Documenti di Didattica
Documenti di Professioni
Documenti di Cultura
Contents
1.
2.
3.
Introduction.......................................................................................................................................... 4
1.1.
1.2.
Operators ......................................................................................................................................... 4
1.3.
2.2.
2.3.
Safety First....................................................................................................................................... 5
2.4.
2.5.
2.6.
2.7.
Transport ......................................................................................................................................... 7
3.2.
3.3.
4.
5.
5.2.
5.3.
5.4.
Compressed Air Supply (required for AWRF and AIR option) ...................................................... 14
5.5.
Drain Water................................................................................................................................... 14
5.6.
5.7.
5.7.1.
6.
Operation of the JUMO dTRON Controller and Conducting the Kesternich Test .................. 16
6.1.
6.2.
Setting Controller Parameters for the Water Condensation Test (CON) .................................... 16
6.3.
Operation of the Kesternich Test with Manual Dosing System (DosiCORR MD) ...................... 19
6.3.1.
Principle of Operation........................................................................................................... 19
6.3.2.
6.3.3.
6.3.4.
7.
8.
Commissioning ................................................................................................................................... 22
7.1.
7.2.
9.
Maintenance ................................................................................................................................. 23
9.2.
9.3.
1. Introduction
1.1. Purpose of this document
This operating manual introduces the users/ operator of the VLM Corrosion Test Cabinet with:
-
1.2. Operators
VLM corrosion testing instruments may only be operated by personnel instructed and authorized by the
owner.
All persons concerned with the installation, commissioning, operation, maintenance and repair of the
instrument must:
-
be appropriately qualified
respect follow the rules and instructions provided in this manual
Please resolve any problem that can affect the safety immediately.
2.5.
Authorized Operators
- Only approved persons are allowed to operate the instrument
- The minimum age of operators is 18
- The operator is responsible for third parties within working area
- The areas of responsibility for the different activities in the relation with the
instrument must be clearly defined and observed. Ambiguous areas of competence are
a safety risk
If the cabinet is stored for a longer period of time make sure that the storage room is dry. The temperature
should not fall below 0C.
Important: Remove all packaging materials such as foam particles from all inlets and outlets.
Be aware of all components under the bottom of the cabinet when you transport the cabinet by
a forklifting or hand pallet truck.
2)
Pressure
6-8 bar
Connection
Nipple size. 5
2-5 bar
No pressure
male thread
PVC hose 25 mm
PU hose 50 mm
4. Technical Description
4.1.
Operating Range
4.2.
Literature:
Standards are available from:
Beuth Verlag GmbH,
Burggrafenstr. 6,
10787 Berlin
ASTM International, 100 Barr Harbor
Drive,
PO Box C700, West Conshohocken,
PA 19428-2959
United States
Annual Book of ASTM Standards Vol
03.02
Note: A decrease in ambient temperature leads to the increase of the amount of water
condensation
According to ISO 6270-2 three phases (Table 2) are defined in the Cyclic Climate test being:
- Water condensation Constant humidity (CH)
- Water Condensation Alternating humidity and temperature (AHT)
- Water condensation Alternating temperature (AT)
The water condensation test (CH) is commonly conducted in the following way:
The trough of the test chamber is filled with purified water such as all four corners of the chamber are
covered and then the water is heated up uniformly to 40C. This allows all test specimens in the chamber
to have a uniform and constant temperature (tolerance is 0,2C).
Option AWRF
The CON test chambers with the AWRF option (Automatic Water Refill) can beside the constant (high)
humidity (CH) phase also facilitate the cooling phase (AT) where the chamber is cooled down to the
environmental temperature with humidity at nearly 100% (with or without water in the chamber).
Option AIR
The CON test chambers with the AIR option can also perform the forced ventilation phase (AHT). The test
chambers without AIR option can perform the AHT phase only by (manually) opening the front door. The
AHT phase can run with or without water in the test chamber.
Table 2 shows the parameters of the water condensation test in more details.
VLM
Cyclic Climate test chambers with AIR option are equipped with solenoid valves and a pneumatically
controlled ball-valve which is closing and opening the ventilation system. For this reason all VLM chambers
fully comply with the DIN 50014 requirements in terms of the ventilation and cooling of the ambient air.
The specification of the chosen ventilators is selected such as to resemble the storage conditions in normal
environmental conditions. The air can flow into the lower rear part of the test chamber through a specially
designed air duct which can be adjusted such as to ensure uniform drying of the test specimens.
The test chamber with AIR option is equipped with fans with adjustable speed in order to meet specific test
standards. The AIR system allows the fastest way for ventilate and cool down the test chamber by
establishing forced ventilation. This replaces the requirement for opening the door
Option: Controlled Water Condensation (CWC)
VLM has developed an innovative water condensation system featuring the patented CWC concept
(Controlled Water Condensation system - Figure 4). This system allows an accurate regulation of preselected condensation parameters such as the temperature difference between the bottom and the roof
of the test chamber. This allows a maximum reproducibility and comparability of test results.
Figure 4 VLMs patented CON AIR CWC method for water condesation
During the salt spray phase, the air under the roof saturated with salt fog acts as a heat insulator. This
insulation is removed after switching to water condensation phase. The battery of fans installed in the roof
construction are pumping the ambient (room) air through the double shelled roof which cools down the air
under the roof in order to keep the required vertical temperature gradient of 1C between the air under
9
the roof and the air above the water bath in the test chamber. In this way a uniform and reproducible
condensation temperature in the test sample zone is controlled to very tight tolerances.
Prerequisites for having such a highly sensitive temperature control system are an advanced software
control and a stainless steel construction of the test chamber coated with PTFE. This makes possible to have
a fast and uniform heat transfer from the heating grid under the floor and behind the back wall of the
chamber. As a result the CWC concept allows a very good horizontal temperature stability and
reproducibility of climate conditions.
4.3.
Figure 5 and on the next page show the front and the rear view of the CON 300-FL AIR CWC AWRF
Roof with CWC
system
Door
Control panel
Test chamber
Tap for drain water (not
applicable for chambers
with AWRF option)
Adjustable foot
4.4.
10
4.5.
Technical Specification
Model
Test Chamber (mm):
Volume test chamber
Dimensions test chamber W/D/H1/H2 (mm)
1100/700/900
740 x 400
11
Air exhaust
(AIR option)
Air inlet
(AIR option)
(AIR
All connections for water supply / water drain as well as electrical connections are in the lower part of the
rear panel.
Figure 9 Water
purification plant
Check if all parts are delivered before starting the installation of the water purification plant. Pay attention
to the instruction manual of the manufacturer of the ion-exchanger cartridges.
12
Figure 11 Digital
conductivity meter
Important!
If there is no drain in the floor a leakage water safety unit (Figure 8) has to be
installed to prevent any damages caused by flooding. In case of a leakage or
burst of a hose the sensor located on the floor will immediately close the
magnetic valve and the water supply will be shut down.
Please follow the following procedure to set up the plant for water purification:
1. Mount the splitter for the purified water on the wall so that it is convenient
Figure 13 Ion-exchange
to be connected and operated.
cartridge
2. Mount the quick connector nipples on the threads on the outlet / inlet of
the ion exchange cartridge.
3. Connect the water outlet of the ion exchanger to the inlet of the splitter. Connect one of the splitter
outlets to the inlet of the test chamber.
4. Connect the water inlet of the ion exchange cartridge to the tap water supply with a supplied hose.
The safety unit should be mounted on the water tap.
5. Screw the second female quick connector on the plastic double-nipple and the conductivity meter
on the other side. Press this unit on the pure water outlet of cartridge (indicated on the cartridge).
Connect this unit with the delivery unit by a hose.
6. Mount the stop-cock on the splitter and connect the hose to it.
7. Put the plug of the conductivity meter into a socket (230 V).
Important!
Note, that the actual conductivity will only be indicated when the water is flowing.
Conductivity meters are shown in Figure 12 and Figure 11
Once you put an ion exchanger cartridge Figure 13 into use pay attention to the fact that the
air will be completely displaced by the water. Open the venting screw at the top of the
cartridge thus the air can escape. Close this screw after there is only water coming out of the
cartridge.
13
5.4. Compressed Air Supply (required for AWRF and AIR option)
The pressure of the compressed air should be between 6 and 8 bar which is required to operate ball valves.
Make sure that the compressed air entering the cabinet is oil free (0,2 mg/m) and particle free (< 5 m).
Be aware of shavings in case new pipes have been installed. These particles may enter the inlet valve and
block it. We strongly recommend the installation of a compressed air maintenance unit which is available
as an accessory (Figure 15).
There is a female connector Size 5 to connect the hose (Figure 14).
In case there is no clean supply of compressed air available VLM can supply a silent compressor which meets
the requirements of the corrosion tests (Figure 16).
1 phase, 230 V mains (50 Hz) supply and consumes 700 W of the electrical power
The conductivity meter in the ion exchange cartridge 230 V
The water leak detector 230 V
Air compressor 230 V
14
The Controller
Figure 18 shows the main control panel with the touch screen, pilot lamps and main switches. The
controller is based on an advanced Jumo dTRON microprocessor controller.
Control light
compressed air (AWRF
and AIR option
Main switch
Toggle switch
Aeration/AT/AHT
(AIR option)
RS232 interface
(option)
15
2.
3.
4.
5.
Attention:
During the filling up of the test chamber with demineralized water the message niv appears
in the green display. When the water level reaches the normal value this message will
disappear. If for any reason the water level during the test drops below the default level this
message will appear again. In this case please check the water supply.
6.2. Setting Controller Parameters for the Water Condensation Test (CON)
Test chamber operates only common water condensation tests (CON). The test starts by pressing the Start
toggle switch (Figure 18) into the upper position. The test can be put on hold (timer is stopped but not
reset) by pressing the toggle switch into Stop position (0). Pressing the toggle switch again into the Start
position will continue the test (timer will continue counting down).
If the AWRF option is available (Automatic Water Refill system) the chamber will be automatically filled
with demineralized water to the required level.
After the CON test is finished the water can be drained from the test chamber by pressing the toggle switch
Start /Stop/Water Drain (Figure 18) into the lower position (Water Drain).
All parameters needed for the standard CON CH test are already stored (preconfigured) in the Jumo dTron
controller. These values are as follows:
16
CON CH test:
The default temperatures are (factory setting):
- Test chamber:
40 C
- Roof temperature:
always 1 C less than the chamber temperature
Important Note: In case the CWC option is available (VLMs patented Controlled Water
Condensation system) the control system will maintain a constant temperature gradient in
the test chamber of exactly T=-1 C between the bottom and the roof of the test chamber.
This gradient temperature is stored in the controller as a parameter (SPdA) and should not
be changed by the operator (should this be required please contact VLM). This implies that
the operator can/should change only the set temperature in the test chamber (SP). The roof
temperature will automatically follow and the temperature gradient of T=-1 C will be kept.
After setting the operating temperature there are two ways run the programmed tests. The first one is in
the so called User mode of the controller and the second one is in the Program (Pro) mode of the controller.
User mode:
In this mode the time of the test duration cannot be set and the test will run as long as the operator does
not stop the test manually. Please note that in this mode only CON CH test can be conducted! In case the
test parameters (chamber temperature) should be changed the operator must do it manually. There is no
time display showing either how long has the test been active or how much time until the end of the test.
During the normal operation of the test chamber the orange pilot lamps are illuminated and blinking.
Table 3 describes the procedure necessary to program the controller in the user mode.
Table 3 Programming procedure in User mode
Step
Mode
Press
PGM
Press
Display
indicator
CON CH
1
User
PGM
In2
CON CH
2
CON CH
3
4
Meaning
SP1
SP
CON CH
CON CH
trun
CON CH
trest
CON CH
5
SPdA
17
Step
Mode
Press
PGM
Press
Display
indicator
Meaning
Name of the controller mode
CON CH
CON CH
PGM
User
2x
PGM
Pro
CON CH
SPP1
CON CH
tP1
CON
AHT/AT
SPP2
CON
AHT/AT
tP2
Once the program has been configured it can be started by pressing the upper arrow on the controller.
The double point on the green part of the display will start blinking indicating that the test (time) runs. The
program can be stopped by pressing the same button on the controller once again.
Please note that normally the water remains in the chamber during the CON AHT/AT phase. Should CON
AHT/AT phase be conducted without water in the test chamber the Water Drain switch should be pressed
on the control panel.
The choice between the AHT and AT phase is made by pressing the toggle switch Aeration / AT/ AHT into
desired position.
18
6.3. Operation of the Kesternich Test with Manual Dosing System (DosiCORR MD)
VLM offers a cost effective system for conducting the Kesternich test by means of manual gas dosing system
DosiCORR MD). In principle this specific system can be fitted to any type of front loading VLM test chamber
designed to conduct (among more) Water Condensation test (CH, AT, AHT).
The Kesternich test is an extended version of the Water Condensation (CON CH) test in which the
predefined volume of the SO2 gas is introduced in the test chamber.
6.3.1. Principle of Operation
The lower container of the glass dosing unit is filled
with the Paraffin oil. This part is connected with the
upper part of the glass container by means of a
multi directional valve. After (manually) opening
the valve (red mark showing upwards) the SO2
flows under pressure into the lower part of the
glass container and the paraffin oil is displaced into
the upper glass container. When the Paraffin oil in
the upper container reaches the level mark
(typically 2 L volume mark) the needle valve has to
be closed.
Multi directional
needle valve
Paraffin oil
Be aware that sulphur dioxide (SO2) is liquid under pressure inside the steel bottle (gascylinder). Always put the gas-cylinder in an upright position and fix it tightly so that it cannot
under no circumstances topple over.
Never place the cylinder in a horizontal position! The liquid sulphur dioxide will flow out of
the bottle instead of the gas when opening the needle valve. The liquid SO2 will expand
instantly in the tubing and the glass container (gas metering device). This handling may result
in severe health hazards.
6.3.2. Putting KES System in Operation
Place the glass container (gas metering device) in the vicinity of the test cabinet. Make sure that it is in a
stable position and cannot topple over. Remove the multidirectional valve and fill the complete volume (ca.
2,5 L) of the Paraffin oil (use a funnel) into the lower part of the glass container (until the oil level reaches
the zero mark. Screw the multi directional valve back and connect the inlet and outlet hoses accordingly.
Connect the vent pipe at the top with the venting system, safety hood or directly to outdoor environment
so that SO2 gas can escape without any danger in case it bubbles through the paraffin oil.
19
Needle valve
20
Open the inlet to the glass dosing device. Turn the multi
directional valve into the position RED up.
2.
3.
Open the needle valve carefully until the SO2 starts slowly
flowing into the lower part of the glass container whilst the
Paraffin oil is being displaced to the upper container.
4.
5.
6.
Close the multi directional valve as soon as the Paraffin oil has
completely filled the lower container.
21
7. Commissioning
7.1. Preparation for Tests
Important!
Make sure that all supply and drain hoses have been connected properly and the fresh water
tap is open.
Press the green main switch and make sure that:
- The door is tightly closed
- The green pilot lamp is illuminated (compressed air supply)
- The chamber heater is on indicated by the orange pilot lamp.
Purity of the water
As mentioned before it is strongly advised to use demineralized water (ion-exchange cartridges) for DIN EN
ISO 6270-2 test. Always watch the conductivity on the measuring gauge and timely replace the cartridge by
a regenerated one.
Regard and treat this cabinet as a testing device. Keep it clean and make sure, that it will be serviced within
the set intervals.
Note that the inside of the test chamber is coated with ECTFE (Halar) which may only be cleaned by a soft
cloth and non-abrasive cleaning agent.
Remove any salt residues on the outer case with a wet cloth.
Protect the surfaces by applying cleaning and protecting sprays.
General Test Procedure
Never put specimens directly on the floor of the chamber.
Attention:
- Make sure that the compressed air at the required pressure is permanently available
(AIR and AWRF option).
- Check if the fresh water tap is open and the pure water supply is guaranteed all the
time
22
When ?
Clean the test chamber, but do not scratch the ECTFE coated base.
Check the door sealing for leakage and if necessary change it
Check the water filter inside the water inlet fitting at the back of the test
cabinet and change it if necessary
Check the filter inside the unit for compressed air, change it if necessary
Clean the drain system by rinsing pure water through the drain
Clean the outer case
Who?
monthly
monthly
quarterly
Operator
Operator
Operator
quarterly
monthly
monthly
Operator
Operator
Operator
In the course of time the elasticity of the silicon foam seal can decrease. Consequently there may be not
enough even surface pressure against the door / lid so the chamber will not be hermetically closed
anymore.
If the seal is damaged for chemical or mechanical reasons it has to be replaced. The seal can be removed
easily as it is not fixed in the gap by adhesives.
23
Description
Main switch 12 A
Switch air purge / spraying
Switch lightning
Clip connector 2 poles
Clip Connector 5 poles
Connector pin block 12 poles
Clip connector 3 poles
Clip connector 4 poles
Temperature controller JUMO dTRON 304
Pilot lamp green (pressure/ air
Pilot lamp yellow (heating/ventilation)
Pilot lamp red (over temperature/low level.
Filter for controller and timer
Relais
Relais
Solid State Relais (ELR/SSR)
Compact fluorescent lamp
Heater testing chamber
Temperature sensor testing chamber Pt 100
Description in the
circuit diagram
Q1
S2
S1
X2-X11
X2-X11
X2/X3/X5/X11
X2/X3/X5/X11
X2/X3/X5/X11
D1A/D1B/D1C
H 13
H1/H2
H3/H4
Z1
K5/K8
K2
V1/V2
E2
E1
B1
V.851.212.000
V.851.212.001
V.851.200.820
V.851.200.010
V.851.220.000
Accessories
Specimen rack 20 acc. To ISO 9227, 26 slits
gap 3,5 mm, length 550 mm
Specimen rack 15 acc. To ISO 6270-2 (High
Humidity CH Constant Humidity, 26 slits gap
3,5 mm, length 550 mm
S-hooks straight (10 Pcs/Unit)
S-hooks twisted by 90 (10 Pcs/Unit)
Specimen support rods
Cross connector
Special specimen holder for steel-discs
Specimen holder for very small specimens
Further individual holder, hooks upon
request
Accessories
24
1 Pc
11 Pc
1U
1U
1 Pc
1 Pc.
1 Pc.
-
1 Pc
V.852.210.100
V.852.221.003
25