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Materials System Specification

01-SAMSS-042
30 December 2013
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services
Document Responsibility: Non-Metallic Standards Committee

Saudi Aramco DeskTop Standards


Table of Contents
1

Scope............................................................. 2

Conflicts and Deviations................................. 2

References..................................................... 2

Responsibilities.............................................. 6

Materials......................................................... 6

Mechanical and Physical Properties............ 12

Fire Performance......................................... 16

Inspections and Acceptance........................ 17

Manufacturer Submittals.............................. 19

10

Packaging, Shipping and Handling.............. 19

11

Quality Program........................................... 20

12

Procurement.. 21

Appendix A Data Sheet..................................... 26


Appendix B Pipe Specification.......................... 27
Appendix C Manufacturer Submittals................ 28
Appendix D Visual Examination........................ 31
Appendix E Elastomeric Seals and Gasket ...... 33

Previous Issue: 27 February 2013

Next Planned Update: 30 December 2018


Page 1 of 37

Primary contact: Mehdi, Mauyed Sahib on +966-13-8809547


CopyrightSaudi Aramco 2013. All rights reserved.

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Scope
This document covers materials specification, manufacture, qualification and
procurement applies to Reinforced Thermoset Resin (RTR) pipe and fittings for use in
High pressure applications including; crude oil flowlines, jumpovers, trunklines, water
injection laterals and pipelines to API 15HR
Exception:
This specification does not apply to RTR pipe intended for use in utilities and fire water
applications as per 01-SAMSS-029 and 01-SAMSS-034.

Conflicts and Deviations


2.1

Any conflicts between this specification and other applicable Saudi Aramco
Materials System Specifications (SAMSSs), Engineering Standards (SAESs),
Standard Drawings (SASDs), or industry standards, codes, and forms shall be
resolved in writing by the Company or Buyer Representative through the
Manager, Consulting Services Department of Saudi Aramco, Dhahran.

2.2

Direct all requests to deviate from this specification in writing to the Company or
Buyer Representative, who shall follow internal company procedure SAEP-302
and forward such requests to the Manager, Consulting Services Department of
Saudi Aramco, Dhahran.

References
The following references in force on the date of the Purchase Order form a supplementary
part of this specification, as applicable:
3.1

Saudi Aramco References


Saudi Aramco Engineering Procedure
SAEP-302

Instructions for Obtaining a Waiver of a Mandatory


Saudi Aramco Engineering Requirement

Saudi Aramco Engineering Standards


SAES-L-610

Nonmetallic Piping in Oily Water Services

SAES-L-620

Design of Nonmetallic Piping in Hydrocarbon and


Water Injection Systems

SAES-L-650

Construction of Nonmetallic Piping in Hydrocarbon


and Water Injection Systems

Page 2 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Saudi Aramco Inspection and Testing Requirements


Form SA 175-012300
3.2

Inspection and Testing Requirements for High


Pressure Reinforced Thermoset Resin (RTR) Pipe

Industry Codes and Standards


American Petroleum Institute
API SPEC 5B

Specification for Threading, Gauging and Thread


Inspection of Casing, Tubing, and Line Pipe
Threads

API SPEC 15HR

Specification for High Pressure Fiberglass Line Pipe

American Society of Mechanical Engineers


ASME B16.5

Pipe Flanges and Flanged Fittings NPS through


NPS 24 Metric/Inch

American Standards for Testing and Materials


ASTM C581

Standard Practice for Determining Chemical


Resistance of Thermosetting Resins Used in
Glass-Fiber-Reinforced Structures Intended for
Liquid Service

ASTM C582

Standard Specification for Contact-Molded


Reinforced Thermosetting Plastic (RTP)
Laminates for Corrosion-Resistant Equipment

ASTM D543

Standard Test Method for Resistance of Plastics to


Chemical Reagents

ASTM D695

Test Method for Compressive Properties of Rigid


Plastics

ASTM D696

Standard Test Method for Coefficient of Linear


Thermal Expansion of Plastics Between -30C
and 30C with a Vitreous Silica Dilatometer

ASTM D790

Test Methods for Flexural Properties of


Unreinforced and Reinforced Plastics and
Electrical Insulating Materials

ASTM D792

Standard Test Methods for Density and Specific


Gravity (Relative Density) of Plastics by
Displacement

ASTM D1598

Standard Test Method for Time-to-Failure of Plastic


Pipe under Constant Internal Pressure
Page 3 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

ASTM D1599

Test Method for Resistance to Short-Time Hydraulic


Pressure of Plastic Pipe, Tubing, and Fittings

ASTM D2105

Test Method for Longitudinal Tensile Properties of


Fiberglass (Glass-Fiber- Reinforced
Thermosetting-Resin) Pipe and Tube

ASTM D638

Standard Test Method for Tensile Properties of


Plastics

ASTM D2143

Standard Test Method for Cyclic Pressure Strength


of Reinforced, Thermosetting Plastic Pipe

ASTM D2290

Standard Test Method for Apparent Hoop Tensile


Strength of Plastic or Reinforced Plastic Pipe by
Split Disk Method

ASTM D2412

Standard Test Method for Determination of External


Loading Characteristics of Plastic Pipe by
Parallel-Plate Loading

ASTM D2584

Standard Test Method for Ignition Loss of Cured


Reinforced Resins

ASTM D2925

Standard Test Method for Beam Deflection of


Fiberglass (Glass-Fiber-Reinforced
Thermosetting Resin) Pipe under Full Bore Flow

ASTM D2992

Practice for Obtaining Hydrostatic or Pressure


Design Basis for Fiberglass (Glass-FiberReinforced Thermosetting-Resin) Pipe and Fittings

ASTM D2996

Filament-Wound Fiberglass (Glass-FiberReinforced Thermosetting-Resin) Pipe

ASTM D3567

Standard Practice for Determining Dimensions of


Fiberglass (Glass-Fiber-Reinforced
Thermosetting Resin) Pipe and Fittings

ASTM D3681

Standard Test Method for Chemical Resistance of


Fiberglass (GlassFiberReinforced
Thermosetting-Resin) Pipe in a Deflected Condition

ASTM D4161

Standard Specification for Fiberglass (GlassFiber-Reinforced Thermosetting-Resin) Pipe


Joints Using Flexible Elastomeric Seals

ASTM E84

Standard Test Methods for Surface Burning


Characteristics of Building Materials

Page 4 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

International Standards Organization


ISO 175

Plastics - Methods of Test for the Determination of


the Effects of Immersion in Liquid Chemicals

ISO 9001

Quality Management Systems Requirements

ISO 14692-1

Petroleum and Natural Gas Industries - GlassReinforced Plastics (GRP) Piping - Part 1:
Vocabulary, Symbols, Applications and Materials

ISO 14692-2

Petroleum and Natural Gas Industries - GlassReinforced Plastics (GRP) Piping - Part 2:
Qualification and Manufacture

ISO 14692-3

Petroleum and Natural Gas Industries - GlassReinforced Plastics (GRP) Piping - Part 3:
System Design

National Association of Corrosion Engineers


NACE TM0298

Evaluating the Compatibility of RTR Pipe and


Tubulars with Oilfield Environments

International Marine Organization


IMO A653 (16)

Recommendation on Improved Fire Test Procedures


for Surface Flammability of Bulkhead, Ceiling
and Deck Finish Materials

American Bureau of Shipping


ABS 137

Guide for Certification of FRP Hydrocarbon


Production Piping Systems

Responsibilities
a)

Saudi Aramco shall develop the Purchase Datasheet Information, Appendix A.

b)

As part of the bid, and based on the Purchase Datasheet Information (Appendix A),
the manufacturer will develop the following information:

Pipe Specifications to cover each material, size and pressure class in the scope
of the bid. The contents of the Pipe Specification shall include, as a minimum,
the information listed in Appendix B.

Basis for the material selection, and material compatibility for pipe, fittings,
components, in accordance with Section 5 of this Specification.

Material certificates including the materials, dimensional, design, physical and


mechanical properties listed in Appendix C.
Page 5 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

c)

d)

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Based on the data submitted by the manufacturer, an experinced nonmetallic


Saudi Aramco engineer shall evaluate:

The completion of the submittal

The suitability of the submittal

Upon acceptance of the manufacturer submittals, the relevant Saudi Aramco


engineer shall use the manufacturer data to develop:

The system design in accordance with the Design Standard SAES-L-620.

The installation procedure in accordance with the Installation Standard


SAES-L-650.

Materials
5.1

5.2

API and ISO Compliance


a)

High pressure pipe and fittings (1,000 psi and higher pressure rating) shall
be fabricated and inspected in accordance with API SPEC 15HR.

b)

The RTR pipe shall be licensed/monogramed to API 15 HR and ISO 9001


certified.

Pipe and Fittings Materials


a)

RTR pipe and fittings shall consist of thermosetting resin reinforced with
glass fiber.

b)

Carbon or aramid fiber may be used to reinforce pipes, fittings or end


joints provided that all API 15HR and ISO 14692 are fulfilled.

c)

RTR Pipes and fittings shall be supplied with integral conductive carbon
fibers when electrical conductivity is needed.

5.2.1

Fiberglass
The glass fiber shall be of the highest quality commercial grade E or EC
glass.

5.2.2

Resin Systems
a)

A premium grade resin shall be used throughout.

b)

Acceptable resins shall be one of the following:

epoxy resin

polyester resin

vinylester resin
Page 6 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

c)

Catalysts and promoters shall be recommended by the resin


manufacturer.

d)

The resins used shall not contain fillers except as required for
viscosity control, fire or smoke retardants, and UV protection.

5.2.2.1

Glass-Reinforced Epoxy
i)

Epoxy is a thermosetting epoxide polymer that cures


(polymerizes and crosslinks) when mixed with a catalyzing
agent or hardener. Curing refers to the toughening or
hardening of a polymer material by cross-linking of
polymer chains, brought about by chemical additives.

ii)

The chemical resistance and temperature resistance of


epoxy resins depend on the choice of curing agent.
Common curing agents are: anhydride, aliphatic amine, or
aromatic amine.

5.2.2.1.1 Anhydride Cured Epoxy: Anhydride cured epoxy is


less susceptible to acid attack due to its acidic
nature.
5.2.2.1.2 Aliphatic and Cycloaliphatic Amine Cured Epoxy:
Aliphatic is a compound composed of carbon and
hydrogen which (unlike aromatic compounds) does
not contain aromatic rings. Cycloaliphatic amines
are comprised of a cyclic hydrocarbon structural
component and an amine functional group external
to that ring.
5.2.2.1.3 Aromatic Amine Cured Epoxy: Aromatic is a
compound composed of carbon and hydrogen which
contains benzene rings or similar rings of atoms.
Amine cured epoxy has excellent chemical resistance
to base environments due to its basic nature.
5.2.2.2

Glass-Reinforced Polyester
Polyester is a category of polymers which contain the ester
functional group (R-COO-R) in its main chain.

5.2.2.3

Glass-Reinforced Vinylester
a)

Vinylester is a low viscosity resin produced by the


esterification of an epoxy resin with an unsaturated
Page 7 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

monocarboxylic acid. It can be used as an alternative to


polyester and epoxy materials in matrix or composite
materials, where its characteristics and strength are
intermediate between polyester and epoxy.
b)
5.2.3

Vinyl ester resins are defined in ASTM C582.

Construction of Corrosion and Abrasion Resistant Liner


The corrosion liner shall refers to the inside portion of the pipe laminate
including resin rich layer; vinyl ester, reinforced with a corrosion veil(s)
and may include chopped strand fiberglass mat. The veil(s) may be
either a corrosion grade fiberglass (C-glass), or an organic veil such as
polyester fiber. An organic veil would be used in environments known
to attack glass, such as sodium hydroxide, hydrofluoric acid, and other
aggressive chemicals. The final thickness of the corrosion liner shall
depend on the aggressiveness of the transported fluid and therefore shall
be agreed upon with a specialized experinced Saudi Aramco engineer.

5.3

5.4

Manufacture
a)

High pressure pipe furnished to this specification shall be produced by


filament winding (FW).

c)

Fittings furnished to this specification shall be produced by compression


molding (CM), filament winding (FW) or resin transfer molding (RTM)
methods.

Material Compatibility
5.4.1

Pipe and Fittings Materials


a)

The manufacturer shall specify the pipe and fitting material


compatibility, given the range of operating parameters.

b)

The manufacturer shall document the basis for the pipe and fitting
material compatibility with the fluid, environment, and operating
conditions, for a minimum of 20 year design life.

c)

A laminate shall be provided which consists of an interior layer and


an exterior layer, to achieve optimum chemical resistance.

d)

The interior layer shall provide abrasion resistance, based on the


Purchase Data Sheet (Appendix A). The internal layer meant to
include resin rich layer, along with synthetic fiber such as
polyester, to combat erosion and corrosion.

Page 8 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

e)

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Material compatibility shall be established by the supplier by one


of the following methods:
Documented proof, with references, of successful field

experience, including fluid, environment, time and operating


conditions
NACE TM0298, Evaluating the Compatibility of RTR Pipe and

Tubulars with Oilfield Environments


ISO 175, Plastics - Methods of Test for the Determination of

the Effects of Immersion in Liquid Chemicals


ASTM C581 for chemical resistance in liquid service
ASTM D3681 for chemical resistance in a deflected condition

(strain corrosion)
ASTM D543 test method for resistance of plastics to chemical

reagents

5.4.2

5.4.3

f)

In all cases, the pipe shall be capable of withstanding the design


pressure (LTHS and short-term burst) at the design temperature,
the bending limit (curvature), and maintain its glass transition
temperature Tg, following the exposure test.

g)

RTR pipe is susceptible to degradation in certain chemicals and


environments, and therefore, RTR pipe manufacturers shall publish
Chemical Resistance tables, indicating the chemical and
temperature for which each pipe is resistant. Examples are
provided in Tables 2.4.1-1 to 2.4.1-4.

Elastomeric Seal Materials and Gaskets


a)

The manufacturer shall specify the seal and gasket material


compatibility in line with fluid composition and design conditions,
given the range of operating parameters. Examples of elastomeric
seals and gasket materials listed in Table E.

b)

The supplier shall document the basis for the seal and gasket
material compatibility with the fluid, environment, and operating
conditions, for a minimum of 20 year design life.

c)

Hardness test as per ASTM D2583.

Ultraviolet (UV) Protection


a)

UV protection is not required for RTR pipes intended for


underground applications.
Page 9 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

b)
5.4.4

5.5

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

UV protection is required for RTR pipes intended for aboveground


applications.

Fire Protection of Buried, aboveground and Offshore Piping


a)

Fire protection is not required for underground applications


provided that the velocity of the transported hydrocarbon is within
the acceptable limit.

b)

Fire protection may be required for RTR piping systems


transporting hydrocarbons in aboveground and offshore
applications. The minimum fire performance for such applications
shall meet the fire performance of IMO Level 2.

Pipe Joints
5.5.1

5.5.2

High Pressure
a)

High pressure pipe shall be threaded, with or without sealing


compound, and shall comply with the requirements of
API SPEC 15HR.

b)

If an elastomeric sealing compound is used, its material shall


comply with ASTM D4161.

c)

Thread dimensions shall comply with API 5B and API SPEC 15HR
Section 5.3.2 and 5.3.4.

d)

High pressure pipe joints are typically threaded (API 5B thread


dimensions) or threaded with an elastomeric seal (O-ring seal).
Some manufacturers add graphite to the threaded joints to improve
their strength and wear resistance.

e)

ASTM D4161 specifies materials and performance requirements


for elastomeric seals used with RTR pipe. The requirements
include materials of manufacture, joining and leak tightness
capability in straight, sheared and deflected pipe joint position.

Flanges
a)

Flange bolt circles, bolt holes and face dimensions shall be drilled
in accordance with ASME B16.5.

b)

The use of ASME B16.5 flanges for RTR pipe is standard practice.
RTR flanges will require washers and a steel or RTR backing ring,
as specified by the manufacturer. ASTM A193 Grade B7 bolts or
studs, and ASTM A194 Grade 2H nuts are commonly used.

Page 10 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Studs, nuts, washers, and bolts shall be coated using a couting a


coating system to be recommended bya coating engineer.
c)
5.6

5.7

5.8

Raised face steel flanges connection to flat face RTR shall require
corrosion resistant spacer ring.

Commercial Sizes
a)

The manufacturer shall determine the pipe size, based on the inner
diameter provided by the Owner and the thickness determined by the
manufacturer based on pressure rating.

b)

Pipes are typically supplied in lengths of approximately 10 meters (33 ft).


Each length of pipe is often called a joint. Examples of high pressure
pipe sizes are listed in Table 2.6-1.

c)

Pipe jointers (two pieces coupled to form one length) are not permitted.

Tolerances
a)

Tolerances shall be in accordance with API SPEC 15HR for high pressure
pipe and fittings. Tolerances for inside diameter, wall thickness and
minimum reinforced wall thickness are provided in API SPEC 15HR.

b)

Dimensional tolerances of supplied pipe, for total wall thickness and


reinforced wall thickness, shall be +22.5% and -0% in accordance with
API SPEC 15HR.

Cut Edges
All cut edges shall be coated with resin so that no glass fibers are exposed and
all voids are filled.

5.9

Markings
Markings shall be in accordance with API SPEC 15HR for high pressure RTR
pipes and fittings. API SPEC 15HR requires the manufacturer name, the symbol
15HR, the nominal size, a unique identification number, the pressure rating,
the date of manufacture. Additional marking shall include Saudi Aramco
purchase order number.

Mechanical and Physical Properties


a)

The mechanical and physical properties for RTR pipe and fittings must be
developed for materials representative of production.

b)

The manufacturer shall demonstrate that the mechanical and design properties
Page 11 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

developed on laboratory specimens apply to the supplied pipe and fittings.


This applicability shall establish, as a minimum, the following equivalency:

c)
6.1

Glass material

Winding angles and thickness

Resin composition

Curing agents

Density

Degree of Cure

Pigments

An example of mechanical and physical properties of RTR pipe is given in Tables


3-1 and 3-2.
Hydrostatic Design Stress SS (ASTM D1598, ASTM D2143, ASTM D2992)
a)

The manufacturer shall provide the hydrostatic design stress of the pipe
and joints, determined in accordance with API 15HR.

b)

The RTR pipe sizing equations in API SPEC 15HR (high pressure pipe)
are based on the Hydrostatic Design Stress (HDS) SS. ASTM D2992
establishes the procedure for obtaining the Hydrostatic Design Stress (HDS)
and, for complex-shaped fittings, the Hydrostatic Design Pressure (HDP),
which are used in design for sizing RTR pipe and fittings. For high pressure
pipe the ASTM D2992 procedure can be described in five steps:
Step 1 - A minimum of 18 specimens are exposed to a series of constant
internal pressures, at a controlled temperature, and the time to
failure is measured for each pressure. These failure tests are
conducted in accordance with ASTM D1598 with some
adjustments described in ASTM D2992. High pressure pipes can
be tested under static pressure or under cyclic pressure in
accordance with procedure ASTM D2143.
Step 2 - The failure pressures (or hoop stress) versus times to failure are
plotted on a log-log scale. The plot is extrapolated to obtain the
Long Term Hydrostatic Strength (LTHS) and the Long Term
Hydrostatic Pressure (LTHP), typically defined for failure
projected at 20-years of service. Since experimental failure plots
contain a statistical scatter, a 95% Lower Confidence Limit (LCL)
is used to obtain the LTHS and LTHP.
Step 3 - The LTHS and LTHP are converted to a Hydrostatic Design Basis
(HDB) for cylindrical pipes and fittings and the Pressure Design
Page 12 of 37

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01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Basis (PDB) for more complex-shaped fiberglass products.


This is done by combining the LTHS and LTHP, in accordance to
a procedure in ASTM D2992. For example, LTHS that fall
between 2400 psi (16500 kPa) to 3010 psi (20700 kPa) are
assigned an HDB of 2500 psi (17200 kPa). For low pressure pipes
tested by cyclic pressure the HDB is labeled HDBC.
Step 4 - Finally, the HDB and PDB are multiplied by a service design
factor (a design margin) to obtain the Hydrostatic Design Stress
(HDS) and Hydrostatic Design Pressure (HDP) respectively.
The design factor is specified in API SPEC 15HR as Sf = 0.67.
For low pressure pipe rated based on cyclic pressure tests the
design factor is Sf = 1.0.
Step 5 - The manufacturer documents the tests used to develop LTHS and
LTHP, the regressions used to develop HDB and PDB, and the
margins used to establish HDS and HDP in a report required by
ASTM D2992.
6.2

6.3

Pressure Rating (API SPEC 15HR, ASTM D2992)


a)

The pressure rating of high pressure RTR pipe shall be established by the
manufacturer in accordance with API SPEC 15HR, Equation (1) or
Equation (2) corrected to include the Service Factor Sf = 0.67.

b)

The manufacturer shall provide the 95% Lower Confidence Limit (LCL)
of the Long-Term Hydrostatic Strength (LTHS) at 20 years, developed in
accordance with ASTM D2992 Procedure B at the specified design
temperature or higher.

c)

The pressure rating of high pressure RTR fittings and components shall be
established by the manufacturer in accordance with API SPEC 15HR,
Section 5.1.2.

d)

The manufacturer shall correct the pressure rating of the piping and fittings
to account for the chemical degradation caused by the fluid for the 20 year
design life. The correction factor for temperature and fluid environment
shall be conducted in accordance with API 15HR Annex G.

Short-Term Burst Pressure (API SPEC 15HR, andASTM D1599)


a)

Fittings and components shall be tested for short-term burst strength in


accordance with API SPEC 15HR Section 5.1.4. The short-term burst
pressure shall exceed the specified short-term burst pressure.

b)

Test procedure ASTM D1599 is established to determine the resistance of


RTR pipe and fittings to short-term over-pressure, at various temperatures.
Page 13 of 37

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Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

The pipe specimens are conditioned at the required temperature, and then
the pressure is steadily raised until failure occurs between 60 to
70 seconds. This test provides useful information if the system will be
subjected to pressure transients (such as water hammer) which exceeds the
rated pressure of the pipe or fitting. It is recommended in the design
standard that a sufficiently thick pipe be selected so that, even in case of
pressure transient, the rated pressure is not exceeded. The maximum
allowed surge pressure is 1.5 design pressure of the pipe.
6.4

6.5

6.6

Longitudinal and Hoop Tensile Properties (ASTM D2105 or ASTM D638,


ASTM D2290)
a)

The manufacturer shall provide at the initial approval process or thereafter


the results for longitudinal tensile and hoop stress tests in accordance with
ASTM D2105 or ASTM D 638 and ASTM D2290 respectively.

b)

The design of RTR piping systems requires determination of the stress-strain


properties of the material, in particular the modulus of elasticity and yield
stress. The longitudinal properties are obtained by tensile tests in
accordance with ASTM D2105. Alternatively, tensile tests with dumbbell
shape specimens from RTR piping can also be performed per ASTM D638.
The hoop properties are obtained in accordance with ASTM D2290.

Parallel Plate Loading (ASTM D2412)


a)

The manufacturer shall provide, at the initial approval process or


thereafter, the pipe ring stiffness test results using the ring deflection
method per ASTM D2412. Ovality shall be measured on a continuous
basis per manufacturers recommended method.

b)

The design of buried RTR pipe requires the determination of the pipe
stiffness (PS), as well as the ovality limit of the pipe. The stiffness shall be
calculated in accordance with D2412 for each pipe. The ovality shall be
measured by the difference in the largest and smallest cross-sectional axes.

External Pressure Resistance (ISO 14692-3)


a)

The manufacturer shall provide calculation for external pressure resistance


of each pipe to ensure that the pipe and fittings have sufficient stiffness to
resist vacuum or external pressure loads in accordance with Section 8.3 of
ISO 14692-3.

b)

The design of RTR pipe may require the pipe to resist external
pressure/vacuum for example when the pipe operates at sub-atmospheric
pressure, or when the pipe is under the water table or vacuum created by
the operation of an upstream valve. The external pressure resistance of
Page 14 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

RTR pipe shall be calculated per ISO-14692-3 to avoid buckling,


compression or leakage.
6.7

6.8

Glass Transition Temperature Tg of RTR Pipe and Fittings


a)

The resin of pipe and fittings shall have a glass transition temperature Tg
greater than or equal to the larger of (a) 95C and (b) the design
temperature plus 30C.

b)

The glass transition temperature Tg shall be established through


differential scanning calorimeter, in accordance with Appendix C of
API SPEC 15HR, at a minimum frequency of once per shift for each resin
system used at each manufacturers facility.

Glass Transition of Adhesives


Where pipes are joined with adhesives, the glass transition temperature of the
cured adhesive shall not be less than 95% of the minimum value quoted by the
manufacturer for the adhesive or resin system.

Fire Performance
Fire endurance requirements for pipes based on system and location are specified in
Section 2, Table 3 of ABS Guide for Certification of FRP Hydrocarbon Production
Piping Systems. However, fire is not a concern for buried crude oil and water injection
application. The fire endurance rating code IMO L1, L2, L3, or L3-WD is to be
assigned to RTR piping components upon the satisfaction of the fire endurance testing
described below.
7.1

Level 1
Piping under dry conditions endures a hydrocarbon fire for a minimum duration
of one hour without loss of integrity is considered to meet IMO Level 1 fire
endurance standard (L1).

7.2

Level 2
Piping under dry conditions endures a hydrocarbon fire for a shorter, but still
appreciable period without loss of integrity is considered to meet IMO Level 2 fire
endurance standard (L2). The duration selected for the L2 test is 30 minutes.

7.3

Level 3
Water filled piping endures a local fire for a minimum duration of 30 minutes
without losing its ability to function satisfactorily after the fire has been
extinguished is considered to meet IMO Level 3 fire endurance standard (L3).
Page 15 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

7.4

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Level 3 Modified Test


Piping having passed the fire endurance test for a minimum duration of
5 minutes in dry condition and 25 minutes in wet condition without loss of
integrity is considered to meet the Wet/Dry fire endurance standard (L3-WD).

7.5

Fire Endurance Coating


A fire protective coating for pipes and fittings shall demonstrate that the coating
is resistant to products which likely to come in contact with the piping. The fire
protection coating characteristics such as thermal expansion, resistance against
vibrations and elasticity are to be taken into account. The fire protection
coatings are to have sufficient resistance to impact to retain their integrity.

7.6

Flame Spread
All pipes except for those fitted on open decks and within tanks, cofferdams,
void spaces; pipe tunnels and ducts are to have low flame spread characteristics.
The test procedures in IMO Resolution A.653 (16), modified for pipes as
described in Section 9, are to be used for determining the flame spread
characteristics. Piping materials giving average values for all of the surface
flammability criteria not exceeding the values listed in IMO Resolution A.653
(16) (surface flammability criteria of bulkhead, wall and ceiling linings) are
considered to meet the requirements for low flame spread. All pipes shall be
certified fire resistant by testing to ASTM E84 with a flame spread rating not to
exceed 20 or by meeting the requirements in IMO Resolution A653 (16).

Inspections and Acceptance


8.1

Manufacturer
8.1.1

Inspection Standard
High pressure pipe and fittings shall be inspected and tested in
accordance with API SPEC 15HR.

8.1.2

Dimensions
The following dimensions shall be determined in accordance with
ASTM D3567:

Internal diameter

Outside diameter

Minimum wall thickness

Page 16 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

8.1.3

Reinforced wall thickness

Laying length

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Glass Content
Glass content shall be inspected in accordance with ASTM D2584,
as a minimum once per lot, but not less often than once per shift.
Glass content shall be in accordance with the manufacturer specification,
but shall not less than 70% for filament wound pipe and 65 % for
filament wound fittings.

8.1.4

Hydrotest
The manufacturer shall hydrotest each high pressure RTR pipe, fitting
and component, at 1.5 times the rated pressure at ambient temperature,
for a minimum of 2 minutes. For every 50th joint the pressure shall be
maintained for a minimum of 10 minutes.

8.1.5

Degree of Cure
The degree of cure shall be determined by DSC according to Section 6.7
of this Specification:

For pipes: at a minimum once per shift for each resin system.

For fittings: at a minimum one fitting per 10 units fabricated.

The Tg shall be not more than 5C below the minimum Tg or the pipe or
fitting.
8.1.6

Short-Term Hydrostatic Failure Test


The short-term hydrostatic failure pressure (ASTM D1599) shall be
conducted once per lot of 5,000 ft of pipe, and once per lot of 50 fitting
or components units. The failure pressure shall be greater than 85% of
the published value.

8.1.7

Visual Inspection
All pipes, fittings and components shall be visually inspected to the
visual standards of Appendix D. Also, test for delamination and voids
by visually inspecting cross section of pipe and fittings.

8.1.8

Retest
If a component fails any of the required tests, the manufacturer shall
retest 2 components of the same lot. If one or both components fail, the
Page 17 of 37

Document Responsibility: Non-Metallic Standards Committee


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Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

whole lot shall be inspected for the failed parameter; each deficient
product of the lot shall be identified and discarded.
8.2

Inspection by Saudi Aramco


a)

The manufacturer shall maintain all materials and fabrication records for a
minimum of 5 years from the date of shipment to Saudi Aramco, and make
the records available to Saudi Aramco upon request, with one week notice.

b)

Saudi Aramco reserves the right to issue inspection notice for plant access,
sub-contractors and suppliers access, compliance, rejection.

Manufacturer Submittals
9.1

Pipe and Fitting Data


The manufacturer shall submit the pipe and fitting specifications (Appendix B),
and the manufacturer Input Sheet (Appendix C) to permit the Owner to verify
the quality of materials, pipes, fittings and components, to design the system, to
inspect and repair the system where necessary.

9.2

10

Field Handling and Installation Instructions


a)

In addition, the manufacturer shall submit the field handling, storage, and
installation requirements for aboveground and buried applications.

b)

The manufacturer shall submit field joining procedures, including required


experience and training of installation personnel.

c)

The manufacturer shall submit field hydrotest limitations.

Packaging, Shipping and Handling


a)

Packing, shipping and handling shall be in accordance to 02-SAMSS-049.

b)

The pipe and fitting ends shall be sealed to prevent damage, and penetration of
dirt, water, humidity or contaminants.

b)

Packing materials will be timber, bubble paper and corrugated paper for fittings
only.

c)

Flange faces shall be protected.

d)

Yard storage shall be in accordance with the manufacturer requirements.

d)

The pipes shall be set on a flat surface, free of sharp edges.

e)

Support pipe on a minimum of four equally spaced racks.

Page 18 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

11

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

f)

Maintain end protectors throughout storage.

g)

If they are to be bundled, pipes and fittings shall be secured by straps; chains are
not permitted.

h)

Precautions shall be in place to tie-down pipes and fittings to prevent overturning


or fall subject to high winds.

i)

Gaskets and adhesive systems and lubricants shall be stored in their original
packing in accordance with the manufacturer recommendations.

j)

The stored adhesive systems or lubricants shall be discarded if they have an


expired shelf life.

k)

Pipes shall be visually inspected for damage before shipment.

Quality Program
a)

The manufacturer quality program shall be in accordance with ISO 9001 and
API SPEC 15HR for high pressure pipe.

d)

The manufacturer shall maintain written procedures for:

Receipt acceptance of raw materials

Storage of raw materials

Mixing procedures

Cure procedures

Fabrication practices

Personnel training and qualification

Inspection and testing procedures

e)

The manufacturer shall have an independent Quality Control inspection function.

f)

All equipment and instruments used in Quality Control shall be identified,


controlled and calibrated at least every 6 months.

g)

Pressure gages shall be accurate within 2% of full scale range.

h)

All pipes, fittings and components shall be traceable, through their markings, to
the manufacturing plant, the lot and its raw material.

i)

The Buyer shall have the right to audit the facilities of the manufacturer, the
Supplier and all their suppliers or sub-contractors upon provision of a two-week
notice of such an audit.

j)

Buyer audit may include but shall not be limited to:


Page 19 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

12

Certification records

Manufacturing records

Manufacturing and storage facilities

Engineering calculations and reports

Testing and Analytical Lab Capabilities

Outsourcing interfaces

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Procurement
12.1

Materials
(Specify the material if it is a re-order, or specify as follows:)

12.2

12.1.1

The Supplier shall select the appropriate pipe and fitting in compliance
with the Design Input Sheet, Appendix A.

12.1.2

The pipe material shall be compatible with the fluid, environment


specified in Appendix A, for a 20-year design life.

12.1.3

The manufacturer shall submit the basis for RTR material selection,
and proof of compatibility with the fluid and environment specified.

12.1.4

Pipe shall be filament wound.

12.1.5

Fittings may be filament wound.

Material Certificates
12.2.1

The Supplier shall submit the material certificates for the fiberglass,
traceable to pipe and fittings.

12.2.2

The Supplier shall submit the material certificates for the resin systems
and curing agents, traceable to pipe and fittings.

12.2.3

The Supplier shall submit the material certificates for graphite fiber
(if used), traceable to pipe and fittings.

12.2.4

Each pipe shall contain a legible, embedded label indicating, as a


minimum:

Manufacturer name

Product code

Traceability to production facility, date, lot


Page 20 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

12.3

12.4

Nominal size

Pressure class

PO Number

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

API Compliance
12.3.1

High Pressure Pipe shall be manufactured by an API SPEC 15HR


certified manufacturer.

12.3.2

Pipes shall be API monogrammed.

12.3.3

Reference standards for physical and mechanical properties shall be in


accordance with Appendix B.

Shipping
Shipping shall be by means of seaworthy crates in cube containers.

12.5

Transport
Transport to the field shall be in original crates or in dedicated (Fiberglass Only)
flat bed trailers, tied-down with straps (not chains).

12.6

Receipt Inspection and Storage


Each delivery shall be inspected by the Buyer. Inspection will include, but not
be limited to:
12.6.1

The trailer load or container load shall be checked for load shifting
which may have occurred during transportation.

12.6.2

The ends shall be checked for missing or broken end protectors.

12.6.3

The quantities of pipes and fittings shall be checked.

12.6.4

Pipe and fittings shall be inspected for conformance to the Purchase


Order.

12.6.5

Joining kits (adhesive bonds, lubricants, etc.) shall be inspected for


conformance to the manufacturer installation manual and the
Engineering Design, and for evidence of damage or tempering.

12.6.7

As a minimum, the label shall confirm the pipe manufacturer, size,


material, and pressure rating.

12.6.8

The product code for each pipe and fitting shall be verified to be
Page 21 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

traceable to the material certificate prior to installation.


12.6.10 Pipes and fittings shall be inspected for evidence of damage or
distortion.
12.6.11 Pipes and fittings which do not pass receipt inspection, shall be marked
and quarantined pending disposition.
12.6.12 Pipe edges shall be coated with resin and inspected to be smooth, not
prone to cutting skin on contact.
12.6.13 Threads type and size shall be inspected to be in accordance with
API 15HR.
12.7

12.8

12.9

Field Support
12.7.1

The Supplier shall provide Installer training and Saudi Aramco


approved certification program.

12.7.2

The Supplier field service representative shall be on site for the


purpose of supervising the installation crew and inspecting of delivered
product.

12.7.3

The Supplier shall specify the crew size needed for handling and
installation of pipe and fittings.

12.7.4

The supplier shall provide technical expertise and onsite assistance,


necessary, to troubleshoot joining or installation problems encountered
should they arise.

Ends Protection
12.8.1

Pipe and fittings shall be sealed and protected with plastic end caps.

12.8.2

The Supplier shall provide suitable cleaning tools.

Adhesives, Lubricants and Sealants


12.9.1

The supplier shall provide a sufficient quantity of adhesives, lubricants


and sealants required to join the quantity of pipe and fittings supplied.

12.9.2

High pressure pipe and fittings: The Supplier shall furnish thread
lubricants and sealants compatible with the fluid, temperature and
pressure specified in Appendix A.

Page 22 of 37

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Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

12.10 Flange Kits


The Supplier shall provide a number of flange kits, as specified in the order.
The flange kit shall include all parts necessary for field joining, including:

Two flange halves compatible with the pipe

Gaskets compatible with the parameters specified in the Design Input Sheet
(Appendix A)

Studs and nuts

Steel or RTR backing rings (if required)

Bolt sequence and torque

Spacer ring

12.11 Make-Up Tools


The Supplier shall provide joint make-up tools for the materials and dimensions
supplied, including strap wrenches and metal friction wrenches and bearing pads
as necessary.
12.12 Field Hydrotest
12.12.1 Hydrotest shall be in accordance to SAES-L-650.
12.12.2 The Supplier shall specify the recommended hydrotest water chemistry.
12.13 Records
The Supplier shall maintain at the manufacturer facility or other facility to be
approved by the Buyer the material records and certificates for all materials
purchased, including compliance to the applicable Standards listed in Appendix B.
12.14 Submittals
12.14.1 The Supplier shall submit a Pressure Rating Report prepared and signed
by the manufacturer to document the basis for the pressure rating,
including pressure transients, in accordance with API SPEC 15HR.
12.14.2 The Supplier shall submit the completed Manufacturer Input Sheet
(Appendix C).
12.14.3 The Supplier shall submit material certificates, traceable to each pipe
or fitting label.

Page 23 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

12.15 Warranty
(Company-specific. Note: RTR pipe and fittings are typically supplied with a one-year
warranty starting 12 months after commissioning date.)

13

Acronyms
RTR

Reinforced Thermoset Resin

GRE

Glass Reinforced Epoxy

GRP

Glass Reinforced Polyester

GRV

Glass Reinforced Vinylester

FRP

Fiber Reinforced Plastic

MAOP

Maximum Allowed Operating Pressure

LTHS

Long Term Hydrostatic Strength

Tg

Glass transition temperature

30 December 2013

Revision Summary
Major revision to be in line with API 15 HR and ISO 14692.

Page 24 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Appendix A Data Sheet


The end user (or representative) should fill out the form below.

Table A Purchase Data Sheet Information


1.

Saudi Aramco Organization/End User


End User

Representative

1.1

Responsible Engineer

1.2

Organization Code

1.3

e-mail

1.4

Telephone No.

2.

Project

2.1

Project Name

2.2

Location

2.3

Type of System (Flowline, piping, etc.)

2.4

Special Operations

3.

Basic Design Data

3.1

Pipe Nominal Diameter, mm (inch)

3.2

Pipe Nominal Internal Diameter, mm (inch)

3.3

Pipe length, meters (ft)

3.4

Design Life, years

3.5

Operational Temperature, C ( F)

Min:

Max:

3.6

Design Temperature, C ( F)

Min:

Max:

3.7

Ambient Temperature, C ( F)

Min:

Max:

3.8

Operational Pressure, psi

Min:

Max:

3.9

Design Pressure, psi

Min:

Max:

MAOP, psi

Min:

Max:

3.10

Expected Cycle Working Pressures, psi

Min:

Max

3.11

Field Hydrostatic Pressure, psi

Min:

Max:

3.12

External Pressure, psi

Min:

Max:

3.13

Load Soil , psi

Min:

Max:

3.14

Road Crossing Requirements

3.15
3.16

Fluid Velocity, m/s (ft/s)


Flow Rate (BPD oil/condensate; BPD water;
MCF/D gas)
Fluid particles Content and Size

Min:

Max:

Min:

Max:

3.17

Page 25 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Table A Purchase Data Sheet Information (contd)


4.

Fluid Service

4.1

Type (gas, water, oil, multiphase)

4.2

Fluid Composition

4.3

If applicable, Oil/Water/Gas Ratio

4.4

CO2 Content

4.5

H2S Content

4.6
4.7
4.8

Other Chemicals (Inhibitor/type, etc.)


Water cut
Fluid Maintenance Requirement
(Acid Cleaning, Hot oil, etc.)
Special Pipe Requirement

5.
5.1

Type of Resin

5.2

Type of Joint System

5.3

Fire Resistance Performance

5.4

Conductivity

5.5

API Monogram requirement

5.6

Abrasion resistance layer

5.7

Sand or suspended solids

6.

Installation Details

6.1

Description of Installation (above/below ground)

6.2

Ground Conditions (Sandy, Rocky, etc.)

6.3

External environment (Temp, sun, etc.)

6.4

Installation Procedure

6.5

External interference hazards

6.6

Routing and spatial

6.7
6.8
6.9

Future Tie-in requirements


End fitting interface requirements
(FF, RF, RJ Flange, other)
Delivery date required

7.

Operational Requirements

7.1

Inspection Requirements Internal/External

7.2

Pigging Requirements

7.3

Reparability Requirements

7.4

Impact resistance requirements

7.5

External wear requirements

Please, attached fluid chemical analysis

Page 26 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Appendix B Pipe Specification


Example of a Pipe Specification Submitted by the Manufacturer
(For Illustration Only)

Table B Example of a Pipe Specification


Size

Pipe

Flange

Fittings

NPS

1.5

2.5
3
4
Spec 1000
-20 to 100F at 1000 psi
Crude Oil Service

10

Mfr. Pr
Class

1500

1000 minimum

Threads

10 rd

5B EUE 8rd

Materials

Glass fiber epoxy composite (Ali. Amine, Aro. Amine, Anh.)

Fabrication

Filament wound pipe only, ASTM D2996, API SPEC 15HR

Pr. Class

Class 600 flat face

Ends

10 rd

Material

Ali. Amine cured Epoxy resin, Glass fiber, Composite (specify)

Fabrication

Filament wound flange only

Pr. Class

1500

1000 minimum, Exceeds pipe

Threads

10 rd

5B EUE 8rd

Material

Ali. Amine cured Epoxy resin, Glass fiber, Composite (specify)

Fabrication

Filament wound fitting only

5B EUE 8 rd

12

5B OD 8rd

5B OD 8rd

5B OD 8rd

Bolting

ASTM A193 Grade B7 bolts, ASTM A194 Grade 2H hex nuts

Gaskets

Spiral wound Teflon-304 stainless steel

Applicable
standards

ISO 14692

Page 27 of 37

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Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Appendix C Manufacturer Submittals


Table C Manufacturer Input Sheet
Product Description
Manufacturer

Notes

Product name
Product code
Pipe designation code (ASTM D2996)
Size
Maximum pressure and maximum temperature
Joining method
Body reinforcement type and supplier
Ends reinforcement type and supplier
Resin
Curing agents
UV protection type and depth (if any)
Repair nipples threaded
Repair nipple flange
API SPEC 15HR Standard and Certifications
Certification (API, ISO)
API SPEC 15HR
20 years

Design life
Fluid Compatibility
Chemical resistance list with technical basis
Application
Sour service limit

Page 28 of 37

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Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Size and Dimensions


Inside diameter (nominal)
Volume capacity (gallons/liters)
Reinforced wall thickness and tolerance
Total wall thickness and tolerance
Outside diameter (nominal)
Length
Size (saddles only)
Connection outside diameter
Thread type, length
Ends insertion depth
Physical Properties
Total weight per joint
Linear weight
Density
Specific gravity (ASTM D792)
Coefficient of thermal conductivity
Coefficient of thermal expansion (ASTM D696)
Tensile modulus of elasticity axial (ambient temperature) (ASTM D2105)
Tensile modulus of elasticity axial (maximum temperature) (ASTM D2105)
Tensile modulus of elasticity hoop (ambient temperature) (ASTM D2105)
Tensile modulus of elasticity hoop (maximum temperature) (ASTM D2105)
Compression modulus of elasticity (ambient temperature) (ASTM D695)
Compression modulus of elasticity (maximum temperature) (ASTM D695)
Beam bending modulus of elasticity (ambient temperature) (ASTM D2925)
Beam bending modulus of elasticity (maximum temperature) (ASTM D2925)

Ring flexural modulus of elasticity (ambient temperature) (ASTM D790)


Ring flexural modulus of elasticity (maximum temperature) (ASTM D790)
Poisson ratio (API SPEC 15HR Appendix F)
Abrasion resistance

Page 29 of 37

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Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Mechanical Design Properties


Pressure rating
Ultimate pressure (ASTM D1599)
Factory hydrotest pressure
Factory hydrotest (100% if each piece is tested)
SS 95% LCL of LTHS (ASTM D2992 Procedure B) (room temperature)
SS 95% LCL of LTHS (ASTM D2992 Procedure B) (maximum temperature)

Ultimate tensile stress (ASTM D2105)


Design tensile stress (ASTM D2105)
Short-term tensile rated force
Axial compression ultimate stress (ASTM D695)
Axial compression design stress (ASTM D695)
Maximum permitted ovalization limit
Permitted bend radius if bent
Flexibility factor of fitting in-plane (ISO 14692-3)
Flexibility factor of fitting out-of-plane (ISO 14692-3)
Stress intensification factor in-plane (ISO 14692-3)
Stress intensification factor out-of-plane (ISO 14692-3)
Design allowable stress envelope (ISO 14692-3)
Beam bending design stress with applied design margin
Ultimate collapse external pressure (ASTM D2924)
Recommended support spacing
Recommended thrust blocks
Design Guide
Hydraulic Design Factors
Hazen-Williams coefficient
Manning coefficient (in or mm)
Surface roughness (in or mm)
Hydrostatic Test
Maximum pressure for field hydrotest

Page 30 of 37

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Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Appendix D Visual Examination


Table D - Visual Examination and Acceptance Criteria
Defect

Description

Criterion

Disposition

Note: The following acceptance criteria apply to the pipe body and fitting body, away from threads or
sealing surfaces. No defects are permitted on threads or sealing surfaces.
Distortion or
Burn
discoloration of the RTR None permitted.
Reject
product surface.
If there are undamaged,
fibers exposed over any
area; or no fibers are
Minor repair
exposed but an area
Small piece broken from
greater than 10 mm x
edge or surface. If
10 mm lacks resin.
Chip
reinforcement fibers are
If there are no fibers
broken, the damage is
exposed, and the area
considered a crack.
Accept
lacking resin is less than
10 mm x 10 mm
If more severe than the
Reject
above
Sharp cut that reaches
Crack
None permitted.
Reject
the reinforcing fibers.
Crack lengths greater
Minor repair
Fine hairline cracks at or
than 25.0 mm.
Crazing
under the surface of the
Crack lengths less than
component.
Accept
25.0 mm.
Area of incomplete
surface film where the
Dry spot
None permitted.
Reject
reinforcement has not
been wetted by resin.
Rupture of the
component with
complete penetration of
Fracture
the laminate. Majority of None permitted.
Reject
fibers broken. Visible as
lighter colored area of
inter-laminar separation.
Discoloration and
possible bubble
reaching the
Impact mark
None permitted
Reject
reinforcement. Impact a
spare sample with a
hammer for reference.
Foreign matter molded
Inclusion
None permitted.
Reject
into the component.

Page 31 of 37

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Next Planned Update: 30 December 2018
Defect

Description

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services
Criterion

Pin hole

Small round pit or


porosity

Superficial, does not


penetrate the
reinforcement, less than
1 mm depth, and less
2
than 1 per m .

UV induced fiber
blooming

Discoloration and
increased roughness of
the pipe surface

None permitted on UVprotected pipe.

Void

Wear scratch

Air bubble

Shallow mark caused by


improper handling,
storage and/or
transportation. If
reinforcement fibers are
broken, the damage is
considered a crack.

Superficial and less than


2 mm diameter and
0.5 mm deep, and less
2
than 4 voids per m
If more severe than the
above.
If there are undamaged,
fibers exposed over any
area; or no fibers are
exposed but an area
greater than 10 mm x
10 mm lacks resin.
If there are no fibers
exposed, and the area
lacking resin is less than
10 mm x 10 mm
If more severe than the
above.

Disposition

Accept

Reject

Accept

Reject

Minor repair

Accept

Reject

Page 32 of 37

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Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Appendix E Elastomeric Seals and Gasket Materials


Table E - Common Elastomeric Seals and Gasket Materials
Material

Description

Buna-N: Nitrile
(NBR)

Commonly used for RTR pipe O-rings.


NBR has good balance of such desirable
working properties as low compression
set, high tensile strength, and high
abrasion resistance.

HNBR

Neoprene

Hydrogenated nitriles have a better


resistance to sour service compared to
NBR.
Commonly used for RTR pipe flange
gasket below 225 psi rated pressure
(Class 150 flange), in the range of 1/8 in
(3 mm) thick. An early developed, oilresistant substitute for Natural Rubber
sunlight and oxygen aging; relatively low
compression set; good resilience and
reasonable cost.

EthylenePropylene
(EPM/EPDM):

Polyurethane:

Viton:

Fluorosilicone

Fluorocarbons
(FS)

Outstanding extrusion and abrasion


resistance, tensile strength, and low
friction qualities.

Combining high temperature toughness


with wide chemical agent compatibility,
with good high temperature compression
set characteristics.
Combining the good high and low
temperature stability of Silicones with the
fuel, oil, and solvent resistance of
fluorocarbons. FS compounds feature
good compression set and resilience
properties. FS compounds are suitable
for exposure to air, sunlight, ozone,
chlorinated and aromatic hydrocarbons.
Organofluorine compounds that contain
only carbon and fluorine. They are
considered resistant to sour gas, if they
are properly formulated.

Applications
Nitrile combines excellent
resistance to petroleum-based oils
and fuels, silicone greases,
hydraulic fluids, water and alcohols
However; they have a limited
resistance to sour service.

Hardness
(ASTM (D2240)

Shore A 40 90

Shore A 40 90

Neoprene features moderate


resistance to petroleum oils; good
resistance to ozone, Freon and
Ammonia.

Featuring good resistance to such


polar solvents as ketones (MEK &
Acetone). EPM/EPDM is also
highly recommended for effective
resistance to steam (to 400F), hot
water, silicone oils and greases,
dilute acids and alkalies, alcohols
and automotive brake fluids.
Cast Polyurethane compounds
feature excellent resistance to
mineral-based oils and petroleum
products, aliphatic solvents,
alcohols and certain polyurethane
elastomers have good resistance to
sour gas service.
Fluorocarbon compounds feature
excellent resistance to petroleum
products and solvents,

Shore A 60 70

Shore A 40 90

Shore A 70 90

Shore A 70 90

Shore A 50 - 80

Shore A 50 - 80

Page 33 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Table 2.4.1-1 General Chemical Resistance


(Actual chemical resistance to be obtained from the manufacturer)
Fluid

Epoxy

Polyester or Vinylester

Inorganic
Dilute acids

Concentrated acids

NR

Oxidizing acids

NR

Alkalis

Acid gases

NR

Ammonia gases

Halogen gases

NR

Salts

Oxidizing salts
Organic

NR

Acids

Anhydride acids

NR

NR

Alcohols

Esters/Ethers

Hydrocarbons aliphatic

Hydrocarbons aromatic

Hydrocarbons halogenated

Natural gas

Synthetic gas

Oils

R = recommended, L = limited usage, NR = not recommended

Table 2.4.1-2 Example of Chemical Resistance of Epoxy-Based RTR Pipe to Hydrocarbons


(Actual chemical resistance to be obtained from manufacturer)
Anhydride
o

Aliphatic Amine
C

Aromatic Amine
o

Crude oil, sweet

150

65

200

93

210

99

Crude oil, sour

150

65

200

93

210

99

Diesel fuel

150

65

200

93

210

99

Fuel oil

150

65

200

93

210

99

Gasoline

150

65

200

93

210

99

Jet fuels

150

65

200

93

150

66

Kerosene

150

65

200

93

210

99

Naphta

100

38

200

93

210

99

Page 34 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Table 2.4.1-3 Example of Chemical Resistance of Epoxy-Based RTR Pipe to Gases


(Actual chemical resistance to be obtained from manufacturer)
Aliphatic
Amine

Anhydride
o

Aromatic
Amine
o

Air, wet and dry

150

65

200

93

210

99

Carbon dioxide, dry, < 800 psi

150

65

175

80

175

80

Carbon dioxide, dry, > 800 psi

NR

NR

150

65

150

65

Carbon dioxide, wet, < 800 psi

150

65

175

80

175

80

Carbon dioxide, wet, > 800 psi

NR

NR

150

65

150

65

Hydrogen sulfide, dry

150

65

175

80

175

80

Methane, natural gas

125

50

150

65

150

65

Sour gas (with < 5% H2S), wet, < 500 psi

100

38

200

93

210

99

Sour gas (with > 5% H2S), wet, < 500 psi

NR

NR

NR

NR

NR

NR

Table 2.4.1-4 Example of Chemical Resistance of Epoxy-Based RTR Pipe to Waters


(Actual chemical resistance to be obtained from manufacturer)
Anhydride

Aliphatic Amine

Aromatic
Amine

Water with brine, salt, KCl, Hard

150

65

200

93

210

99

Water, chlorinated (to 100 ppm)

100

38

150

65

150

66

Water, demineralized, distilled

100

38

200

93

200

93

Water, produced, sweet (CO2)

150

65

200

93

210

99

Water, produced, sour (H2S)

150

65

200

93

210

99

Water, sea

150

65

200

93

210

99

Page 35 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Table 2.6-1 Example of Pipe Size and Pressure Rating for High Pressure Line Pipe
(For actual sizes and pressure rating consult the pipe manufacturer)
Rating at 150F
o
(65.6 C)
(psi)
500
1000
1500
2000
2500
3000

Nominal
Size

Outer
Diameter
in (mm)

Wall
Thickness
in (mm)

Failure
Pressure
Psi (MPa)

3 min

Max. Support
Span
ft (m)

3.14 (79,8)

0.07 (1,8)

1500 (10,3)

10 (3,1)

8 max

7.75 (196,9)

0.13 (3,2)

1100 (7,6)

14 (4,3)

2 min

2.14 (54,4)

0.07 (1,8)

2200 (15,2)

9 (2,8)

8 max

8.00 (203,2)

0.25 (6,4)

2100 (14,5)

17 (5,2)

1.5 min

1.65 (41,9)

0.08 (1,9)

3100 (21,4)

8 (2,5)

8 max

8.25 (209,6)

0.38 (9,5)

3100 (21,4)

18 (5,5)

1.5 min

1.71 (43,4)

0.11 (2,7)

4300 (29,6)

9 (2,8)

8 max

9.08 (230,6)

0.55 (14,0)

4200 (29,0)

20 (6,2)

1.5 min

1.76 (44,7)

0.13 (3,3)

5200 (35,9)

9 (2,8)

4 max

4.59 (116,6)

0.34 (8,6)

5200 (35,9)

15 (4,6)

1.5 min

1.82 (46,2)

0.16 (4,1)

6300 (43,4)

9 (2,8)

4 max

4.55 (115,6)

0.40 (10,2)

6300 (43,4)

15 (4,6)

Table 3-1 Approximate Physical and Mechanical Properties


(Actual RTR pipe properties to be obtained from the manufacturer)
Epoxy

Polyester

Vinylester

1.90

1.60

1.90

0.03

0.03

0.03

35,000

35,000

35,000

9,000

9,000

9,000

1.4

1.4

1.4

> 20,000

> 20,000

> 20,000

> 25

> 25

> 25

14

14

14

Thermal Conductivity (BTU/hr.ft . F.in)

1.8

1.3

1.3

Supports Combustion

No

Yes

Yes

Temperature limit (C)

66 to 100

70

100

- 35

- 35

- 35

Specific Gravity
o

Water Absorption [% 24 hours at 73 F (23C)]


Hoop Tensile Strength [psi at 78F (26C)]
Axial Tensile Strength [psi at 78F (26C)]
o

Modulus of Elasticity in Tension [psi at 73 F (23C) x 10 ]


Flexural Strength [psi at 73F (23C)]
Impact Strength (Izod, ft-lb/in, notch)
-6

Hoop Coefficient of Thermal Expansion (1/F x 10 )


-6

Axial Coefficient of Thermal Expansion (1/F x 10 )


2

Minimum operating temperature (C)

Page 36 of 37

Document Responsibility: Non-Metallic Standards Committee


Issue Date: 30 December 2013
Next Planned Update: 30 December 2018

01-SAMSS-042
Reinforced Thermoset Resin (RTR) Pipe and
Fittings in Water and Hydrocarbon Services

Table 3-2 Example of Physical and Mechanical Properties


of High Pressure Epoxy Resin Line Pipe
(Actual RTR pipe properties to be obtained from the manufacturer)
Property
Maximum temperature F (C)
Life expectancy
20 year Average long term hydrostatic
strength

(LTHS ASTM D2992-B)


20 year Lower confidence limit
(LCL ASTM D2992-B)
Density
Specific gravity
Coefficient of thermal conductivity
Coefficient of thermal expansion
Hoop modulus of elasticity
Axial modulus of elasticity
Poisson ratio

Anhydride

Aliphatic Amine

Aromatic Amine

150F
65.6C

200F
93.3C

212F
100C

20 years

20 years

20 years

23,270 psi at 150F


160,5 MPa at
65.6C
21,400 psi at 150F
147,6 Mpa at
65.6C
3
121 lb/ft
-3
3
1,94 10 kg/cm

18,410 psi at 200F


126,9 Mpa at
93.3C
17,554 psi at 200F
121,0 Mpa at
93.3C
3
124 lb/ft
-3
3
1,93 10 kg/cm

16,945 psi at 200F


116,8 Mpa at
93.3C
14,654 psi at 200F
101,0 Mpa at
93.3C
3
112 lb/ft
-3
3
1,8 10 kg/cm

1.94
0.23 BTU/ft.hr.F
0.14 W/m.C
-6
12.5 10 1/F
-6
22,6 10 1/C
6
3.5 10 psi
24,1 GPa
6
1.5 10 psi
10,3 GPa

1.99
0.23 BTU/ft.hr.F
0.14 W/m.C
-6
8.7 10 1/F
-6
15,7 10 1/C
6
3.3 10 psi
22,8 GPa
6
2.0 10 psi
13,8 GPa

1.80
0.23 BTU/ft.hr.F
0.14 W/m.C
-6
8.8 10 1/F
-6
15,8 10 1/C
6
3.2 10 psi
22,8 GPa
6
1.82 10 psi
12,6 GPa

0.38

0.39

0.38

Page 37 of 37

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