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RESEARCH PAPER
RP612
Kessler
ABSTRACT
Since the hardness testing devices in general use are not well adapted to floor
In order to
surfacing materials, an apparatus for this purpose was designed.
determine if the results of tests with this device bear a definite ratio to wear in
had
on
stair treads
been
service, a comparison was made with 22 materials which
under service conditions and which represented about 10 percent of the total
number received for tests. The degree of correlation between the tests and
actual wear was found to be high and, hence, the test values should enable one
Subsequently samples
to predict service wear with a fair degree of accuracy.
representing the marbles, limestones, slates, etc., commonly used in floor surfaces
were tested, and the approximate values for the different types range as follows:
Marbles, from 7 to 42; limestones, 2 to 24; sandstones, 2 to 26; slates, 6 to 12;
On this scale the
granites, 44 to 66; serpentines, 15 to 111; travertines, 5 to 17.
most resistant material (quartz) showed a value of 180. Materials used for
general flooring purposes in this country show values between 15 and 20.
CONTENTS
Fafft
I.
II.
635
637
637
637
637
638
Introduction
Development
1.
of
Test procedure
(6)
Service tests
3. Correlation of preliminary laboratory
values
III. Results of Laboratory Tests
2.
3.
Marble
Limestone
Sandstone
4.
Slate
1.
2.
639
640
640
642
643
643
644
645
645
646
646
648
Granite
Serpentine
7. Travertine
8. Miscellaneous materials
IV. Discussion of Results
V. Conclusions
5.
6.
I.
INTRODUCTION
The purpose of this investigation was to determine the comparative resistance to wear of the natural stones commonly used in floor
surfaces and other parts of buildings exposed to the abrasive action
of traffic.
For several years there has been a growing demand for
information on this subject which could not be adequately supplied
_
tests.
The United States Bureau
has published a large amount of valuable data on
Bureau
of
Roads
Dept.
of Agriculture,
635
636
of Research
[Vol. it
tests with the Dorry and Deval machines, but the materials referred
to usually do not correspond with those used in floors.
The rate of
wear on heavy duty floors is of considerable importance and due consideration to wearing qualities in the selection of materials may often
prevent annoyance or replacement.
floors are made a decorative feature of the building the design often requires the selection of
materials for color effect.
In the absence of comparative data on the
wearing qualities of the different materials one may select an unfortunate combination that will soon result in an uneven surface.
The subject of accidents in public buildings has been a matter of
some concern. While the question of slipperiness is not within the
scope of this study, it seems probable that irregular surfaces, espeSome
cially on stair treads, are a contributing factor to accidents.
varieties of stone which have high decorative values due to their
When
veined or mottled appearance may wear unevenly. Where a considerable range in wear resistance is shown for different specimens of a
sample the material may be expected to wear unevenly in service.
An examination of the methods and apparatus employed for hardness determinations shows various conceptions of this property.
These methods may be roughly classified as follows: the determination of the resistance of the material to (1) penetration of a spherical
surface or conical point (Brinell 2 and Rockwell 2 tests); (2) scratching with materials of standard hardness (Moh's hardness scale 3 );
(3) abrasion with loose, granular materials of standard hardness
(Dorry 4 and Amsler 5 tests) (4) the cutting action of a hard granular
substance of standard hardness under impact (sandblast) (5) a combination of impact and abrasion between broken fragments of the
sample (Deval test 6 ); (6) cutting with a tool of standard hardness
(Bauer drill test 7 for metals and Jagger's boring test 8 for minerals).
The test for flooring materials should simulate closely the conditions to which a floor is exposed.
Although the surface of a floor is
evidently subjected to a mild form of impact, the greatest amount of
wear is probably due to cutting or scratching of hard particles forced
into or rolled over the surface under pressure.
While the Deval test
combines the two factors assumed to be largely concerned in the wear
on floors, the impact action is much greater than the abrasive action.
Besides, the type of floor samples usually received for test purposes
are not well adapted to this apparatus.
The Dorry and Amsler
machines produce an abrasive action similar to that occurring on
floors, but some modifications would be necessary to adapt them to
the test samples. It was considered more feasible to design an apparatus of compact form and determine experimentally whether it pro;
floors.
The
3
*
8
See footnote 4.
B. S. Tech. Paper No.
Am.
4,
11,
Ralph P. Devries.
p. 399, 1897,
T. A. Jagger,
Jr.
Figure
1.
RP612
testing.
A, Grinding lap; B, specimen holder; C, specimen holder guide rings; D, spinning rods; E, spinning
gear; F, weight hoppers; G, spinning drive; H, abrasive conduit; I, abrasive hopper; K, guide ring
support; L, guide ring clamp.
Wear
Kessier)
637
The samples tested were supplied by the producers as being representative of the various quarries or grades. Variations occur in all
quarries and hence the test results can be only as representative as
the samples were.
II.
1.
(a)
LABORATORY TEST
DESIGN OF APPARATUS
(b)
TEST PROCEDURE
The specimens
Proc.A.S.T.M., D.
W.
Kessier.
was found to be more convenient to keep the superimposed weight constant and apply a correction
for the specimen weight.
The rate of abrasion was found to be proportional to the pressure; for example,
with 4,000 grams load the abrasion was twice that for 2.000 grams load. The correction factor is
10
It
2,000
W,+2,000
where W,
is
638
oj Research
[vol.
W
W
W W
Vnoo
f r
^ ne
weight of specimen,
the
formula becomes:
+ 2,000)G
,'{
TT _ 10(W,
aa
2,0G01F
{l)
where
is
a is
the
mean
2.
SERVICE TESTS
Wear
Kessler]
639
Vhite
marble
Z- Black
3- Pink
KncfliALS
( Vt.)
Be/gum)
(Tenn)
mo
Their designations
4- while
(Ala )
l56ray
16- Blue gray
5- Buff
'
(Italy)
17-
Iff-
6-7raveriine( Italy)
on
6iwh
OMm
X 5m
slate (Pa.)
'
(Pa)
(Pa)
5
z
<
JZ-
zo
(My.)
(ind)
(Ind)
---''
,
'-'"
.,~-'
-2
,-'-"'
06
>""
--'
Zi
""
0.1
Figure
3.
2.
'
*?
4--', 18
+15
?
-4 '+
9
OS
06
Relation between
Ha
02
0.3
04
I.I
0.7
08
03
1.0
Average Reciprocal Wear Rat/as
1.3
1.8
1.4
1.5
16
1.7
WEAR
In figure 2 the a values are plotted against the wear ratio reciprocals for all materials subjected to the service test except the serpentine.
The deviations from a linear relation are probably within the
precision of the tests.
The correlation coefficient (r) was computed for the values of the
two variables given in figure 2 by the formula
S(a?)S(y)
(xy)
r=
(2)
V(-^<>
(3/A
K=
640
Bureau
random
[Vol. it
linear relation
III.
MARBLE
Table
28 imported.
Table
1.
Results of
tests
on marble
[Note. Column
Serial
num-
Variety
bers of
Source
samples
Num Num
ber of
samples
Vermont
do._.
do._.
do._.
do.-.
White
calcite
Black
calcite (fossiliferous).
calcite..
Maxi-
Mini-
4b
4b
14.6
12.8
14.3
10.8
15.4
13.3
11.7
9.5
10.4
15.3
13.8
12.3
10.8
10.5
15.4
13.0
14.2
6.7
33.9
9.1
12.0
13.6
6.7
24.6
7.6
12.4
13.9
6.7
30.9
8.4
26.0
22.9
12.1
14.8
15.6
10.5
9.0
14.0
24.8
12.0
11.2
13.5
14.9
10.8
13.6
17.1
18.6
15.4
10.0
11.6
15.3
18.2
13.5
10.3
12.5
16.6
18.3
14.6
13.2
13.4
43.5
21.9
18.8
12.8
12.1
38.9
18.9
17.8
13.0
12.9
41.7
20.2
18.4
4b
4b
4b
4b
5
calcite.
White dolomite
Pink fossiliferous calcite...
Gray fossiliferous calcite. ..
Gray calcite..
White dolomite.
Buff dolomite
Black calcite
Pink calcite
Chocolate colored
calcite.
mum
mum
do
do
- do
New
York.
....do
....do
tests
ber of
4b
4b
Abrasive hardness
4b
4b
3
do
4b
Massachusetts.
4b
Maryland
Virginia
3
7
Tennessee
do...
4b
4b
Aver-
Wear
Kessler]
Table
1.
Results of
tests
on marble
Source
Variety
Continued
Num- Num
ber of
samples
tests
Tennessee
do
do.._
do
4b
4b
Blue
North Carolina.
4b
calcite.
....do..
do..
Georgia.
do.do..
calcite
Alabama.
Pink
calcite.
calcite.
calcite.
calcite
White dolomite
White and black calcite
Light-gray calcite
do--_
calcite
Gray
calcite
Pink
Gray
calcite.
do...
do...
Missouri .
calcite.
calcite
do
calcite
(dolomitic).
Buff
55
fossiliferous calcite
Violet pink calcite
Light pink calcite.
Gray
calcite (fossiliferous)
calcite
Dark-veined white
calcite.
.do.
17.5
17.3
8.9
16.2
18.8
15.6
12.5
8.3
14.4
17.2
4
3
19.3
14.3
14.3
20.2
14.9
16.9
13.5
13.8
19.1
12.1
10
21.0
7.8
33.4
15.5
14.9
12.1
7.5
28.7
14.0
13.3
33.5
15.3
16.2
28.2
35.2
27.7
10.2
13.5
20.7
29.0
25.9
35.6
33.1
31.2
15.2
25.4
33.8
29.0
30.8
14.9
30.9
14.1
34.4
33.4
34.0
29.6
11.0
32.9
27.1
33.7
12.7
16.5
14.5
25.7
11.4
12.2
13.4
13.8
23.5
9.4
28.8
27.0
27.0
31.5
26.4
25.0
23.8
24.3
29.5
25.0
22.5
26.7
25.6
20.4
24.2
17.3
4b
4b
3
3
4b
Yellow-veined black
Brown
calcite.
calcite.
4b
California.
Belgium.
4b
Norway.
France .
.....do
4
4
4
4
4
4b
calcite
Italy..
do.
do.
dodo.
.do.
.do.
.do.
.do.
4b
4b
4
....do.
....do.
....do.
..._do.
4b
Germany.
.do.
.do.
Algeria.
mum
24.0
17.5
12.3
11.5
10.9
3
5
3
3
Alaska
.do.
.do.
_do.
Mini-
25.7
18.5
15.4
12.6
11.7
2a
Utah
do
mum
17.8
18.7
21.0
19.2
16.8
do.
.do.
White
Arkansas..
Colorado..
Maxi-
19.0
19.5
21.3
20.3
17.4
do
do
do
White calcite
Gray calcite (fossiliferous) . .
Abrasive hardness
ber of
Gray calcite.
Pink calcite.
Gray
641
4
3
Average
The results do not indicate that the dolomites are more resistant to
abrasion than the calcites, although mineralogists assign a higher
hardness value to dolomite than calcite. It appears from the tests
that the abrasive resistance is influenced more by the compactness of
the material than by differences in hardness of constituent minerals.
The highest a value obtained on dolomitic marble was 30.9 (no. 9)
and the lowest 12.5 (no. 17). The highest value for any calcitic
marble was 41.7 (no. 23) and the lowest 6.7 (no. 8).
642
[Vol. it
LIMESTONE
floors
and
steps.
Table
2.
Serial
num-
Variety
bers of
Source
Num Numberof
sam-
(crystalline)
(oolitic)
19.6
6.8
6.7
7.1
11.6
18.5
6.4
5.0
6.6
7.3
19.2
6.6
6.1
6.9
6.3
5.7
6.6
5.1
4.7
6.1
5.0
6.4
5.1
4.6
6.2
5.4
6.5
5.1
4.6
.do.
.do.
.do.
.do.
.do.
5.7
8.4
18.3
6.4
6.2
4.1
7.9
14.8
6.2
6.2
4.8
8.1
16.9
6.3
6.2
do
6.7
24.9
15.5
5.6
9.7
6.3
22.9
13.9
4.5
4.9
6.5
24.1
14.9
4.9
1.5
10.2
10.0
8.3
2.1
11.0
11.2
10.0
9.9
mum
New York.
Indiana
do
do
Select gray (oolitic).
Hard
buff (oolitic)
Rustic buff (oolitic)...
Standard buff (oolitic).
do.
Rustic buff
(oolitic)
. .
..do
....
Select gray (oolitic).
Hard gray (oolitic)
do.
Select buff (oolitic)
Standard. buff
Gray
Gray
Gray
(oolitic).
.do.
.do.
.do.
(crystalline)
....do
(dolomitic)
Illinois
(oolitic)
Kentucky.
Alabama-
do
Light buff (earthy).
Florida
Pink (dolomitic)
Yellow (dolomitic)
Minnesota.
do
14
Buff (dolomitic)
Gray
(dolomitic)...
Gray
(oolitic)
Buff (semicrystalline)
Gray
(semicrystalline).
Light gray
Light buff
(oolitic)
(fossiliferous)
mum
10.2
Aver-
9.0
.do.
.do.
.do.
.do.
9.2
11.2
7.6
8.5
3.7
7.7
9.2
7.1
7.7
3.5
8.6
10.3
7.3
8.2
3.6
Oklahoma-
8.0
7.8
7.2
6.6
4.6
1.0
12.3
7.6
7.1
4.8
1.3
14.6
11.4
4.5
14
Texas
do
France.
5.1
1.8
17.6
Italy.
16.0
7.3
6.4
9.0
do-
Buff
Light buff (semicrystalline)
Buff (oolitic)...
Pink
Mini-
ples
Statuary buff
Maxi-
samples
Dark gray
Abrasive hardness
ber of
4.2
7.6
7.2
5.2
8.4
Wear
Kessler]
643
SANDSTONE
Table
3.
Serial
num-
Source
Variety
bers of
10.8
10.4
9.7
15.1
11.7
10.8
13.5
14.3
18.8
14.7
do
Pennsylvania.
do
do
do
17.6
11.3
25.5
29.8
17.2
12.6
8.9
19.0
19.2
13.8
15.5
10.1
23.3
26.4
15.6
do.
do.
Ohio...
do.
15.0
23.2
5.2
4.3
1.8
12.2
13.1
4.9
4.0
1.4
14.0
18.2
5.1
4.2
1.6
8.8
4.5
9.2
12.0
46.0
5.2
3.7
6.0
7.2
9.6
6.3
4.0
7.3
29.0
20.4
15.5
14.7
11.0
17.7
12.9
New York
New Jersey
do
.do.
flagstone.
Red
flagstone
Blue flagstone..
Bluestone
Gray sandstoneBuff sandstone..
do
.do.
Tennessee.
Gray
....do
.do.
.do.
do
Kentucky-
(fine grained)..
California.
4.
10.8
18.9
20.1
20.7
18.5
Massachusetts.
Bluestone
Purple flagstone.
Blue flagstone...
Brown
Mini-
Brownstone
flagstone...
sam
Abrasive hardness
berof
Maxi-
samples
Gray
Num Num
berof
tests
mum
mum
Aver-
9.
SLATE
644
Bureau
Table
[Note. Column
number
Results of
4.
Where "a"
tests
on
slate
number, 2
where "b" follows the number, tests were repeated on 2 of the
number, 3 tests were made on each of 3 specimens]
5 gives the
of tests.
follows the
of 3 specimens;
follows the
Num- Num-
Serial
num-
Variety
bers of
Source
samples
ber of
samples
Vermont.
Purple
Unfading green. ..
do...
do...
do...
do...
Maine
Red
New
5b
6a
5b
5b
9.0
8.1
8.5
7.9
7.3
6.9
7.0
7.6
7.5
6.7
8.3
7.6
8.0
7.7
9.2
12.0
12.2
8.8
8.1
7.4
8.8
10.7
9.0
9.6
7.9
9.4
11.4
7.8
7.2
15.2
8.0
7.6
7.3
7.0
7.4
7.6
7.2
7.5
7.1
11.7
7.7
7.5
7.0
7.7
6.6
7.2
7.2
5.8
7.5
6.3
6.3
6.2
7.8
7.7
7.7
7.2
6.4
7.4
7.0
5.8
6.2
5.6
7.2
5.8
9.3
5.7
12.2
6.5
5.5
6.8
5.5
9.9
10.9
7.0
3.5
8.5
6.8
6a
5b
Pennsylvania.
do
do
do
do
Blue-gray, clear.
do
....do
.do
.do
Blue-gray, ribbon.
Blue-gray, clear...
3
3
5b
15
.do.
.do.
-do.do.
.do.
do
Blue-gray, ribbon.
Blue-gray, clear. ,.
3
3
29
15
12
Dark gray
do
do
do
Maryland-
do
Virginia. ..
5b
Green
Georgia...
Tennessee.
5b
Blue-gray, ribbon.
Blue-gray, clear...
Hard vein
do.
5.
Mini-
5b
5b
Weathering green.
Unfading green. _.
Maxi-
York.
Abrasive hardness
tests
5b
Silver gray
ber of
do
do
do
....do
[Vol.
9c
3
mum
mum
7.1
7.5
7.4
6.5
5.6
8.2
5.6
GRANITE
finishing process.
Wear
Kessler]
Table
[Note. Column
of 3
5 gives the
number
specimens; where
"b"
5.
Results of
tests
Where "a"
of tests.
follows the
number,
on granite
follows the
3 tests
number,
Abrasive hardness
Num- Xum
Variety
bers of
ber of
Source
sam-
samples
ples
Pink
biotite granite
Maxi-
tests
mum
3
3
do
do
Vermont
Massachusetts..
6a
do
55.0
55.7
76.0
98.4
53.9
65.2
3
3
do
6.
69.2
48.5
72.5
72.9
75.1
do.
New Hampshire
ber of
Maine.
on each
Serial
num-
645
North Carolina.
Colorado
9b
Mini-
mum
Average
63.2
45.9
64.0
66.4
66.3
56.6
60.2
37.0
50.0
59.0
77.3
44.6
42.9
43.9
53.2
67.7
87.9
50.5
59.5
SERPENTINES
Table
[Note. Column
5 gives the
number
Results of
6.
of tests.
tests
Where "a"
on serpentine
follows the
number
2 tests
of 2 specimens]
Serial
num-
Source
Variety
bers of
samples
Num- Num
ber of
samples
Vermont
Sweden.
Emerald-green
Green, white veins.
Red, white, and green...
Dark green, white veins
Green, white veins
Italy....
Dark
tests
Massachusetts.
New
Jersey
Maryland
Georgia
do..
do..
France..
Greece..
Abrasive hardness
ber of
4
3
4a
4
Maxi-
Mini-
97.6
16.7
40.6
158.0
26.9
86.1
12.9
30.2
75.0
23.0
92.6
15.0
35.3
111.4
24.9
22.7
37.6
81.0
21.0
15.3
80.0
15.6
31.7
65.0
16.0
10.2
74.3
18.8
34.8
74.2
17.8
13.3
77.2
mum
mum
Average
TRAVERTINES
products.
1331733
Some
6
646
of Research
[Vol. 11
igneous rock.
1, 2, 3,
and
9) are
cellular structure.
Table
[Note. Column
5 gives the
number
7.
of tests.
number,
2 tests
Num- Num-
Serial
num-
sam- berof
tests
samples
Buff (sedimentary).
Buff (fossiliferous) Buff (sedimentary).
Buff
Florida
Georgia
Minnesota.
Montana
.do
.do.
Pink
Gray
Pinkish-buff
Buff.
Light buff (sedimentary)
Buff
Black (vesicular basalt) ...
8.
Abrasive hardness
ber of
Source
Variety
bers of
ColoradoItaly
France
Germany.
__do-
Maxi-
mum
Mini-
mum
Average
17.6
13.4
12.5
14.4
13.3
5.6
11.7
10.0
14.1
8.8
12.4
12.6
11.2
14.3
11.4
5.8
8.8
16.7
.6
18.4
50.7
5.0
8.3
15.2
.6
15.3
35.6
5.4
8.6
15.7
.6
16.5
40.6
MISCELLANEOUS MATERIALS
and
Table
8.
5 gives the number of tests. Where "a" follows the number, 5 tests were
specimens; where "b" follows the number, 3 tests were made on 1 specimen]
[Note. Column
Num- Num-
Serial
num-
ber
Source
Variety
bers of
of
sam-
sam-
ples
ples
2
3
4
5
6
7
8
9
10
11
do
do
do
"do.
do
do
do
do
do
Chloritic amphibole
do
New York
Feldspar (orthoclase)
Feldspar (albite)
Quartz
IV.
made on
Abrasive hardness
ber
of
tests
Maxi-
Mini-
2
2
2
2
2
23.2
10.0
5.6
4.9
4.4
22.0
9.6
5.4
4.2
4.2
22.6
9.8
5.5
4.6
4.3
14
3
21.6
16.2
9.9
55.0
89.8
187.0
11.7
15.7
5.6
50.5
75.0
176.0
16.3
16.0
7.2
52.7
80.9
179.7
11
3
5 a
Brazil
3b
mum
mum
Average
DISCUSSION OF RESULTS
the
This
may
Wear
Kessier]
647
which minerals occur. The mineralogist deals usually with individual crystals of the substance while rocks are mainly aggregations
Loosely bonded aggregations of hard minerals in
of small crystals.
This is illustrated
this test invariably show low resistance to wear.
by the tests on some of the sandstones which were almost entirely
quartz but gave lower
The
a values than most of the limestones.
abrasive resistance of sandstone seems to depend mainly on its coThe correlation coefficient (r) between the
hesive strength.
a
values and modulus of rupture values for 21 sandstones, computed
in
by formula
was found
mean
percentage variation
648
Bureau
[Vol.
V.
CONCLUSIONS
weathering.
11. Since the values for most of the types of stone tested overlap in
many instances, it is not possible to evaluate the relative wear resistance of materials by type alone.
Washington, August
30, 1933.