Northwest ISD 2016 Lead Testing Lab Results

Analytical Report 534731
for
Northwest Independent School District
Project Manager: Jim Sadler
----16-AUG-16
Collected By: Client
9701 Harry Hines Blvd

Dallas, TX 75220
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400)
Xenco-San Antonio: Texas (T104704534)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Page 1 of 44
Final 1.000
Table of Contents
Cover Page
Cover Letter
Sample ID Cross Reference
Case Narrative
Certificate of Analysis (Detailed Report)
QC Summary
35
Explanation of Qualifiers (Flags)
37
Chain of Custody
38
Sample Receipt Conformance Report
44
Page 2 of 44
Final 1.000
16-AUG-16
1800 Hwy 114
Justin, TX 76247
Reference: XENCO Report No(s): 534731
--Project Address: --Jim Sadler :
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 534731. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 534731 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
Gale Denman
Project Manager
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Page 3 of 44
Final 1.000
Sample Cross Reference 534731

Northwest Independent School District, Justin, TX
--Sample Id
A0001
A0002
A0003
A0004
A0005
A0006
A0007
B0008
B0009
B0010
B0011
B0012
B0013
B0014
B0015
B0016
B0017
B0018
C0019
C0020
C0021
C0022
C0023
C0024
C0025
C0026
C0027
C0028
C0029
Matrix
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
Date Collected
Sample Depth
08-09-16 09:13
08-09-16 09:26
08-09-16 09:37
08-09-16 09:56
08-09-16 09:59
08-09-16 10:04
08-09-16 10:10
08-09-16 10:50
08-09-16 11:00
08-09-16 11:05
08-09-16 11:10
08-09-16 11:15
08-09-16 12:40
08-09-16 12:50
08-09-16 12:55
08-09-16 13:00
08-09-16 13:05
08-09-16 13:12
08-09-16 13:49
08-09-16 13:53
08-09-16 14:00
08-09-16 14:02
08-09-16 14:06
08-09-16 14:10
08-09-16 14:12
08-09-16 14:15
08-09-16 14:22
08-09-16 14:36
08-09-16 14:38
Page 4 of 44
Lab Sample Id
534731-001
534731-002
534731-003
534731-004
534731-005
534731-006
534731-007
534731-008
534731-009
534731-010
534731-011
534731-012
534731-013
534731-014
534731-015
534731-016
534731-017
534731-018
534731-019
534731-020
534731-021
534731-022
534731-023
534731-024
534731-025
534731-026
534731-027
534731-028
534731-029
Final 1.000
CASE NARRATIVE
Client Name: Northwest Independent School District
Project Name: --Report Date: 16-AUG-16
Date Received: 08/10/2016
Project ID:
--Work Order Number(s): 534731
Sample receipt non conformances and comments:
Sample receipt non conformances and comments per sample:

None
Page 5 of 44
Final 1.000
Certificate of Analytical Results 534731

--Sample Id:
Matrix:
A0001
Lab Sample Id: 534731-001
Water
Date Received:08.10.16 09.05
Date Collected: 08.09.16 09.13
Analytical Method: Metals per ICP by EPA 200.7

Tech:
DAT
Analyst:
DAT
Prep Method: E200.7P

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 10.33
Page 6 of 44
Final 1.000

--Sample Id:
Matrix:
A0002
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 10.36
Page 7 of 44
Final 1.000

--Sample Id:
Matrix:
A0003
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 10.39
Page 8 of 44
Final 1.000

--Sample Id:
Matrix:
A0004
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 10.42
Page 9 of 44
Final 1.000

--Sample Id:
Matrix:
A0005
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 10.45
Page 10 of 44
Final 1.000

--Sample Id:
Matrix:
A0006
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 10.48
Page 11 of 44
Final 1.000

--Sample Id:
Matrix:
A0007
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 10.51
Page 12 of 44
Final 1.000

--Sample Id:
Matrix:
B0008
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 11.03
Page 13 of 44
Final 1.000

--Sample Id:
Matrix:
B0009
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 11.06
Page 14 of 44
Final 1.000

--Sample Id:
Matrix:
B0010
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 05.45
Date Prep:
Seq Number: 999735

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 11.08
Page 15 of 44
Final 1.000

--Sample Id:
Matrix:
B0011
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 12.31
Page 16 of 44
Final 1.000

--Sample Id:
Matrix:
B0012
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 12.34
Page 17 of 44
Final 1.000

--Sample Id:
Matrix:
B0013
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 12.37
Page 18 of 44
Final 1.000

--Sample Id:
Matrix:
B0014
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 12.40
Page 19 of 44
Final 1.000

--Sample Id:
Matrix:
B0015
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 12.43
Page 20 of 44
Final 1.000

--Sample Id:
Matrix:
B0016
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 12.46
Page 21 of 44
Final 1.000

--Sample Id:
Matrix:
B0017
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
0.0124
RL
Units
Analysis Date
0.0120
mg/L
08.12.16 12.49
Page 22 of 44
Final 1.000
Flag
Dil
1

--Sample Id:
Matrix:
B0018
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 13.00
Page 23 of 44
Final 1.000

--Sample Id:
Matrix:
C0019
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 13.03
Page 24 of 44
Final 1.000

--Sample Id:
Matrix:
C0020
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.12.16 06.15
Date Prep:
Seq Number: 999740

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.12.16 13.06
Page 25 of 44
Final 1.000

--Sample Id:
Matrix:
C0021
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 09.48
Page 26 of 44
Final 1.000

--Sample Id:
Matrix:
C0022
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.05
Page 27 of 44
Final 1.000

--Sample Id:
Matrix:
C0023
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.16
Page 28 of 44
Final 1.000

--Sample Id:
Matrix:
C0024
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.19
Page 29 of 44
Final 1.000

--Sample Id:
Matrix:
C0025
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.22
Page 30 of 44
Final 1.000

--Sample Id:
Matrix:
C0026
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.25
Page 31 of 44
Final 1.000

--Sample Id:
Matrix:
C0027
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.28
Page 32 of 44
Final 1.000

--Sample Id:
Matrix:
C0028
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.31
Page 33 of 44
Final 1.000

--Sample Id:
Matrix:
C0029
Water

Tech:
DAT
Analyst:
DAT

% Moisture:
08.15.16 05.30
Date Prep:
Seq Number: 999802

Parameter
Lead
Cas Number
7439-92-1
Result
<0.0120
RL
Units
Analysis Date
Flag
Dil
0.0120
mg/L
08.15.16 10.34
Page 34 of 44
Final 1.000
QC Summary
534731

--Prep Method: E200.7P
Date Prep: 08.12.16
LCSD Sample Id: 711995-1-BSD

Seq Number:
999735
Matrix: Water
LCS
Sample
Id: 711995-1-BKS
711995-1-BLK
MB Sample Id:
Parameter
Lead
MB
Result
Spike
Amount
LCS
Result
LCS
%Rec
LCSD
Result
LCSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
<0.0120
1.00
1.05
105
1.04
104
85-115
20
mg/L
08.12.16 10:21

Date Prep: 08.12.16

Seq Number:
999740
Matrix: Water
LCS Sample Id: 711997-1-BKS
711997-1-BLK
MB Sample Id:
Parameter
Lead
MB
Result
Spike
Amount
LCS
Result
LCS
%Rec
LCSD
Result
LCSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
<0.0120
1.00
1.06
106
1.07
107
85-115
20
mg/L
08.12.16 12:19
Lead
MB
Result
Spike
Amount
LCS
Result
LCS
%Rec
LCSD
Result
LCSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
<0.0120
1.00
1.05
105
1.05
105
85-115
20
mg/L
08.15.16 09:37

Seq Number:
999735
534853-001
Parent Sample Id:
Matrix: Water
MS Sample Id: 534853-001 S
Parent
Result
Spike
Amount
MS
Result
MS
%Rec
MSD
Result
MSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
Lead
<0.120
10.0
10.3
103
10.4
104
75-125
20
mg/L
08.12.16 11:14
Parent
Result
Spike
Amount
MS
Result
MS
%Rec
MSD
Result
MSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
Lead
<0.120
10.0
10.6
106
10.7
107
75-125
20
mg/L
08.12.16 12:04
Flag

Date Prep: 08.12.16
MSD Sample Id: 534754-005 SD
Matrix: Water
Parameter
Parent
Result
Spike
Amount
MS
Result
MS
%Rec
MSD
Result
MSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
Lead
<0.0120
1.00
1.04
104
1.04
104
75-125
20
mg/L
08.12.16 13:25
Page 35 of 44
Flag

Date Prep: 08.12.16
Matrix: Water
Parameter

Seq Number:
999740
534754-005
Parent Sample Id:
Flag

Date Prep: 08.12.16
Parameter

Seq Number:
999735
Parent Sample Id:
534853-010
Flag

Date Prep: 08.15.16

Seq Number:
999802
Matrix: Water
LCS Sample Id: 712042-1-BKS
712042-1-BLK
MB Sample Id:
Parameter
Flag
Final 1.000
Flag
QC Summary
534731

--Analytical Method: Metals per ICP by EPA 200.7
Seq Number:
999740
Parent Sample Id:
534754-008

Date Prep: 08.12.16
Matrix: Water
Parameter
Parent
Result
Spike
Amount
MS
Result
MS
%Rec
MSD
Result
MSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
Lead
<0.0120
1.00
1.04
104
1.04
104
75-125
20
mg/L
08.12.16 13:56

Seq Number:
999802
Parent Sample Id:
534731-021

Date Prep: 08.15.16
Matrix: Water
Parameter
Parent
Result
Spike
Amount
MS
Result
MS
%Rec
MSD
Result
MSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
Lead
<0.0120
1.00
0.996
100
1.00
100
75-125
20
mg/L
08.15.16 09:51

Seq Number:
999802
Parent Sample Id:
534947-004
Flag
Prep Method: SW3010A

Date Prep: 08.15.16
Matrix: Water
Parameter
Parent
Result
Spike
Amount
MS
Result
MS
%Rec
MSD
Result
MSD
%Rec
Limits
%RPD
RPD
Limit
Units
Analysis
Date
Lead
<0.0120
1.00
0.883
88
0.889
89
75-125
20
mg/L
08.15.16 11:20
Page 36 of 44
Flag
Final 1.000
Flag
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit
SDL Sample Detection Limit
LOD Limit of Detection
PQL Practical Quantitation Limit
MQL Method Quantitation Limit
LOQ Limit of Quantitation
DL Method Detection Limit

NC Non-Calculable
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation

Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
Phone
(281) 240-4200
(214) 902 0300
(210) 509-3334
(432) 563-1800
(602) 437-0330
4147 Greenbriar Dr, Stafford, TX 77477

9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
1211 W Florida Ave, Midland, TX 79701
2525 W. Huntington Dr. - Suite 102, Tempe AZ 85282
Page 37 of 44
Fax
(281) 240-4280
(214) 351-9139
(210) 509-3335
(432) 563-1713
Final 1.000
Page 38 of 44
Final 1.000
Page 39 of 44
Final 1.000
Page 40 of 44
Final 1.000
Page 41 of 44
Final 1.000
Page 42 of 44
Final 1.000
Page 43 of 44
Final 1.000
XENCO Laboratories
Prelogin/Nonconformance Report- Sample Log-In
Client: Northwest Independent School District
Date/ Time Received: 08/10/2016 09:05:00 AM
Acceptable Temperature Range: 0 - 6 degC

Air and Metal samples Acceptable Range: Ambient
Work Order #: 534731
Temperature Measuring device used : XDA

Comments
Sample Receipt Checklist

#1 *Temperature of cooler(s)?
#2 *Shipping container in good condition?

#3 *Samples received on ice?
Yes
Yes
#4 *Custody Seal present on shipping container/ cooler?

#5 *Custody Seals intact on shipping container/ cooler?
Yes
Yes
#6 Custody Seals intact on sample bottles?

#7 *Custody Seals Signed and dated?
N/A
Yes
#8 *Chain of Custody present?

#9 Sample instructions complete on Chain of Custody?
Yes
Yes
#10 Any missing/extra samples?

#11 Chain of Custody signed when relinquished/ received?
No
Yes
#12 Chain of Custody agrees with sample label(s)?

#13 Container label(s) legible and intact?
Yes
Yes
#14 Sample matrix/ properties agree with Chain of Custody?

#15 Samples in proper container/ bottle?
Yes
Yes
#16 Samples properly preserved?

#17 Sample container(s) intact?
Yes
Yes
#18 Sufficient sample amount for indicated test(s)?

#19 All samples received within hold time?
Yes
Yes
#20 Subcontract of sample(s)?

#21 VOC samples have zero headspace (less than 1/4 inch bubble)?
No
N/A
#22 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#23 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
N/A
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: CG
PH Device/Lot#: 213315
Checklist completed by:
Date: 08/10/2016
Angelica Martinez
Checklist reviewed by:

Date: 08/10/2016
Gale Denman
Page 44 of 44
Final 1.000

for
Project Manager: Rusty Stierwalt
----19-AUG-16

Dallas, TX 75220
Oklahoma (9218)
Page 1 of 39
Final 1.000
Table of Contents
Cover Page
Cover Letter
Case Narrative
25
LCS / LCSD Recoveries
26
MS / MSD Recoveries
28
Chain of Custody
31
39
Page 2 of 39
Final 1.000
19-AUG-16
1800 Hwy 114
Justin, TX 76247
--Project Address: --Rusty Stierwalt :
Respectfully,
Gale Denman
Project Manager
Page 3 of 39
Final 1.000

--Sample Id
D0030
D0031
D0032
D0033
D0034
D0035
D0036
D0037
D0038
D0039
D0040
D0041
D0042
D0043
D0044
D0045
D0046
D0047
D0048
D0049
E0050
E0051
E0052
E0053
F0054
F0055
F0056
F0057
F0058
G0059
G0060
G0061
G0062
G0063
G0064
G0065
G0066
G0067
G0068
G0069
G0070
G0071
G0072
Matrix
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
Date Collected
Sample Depth
534875-001
534875-002
534875-003
534875-004
534875-005
534875-006
534875-007
534875-008
534875-009
534875-010
534875-011
534875-012
534875-013
534875-014
534875-015
534875-016
534875-017
534875-018
534875-019
534875-020
534875-021
534875-022
534875-023
534875-024
534875-025
534875-026
534875-027
534875-028
534875-029
534875-030
534875-031
534875-032
534875-033
534875-034
534875-035
534875-036
534875-037
534875-038
534875-039
534875-040
534875-041
534875-042
534875-043
08-10-16 12:48
08-10-16 12:56
08-10-16 13:02
08-10-16 13:05
08-10-16 13:06
08-10-16 13:08
08-10-16 13:16
08-10-16 13:19
08-10-16 13:23
08-10-16 13:26
08-10-16 13:36
08-10-16 13:40
08-10-16 13:44
08-10-16 13:46
08-10-16 13:48
08-10-16 13:51
08-10-16 13:54
08-10-16 13:56
08-10-16 14:00
08-10-16 14:03
08-10-16 14:35
08-10-16 14:43
08-10-16 14:46
08-10-16 14:48
08-10-16 15:13
08-11-16 08:34
08-11-16 08:36
08-11-16 08:45
08-11-16 08:52
08-11-16 09:52
08-11-16 09:57
08-11-16 10:00
08-11-16 10:04
08-11-16 10:07
08-11-16 10:10
08-11-16 10:14
08-11-16 10:17
08-11-16 10:21
08-11-16 10:25
08-11-16 10:30
08-11-16 10:34
08-11-16 10:37
08-11-16 10:39
Version: 1.%
Page 4 of 39
Lab Sample Id
Final 1.000

--G0073
G0074
G0075
G0076
G0077
G0078
H0079
H0080
H0081
H0082
H0083
H0084
H0085
H0086
I0087
I0088
I0089
I0090
I0091
I0092
I0093
I0094
I0095
I0096
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
08-11-16 10:43
08-11-16 10:45
08-11-16 10:47
08-11-16 10:51
08-11-16 10:55
08-11-16 11:00
08-11-16 13:47
08-11-16 13:53
08-11-16 13:57
08-11-16 14:02
08-11-16 14:07
08-11-16 14:12
08-11-16 14:19
08-11-16 14:24
08-11-16 15:07
08-11-16 15:12
08-11-16 15:17
08-11-16 15:20
08-11-16 15:25
08-11-16 15:30
08-11-16 15:33
08-11-16 15:36
08-11-16 15:41
08-11-16 15:46
534875-044
534875-045
534875-046
534875-047
534875-048
534875-049
534875-050
534875-051
534875-052
534875-053
534875-054
534875-055
534875-056
534875-057
534875-058
534875-059
534875-060
534875-061
534875-062
534875-063
534875-064
534875-065
534875-066
534875-067
Version: 1.%
Page 5 of 39
Final 1.000
CASE NARRATIVE
Project ID:
This laboratory is NELAC accredited under the Texas Laboratory Accreditation Program for all the
methods, analytes, and matrices reported in this data package except as noted. The data have been
reviewed and are technically compliant with the requirements of the methods used, except where noted by
the laboratory.

None
Page 6 of 39
Final 1.000
Certificate of Analytical Results

534875
--Sample Id:
Matrix:
D0030
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00
Date Received: 08.12.16 09.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00750
Matrix:
D0031
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 07:34
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00950
Matrix:
D0032
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 07:37
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00720
Matrix:
D0033
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 07:40
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep seq: 712076
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00690
Page 7 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 07:43
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
D0034
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00900
Matrix:
D0035
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 07:46
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00810
Matrix:
D0036
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 07:49
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00760
Matrix:
D0037
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 07:52
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep seq: 712076
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00610
Page 8 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 08:03
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
D0038
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00600
Matrix:
D0039
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 08:06
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00770
Matrix:
D0040
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 08:09
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00960
Matrix:
D0041
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 08:12
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep seq: 712076
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00800
Page 9 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 08:15
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
D0042
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0102
Matrix:
D0043
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 08:18
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00840
Matrix:
D0044
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 08:21
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00980
Matrix:
D0045
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 08:24
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep seq: 712076
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00620
Page 10 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 08:50
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
D0046
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00950
Matrix:
D0047
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 08:53
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00850
Matrix:
D0048
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00
Flag
mg/L
08.16.16 08:56
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00860
Matrix:
D0049
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 08:59
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00

Prep seq: 712076
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00750
Page 11 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 09:07
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
E0050
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0120
Matrix:
E0051
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 11:28
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
E0052
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 11:31
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00660
Matrix:
E0053
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 11:34
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep seq: 712077
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00720
Page 12 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 11:58
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
F0054
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00870
Matrix:
F0055
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 12:01
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00460
Matrix:
F0056
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 12:04
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00650
Matrix:
F0057
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 12:06
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep seq: 712077
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 13 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 12:09
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
F0058
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00870
Matrix:
G0059
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 12:12
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00590
Matrix:
G0060
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 12:15
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
G0061
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 12:18
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep seq: 712077
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00760
Page 14 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 12:21
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
G0062
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00780
Matrix:
G0063
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 12:23
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
G0064
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 12:34
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0101
Matrix:
G0065
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 12:37
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep seq: 712077
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00470
Page 15 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 12:40
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
G0066
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
G0067
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999914
Date Prep: 08.15.16 12.15
Flag
mg/L
08.16.16 12:43
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0132
Matrix:
G0068
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15
mg/L
Flag
Dil Factor
08.16.16 12:46
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00600
Matrix:
G0069
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 12:49
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999914
Date Prep: 08.15.16 12.15

Prep seq: 712077
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00510
Page 16 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 12:57
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
G0070
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
G0071
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 13:20
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
G0072
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 13:22
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00440
Matrix:
G0073
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 13:25
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep seq: 712078
Parameter
Lead
CAS
Number
7439-92-1
Result
0.0126
Page 17 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Units
mg/L
08.16.16 13:28
Final 1.000
Flag
Dil Factor
1

534875
--Sample Id:
Matrix:
G0074
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00850
Matrix:
G0075
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 13:31
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00490
Matrix:
G0076
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 13:34
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00650
Matrix:
G0077
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 13:36
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep seq: 712078
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00630
Page 18 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 13:48
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
G0078
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00620
Matrix:
H0079
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 13:51
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0194
Matrix:
H0080
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30
mg/L
Flag
Dil Factor
08.16.16 13:53
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00890
Matrix:
H0081
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 14:10
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep seq: 712078
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00460
Page 19 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 14:12
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
H0082
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00690
Matrix:
H0083
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 14:24
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00760
Matrix:
H0084
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 14:26
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
H0085
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 14:29
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep seq: 712078
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00760
Page 20 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 14:32
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
H0086
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0109
Matrix:
I0087
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 14:35
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00670
Matrix:
I0088
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30
Flag
mg/L
08.16.16 14:38
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
I0089
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 14:46
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30

Prep seq: 712078
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00990
Page 21 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 14:49
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
I0090
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999888
Date Prep: 08.16.16 05.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712102

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00840
Matrix:
I0091
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999888
Date Prep: 08.16.16 05.15
Flag
mg/L
08.16.16 09:57
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712102

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0105
Matrix:
I0092
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999888
Date Prep: 08.16.16 05.15
Flag
mg/L
08.16.16 10:00
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712102

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0113
Matrix:
I0093
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.16.16 10:02
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999888
Date Prep: 08.16.16 05.15

Prep seq: 712102
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00760
Page 22 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 10:05
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
I0094
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
999888
Date Prep: 08.16.16 05.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712102

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0117
Matrix:
I0095
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
999888
Date Prep: 08.16.16 05.15
Flag
mg/L
08.16.16 10:08
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712102

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00420
Matrix:
I0096
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
999888
Date Prep: 08.16.16 05.15
Flag
mg/L
08.16.16 10:11
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712102

Parameter
Lead
CAS
Number
7439-92-1
Result
0.00660
Page 23 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 10:27
Units
mg/L
Final 1.000
Dil Factor
1

534875
--Sample Id:
Matrix:
712076-1-BLK
Lab Sample Id: 712076-1-BLK
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
999857
Date Prep: 08.15.16 12.00
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712076

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712077-1-BLK
MQL
0.0120
SDL
0.00400
Seq Number:
Flag
mg/L
08.16.16 07:31
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
Analysis
Date
Units
DAT
% Moist:
999914
Date Prep: 08.15.16 12.15
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712077

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712078-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 11:25
Units
mg/L
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
999938
Date Prep: 08.15.16 12.30
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712078

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712102-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 13:17
Units
mg/L
Date Collected:
Date Received:
Prep Method:
E200.7P
Tech:
DAT

DAT
% Moist:
Seq Number:
999888
Date Prep: 08.16.16 05.15
Sample Depth:
Water
Analyst:
Dil Factor
Prep seq: 712102

Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 24 of 39
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.16.16 09:29
Units
mg/L
Final 1.000
Dil Factor
1
Flagging Criteria
RL Reporting Limit

NC Non-Calculable

Phone
(281) 240-4200
(214) 902 0300
(210) 509-3334
(432) 563-1800
(602) 437-0330

Page 25 of 39
Fax
(281) 240-4280
(214) 351-9139
(210) 509-3335
(432) 563-1713
Final 1.000
BS / BSD Recoveries
Project Name: --Project ID: ---

Date Prepared: 08/15/2016
DAT
Analyst:
Lab Batch ID: 999857
Sample: 712076-1-BKS
Batch #: 1
mg/L
Units:
Blank
Sample Result
[A]
Analytes
Lead
<0.00400
DAT
Lead
Blank
Sample Result
[A]
<0.00400
DAT
1.06
106
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.06
Spike
Added
Blk. Spk
Dup.
%R
[G]
106
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
Date Analyzed: 08/16/2016

Matrix: Water
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.07
Blank
Spike
%R
[D]
107
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.06
Spike
Added

mg/L
Units:
1.00
Blank
Spike
%R
[D]
Batch #: 1
Analytes
[B]
Blank
Spike
Result
[C]
BLANK /BLANK SPIKE / BLANK SPIKE DUPLICATE RECOVERY STUDY
Metals per ICP by EPA 200.7
Analyst:
Spike
Added
mg/L
Units:
Matrix: Water
Analyst:
106
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
Blk. Spk
Dup.
%R
[G]
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.07
Blank
Spike
%R
[D]
107
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.07
Spike
Added
Blk. Spk
Dup.
%R
[G]
107
Relative Percent Difference RPD = 200*|(C-F)/(C+F)|

Blank Spike Recovery [D] = 100*(C)/[B]
Blank Spike Duplicate Recovery [G] = 100*(F)/[E]
All results are based on MDL and Validated for QC Purposes
Version: 1.%
Page 26 of 39
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
BS / BSD Recoveries

DAT
Analyst:

mg/L
Units:
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.06
Blank
Spike
%R
[D]
106
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.06
Spike
Added
Blk. Spk
Dup.
%R
[G]
106

Version: 1.%
Page 27 of 39
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
Form 3 - MS / MSD Recoveries

Project Name: --Work Order # :
534875
Lab Batch ID:
999857
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
999857
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
999888
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead
Matrix Spike Percent Recovery [D] = 100*(C-A)/B

Project ID: --QC- Sample ID: 534875-015 S

Batch #:
Matrix: Water
Analyst: DAT
MATRIX SPIKE / MATRIX SPIKE DUPLICATE RECOVERY STUDY

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00980
1.00
Spiked Sample Spiked

Result
Sample
[C]
%R
[D]
1.02
QC- Sample ID: 534875-019 S

101
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.04
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
103
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00860
1.00

Result
Sample
[C]
%R
[D]
1.04

103
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.04
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
103
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00420
1.00

Result
Sample
[C]
%R
[D]
1.03
103
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.05
Matrix Spike Duplicate Percent Recovery [G] = 100*(F-A)/E
ND = Not Detected, J = Present Below Reporting Limit, B = Present in Blank, NR = Not Requested, I = Interference, NA = Not Applicable
N = See Narrative, EQL = Estimated Quantitation Limit, NC = Non Calculable - Sample amount is > 4 times the amount spiked.
Page 28 of 39
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
105
75-125
20
Flag

534875
Lab Batch ID:
999888
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
999914
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
999914
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead


Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.0200
5.00

Result
Sample
[C]
%R
[D]
5.29

106
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
5.00
Batch #:
5.31
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
106
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00660
1.00

Result
Sample
[C]
%R
[D]
1.03

102
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.03
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
102
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00600
1.00

Result
Sample
[C]
%R
[D]
1.03
102
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.02
Page 29 of 39
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
101
75-125
20
Flag

534875
Lab Batch ID:
999938
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
999938
Date Analyzed:
08/16/2016
Reporting Units:
mg/L

Analytes
Lead

Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.0194
1.00

Sample
Result
%R
[C]
[D]
1.02
100
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.01
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
99
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00670
1.00

Sample
Result
%R
[C]
[D]
1.03
102
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.02
Page 30 of 39
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
101
75-125
20
Flag
Page 31 of 39
Final 1.000
Page 32 of 39
Final 1.000
Page 33 of 39
Final 1.000
Page 34 of 39
Final 1.000
Page 35 of 39
Final 1.000
Page 36 of 39
Final 1.000
Page 37 of 39
Final 1.000
Page 38 of 39
Final 1.000
XENCO Laboratories


Comments

1.3

Yes
Yes

N/A
N/A

N/A
Yes

Yes
Yes

No
Yes

Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

No
N/A
analysts.
Yes
N/A
Analyst: CG
Date: 08/12/2016
Angelica Martinez

Date: 08/12/2016
Gale Denman
Page 39 of 39
Final 1.000

for
2016 drinking water- Northwest ISD
19-AUG-16

Dallas, TX 75220
Oklahoma (9218)
Page 1 of 52
Final 1.000
Table of Contents
Cover Page
Cover Letter
Case Narrative
31
32
MS / MSD Recoveries
34
Chain of Custody
38
52
Page 2 of 52
Final 1.000
19-AUG-16
1800 Hwy 114
Justin, TX 76247
Project Address:
Rusty Stierwalt :
Respectfully,
Gale Denman
Project Manager
Page 3 of 52
Final 1.000

Sample Id
J0097
J0098
J0099
J0100
J0101
K0102
K0103
K0104
K0105
K0106
K0107
K0108
K0109
K0110
K0111
K0112
K0113
L0114
L0115
L0116
L0117
L0118
M0119
M0120
M0121
M0122
M0123
M0124
M0125
M0126
M0127
M0128
M0129
M0130
N0131
N0132
N0133
N0134
N0135
N0136
N0137
N0138
N0139
Matrix
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
Date Collected
Sample Depth
534987-001
534987-002
534987-003
534987-004
534987-005
534987-006
534987-007
534987-008
534987-009
534987-010
534987-011
534987-012
534987-013
534987-014
534987-015
534987-016
534987-017
534987-018
534987-019
534987-020
534987-021
534987-022
534987-023
534987-024
534987-025
534987-026
534987-027
534987-028
534987-029
534987-030
534987-031
534987-032
534987-033
534987-034
534987-035
534987-036
534987-037
534987-038
534987-039
534987-040
534987-041
534987-042
534987-043
08-12-16 10:33
08-12-16 10:37
08-12-16 10:43
08-12-16 10:46
08-12-16 10:53
08-12-16 13:11
08-12-16 13:17
08-12-16 13:23
08-12-16 13:26
08-12-16 13:30
08-12-16 13:34
08-12-16 13:37
08-12-16 13:40
08-12-16 13:43
08-12-16 13:49
08-12-16 13:55
08-12-16 14:05
08-13-16 08:29
08-13-16 08:33
08-13-16 08:36
08-13-16 08:40
08-13-16 08:44
08-13-16 09:15
08-13-16 09:18
08-13-16 09:23
08-13-16 09:26
08-13-16 09:29
08-13-16 09:33
08-13-16 09:36
08-13-16 09:38
08-13-16 09:41
08-13-16 09:45
08-13-16 09:50
08-13-16 09:55
08-13-16 10:39
08-13-16 10:44
08-13-16 11:05
08-13-16 11:09
08-13-16 11:17
08-13-16 11:50
08-13-16 11:57
08-13-16 12:05
08-13-16 12:10
Version: 1.%
Page 4 of 52
Lab Sample Id
Final 1.000

O0140
O0141
O0142
O0143
O0144
O0145
O0146
O0147
O0148
O0149
P0150
P0151
P0152
P0153
P0154
P0155
P0156
Q0157
Q0158
Q0159
Q0160
Q0161
Q0162
Q0163
Q0164
Q0165
Q0166
Q0167
Q0168
R0169
R0170
R0171
R0172
R0173
R0174
R0175
R0176
R0177
R0178
R0179
R0180
R0181
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
08-13-16 12:40
08-13-16 12:45
08-13-16 12:49
08-13-16 12:55
08-13-16 13:00
08-13-16 13:04
08-13-16 13:07
08-13-16 13:10
08-13-16 13:14
08-13-16 13:17
08-13-16 13:35
08-13-16 13:50
08-13-16 14:00
08-13-16 14:05
08-13-16 14:10
08-13-16 14:15
08-13-16 14:20
08-13-16 14:50
08-13-16 14:54
08-13-16 14:58
08-13-16 15:02
08-13-16 15:06
08-13-16 15:10
08-13-16 15:14
08-13-16 15:18
08-13-16 15:23
08-13-16 15:27
08-13-16 15:30
08-13-16 15:34
08-15-16 09:20
08-15-16 09:23
08-15-16 09:26
08-15-16 09:33
08-13-16 09:37
08-15-16 09:40
08-15-16 09:44
08-15-16 09:50
08-15-16 09:56
08-15-16 10:00
08-15-16 10:04
08-15-16 10:07
08-15-16 10:11
534987-044
534987-045
534987-046
534987-047
534987-048
534987-049
534987-050
534987-051
534987-052
534987-053
534987-054
534987-055
534987-056
534987-057
534987-058
534987-059
534987-060
534987-061
534987-062
534987-063
534987-064
534987-065
534987-066
534987-067
534987-068
534987-069
534987-070
534987-071
534987-072
534987-073
534987-074
534987-075
534987-076
534987-077
534987-078
534987-079
534987-080
534987-081
534987-082
534987-083
534987-084
534987-085
Version: 1.%
Page 5 of 52
Final 1.000
CASE NARRATIVE
Project Name: 2016 drinking water- Northwest ISD
Report Date: 19-AUG-16
Project ID:
Work Order Number(s): 534987
the laboratory.

None
Page 6 of 52
Final 1.000

534987
Sample Id:
Matrix:
J0097
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00780
Matrix:
J0098
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999995
Date Prep: 08.16.16 06.30
Flag
mg/L
08.17.16 10:40
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00650
Matrix:
J0099
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30
Flag
mg/L
08.17.16 10:43
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
J0100
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.17.16 10:45
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30

Prep seq: 712103
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 7 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 10:48
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
J0101
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00550
Matrix:
K0102
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999995
Date Prep: 08.16.16 06.30
Flag
mg/L
08.17.16 10:51
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
K0103
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30
Flag
mg/L
08.17.16 11:02
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00830
Matrix:
K0104
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.17.16 11:05
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30

Prep seq: 712103
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 8 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 11:08
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
K0105
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
K0106
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
999995
Date Prep: 08.16.16 06.30
Flag
mg/L
08.17.16 11:11
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00410
Matrix:
K0107
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30
Flag
mg/L
08.17.16 11:13
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
K0108
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.17.16 11:16
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30

Prep seq: 712103
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 9 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 11:19
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
K0109
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
K0110
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 11:22
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
K0111
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 11:49
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
K0112
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 11:52
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep seq: 712104
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 10 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 12:17
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
K0113
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
L0114
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 12:20
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00570
Matrix:
L0115
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 12:23
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
L0116
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.17.16 12:26
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep seq: 712104
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00440
Page 11 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 12:29
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
L0117
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
L0118
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 12:32
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0119
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 12:35
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0120
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 12:38
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep seq: 712104
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 12 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 12:41
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
M0121
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0122
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 12:44
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0123
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 12:56
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0124
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 12:59
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep seq: 712104
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 13 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 13:02
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
M0125
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0126
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 13:05
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0127
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45
Flag
mg/L
08.17.16 13:14
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
M0128
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 13:17
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep seq: 712104
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 14 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 13:20
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
M0129
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000021
Date Prep: 08.16.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
M0130
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 13:23
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
N0131
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 13:47
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00450
Matrix:
N0132
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.17.16 14:04
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep seq: 712105
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 15 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 14:16
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
N0133
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
N0134
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 14:19
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
N0135
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 14:22
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
N0136
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 14:25
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep seq: 712105
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 16 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 14:28
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
N0137
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
N0138
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 14:31
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
N0139
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 14:34
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
O0140
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 14:37
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep seq: 712105
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 17 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 14:40
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
O0141
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
O0142
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 14:57
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
O0143
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 15:00
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
O0144
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 15:03
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep seq: 712105
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 18 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 15:06
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
O0145
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
O0146
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 15:10
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
O0147
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00
Flag
mg/L
08.17.16 15:13
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
O0148
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 15:16
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep seq: 712105
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 19 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 15:19
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
O0149
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
P0150
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.17.16 15:22
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0173
Matrix:
P0151
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15
mg/L
Flag
Dil Factor
08.19.16 08:18
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.136
Matrix:
P0152
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Units
mg/L
Flag
Dil Factor
08.19.16 08:21
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep seq: 712106
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00870
Page 20 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 08:25
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
P0153
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00950
Matrix:
P0154
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 08:28
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00860
Matrix:
P0155
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 08:31
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00860
Matrix:
P0156
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 08:34
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep seq: 712106
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00900
Page 21 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 08:37
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
Q0157
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00820
Matrix:
Q0158
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 09:03
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00790
Matrix:
Q0159
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 09:06
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00620
Matrix:
Q0160
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 09:09
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep seq: 712106
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00750
Page 22 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 09:12
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
Q0161
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00610
Matrix:
Q0162
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 09:29
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00590
Matrix:
Q0163
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 09:32
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00650
Matrix:
Q0164
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 09:35
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep seq: 712106
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00780
Page 23 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 09:38
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
Q0165
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00870
Matrix:
Q0166
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 09:41
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00750
Matrix:
Q0167
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15
Flag
mg/L
08.19.16 09:44
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00570
Matrix:
Q0168
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 09:48
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep seq: 712106
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00660
Page 24 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 09:51
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
R0169
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712106

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00460
Matrix:
R0170
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000181
Date Prep: 08.19.16 06.00
Flag
mg/L
08.19.16 09:54
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0101
Matrix:
R0171
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00
Flag
mg/L
08.19.16 10:18
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00610
Matrix:
R0172
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 10:21
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00

Prep seq: 712781
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00490
Page 25 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 10:47
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
R0173
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
R0174
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000181
Date Prep: 08.19.16 06.00
Flag
mg/L
08.19.16 10:50
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00510
Matrix:
R0175
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00
Flag
mg/L
08.19.16 10:53
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
R0176
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 10:56
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00

Prep seq: 712781
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 26 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 10:59
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
R0177
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
R0178
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000181
Date Prep: 08.19.16 06.00
Flag
mg/L
08.19.16 11:02
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00410
Matrix:
R0179
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00
Flag
mg/L
08.19.16 11:05
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00880
Matrix:
R0180
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 11:08
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00

Prep seq: 712781
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00720
Page 27 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 11:11
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
R0181
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

Parameter
Lead
CAS
Number
7439-92-1
Result
0.00550
Page 28 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 11:14
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
712103-1-BLK
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
999995
Date Prep: 08.16.16 06.30
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712103

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712104-1-BLK
MQL
0.0120
SDL
0.00400
Seq Number:
Flag
mg/L
08.17.16 09:55
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
Analysis
Date
Units
DAT
% Moist:
1000021
Date Prep: 08.16.16 06.45
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712104

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712105-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 11:46
Units
mg/L
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
1000047
Date Prep: 08.16.16 07.00
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712105

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712106-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.17.16 13:44
Units
mg/L
Date Collected:
Date Received:
Prep Method:
E200.7P
Tech:
DAT

DAT
% Moist:
Seq Number:
1000171
Date Prep: 08.16.16 07.15
Sample Depth:
Water
Analyst:
Dil Factor
Prep seq: 712106

Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 29 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 08:15
Units
mg/L
Final 1.000
Dil Factor
1

534987
Sample Id:
Matrix:
712781-1-BLK
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
1000181
Date Prep: 08.19.16 06.00
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712781

Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 30 of 52
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 10:15
Units
mg/L
Final 1.000
Dil Factor
1
Flagging Criteria
RL Reporting Limit

NC Non-Calculable

Phone
(281) 240-4200
(214) 902 0300
(210) 509-3334
(432) 563-1800
(602) 437-0330

Page 31 of 52
Fax
(281) 240-4280
(214) 351-9139
(210) 509-3335
(432) 563-1713
Final 1.000
BS / BSD Recoveries
Project ID:
DAT
Analyst:
Batch #: 1
mg/L
Units:
Blank
Sample Result
[A]
Analytes
Lead
<0.00400
DAT
Lead
Blank
Sample Result
[A]
<0.00400
DAT
1.08
108
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.09
Spike
Added
Blk. Spk
Dup.
%R
[G]
109
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

Matrix: Water
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.10
Blank
Spike
%R
[D]
110
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.09
Spike
Added

mg/L
Units:
1.00
Blank
Spike
%R
[D]
Batch #: 1
Analytes
[B]
Blank
Spike
Result
[C]
Analyst:
Spike
Added
mg/L
Units:
Matrix: Water
Analyst:
109
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
Blk. Spk
Dup.
%R
[G]
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.09
Blank
Spike
%R
[D]
109
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.08
Spike
Added
Blk. Spk
Dup.
%R
[G]
108

Version: 1.%
Page 32 of 52
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
BS / BSD Recoveries
Project ID:
DAT
Analyst:

Batch #: 1
mg/L
Units:
Blank
Sample Result
[A]
Analytes
Lead
<0.00400
DAT
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.04
Blank
Spike
%R
[D]
104
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.03
Spike
Added

mg/L
Units:
Matrix: Water
Analyst:
103
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
Blk. Spk
Dup.
%R
[G]
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.02
Blank
Spike
%R
[D]
102
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.03
Spike
Added
Blk. Spk
Dup.
%R
[G]
103

Version: 1.%
Page 33 of 52
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

Work Order # :
534987
Lab Batch ID:
999995
Date Analyzed:
08/17/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
999995
Date Analyzed:
08/17/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000021
Date Analyzed:
08/17/2016
Reporting Units:
mg/L

Analytes
Lead

Project ID:
Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.250
25.0

Result
Sample
[C]
%R
[D]
27.0

107
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
25.0
Batch #:
27.5
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
109
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.06

106
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.06
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
106
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.06
106
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.05
Page 34 of 52
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
105
75-125
20
Flag

Work Order # :
534987
Lab Batch ID:
1000021
Date Analyzed:
08/17/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000047
Date Analyzed:
08/17/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000047
Date Analyzed:
08/17/2016
Reporting Units:
mg/L

Analytes
Lead

Project ID:
Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.05

105
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.05
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
105
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.05

105
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.05
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
105
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.05
105
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.06
Page 35 of 52
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
106
75-125
20
Flag

Work Order # :
534987
Lab Batch ID:
1000171
Date Analyzed:
08/19/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000171
Date Analyzed:
08/19/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000181
Date Analyzed:
08/19/2016
Reporting Units:
mg/L

Analytes
Lead

Project ID:
Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00900
1.00

Result
Sample
[C]
%R
[D]
0.918

91
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
0.918
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
91
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00750
1.00

Result
Sample
[C]
%R
[D]
1.01

100
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.01
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
100
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00610
1.00

Result
Sample
[C]
%R
[D]
1.02
101
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.01
Page 36 of 52
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
100
75-125
20
Flag

Work Order # :
534987
Lab Batch ID:
1000181
Date Analyzed:
08/19/2016
Reporting Units:
mg/L

Analytes
Lead

Project ID:
Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.0200
5.00

Result
Sample
[C]
%R
[D]
5.04
101
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
5.00
5.00
Page 37 of 52
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
100
75-125
20
Flag
Page 38 of 52
Final 1.000
Page 39 of 52
Final 1.000
Page 40 of 52
Final 1.000
Page 41 of 52
Final 1.000
Page 42 of 52
Final 1.000
Page 43 of 52
Final 1.000
Page 44 of 52
Final 1.000
Page 45 of 52
Final 1.000
Page 46 of 52
Final 1.000
Page 47 of 52
Final 1.000
Page 48 of 52
Final 1.000
Page 49 of 52
Final 1.000
Page 50 of 52
Final 1.000
Page 51 of 52
Final 1.000
XENCO Laboratories


Comments

1.8

Yes
Yes

Yes
Yes

N/A
N/A

Yes
Yes

No
Yes

Yes
Yes

Yes
Yes

No
Yes

Yes
Yes

No
N/A
analysts.
N/A
SX 58 added HNO3
N/A
Analyst: CG
Date: 08/15/2016
Cindy Guerra

Date: 08/16/2016
Gale Denman
Page 52 of 52
Final 1.000

for
----24-AUG-16

Dallas, TX 75220
Oklahoma (9218)
Page 1 of 40
Final 1.000
Table of Contents
Cover Page
Cover Letter
Case Narrative
24
25
MS / MSD Recoveries
27
Chain of Custody
30
40
Page 2 of 40
Final 1.000
24-AUG-16
1800 Hwy 114
Justin, TX 76247
--Project Address: ---Rusty Stierwalt :
Respectfully,
Gale Denman
Project Manager
Page 3 of 40
Final 1.000

--Sample Id
S0182
S0183
S0184
S0185
S0186
S0187
S0188
S0189
S0190
S0191
S0192
S0193
S0194
T0195
T0196
T0197
T0198
T0199
T0200
T0201
T0202
T0203
T0204
T0205
T0206
U0207
U0208
U0209
U0210
U0211
U0212
U0213
U0214
U0215
U0216
U0217
U0218
V0219
V0220
V0221
V0222
V0223
V0224
Matrix
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
Date Collected
Sample Depth
535098-001
535098-002
535098-003
535098-004
535098-005
535098-006
535098-007
535098-008
535098-009
535098-010
535098-011
535098-012
535098-013
535098-014
535098-015
535098-016
535098-017
535098-018
535098-019
535098-020
535098-021
535098-022
535098-023
535098-024
535098-025
535098-026
535098-027
535098-028
535098-029
535098-030
535098-031
535098-032
535098-033
535098-034
535098-035
535098-036
535098-037
535098-038
535098-039
535098-040
535098-041
535098-042
535098-043
08-15-16 12:50
08-15-16 12:55
08-15-16 13:00
08-15-16 13:05
08-15-16 13:10
08-15-16 13:13
08-15-16 13:16
08-15-16 13:20
08-15-16 13:23
08-15-16 13:27
08-15-16 13:34
08-15-16 13:39
08-15-16 13:43
08-15-16 14:15
08-15-16 14:20
08-15-16 14:25
08-15-16 14:30
08-15-16 14:34
08-15-16 14:37
08-15-16 14:42
08-15-16 14:46
08-15-16 14:50
08-15-16 14:55
08-15-16 15:00
08-15-16 15:06
08-16-16 08:50
08-16-16 08:55
08-16-16 08:59
08-16-16 09:04
08-16-16 09:10
08-16-16 09:14
08-16-16 09:18
08-16-16 09:21
08-16-16 09:26
08-16-16 09:30
08-16-16 09:34
08-16-16 09:40
08-16-16 10:25
08-16-16 10:30
08-16-16 10:35
08-16-16 10:40
08-16-16 10:45
08-16-16 10:51
Page 4 of 40
Lab Sample Id
Final 1.000

--V0225
W0226
W0227
W0228
W0229
W0230
W0231
W0232
W0233
W0234
W0235
W0236
W0237
W0238
W0239
W0240
W0241
W0242
W0243
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
535098-044
535098-045
535098-046
535098-047
535098-048
535098-049
535098-050
535098-051
535098-052
535098-053
535098-054
535098-055
535098-056
535098-057
535098-058
535098-059
535098-060
535098-061
535098-062
08-16-16 10:57
08-16-16 12:30
08-16-16 12:36
08-16-16 12:42
08-16-16 12:47
08-16-16 12:55
08-16-16 13:00
08-16-16 13:04
08-16-16 13:07
08-16-16 13:11
08-16-16 13:15
08-16-16 13:20
08-16-16 13:24
08-16-16 13:30
08-16-16 13:35
08-16-16 13:40
08-16-16 13:45
08-16-16 13:55
08-16-16 14:00
Page 5 of 40
Final 1.000
CASE NARRATIVE
Project ID:
the laboratory.

None
Page 6 of 40
Final 1.000

535098
--Sample Id:
Matrix:
S0182
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00730
Matrix:
S0183
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 12:17
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00980
Matrix:
S0184
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 12:20
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00780
Matrix:
S0185
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 12:46
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep seq: 712782
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00580
Page 7 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 12:49
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
S0186
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00630
Matrix:
S0187
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 12:52
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00740
Matrix:
S0188
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 12:55
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00470
Matrix:
S0189
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 12:58
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep seq: 712782
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00760
Page 8 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 13:02
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
S0190
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00560
Matrix:
S0191
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 13:05
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00660
Matrix:
S0192
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 13:08
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00750
Matrix:
S0193
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 13:11
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep seq: 712782
Parameter
Lead
CAS
Number
7439-92-1
Result
0.0108
Page 9 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 13:14
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
S0194
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00670
Matrix:
T0195
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 13:32
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00480
Matrix:
T0196
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 13:35
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
T0197
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 13:38
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep seq: 712782
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 10 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 13:41
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
T0198
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00600
Matrix:
T0199
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 13:44
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00410
Matrix:
T0200
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15
Flag
mg/L
08.19.16 13:47
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00780
Matrix:
T0201
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.19.16 13:50
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15

Prep seq: 712782
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00470
Page 11 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.19.16 13:53
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
T0202
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
T0203
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 11:40
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
T0204
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 11:43
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
T0205
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 11:46
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep seq: 712783
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 12 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 11:49
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
T0206
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0207
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 11:52
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0208
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 11:55
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0209
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 12:21
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep seq: 712783
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 13 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 12:24
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
U0210
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0211
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 12:27
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0212
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 12:30
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0213
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 12:33
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep seq: 712783
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 14 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 12:36
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
U0214
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0215
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 12:39
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0216
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 12:51
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
U0217
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 12:54
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep seq: 712783
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 15 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 12:57
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
U0218
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
V0219
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 13:06
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
V0220
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30
Flag
mg/L
08.22.16 13:09
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
V0221
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 13:12
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000292
Date Prep: 08.19.16 06.30

Prep seq: 712783
Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 16 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 13:15
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
V0222
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00740
Matrix:
V0223
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 08:21
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00770
Matrix:
V0224
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 08:24
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00750
Matrix:
V0225
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.23.16 08:27
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep seq: 712784
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00730
Page 17 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 08:30
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
W0226
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00580
Matrix:
W0227
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 08:33
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00660
Matrix:
W0228
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 08:36
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00750
Matrix:
W0229
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.23.16 08:39
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep seq: 712784
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00750
Page 18 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 09:05
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
W0230
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00710
Matrix:
W0231
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 09:08
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00770
Matrix:
W0232
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 09:11
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00740
Matrix:
W0233
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.23.16 09:14
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep seq: 712784
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00820
Page 19 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 09:17
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
W0234
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00760
Matrix:
W0235
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 09:29
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00780
Matrix:
W0236
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 09:32
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00690
Matrix:
W0237
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.23.16 09:35
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep seq: 712784
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00710
Page 20 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 09:38
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
W0238
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00820
Matrix:
W0239
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 09:46
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00730
Matrix:
W0240
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45
Flag
mg/L
08.23.16 09:49
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00650
Matrix:
W0241
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.23.16 09:52
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45

Prep seq: 712784
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00660
Page 21 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 09:55
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
W0242
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000366
Date Prep: 08.23.16 06.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712898

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00900
Matrix:
W0243
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000366
Date Prep: 08.23.16 06.00
Flag
mg/L
08.23.16 10:20
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712898

Parameter
Lead
CAS
Number
7439-92-1
Result
0.00930
Page 22 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 10:37
Units
mg/L
Final 1.000
Dil Factor
1

535098
--Sample Id:
Matrix:
712782-1-BLK
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
1000201
Date Prep: 08.19.16 06.15
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712782

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712783-1-BLK
MQL
0.0120
SDL
0.00400
Seq Number:
Flag
mg/L
08.19.16 12:14
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
Analysis
Date
Units
DAT
% Moist:
1000292
Date Prep: 08.19.16 06.30
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712783

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712784-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.22.16 11:37
Units
mg/L
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
1000351
Date Prep: 08.19.16 06.45
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712784

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712898-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 08:18
Units
mg/L
Date Collected:
Date Received:
Prep Method:
E200.7P
Tech:
DAT

DAT
% Moist:
Seq Number:
1000366
Date Prep: 08.23.16 06.00
Sample Depth:
Water
Analyst:
Dil Factor
Prep seq: 712898

Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 23 of 40
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 10:17
Units
mg/L
Final 1.000
Dil Factor
1
Flagging Criteria
RL Reporting Limit

NC Non-Calculable

Phone
(281) 240-4200
(214) 902 0300
(210) 509-3334
(432) 563-1800
(602) 437-0330

Page 24 of 40
Fax
(281) 240-4280
(214) 351-9139
(210) 509-3335
(432) 563-1713
Final 1.000
BS / BSD Recoveries

Analyst:
DAT
Batch #: 1
mg/L
Units:
Blank
Sample Result
[A]
Analytes
Lead
<0.00400
DAT
Lead
Blank
Sample Result
[A]
<0.00400
DAT
1.03
103
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.03
Spike
Added
Blk. Spk
Dup.
%R
[G]
103
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

Matrix: Water
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.07
Blank
Spike
%R
[D]
107
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.06
Spike
Added

mg/L
Units:
1.00
Blank
Spike
%R
[D]
Batch #: 1
Analytes
[B]
Blank
Spike
Result
[C]
Analyst:
Spike
Added
mg/L
Units:
Matrix: Water
Analyst:
106
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
Blk. Spk
Dup.
%R
[G]
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.04
Blank
Spike
%R
[D]
104
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.04
Spike
Added
Blk. Spk
Dup.
%R
[G]
104

Page 25 of 40
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
BS / BSD Recoveries

Analyst:
DAT

mg/L
Units:
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.05
Blank
Spike
%R
[D]
105
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.05
Spike
Added
Blk. Spk
Dup.
%R
[G]
105

Page 26 of 40
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

535098
Lab Batch ID:
1000201
Date Analyzed:
08/19/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000201
Date Analyzed:
08/19/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000292
Date Analyzed:
08/22/2016
Reporting Units:
mg/L

Analytes
Lead

Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00980
1.00

Result
Sample
[C]
%R
[D]
0.985
98
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
0.984
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
97
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.0108
1.00

Result
Sample
[C]
%R
[D]
0.988

98
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
0.989
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
98
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.03
103
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.02
Page 27 of 40
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
102
75-125
20
Flag

535098
Lab Batch ID:
1000292
Date Analyzed:
08/22/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000351
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000351
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead


Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.04

104
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.05
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
105
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00750
1.00

Result
Sample
[C]
%R
[D]
1.01

100
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.00
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
99
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00710
1.00

Result
Sample
[C]
%R
[D]
1.01
100
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.01
Page 28 of 40
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
100
75-125
20
Flag

535098
Lab Batch ID:
1000366
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000366
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead

Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00900
1.00

Sample
Result
%R
[C]
[D]
1.02
101
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.02
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
101
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.0132
1.00

Sample
Result
%R
[C]
[D]
1.05
104
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.05
Page 29 of 40
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
104
75-125
20
Flag
Page 30 of 40
Final 1.000
Page 31 of 40
Final 1.000
Page 32 of 40
Final 1.000
Page 33 of 40
Final 1.000
Page 34 of 40
Final 1.000
Page 35 of 40
Final 1.000
Page 36 of 40
Final 1.000
Page 37 of 40
Final 1.000
Page 38 of 40
Final 1.000
Page 39 of 40
Final 1.000
XENCO Laboratories


Comments

1.5

Yes
Yes

Yes
Yes

N/A
Yes

Yes
Yes

No
Yes

Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

No
N/A
analysts.
Yes
N/A
Analyst: CG
Date: 08/17/2016
Angelica Martinez

Date: 08/18/2016
Gale Denman
Page 40 of 40
Final 1.000

for
----26-AUG-16

Dallas, TX 75220
Oklahoma (9218)
Page 1 of 37
Final 1.000
Table of Contents
Cover Page
Cover Letter
Case Narrative
22
23
MS / MSD Recoveries
25
Chain of Custody
28
37
Page 2 of 37
Final 1.000
26-AUG-16
1800 Hwy 114
Justin, TX 76247
Respectfully,
Gale Denman
Project Manager
Page 3 of 37
Final 1.000

--Sample Id
AA0286
AA0287
AA0288
BB0289
BB0290
BB0291
BB0292
BB0293
CC0294
CC0295
CC0296
CC0297
X0244
X0245
X0246
X0247
X0248
X0249
X0250
X0251
X0252
X0253
X0254
X0255
X0256
X0257
X0258
X0259
X0260
Y0261
Y0262
Y0263
Y0264
Y0265
Y0266
Y0267
Y0268
Y0269
Y0270
Y0271
Y0272
Y0273
Y0274
Matrix
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
Date Collected
Sample Depth
535422-001
535422-002
535422-003
535422-004
535422-005
535422-006
535422-007
535422-008
535422-009
535422-010
535422-011
535422-012
535422-013
535422-014
535422-015
535422-016
535422-017
535422-018
535422-019
535422-020
535422-021
535422-022
535422-023
535422-024
535422-025
535422-026
535422-027
535422-028
535422-029
535422-030
535422-031
535422-032
535422-033
535422-034
535422-035
535422-036
535422-037
535422-038
535422-039
535422-040
535422-041
535422-042
535422-043
08-19-16 12:50
08-19-16 12:55
08-19-16 13:03
08-19-16 14:40
08-19-16 14:45
08-19-16 14:50
08-19-16 15:00
08-19-16 15:05
08-19-16 15:15
08-19-16 15:19
08-19-16 15:24
08-19-16 15:30
08-17-16 13:25
08-17-16 13:30
08-17-16 13:36
08-17-16 13:40
08-17-16 13:45
08-17-16 13:50
08-17-16 13:54
08-17-16 14:03
08-17-16 14:07
08-17-16 14:11
08-17-16 14:30
08-17-16 14:35
08-17-16 14:40
08-17-16 14:50
08-17-16 15:00
08-17-16 15:20
08-17-16 15:30
08-19-16 07:55
08-19-16 08:05
08-19-16 08:08
08-19-16 08:12
08-19-16 08:17
08-19-16 08:20
08-19-16 08:24
08-19-16 08:29
08-19-16 08:35
08-19-16 08:39
08-19-16 08:44
08-19-16 08:50
08-19-16 08:55
08-19-16 09:00
Version: 1.%
Page 4 of 37
Lab Sample Id
Final 1.000

--Y0275
Y0276
Y0277
Y0278
Z0279
Z0280
Z0281
Z0282
Z0283
Z0284
Z0285
DD0298
DD0299
W
W
W
W
W
W
W
W
W
W
W
W
W
535422-044
535422-045
535422-046
535422-047
535422-048
535422-049
535422-050
535422-051
535422-052
535422-053
535422-054
535422-055
535422-056
08-19-16 09:05
08-19-16 09:10
08-19-16 09:20
08-19-16 09:25
08-19-16 10:00
08-19-16 10:05
08-19-16 10:10
08-19-16 10:15
08-19-16 10:18
08-19-16 10:23
08-19-16 10:27
08-19-16 15:35
08-19-16 15:40
Version: 1.%
Page 5 of 37
Final 1.000
CASE NARRATIVE
Project ID:
the laboratory.

None
Page 6 of 37
Final 1.000

535422
--Sample Id:
Matrix:
AA0286
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00510
Matrix:
AA0287
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 09:12
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00620
Matrix:
AA0288
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 09:15
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00490
Matrix:
BB0289
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 09:18
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep seq: 712901
Parameter
Lead
CAS
Number
7439-92-1
Result
0.0105
Page 7 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 09:21
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
BB0290
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00530
Matrix:
BB0291
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 09:24
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00720
Matrix:
BB0292
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 09:27
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00590
Matrix:
BB0293
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 09:30
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep seq: 712901
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00450
Page 8 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 09:56
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
CC0294
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0108
Matrix:
CC0295
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 09:59
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00570
Matrix:
CC0296
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 10:02
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00720
Matrix:
CC0297
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 10:05
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep seq: 712901
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00430
Page 9 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 10:08
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
X0244
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00710
Matrix:
X0245
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 10:20
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00710
Matrix:
X0246
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 10:24
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00610
Matrix:
X0247
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 10:32
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep seq: 712901
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00560
Page 10 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 10:35
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
X0248
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00460
Matrix:
X0249
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 10:38
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00490
Matrix:
X0250
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00
Flag
mg/L
08.25.16 10:41
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00570
Matrix:
X0251
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 10:44
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000558
Date Prep: 08.23.16 07.00

Prep seq: 712901
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00530
Page 11 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 10:48
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
X0252
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00450
Matrix:
X0253
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 11:12
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00540
Matrix:
X0254
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 11:15
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00710
Matrix:
X0255
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 11:18
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep seq: 712902
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00510
Page 12 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 11:21
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
X0256
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00490
Matrix:
X0257
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 11:24
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00530
Matrix:
X0258
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 11:27
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00820
Matrix:
X0259
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 11:53
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep seq: 712902
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00580
Page 13 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 11:56
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
X0260
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00540
Matrix:
Y0261
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 11:59
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00510
Matrix:
Y0262
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 12:02
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00430
Matrix:
Y0263
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 12:20
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep seq: 712902
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00510
Page 14 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 12:23
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
Y0264
Sample Depth:
Water

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00540
Matrix:
Y0265
MQL
0.0120
SDL
0.00400

Analyst:
Seq Number:
DAT
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 12:26
Dil Factor
1
Sample Depth:
Water
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
Y0266
MQL
0.0120
SDL
0.00400

DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 12:29
Dil Factor
1
Sample Depth:
Water
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00450
Matrix:
Y0267
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 12:32
Units
mg/L
Dil Factor
1
Sample Depth:
Water

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep seq: 712902
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00540
Page 15 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 12:35
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
Y0268
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00520
Matrix:
Y0269
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 12:38
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00460
Matrix:
Y0270
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30
Flag
mg/L
08.25.16 12:41
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
Lead
Sample Id:
7439-92-1
Result
<0.00400
Matrix:
Y0271
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 12:44
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30

Prep seq: 712902
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00520
Page 16 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 12:47
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
Y0272
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0102
Matrix:
Y0273
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000530
Date Prep: 08.23.16 10.00
Flag
mg/L
08.25.16 07:04
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.0115
Matrix:
Y0274
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00
Flag
mg/L
08.25.16 07:07
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00510
Matrix:
Y0275
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 07:33
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00

Prep seq: 712917
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00670
Page 17 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 07:36
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
Y0276
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00450
Matrix:
Y0277
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000530
Date Prep: 08.23.16 10.00
Flag
mg/L
08.25.16 07:39
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00580
Matrix:
Y0278
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00
Flag
mg/L
08.25.16 07:42
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00600
Matrix:
Z0279
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 07:45
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00

Prep seq: 712917
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00540
Page 18 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 07:48
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
Z0280
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00500
Matrix:
Z0281
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000530
Date Prep: 08.23.16 10.00
Flag
mg/L
08.25.16 07:51
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00430
Matrix:
Z0282
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00
Flag
mg/L
08.25.16 07:54
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00400
Matrix:
Z0283
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.25.16 07:58
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00

Prep seq: 712917
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00690
Page 19 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 08:01
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
Z0284
Water
Sample Depth:

Analyst:
DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00670
Matrix:
Z0285
MQL
0.0120
SDL
0.00400
Water

Analyst:
Seq Number:
DAT
1000530
Date Prep: 08.23.16 10.00
Flag
mg/L
08.25.16 08:15
Dil Factor
1
Sample Depth:
% Moist:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712917

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00580
Matrix:
DD0298
MQL
0.0120
SDL
0.00400
Water

DAT
% Moist:
Seq Number:
1000387
Date Prep: 08.23.16 06.30
Flag
mg/L
08.25.16 08:18
Dil Factor
1
Sample Depth:
Analyst:
Analysis
Date
Units

Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712900

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
0.00630
Matrix:
DD0299
MQL
0.0120
SDL
0.00400
Water
Analysis
Date
Flag
08.23.16 13:15
Units
mg/L
Dil Factor
1
Sample Depth:

Prep Method:
E200.7P
Tech:
DAT

Analyst:
DAT
% Moist:
Seq Number:
1000387
Date Prep: 08.23.16 06.30

Prep seq: 712900
Parameter
Lead
CAS
Number
7439-92-1
Result
0.00720
Page 20 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.23.16 13:18
Units
mg/L
Final 1.000
Dil Factor
1

535422
--Sample Id:
Matrix:
712900-1-BLK
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
1000387
Date Prep: 08.23.16 06.30
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712900

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712901-1-BLK
MQL
0.0120
SDL
0.00400
Seq Number:
Flag
mg/L
08.23.16 12:17
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
Analysis
Date
Units
DAT
% Moist:
1000558
Date Prep: 08.23.16 07.00
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712901

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712902-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 09:09
Units
mg/L
Dil Factor
1
Sample Depth:
Water
Date Collected:
Date Received:

Analyst:
DAT
% Moist:
Seq Number:
1000584
Date Prep: 08.23.16 07.30
Prep Method:
E200.7P
Tech:
DAT
Prep seq: 712902

CAS
Number
Parameter
7439-92-1
Lead
Sample Id:
Result
<0.00400
Matrix:
712917-1-BLK
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 11:09
Units
mg/L
Date Collected:
Date Received:
Prep Method:
E200.7P
Tech:
DAT

DAT
% Moist:
Seq Number:
1000530
Date Prep: 08.23.16 10.00
Sample Depth:
Water
Analyst:
Dil Factor
Prep seq: 712917

Parameter
Lead
CAS
Number
7439-92-1
Result
<0.00400
Page 21 of 37
MQL
0.0120
SDL
0.00400
Analysis
Date
Flag
08.25.16 07:01
Units
mg/L
Final 1.000
Dil Factor
1
Flagging Criteria
RL Reporting Limit

NC Non-Calculable

Phone
(281) 240-4200
(214) 902 0300
(210) 509-3334
(432) 563-1800
(602) 437-0330

Page 22 of 37
Fax
(281) 240-4280
(214) 351-9139
(210) 509-3335
(432) 563-1713
Final 1.000
BS / BSD Recoveries

DAT
Analyst:
Batch #: 1
mg/L
Units:
Blank
Sample Result
[A]
Analytes
Lead
<0.00400
DAT
Lead
Blank
Sample Result
[A]
<0.00400
DAT
1.06
106
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.05
Spike
Added
Blk. Spk
Dup.
%R
[G]
105
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

Matrix: Water
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.05
Blank
Spike
%R
[D]
105
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.05
Spike
Added

mg/L
Units:
1.00
Blank
Spike
%R
[D]
Batch #: 1
Analytes
[B]
Blank
Spike
Result
[C]
Analyst:
Spike
Added
mg/L
Units:
Matrix: Water
Analyst:
105
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
Blk. Spk
Dup.
%R
[G]
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.06
Blank
Spike
%R
[D]
106
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.07
Spike
Added
Blk. Spk
Dup.
%R
[G]
107

Version: 1.%
Page 23 of 37
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag
BS / BSD Recoveries

DAT
Analyst:

mg/L
Units:
Batch #: 1
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
<0.00400
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.07
Blank
Spike
%R
[D]
107
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.06
Spike
Added
Blk. Spk
Dup.
%R
[G]
106

Version: 1.%
Page 24 of 37
Final 1.000
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

535422
Lab Batch ID:
1000387
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000387
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000530
Date Analyzed:
08/25/2016
Reporting Units:
mg/L

Analytes
Lead

Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.00400
1.00

Result
Sample
[C]
%R
[D]
1.05
105
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.05
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
105
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.0492
1.00

Result
Sample
[C]
%R
[D]
0.907

86
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
0.909
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
86
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.0115
1.00

Result
Sample
[C]
%R
[D]
1.03
102
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.03
Page 25 of 37
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
102
75-125
20
Flag

535422
Lab Batch ID:
1000530
Date Analyzed:
08/25/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000558
Date Analyzed:
08/25/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000558
Date Analyzed:
08/25/2016
Reporting Units:
mg/L

Analytes
Lead


Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00450
1.00

Result
Sample
[C]
%R
[D]
1.06

106
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.06
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
106
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00590
1.00

Result
Sample
[C]
%R
[D]
1.04

103
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.04
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
103
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00710
1.00

Result
Sample
[C]
%R
[D]
1.02
101
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.02
Page 26 of 37
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
101
75-125
20
Flag

535422
Lab Batch ID:
1000584
Date Analyzed:
08/25/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000584
Date Analyzed:
08/25/2016
Reporting Units:
mg/L

Analytes
Lead

Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00530
1.00

Sample
Result
%R
[C]
[D]
1.02
101
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.02
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
101
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.00510
1.00

Sample
Result
%R
[C]
[D]
1.04
103
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.05
Page 27 of 37
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
104
75-125
20
Flag
Page 28 of 37
Final 1.000
Page 29 of 37
Final 1.000
Page 30 of 37
Final 1.000
Page 31 of 37
Final 1.000
Page 32 of 37
Final 1.000
Page 33 of 37
Final 1.000
Page 34 of 37
Final 1.000
Page 35 of 37
Final 1.000
Page 36 of 37
Final 1.000
XENCO Laboratories


Comments

1.5

Yes
Yes

N/A
N/A

N/A
N/A

Yes
Yes
Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

No
N/A
analysts.
Yes
Received two extra samples not

listed on COC
DD0298 (0819/16 03:35) and
DD0299 (08/19/16 03:40)
N/A
Analyst: ana
Date: 08/22/2016
Angelica Martinez

Date: 08/23/2016
Gale Denman
Page 37 of 37
Final 1.000

for
----24-AUG-16

Dallas, TX 75220
Oklahoma (9218)
Page 1 of 9
Final 1.000
Table of Contents
Cover Page
Cover Letter
Certificate of Analysis Summary
MS / MSD Recoveries
Chain of Custody
Page 2 of 9
Final 1.000
24-AUG-16
1800 Hwy 114
Justin, TX 76247
Respectfully,
Gale Denman
Project Manager
Page 3 of 9
Final 1.000
Certificate of Analysis Summary 535423

Project Name: --Project Id:
---
Contact:
Project Location:
Rusty Stierwalt
---
Analysis Requested
Date Received in Lab: Mon Aug-22-16 11:40 am

Report Date: 24-AUG-16
Project Manager: Gale Denman
Lab Id:
535423-001
535423-002
Field Id:
P0150
P0151
Depth:
Matrix:
WATER
WATER
Sampled:
Aug-22-16 09:05
Aug-22-16 09:10
Extracted:
Aug-23-16 06:30
Aug-23-16 06:30
Analyzed:
Aug-23-16 13:34
Aug-23-16 13:37
Units/RL:
Lead
mg/L
0.0150
RL
0.0120
mg/L
<0.0120
RL
0.0120
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.
The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.
XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.
Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
________________________________
Gale Denman
Project Manager
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 4 of 9
Final 1.000
Flagging Criteria
RL Reporting Limit

NC Non-Calculable

Phone
(281) 240-4200
(214) 902 0300
(210) 509-3334
(432) 563-1800
(602) 437-0330

Page 5 of 9
Fax
(281) 240-4280
(214) 351-9139
(210) 509-3335
(432) 563-1713
Final 1.000
BS / BSD Recoveries

Analyst:
DAT

Batch #: 1
mg/L
Units:
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
<0.0120
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.06
Blank
Spike
%R
[D]
106
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.05
Spike
Added
Blk. Spk
Dup.
%R
[G]

Page 6 of 9
Final 1.000
105
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

535423
Lab Batch ID:
1000387
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
1000387
Date Analyzed:
08/23/2016
Reporting Units:
mg/L

Analytes
Lead

Batch #:
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.0120
1.00

Sample
Result
%R
[C]
[D]
1.05
105
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
1.05
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
105
75-125
20
Flag
Matrix: Water
Analyst: DAT

Parent
Sample
Result
[A]
Spike
Added
[B]
0.0492
1.00

Sample
Result
%R
[C]
[D]
0.907
86
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
0.909
Page 7 of 9
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
86
75-125
20
Flag
Page 8 of 9
Final 1.000
XENCO Laboratories


Comments

1.5

Yes
Yes

N/A
N/A

N/A
N/A

Yes
Yes

No
Yes

Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

No
N/A
analysts.
Yes
N/A
Analyst: ana
Date: 08/22/2016
Angelica Martinez

Date: 08/22/2016
Gale Denman
Page 9 of 9
Final 1.000

for
----04-NOV-16

Dallas, TX 75220
Oklahoma (9218)
Page 1 of 9
Final 1.000
Table of Contents
Cover Page
Cover Letter
Certificate of Analysis Summary
MS / MSD Recoveries
Chain of Custody
Page 2 of 9
Final 1.000
04-NOV-16
1800 Hwy 114
Justin, TX 76247
--Project Address: --Jim Sadler :
Respectfully,
Gale Denman
Project Manager
Page 3 of 9
Final 1.000
Certificate of Analysis Summary 539698

Project Name: --Project Id:
---
Contact:
Project Location:
Jim Sadler
---
Analysis Requested
Date Received in Lab: Thu Nov-03-16 12:37 pm

Report Date: 04-NOV-16
Project Manager: Gale Denman
Lab Id:
539698-001
Field Id:
H0079
Depth:
Matrix:
Nov-03-16 11:20
Extracted:
Nov-03-16 13:40
Analyzed:
Nov-04-16 11:43
Units/RL:
Lead
DRINKING WATER
Sampled:
mg/L
<0.0120
RL
0.0120
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.
The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.
XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.
Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
________________________________
Gale Denman
Project Manager
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Version: 1.%
Page 4 of 9
Final 1.000
Flagging Criteria
RL Reporting Limit

NC Non-Calculable

Phone
(281) 240-4200
(214) 902 0300
(210) 509-3334
(432) 563-1800
(602) 437-0330

Page 5 of 9
Fax
(281) 240-4280
(214) 351-9139
(210) 509-3335
(432) 563-1713
Final 1.000
BS / BSD Recoveries

LEO
Analyst:

Batch #: 1
mg/L
Units:
Matrix: Water

Blank
Sample Result
[A]
Analytes
Lead
<0.0120
Spike
Added
[B]
Blank
Spike
Result
[C]
1.00
1.10
Blank
Spike
%R
[D]
110
[E]
Blank
Spike
Duplicate
Result [F]
1.00
1.11
Spike
Added
Blk. Spk
Dup.
%R
[G]

Version: 1.%
Page 6 of 9
Final 1.000
111
RPD
%
Control
Limits
%R
Control
Limits
%RPD
85-115
20
Flag

539698
Lab Batch ID:
3003262
Date Analyzed:
11/04/2016
Reporting Units:
mg/L

Analytes
Lead
Lab Batch ID:
3003262
Date Analyzed:
11/04/2016
Reporting Units:
mg/L

Analytes
Lead

Batch #:
Matrix: Ground Water
Analyst: LEO

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.0120
1.00

Sample
Result
%R
[C]
[D]
0.997
100
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
Batch #:
0.992
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
99
75-125
20
Flag
Matrix: Ground Water
Analyst: LEO

Parent
Sample
Result
[A]
Spike
Added
[B]
<0.0120
1.00

Sample
Result
%R
[C]
[D]
1.00
100
Duplicate
Spike Spiked Sample
Added
Result [F]
[E]
1.00
1.00
Page 7 of 9
Final 1.000
Spiked
Dup.
%R
[G]
RPD
%
Control
Limits
%R
Control
Limits
%RPD
100
75-125
20
Flag
Page 8 of 9
Final 1.000
XENCO Laboratories
Date/ Time Received: 11/03/2016 12:37:00 PM


Comments

13.7

Yes
No

N/A
N/A

N/A
N/A

Yes
Yes

No
Yes

Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

No
N/A
analysts.
Yes
N/A
Analyst: ana
Date: 11/03/2016
Angelica Martinez

Date: 11/03/2016
Gale Denman
Page 9 of 9
Final 1.000

Dallas, TX 75220
August 23, 2016

Rusty Stierwalt
1800 Hwy 114 Justin, TX 76247
Please find the attached Confirmation of Sample Receipt for samples received by our laboratory on
08/22/2016. The samples have been logged in for a Standard TAT turnaround with results due
08/29/2016. The following is our understanding of your project requirements as described on the
enclosed chain of custody form. To ensure that your needs are met, please take a moment to verify
that:
1. The number and type of samples received are correct.
2. The analytical methods specified are correct.
3. Due dates for analytical results are correct.
4. Address, phone and fax information are correct.
Your samples will be retained for a period of 60 business days following receipt of the samples.
After that time, they will be properly disposed of without further notice, unless there is an
acknowledged written request. We reserve the right to return any unused samples, extracts or
related solutions that have been identified as hazardous waste, are controlled substances under
regulated protocols or have sample sizes exceeding standard analytical practices.
If there are any questions, please do not hesitate to contact your Project Manager and reference
work order number 535422
Page 1 of 13
Confirmation of Sample Receipt # 535422

The following samples were received on Aug 22,2016 and will be analyzed as follows:
Client:
Lab PM:
Project ID:
Project Name:
Location:
QC Package:
EDD Type:

Gale Denman
------TRRP and QCs (Texas-UST)
Turnaround: Standard TAT

Results Due: Aug-29-2016 17:00
Report to
Rusty Stierwalt
Client Sample ID
Lab ID
Method Name (Analysis)
AA0286
535422-001
Water
08/19/16 12:50
AA0287
535422-002
Water
08/19/16 12:55
AA0288
535422-003
Water
08/19/16 13:03
BB0289
535422-004
Water
08/19/16 14:40
BB0290
535422-005
Water
08/19/16 14:45
BB0291
535422-006
Water
08/19/16 14:50
BB0292
535422-007
Water
08/19/16 15:00
BB0293
535422-008
Water
08/19/16 15:05
CC0294
535422-009
Water
08/19/16 15:15
CC0295
535422-010
Water
08/19/16 15:19
CC0296
535422-011
Water
08/19/16 15:24
CC0297
535422-012
Water
08/19/16 15:30
X0244
535422-013
Water
08/17/16 13:25
X0245
535422-014
Water
08/17/16 13:30
X0246
535422-015
Water
08/17/16 13:36
X0247
535422-016
Water
08/17/16 13:40
X0248
535422-017
Water
08/17/16 13:45
X0249
535422-018
Water
08/17/16 13:50
X0250
535422-019
Water
08/17/16 13:54
X0251
535422-020
Water
08/17/16 14:03
X0252
535422-021
Water
08/17/16 14:07
X0253
535422-022
Water
08/17/16 14:11
X0254
535422-023
Water
08/17/16 14:30
X0255
535422-024
Water
08/17/16 14:35
X0256
535422-025
Water
08/17/16 14:40
X0257
535422-026
Water
08/17/16 14:50
X0258
535422-027
Water
08/17/16 15:00
X0259
535422-028
Water
08/17/16 15:20
X0260
535422-029
Water
08/17/16 15:30
Y0261
535422-030
Water
08/19/16 07:55
Y0262
535422-031
Water
08/19/16 08:05
Y0263
535422-032
Water
08/19/16 08:08
Y0264
535422-033
Water
08/19/16 08:12
Y0265
535422-034
Water
08/19/16 08:17
Y0266
535422-035
Water
08/19/16 08:20
Page 2 of 13
Matrix
Sampled
Client:
Lab PM:
Project ID:
Project Name:
Location:
QC Package:
EDD Type:

Gale Denman
------TRRP and QCs (Texas-UST)

Report to
Rusty Stierwalt
Client Sample ID
Lab ID
Y0267
535422-036
Water
08/19/16 08:24
Y0268
535422-037
Water
08/19/16 08:29
Y0269
535422-038
Water
08/19/16 08:35
Y0270
535422-039
Water
08/19/16 08:39
Y0271
535422-040
Water
08/19/16 08:44
Y0272
535422-041
Water
08/19/16 08:50
Y0273
535422-042
Water
08/19/16 08:55
Y0274
535422-043
Water
08/19/16 09:00
Y0275
535422-044
Water
08/19/16 09:05
Y0276
535422-045
Water
08/19/16 09:10
Y0277
535422-046
Water
08/19/16 09:20
Y0278
535422-047
Water
08/19/16 09:25
Z0279
535422-048
Water
08/19/16 10:00
Z0280
535422-049
Water
08/19/16 10:05
Z0281
535422-050
Water
08/19/16 10:10
Z0282
535422-051
Water
08/19/16 10:15
Z0283
535422-052
Water
08/19/16 10:18
Z0284
535422-053
Water
08/19/16 10:23
Z0285
535422-054
Water
08/19/16 10:27
DD0298
535422-055
Water
08/19/16 15:35
DD0299
535422-056
Water
08/19/16 15:40
Special Instructions:
Dallas: Metals (Pb)
Page 3 of 13
Matrix
Sampled
Page 4 of 13
Page 5 of 13
Page 6 of 13
Page 7 of 13
Page 8 of 13
Page 9 of 13
Page 10 of 13
Page 11 of 13
Page 12 of 13
XENCO Laboratories


Comments

1.5

Yes
Yes

N/A
N/A

N/A
N/A

Yes
Yes
Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

No
N/A
analysts.
Yes
Received two extra samples not

listed on COC
DD0298 (0819/16 03:35) and
DD0299 (08/19/16 03:40)
N/A
Analyst: ana
Date: 08/22/2016
Angelica Martinez

Date: 08/23/2016
Gale Denman
Page 13 of 13

Dallas, TX 75220
August 12, 2016

Rusty Stierwalt
1800 Hwy 114 Justin, TX 76247
Please find the attached Confirmation of Sample Receipt for samples received by our laboratory on
08/12/2016. The samples have been logged in for a Standard TAT turnaround with results due
08/19/2016. The following is our understanding of your project requirements as described on the
enclosed chain of custody form. To ensure that your needs are met, please take a moment to verify
that:
1. The number and type of samples received are correct.
2. The analytical methods specified are correct.
3. Due dates for analytical results are correct.
4. Address, phone and fax information are correct.
Your samples will be retained for a period of 60 business days following receipt of the samples.
After that time, they will be properly disposed of without further notice, unless there is an
acknowledged written request. We reserve the right to return any unused samples, extracts or
related solutions that have been identified as hazardous waste, are controlled substances under
regulated protocols or have sample sizes exceeding standard analytical practices.
If there are any questions, please do not hesitate to contact your Project Manager and reference
work order number 534875
Page 1 of 13

The following samples were received on Aug 12,2016 and will be analyzed as follows:
Client:
Lab PM:
Project ID:
Project Name:
Location:
QC Package:
EDD Type:

Gale Denman
------Summary and QCs

Report to
Rusty Stierwalt
Client Sample ID
Lab ID
D0030
534875-001
Water
08/10/16 12:48
D0031
534875-002
Water
08/10/16 12:56
D0032
534875-003
Water
08/10/16 13:02
D0033
534875-004
Water
08/10/16 13:05
D0034
534875-005
Water
08/10/16 13:06
D0035
534875-006
Water
08/10/16 13:08
D0036
534875-007
Water
08/10/16 13:16
D0037
534875-008
Water
08/10/16 13:19
D0038
534875-009
Water
08/10/16 13:23
D0039
534875-010
Water
08/10/16 13:26
D0040
534875-011
Water
08/10/16 13:36
D0041
534875-012
Water
08/10/16 13:40
D0042
534875-013
Water
08/10/16 13:44
D0043
534875-014
Water
08/10/16 13:46
D0044
534875-015
Water
08/10/16 13:48
D0045
534875-016
Water
08/10/16 13:51
D0046
534875-017
Water
08/10/16 13:54
D0047
534875-018
Water
08/10/16 13:56
D0048
534875-019
Water
08/10/16 14:00
D0049
534875-020
Water
08/10/16 14:03
E0050
534875-021
Water
08/10/16 14:35
E0051
534875-022
Water
08/10/16 14:43
E0052
534875-023
Water
08/10/16 14:46
E0053
534875-024
Water
08/10/16 14:48
F0054
534875-025
Water
08/10/16 15:13
F0055
534875-026
Water
08/11/16 08:34
F0056
534875-027
Water
08/11/16 08:36
F0057
534875-028
Water
08/11/16 08:45
F0058
534875-029
Water
08/11/16 08:52
G0059
534875-030
Water
08/11/16 09:52
G0060
534875-031
Water
08/11/16 09:57
G0061
534875-032
Water
08/11/16 10:00
G0062
534875-033
Water
08/11/16 10:04
G0063
534875-034
Water
08/11/16 10:07
G0064
534875-035
Water
08/11/16 10:10
Page 2 of 13
Matrix
Sampled
Client:
Lab PM:
Project ID:
Project Name:
Location:
QC Package:
EDD Type:

Gale Denman

Report to
Rusty Stierwalt
Client Sample ID
Lab ID
G0065
534875-036
Water
08/11/16 10:14
G0066
534875-037
Water
08/11/16 10:17
G0067
534875-038
Water
08/11/16 10:21
G0068
534875-039
Water
08/11/16 10:25
G0069
534875-040
Water
08/11/16 10:30
G0070
534875-041
Water
08/11/16 10:34
G0071
534875-042
Water
08/11/16 10:37
G0072
534875-043
Water
08/11/16 10:39
G0073
534875-044
Water
08/11/16 10:43
G0074
534875-045
Water
08/11/16 10:45
G0075
534875-046
Water
08/11/16 10:47
G0076
534875-047
Water
08/11/16 10:51
G0077
534875-048
Water
08/11/16 10:55
G0078
534875-049
Water
08/11/16 11:00
H0079
534875-050
Water
08/11/16 13:47
H0080
534875-051
Water
08/11/16 13:53
H0081
534875-052
Water
08/11/16 13:57
H0082
534875-053
Water
08/11/16 14:02
H0083
534875-054
Water
08/11/16 14:07
H0084
534875-055
Water
08/11/16 14:12
H0085
534875-056
Water
08/11/16 14:19
H0086
534875-057
Water
08/11/16 14:24
I0087
534875-058
Water
08/11/16 15:07
I0088
534875-059
Water
08/11/16 15:12
I0089
534875-060
Water
08/11/16 15:17
I0090
534875-061
Water
08/11/16 15:20
I0091
534875-062
Water
08/11/16 15:25
I0092
534875-063
Water
08/11/16 15:30
I0093
534875-064
Water
08/11/16 15:33
I0094
534875-065
Water
08/11/16 15:36
I0095
534875-066
Water
08/11/16 15:41
I0096
534875-067
Water
08/11/16 15:46
Special Instructions:
Dallas Metals (Pb)

Page 3 of 13
Matrix
Sampled
Client:
Lab PM:
Project ID:
Project Name:
Location:
QC Package:
EDD Type:

Gale Denman

Report to
Rusty Stierwalt
Page 4 of 13
Page 5 of 13
Page 6 of 13
Page 7 of 13
Page 8 of 13
Page 9 of 13
Page 10 of 13
Page 11 of 13
Page 12 of 13
XENCO Laboratories


Comments

1.3

Yes
Yes

N/A
N/A

N/A
Yes

Yes
Yes

No
Yes

Yes
Yes

Yes
Yes

Yes
Yes

Yes
Yes

No
N/A
analysts.
Yes
N/A
Analyst: CG
Date: 08/12/2016
Angelica Martinez

Date: 08/12/2016
Gale Denman
Page 13 of 13

Northwest ISD 2016 Lead Testing Lab Results

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Northwest ISD 2016 Lead Testing Lab Results

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Analytical Report 534731

9701 Harry Hines Blvd

Sample ID Cross Reference

Certificate of Analysis (Detailed Report)

Explanation of Qualifiers (Flags)

Sample Receipt Conformance Report

Sample Cross Reference 534731

Sample receipt non conformances and comments:

Sample receipt non conformances and comments per sample:

Certificate of Analytical Results 534731

Lab Sample Id: 534731-001

Date Received:08.10.16 09.05

Date Collected: 08.09.16 09.13

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P

Seq Number: 999735

Certificate of Analytical Results 534731

Lab Sample Id: 534731-002

Date Received:08.10.16 09.05

Date Collected: 08.09.16 09.26

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P

Seq Number: 999735

Certificate of Analytical Results 534731

Lab Sample Id: 534731-003

Date Received:08.10.16 09.05

Date Collected: 08.09.16 09.37

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P

Seq Number: 999735

Certificate of Analytical Results 534731

Lab Sample Id: 534731-004

Date Received:08.10.16 09.05

Date Collected: 08.09.16 09.56

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P

Seq Number: 999735

Certificate of Analytical Results 534731

Lab Sample Id: 534731-005

Date Received:08.10.16 09.05

Date Collected: 08.09.16 09.59

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P

Seq Number: 999735

Certificate of Analytical Results 534731

Lab Sample Id: 534731-006

Date Received:08.10.16 09.05

Date Collected: 08.09.16 10.04

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P

Seq Number: 999735

Certificate of Analytical Results 534731

Lab Sample Id: 534731-007

Date Received:08.10.16 09.05

Date Collected: 08.09.16 10.10

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P

Seq Number: 999735

Certificate of Analytical Results 534731

Lab Sample Id: 534731-008

Date Received:08.10.16 09.05

Date Collected: 08.09.16 10.50

Analytical Method: Metals per ICP by EPA 200.7

Prep Method: E200.7P