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Petrochemical
Engineering.
Asphalt Technology.
Second Stage.
Softening point
Prepared by : MUHAMMAD Akram
Place of the test: laboratory of duhok polytechnic University
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Definition
Softening point is the temperature at which a disk of the sample held
within a horizontal ring is forced download a distance of 1 in under the
weight of a steel ball as the sample is heated at a prescribed rate in a
water or glycerine bath.
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Apparatus:
Ring-a brass ring 5/8 dia.
Ball-A steel ball,9.53 mm (3/8) in diameter, weighting between
3.45 and 3.55 g
Ball centering guide-A guide for centering the ball
Batch. A glass vessel , capable of being heated, not less than
8.5cm in diameter and not less than 12cm in depth from the
bottom of the flare
Ring Holder. The rings shall be supported on the ring holder as
shown in the assembly figure below.
Ring shall be supported in a horizontal position with bottom of the
ring 1 in above the upper surface of the vessel bottom. The depth
of liquid in the bath should be not less than 4 in
Thermometers , An ASTM Low softening point having a range -2
to 80 0C
An ASTM high softening point having a range of 30 to 200 0C
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Liquid asphalt
Steel ball in
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center of mold
Ring a brass
Steel ball
Preparation of Sample:
than
expected
softening
point
for
asphalt.
Avoid
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thermometer and ball centering guides in position and fill the bath
with freshly boiled distilled water 51 0C TO a depth not less than 4
in and not more than 4.25 in in maintain the bath temperature at 5
0
shields if necessary.
reject all tests in which the rate of rise does not fall within these
limits
trail
Ball 1
Ball 2
48 C0
49 C0
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48.5 C0
Discussion:
Softening point / its a Soften of asphalt whishs determine sensitive
of asphalt with temperature till temperature increase the sensitive
asphalt will be decreased the asphalt is so good, but until the
temperature is lowed the sensitive asphalt will be increased.
Till the sensitive asphalt high it means that asphalt will be used in cold
place and until the sensitive low it means that asphalt will be used in
hot place.
However our machine was breaking down and we did not use it perfectly
so, our result was not a real softening point but
48.9 (C0)
was
good result .
Too many factor have effect to incorrect determine for instance
temperature of water need to gradually increase but we heated rapidly.
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but 1(C0)