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Staple Fibre
Length
Staple length determines the strength of yarn and optimum twist
factor. Extra long staple fibres (50-64mm) require a lower twist
factor and enable higher spindle speeds. At the same time, they are
more prone to nep generation and result in inferior yarn appearance.
Staple fibre yarns from 38mm enjoy a premium over those made from
52mm fibre. In the case of cut staple fibres, fibre length is measured
by laying the fibre on a glass plate smeared with paraffin oil to enable
straightening of fibre (BISFA, ASTM D5103-07). With highly crimped
fibres straightening may be difficult and in this case fibre has to be
fixed between two clamps and a slight tension has to be applied to
one of the clamps. The amount of tension should be just sufficient to
remove crimp and is determined by preliminary tests. Length of fibre
is measured on a scale or by a sliding microscope. Roughly about 1015 fibres are tested and average is determined.
In the case of variable staple fibre and synthetic tops used in worsted
spinning system, automatic fibre diagram machine by SDL or WIRA is
used. Cut square method is used to draw a tuft of fibres from the
sliver and tuft is passed between the plates of capacitor. A measure is
thus obtained of number of fibres in the tuft from the base to tip,
from which cumulative fibre distribution is obtained. The
measurement is fully automated and the fibre diagram together with
results of mean length, upper half mean and CV are automatically
displayed. While preparing a cut square sample, precaution should be
taken to avoid breakage of fibres.
Fibre Fineness
Fineness in the case of staple fibres determines the count to which
the fibre can be spun. It also determines the strength, evenness and
imperfections of yarn and also the end breaks in spinning. Fibre
fineness is determined gravimetrically or air-flow method or by
vibration method.
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o
Gravimetric method
Airflow method
Vibration Method
The fibre, hung vertically, is taken over a knife edge and tensioned
by a pre determined weight and is subjected to transverse
vibrations at variable frequency (ASTM D1577). The frequency at
which maximum amplitude is obtained, which is resonance
frequency, is determined, from which fineness is determined by
the following formulae.
107
Where T = tension in Newton
F= Frequency in Hertz
L = Length in metres
Vibromat by Textechno Herbertstein and Vibroscop by Lenzing are
based on this principle. The equipment is fully automatic and upon
testing a number of fibres randomly selected (around 8-10), mean
fibre fineness and CV are displayed. The method is very fast with a
total testing time of 5 - 6 sec. However determination of
resonance frequency is not precise with some fibres.
Tensile properties
Fibre Strength
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and elongation and their variability critically affect performance in
weaving and knitting. Single fibre testing is normally done (ASTM
3822 - 07) at constant rate of elongation with a gauge length of 1
cm. Fibre is clamped preferably pneumatically between two jaws
at a predetermined tension. Lower jaw is traversed at a constant
rate while upper jaw is attached to a sensitive load cell of 50100cN capacity. The load extension curve, breaking load,
elongation, work of rupture and modulus are determined and
displayed. Load at 7% and 10% elongation are also determined
for synthetic fibres blended with cotton/viscose. Strength at 7%
and 10% elongation,T7 and T10, have to be close to cotton/viscose
breaking strength to minimise strength losses in blending. Facility
is also offered in some instruments to carry out tests under liquid
and for carrying out cyclic loading test. Fafegraph and Favimat by
Textechno Herbert stein and Vibroskop and Vibrodyn by Lenzing
are some commonly used instruments. At least 10 fibres should be
tested for getting a reliable mean. Considerable automation has
taken place in transferring the fibre to the jaws through use of
transfer clamp actuated by robot. Manual involvement in testing
is restricted to clamping the fibre between two paper clips and
mounting it on a magazine. After that all operations are carried
out automatically. Single testing instrument that carries out
fineness, strength and crimp all, at one place, have also been
developed. Not only testing time is reduced but also the different
tests are carried out on the same fibre. Bundle strength in
stelometer is not recommended because of fibre slippage under
the jaws.
Loop/knot test
To get an estimate of brittleness of fibre, fibre is tested in loop or
knot configurations and resulting strength compared with normal
strength (ASTM D 3217). Fig 2 shows strength testing of loop and
knot. Two filaments are used to form the loop and the ends of loop
are clamped on the clamps of the strength tester. Knot is formed
on fibre and the fibre/filament with knot is placed between the
clamps and tested.
Crimp
Crimp is an important property that determines processing behaviour
in carding, drafting and fault incidences in yarn. Crimp frequency,
amplitude, crimp stability, crimp elongation, decrimping point are
some of the important properties that determine crimp. Crimp
stability is an important property as it indicates the extent to which
fibre retains the original crimp during opening, carding and drawing.
ASTM D3937 describes a simple method for determining crimp
frequency. Crimp frequency and amplitude may be determined by
projecting a magnified image of fibre on screen. Opto electronic
sensor is used in some equipments to provide digital representation
of fibre held between two clamps at very low tension and for
determination of crimp geometry. Tensile tests using an extremely
sensitive force measuring system with measuring accuracy of 1mN,
enables the measurement of the curve of crimp force vs elongation,
crimp extension, decrimping point and crimp stability. The fibre is
subjected to gradual loading and crimp is measured in two ways 1.
Extension at 1cN/tex and 2. Extension at the inflexion point given by
tangent1 (Fig 3)
Spin Finish
Nature and quantum of spin finish has critical influence on
performance of fibre. Lap licking, cylinder loading and roller lapping
are often traced to improper spin finish. Spin finish is traditionally
estimated by extraction with a solvent like carbon tetrachloride or
benzene on Soxhlet's apparatus. The amount of extracted material is
determined gravimetrically or by infrared spectroscopy. This is time
consuming though accurate. ALFA 300 by Lenzing and Rapid
extraction apparatus by SDL are rapid methods for determining spin
finish. Known quantity of fibre is packed in a vessel and spin finish is
removed by means of a solvent through constant stirring and the
resultant emulsion is subjected to an analyser where organic carbon
content is determined. %of oil and finish are separately determined.
The equipment is suitable for fibre as well as filament. Low resolution
Nuclear Magnetic Resonance is a faster and solvent free method for
determining spin finish and is offered, among others by Lenzing and
Oxford instruments.
Oil content in filament is an important property. Filament sample is
extracted in water and the extraction is conveyed to a furnace. Oil in
water is burned and oxidised and the generated gas is analysed for
carbon-dioxide content in Infra red analyser.
Static Generation
One of the problems encountered with synthetic fibres is generation
of static electricity. Static generation is a cause for lap licking,
cylinder loading, web falling incidences and coiler choke up in carding
and roller lapping in draw frame to ring frame. High hairiness in yarn,
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fabric defects like stitches and floats are also attributed static
electricity. Sparking may take place due to static in synthetic carpets.
Accurate instruments are available for estimating the amount static
charge and half decay time. Half decay time denotes the time taken
for static charge to come down to half its level and a low value is
desirable. Sample held in a holder is rubbed for a known duration of
time and static charge sensing unit measures the charge and decay of
charge with time. This method is not normally preferred as it is
dependent on rubbing material and conditions. Honestometer which
works on the principle of charging the material by irradiating it with
air ions generated in a corona discharge field is commonly used.
Developed charge, decay curve and half decay time are measured
afterwards (Fig 5).
Drafting Force
Drafting behaviour of fibre can be estimated by determining drafting
force and its variability. Cohesion testers have been developed for
this purpose. The sliver or roving is passed between two pairs of
drafting rollers with front pair mounted on a lever fitted to strain
gauge. As the material is drafted, front pair of rollers oscillates to and
fro as per drafting force and the strain gauge measures the force
continuously, amplifies and records it on a chart. Mean and coefficient
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of variation of drafting force are measured. The equipment is also
useful in assessing the quality of spin finish and oil applied on fibre.
Abnormalities in fibre
Presence of extraneous agglomerations on the surface of fibre, fused
and undrawn fibres, over length fibres are some of the abnormalities
in fibre. High precision microscope like Projectina is useful to detect
such abnormalities in fibre. Modified Baer sorter of a longer length
with double the number of combs is sometimes used for estimating
over length fibres. ASTM D3513-02 prescribes a method for
determining over length fibres. Over length fibres are the main source
of crackers in yarn and should be below .01%. Undrawn and fused
fibres cause slubs and long thick places in yarn.
UV Stability
Resistance to degradation by UV requires to be tested in geotextiles,
automobile materials and others continuously exposed to sunlight.
Weather-o-meter is used for finding UV stability. The instrument uses
UV lamp which simulates the ultra violet rays found in sunlight. After
exposing the specimen for a specified duration, strength is tested to
assess degradation if any. Polypropylene and nylon have lower UV
stability compared to polyester.
Dyeability of fibre
Laboratory model dyeing equipments are offered by various
manufacturers for dyeing small samples of fibre up to 5 gm, to check
uniformity of dye pick up.
Molecular Orientation
Variations in whiteness in grey material and colour in dyed fibre from lot to
lot is a source of streakiness and weft bars in fabric. To maintain
consistency in whiteness and colour of fabric, raw material should be
checked for whiteness, degree of yellowness and colour. Instruments are
available for estimating whiteness and degree of yellowness. Bench type
spectrophotometer is used for testing and matching of colour.
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Filaments and Yarns
Tensile properties
Breaking load, elongation and work of rupture are some of the
important characteristics of filaments and staple fibre yarns. Lea and
single thread strength are the commonly used measures of yarn
strength and their relative merits have been discussed elsewhere 2.
o Single thread strength
Tensile testers may be classified as
Constant rate of loading type
Constant rate of elongation type
Constant rate of traverse type
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Gauge Length
Gauge length has considerable influence on strength.
With increase in gauge length, strength will decrease
because of increased chances of occurrence of more
weak places and the weak place being weaker. So gauge
length has to be standardised. Normally 50 cm gauge
length is used except in POY yarns where 20cm gauge
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Elastomeric yarns
Elastomeric yarns like spandex have a very elongation and special
testers have to be used to ensure that the material is transferred to
force measuring area at very low pre tension, and pre tension level is
set at as low a value of .01 cN/tex (ASTM D2653-07). Force
measuring system should have a high resolution of the order of 10N.
Breaking load, tenacity and elongation are determined at first
filament break (FFB). Special clamps have to be used to avoid
slippage. Eccentric roller grips and rubber grip grips are some of the
grips used to prevent slippage. If pneumatic clamps are used
pressure is set at 415 kPa(60 psi)
Creep testing
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Creep is a very important property in composites used in construction
and geotextiles. Creep and relaxation testing of yarn can be done by
subjecting loops of yarn to loading for a long time. Load is removed
and length is tested. Creep tester has facility for simultaneous testing
of 10 20 yarns.
Count
Count of the yarn is determined along with the lea test by weighing
the broken leas. Auto sorter is used to determine mean, minimum,
maximum, S.D., CV, Confidence limits and other statistics from count
tests of leas from within and from different packages. The instrument
consists of an electronic balance to measure the weight of leas. This
is equipped with a software for determining the various statistics.
Some manufacturers have developed instruments for automatically
determining count. This consists of drive rollers which withdraw a
known length of yarn from a package and deposit it on an electronic
balance for weighing and estimating count and related statistics.
Irregularity
Irregularity is an important quality characteristic of staple fibre
yarns. It determines the appearance of yarn and fabric, feel of fabric,
performance of yarn in further processes and the strength realisation
of fibre in yarn. Irregularity is commonly measured by capacitance
type irregularity tester (ASTM D 1425/1425M-09. Uster Evenness
tester is the widely used instrument for measuring irregularity. The
yarn is passed between two capacitance plates at a constant speed.
The capacitance of the condenser varies according to weight per unit
length of yarn. The variations in capacitance are converted into
voltage and amplified. A continuous record of variations is obtained in
a recorder chart. Instantaneous values of Mean Deviation%(U%) or
Coefficient of variation(CV%) of the variations is computed by an
integrator and displayed. A number Condenser slots of different sizes
are used for testing slivers, rovings and yarns as per their count.
Apart from short term variation, the instrument has also facility for
determining medium term term variations and variance length curve
of the yarn. Module for diameter variation is also available in most
electronic evenness testers.
Imperfection Tester
This is an attachment for determining the extreme places. Thick
places, Thin places, Neps, each of 4 categories based on their size,
are measured by the instrument.
Faults
While imperfections are frequently occurring defects, faults occur at
longer interval of time. Faults have a very critical influence on fabric
appearance, rejections and performance of yarn in winding and
subsequent stages. Measurement of faults is done by classimat on a
laboratory winding unit (ASTM D6197-99).In the winding unit yarn
passes through a capacitance sensing unit which counts faults as per
their size and length. 23 classes of faults to cover short and long thick
places, spinners doubles and long thin places are measured in Uster
Classimat. A more detailed article on measurement of faults, their
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source of occurrence and measures to control them are discussed in
an earlier article3,5. 10 bobbins are tested for evenness and
imperfections and faults. Faults are also tested before and after
winding to check the efficiency of clearing unit.
Spectrograph
Spectrogrpah carries out a fourier analysis of mass variations in the
material and displays a curve showing the amplitude of different
wavelengths present in the material. With constant staple fibres,
spectrograph will have two peaks one at2.7l and another at
which
is a lower harmonic (Fig 6). The peaks will be seen even if the yarn is
random with no extra irregularities. In mills peak at half the fibre
length have been often found in polyester/viscose blend and the
technicians and management used to be unnecessarily perturbed by
their presence.
Conditioning
Conditioning of material to test room is important, when test
room humidity varies considerably from manufacturing room.
One hour in the case of yarns and 2-3 hours in the case of
rovings, of conditioning would be adequate. The bobbins should
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o
o
Yarn Roundness
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Hairiness
Though hairiness in staple fibre yarns adds to the textile character of
fabric and contributes to comfort and skin friendliness, excessive
hairiness adversely affects appearance of yarn and performance of
material in subsequent stages. Hairiness is generally higher in staple
fibre yarns and blends than in cotton yarns. Several instruments
based on photoelectric principle are available for measuring hairiness
(ASTM D5647-01). An LCD beam is projected on yarn and a photocell
placed behind the yarn, counts the number of interruptions made by
the protruding hairs. Measurement of hairiness as per the length of
protruding hair is carried out. Portable models are also available for
measuring hairiness during production. Uster Evenness tester has a
hairiness attachment, which gives an estimate of total length of
protruding hairs in a cm length, termed as Hairiness index. More
detailed information on the causes of hairiness, measurement and the
effect of on performance of yarn is given in another article 7.
Twist tester
Twist in staple fibre yarns is measured by clamping 2.5 cm length of
yarn between two clamps under tension. One of clamps can be
rotated to remove the twist and other clamp can be moved to fix the
test length.. A microscope or magnifying glass placed over the yarn
enables to determine the point at which twist is fully removed and
fibres become parallel. Counter fixed on the rotating clamp
determines the twist. This is a time consuming method and is
subjective. Untwist twist method represents a quicker method for
estimating twist. A length of yarn mounted under a given initial
tension is untwisted till the yarn extends to a preset level and then
retwisted in opposite direction till original length and tension are
reached. Half of the number of turns (during twisting and untwisting)
divided by gauge length gives twist/unit length. Fully automatic
electronic testers have been developed based on this principle
(ASTM.1423-08). This method is not quite accurate as some twist is
set in yarn and cannot be removed during untwisting.
Lint Generation
Lint generation during weaving and knitting is experienced especially
in yarns with high hairiness. Lawson Hemphill has developed a lint
generation tester as an attachment to Constant tension tester. The
lint generated during running of yarn at 360m/min for 1 km length is
estimated.
Draw Force
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force, variations in molecular orientation, shrinkage and dyeing
characteristics of the material can be assessed. Testing of draw force
under dynamic conditions has the merit of high speed testing and
continuous recording of variations in draw force. Crimp force or crimp
rigidity of textured yarns and shrinkage force of flat and textured yarns
are also important quality characteristics that determine in fault
incidence in fabric. For measuring draw force, the yarn is passed
between two godets at high speed. The measuring roll of force
measuring system senses the yarn in between the two godets. Below the
measuring system, the yarn is heated by a heating system to high
temperature. There is usually facility to run the tester either with
constant extension or contraction for continuous measurement of yarn
tension, or with constant tension for continuous measurement of
extension or contraction.
o
POY yarns
The yarn is run at constant extension and draw force is
continuously measured and recorded.
Textured yarns
Overfeed is kept between two godets to determine shrinkage.
The test is carried out at low speed and high temperature to
determine shrinkage. Alternatively the yarn is tested at high
speed and low yarn temperature to determine crimp
contraction or crimp rigidity.
Flat yarns
Shrinkage is tested by running yarn at high yarn temperature
Lawson-Hemphill have developed hot draw knitter with draw
force tester to assess the uniformity of dyeing of POY yarns. It
employs a knitting machine with precision stitch control and
draw force measurement conforming to ASTM D 5344.
Shrinkage Elasiticity
Yarn is extended at a slow rate to 3-5% of original length. Tension is
then released and length is measured after 2-3 min. The difference
between original length and final length expressed as % of former
gives elasticity of yarn.
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19
Crimp Modulus % =
Crimp stability % =
.
Fig 8 : Crimp tester for textured yarns
Residual shrinkage, crimp contraction and their variability can also be
estimated by an automated tester(ASTM D 6774).Online instruments
for measuring crimp in a running tow are also available which
ensures satisfactory processing at later stages.
Broken Filaments
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units are also fitted in the unit to warn the operator of a sensor not
functioning properly because of contamination.
Entanglement Tester
Friction
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22
Yarn Abrasion
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Monofilament
Roundness, diameter and variability in diameter are measured using
multiaxis optical measuring system. Online measuring systems are also
available, among others by BSC Electronics.
Dyeability of yarn/filament
Dye pick up, uniformity in dyeing are estimated by knitting the yarn on a
sample knitting machine and examining the appearance of the product. Lot
to lot variability in yarn in regard to dye pick up, which is a source of weft
bars and bands, can also be assessed by this method. Instruments are also
available for continuous dyeing of yarn and evaluating the streakiness by an
automatic inspection system. Amount of light transmitted and reflected by
the dyed yarn are compared to assess lack of uniformity.
Vicosity
The chips used for manufacturing synthetic fibre should be checked for
degree of polymerisation by viscosity tester. Automatic viscometers are
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available by charging the chips in an extruder and measuring the viscosity
of molten material. The molten polymer obtained by heating the chips is
allowed to flow capillary tube and discharge pump. Pressure at capillary at
entrance and exit point are measured by a displacement pump pressure
sensing unit (Fig 12). The difference in pressure is used to measure
viscosity.
Where = Viscosity
r = Cpillary tube radius
l = Capillary tube length
q = Flow rate
Melt flow rate and melt volume rate are determined as per DIN 53735 to
check the quality of polymer chip.
Package Analyser
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Moisture Content