult to clean. Method
s filter hot hot filtration is used when you want to separate the insoluble impu
rities in the solvent used in the solution of the substance to be purified. Hot
Filtration:
a) Simple ï ¨ for filterable solid impurities by filter paper. b) bed of Celite ï ¨
for impurities that could pass through the filter paper (turbulent solutions, im
purities in suspension, etc.).
c) decolorizing charcoal (activated) ï ¨ soluble colored impurities. The bed is us
ed to hold coal.
Recommendations for filtering hot to be taken into account the precaution of hea
ting the funnel before filtering. To do this it can be dipped in a bath of boili
ng water or placed in an electric heater to proper temperature where it is remov
ed at the time of filtering. (If no water is used as solvent the funnel must be
dry). Keep the hot filtered solution throughout the operation and once past all
the liquid rinse the container with small portions of hot solvent. b), c) Suctio
n filtration. Recommendations. â ¢ â ¢ You can use the Buchner or Hirsch funnel, dep
ending on whether the fluid volume is large or small respectively. By applying s
uction can cause rapid evaporation of the solvent causing the recrystallization
of the compound in the stem of the funnel. Therefore placing an additional amoun
t of solvent in the solution before filtering. The filtrate was heated again and
redissolved the crystals, thus falling in solution those who were trapped in th
e vessel walls.
â ¢
How is the bed of celite weapon? 1) Assemble the filtration apparatus with sucti
on in the conventional manner (Fig. 2). The funnel should be hot. 2) Place the f
ilter paper making sure all holes are covered and not touching the walls of the
funnel. 3) In a glass of ppdos. prepare a hot suspension of Celite in the same s
olvent used for recrystallization (the suspension should look like cream. See.)
4) Without applying suction tip over the grout on paper evenly and immediately a
pply suction. The celite bed should have a thickness of 1-2 mm and be equal, sho
uld not be allowed to dry for cracks decreasing its effectiveness. 5) Filter in
a conventional manner. Note: when should the procedure charcoal filter is the sa
me except that he added to the solution of the compound no more than 2% by weigh
t (relative to the amount of dry sample) of activated charcoal prior to filtrati
on.