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DistillationColumn:ColumnInternals,Bubblecaptrays,Valvetrays,Sievetrays,Structuredpacking
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Distillation Columns: Column Internals


Trays and Plates
Bubble cap trays
Abubblecaptrayhasriserorchimneyfittedovereachhole,andacapthatcoverstheriser.Thecapis
mountedsothatthereisaspacebetweenriserandcaptoallowthepassageofvapour.Vapourrises
throughthechimneyandisdirecteddownwardbythecap,finallydischargingthroughslotsinthecap,
andfinallybubblingthroughtheliquidonthetray.

Sieve trays
Sievetraysaresimplymetalplateswithholesinthem.Vapourpassesstraightupwardthroughthe
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liquidontheplate.Thearrangement,numberandsizeoftheholesaredesignparameters.

Valve trays
Invalvetrays,perforationsarecoveredbyliftablecaps.Vapourflowsliftsthecaps,thusselfcreatinga
flowareaforthepassageofvapour.Theliftingcapdirectsthevapourtoflowhorizontallyintothe
liquid,thusprovidingbettermixingthanispossibleinsievetrays.

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ThisFLEXITRAYTMvalvetrayisasteelsheetonwhichliftablevalvesaremounted.Theyaremuch
moreefficientthansievetrays.PictureofKochGlitsch,LP.

Liquid and Vapour Flows in a Tray Column


Theimagebelowshowthedirectionofvapourandliquidflowacrossatray,andacrossacolumn.
Eachtrayhas2conduits,oneoneachside,calleddowncomers.Liquidfallsthroughthedowncomersby
gravityfromonetraytotheonebelowit.

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Aweironthetrayensuresthatthereisalwayssomeliquid(holdup)onthetrayandisdesignedsuch
thatthetheholdupisatasuitableheight,e.g.suchthatthebubblecapsarecoveredbyliquid.
Beinglighter,vapourflowsupthecolumnandisforcedtopassthroughtheliquid,viatheopeningson
eachtray.Theareaallowedforthepassageofvapouroneachtrayiscalledtheactivetrayarea.

Tray Designs
Atrayessentiallyactsasaminicolumn,eachaccomplishingafractionoftheseparationtask.Fromthis
wecandeducethatthemoretraysthereare,thebetterthedegreeofseparationandthatoverall
separationefficiencywilldependsignificantlyonthedesignofthetray.Traysaredesignedtomaximise
vapourliquidcontactbyconsideringthe
liquiddistributionand
vapourdistribution
onthetray.Thisisbecausebettervapourliquidcontactmeansbetterseparationateachtray,
translatingtobettercolumnperformance.Lesstrayswillberequiredtoachievethesamedegreeof
separation.Attendantbenefitsincludelessenergyusageandlowerconstructioncosts.

Structured packing
Thetermstructuredpackingreferstoarangeofspeciallydesignedmaterialsforuseinabsorptionand
distillationcolumns.Structuredpackingstypicallyconsistofthincorrugatedmetalplatesorgauzes
arrangedinawaythattheyforcefluidstotakecomplicatedpathsthroughthecolumn,thereby
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creatingalargesurfaceareaforcontactbetweendifferentphases.

Structuredpackingisformedfromcorrugatedsheetsofperforatedembossedmetalorwiregauze.The
resultisaveryopenhoneycombstructurewithinclinedflowchannelsgivingarelativelyhighsurface
areabutwithverylowresistancetogasflow.
Thesurfaceenhancementshavebeenchosentomaximizeliquidspreading.Thesecharacteristicstend
toshowsignificantperformancebenefitsinlowpressureandlowirrigationrateapplications.

Packings versus Trays


Atraycolumnthatisfacingthroughputproblemsmaybedebottleneckedbyreplacingasectionof
trayswithpackings.Thisisbecause:
packingsprovideextrainterfacialareaforliquidvapourcontact
efficiencyofseparationisincreasedforthesamecolumnheight
packedcolumnsareshorterthantrayedcolumns
Packedcolumnsarecalledcontinuouscontactcolumnswhiletrayedcolumnsarecalledstagedcontact
columnsbecauseofthemannerinwhichvapourandliquidarecontacted.

Part 1:WhatareDistillationColumns?
Part 2:DistillationColumn:ColumnInternals
Foramoreexpandedarticleaboutdistillation,pleasevisit:

http://lorien.ncl.ac.uk

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GraphiccourtesyofBismarckStateCollegeNationalEnergyCenterofExcellence

WernerSlken20082015.Allrightsreserved.
DonotworryaboutyourdifficultiesinMathematics.Icanassureyouminearestillgreater.AlbertEinstein

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