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Abstract
This paper presents the results of X-ray scans in vuggyfractured limestone core studies to determine porosity rock
distribution and residual oil and water saturations for mexican
core samples. Iodine as the injecting fluid provided a means
for detecting water saturation and residual oil saturation. Xray Computerized Tomography (CT) was applied as an
approach for oil and water saturation determination. The
tracer (iodine) studies indicated that the water invasion
increases with time until to get conduction porosity.
CT
scans measure the density distribution inside of vuggyfractured cores and block models samples during X-ray CT
laboratory experiments. Firstly, an image processing method
for determining, simultaneously, some of basic geometrical
characteristics of homogeneous and vuggy-fractured porous
media such as secondary porosity, specific surface, mean pore
width, mean block thickness, mean fracture width, and
absolute permeability is applied in order to characterize the
core. Then, oil recovery mechanisms from vuggy-fractured
reservoirs were studied because of the large reserves contained
in such formations. The estimation of saturation of residual
oil is fundamental to oil recovery from vuggy-fractured
reservoirs under primary and enhanced recovery processes of
practical interest. Saturation of residual oil depends of several
petrophysical parameters such as conduction porosity,
stagnation porosity, cementation exponent and fluid properties
like viscosity of wetting and nonwetting phases. In this paper
we present our recent work on imaging dynamic
characterization in a vuggy-fractured core (calcareous) with
X-ray tomographic techniques.
We also perform forced
displacement experiment to get two liquid phases inside the
vuggy -fractured limestone core.
Introduction
In this paper some results are presented that the authors
tot =
(1)
Sf =
Vf
Vpc
(2)
So + S w + S g =
=1
Vo + Vw + Vg
=1
V pc
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FR = m
where m is the cementation factor.
.. (7)
(3)
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3 D Quantification of Vugs and Fractures Networks in Limestone Cores
3
unidirectional forced displacement of oil by water (forced
the stagnation porosity tends to zero and where it is not
imibition) like in oil secondary recovery processes that
possible the existence of traps because the blocks of
the total or effective porous space is divided in two great
solids lose cohesion.
domains: fluid flow channels and traps regions, like it is
The third postulate of the theory constituted it the
shown schematically in the Figure 1b.
Fluid flow
discovery that the equation of Maxwell-Fricke, can be
channels, indicated by the blue color, are those parts of
generalized easily, to make it applicable to vuggythe calcareous rock that really participate in the
fractured calcareous rocks, packings of particles in a
conduction of fluids and they are represented on the part
simple ways (cubes, spheres) and consolidated porous
of the vugs and part of the areas of micro fractures,
media, by means of the logical modification, firstly,
while the traps, indicated by the black color or letter T,
proposed by Prez-Rosales, consisting in substituting
are stagnation regions and they are represented as
the effective porosity for the porosity of conduction of
porosity areas, however, they don't participate in the
fkuids defined by the Equations 8 and 9.
In
displacement of the oil by water and they are strongly
consequence, the third postulate can be expressed as
related with the saturation of residual oil at the end of the
folowws:
experiment.
G 1 con
(10)
FR = 1 +
con
The traps are not necessarily constituted by closed vugs
where G is a general form of the parameter P of the
in one of their ends, like one can observe in Figure 1b,
but rather they can also consist on open spaces, but that
Eq.5. Combining the Equations 9 and 10, we arrive to
the interesting relationship
for symmetry reasons they generate stagnation regions,
m
like it is illustrated in the same Figure 1b.
Here the
FR = 1 + G con 1
(11)
region indicated by black color could not drive fluids, due
This
is
a
formula,
proposed
by
Prez
-Rosales
in
1981
to the equality of local conditions of pressure that exist in
that it allows to put on approval the theory developed for
the two nearer channels.
Because of these
vuggy -fractured calcareous rocks, since so much FR as
observations, on the displacement of oil by water, the
con both can be measured in the X-rays tomography
first postulate of the theory establishes that the total
laboratory.
porosity can be divided in two main parts: a porosity of
(8)
con = tot
(9)
FR = G con
+ (1 G )
(12)
-m
FR = G con
(13)
tot =
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(16)
con = totm
(9)
m
est = tot tot
(17)
Graphing relationships as of the equations 9 and 17, for
different values of the cementation exponent m, it has
been observed that they have problems when they try to
interpret values of total porosity tot in the limits of the
values reported in the literature, mainly for further values
that the critical porosity and smaller than the porosity of
percolation. It influences of the porosity of percolation
and the critical porosity.
The physical limits of porosity, so that the flow of fluids
exists inside sedimentary rocks, they are given by two
porosity limits: the porosity of percolation and the critical
porosity. These limits define three physical regions of
porosity of a porous medium (fractured, vugged or
homogeneous), and they are particular for each
reservoir, well, core or study rock.
These regions can be detected by means of several
techniques in the laboratory of X-rays tomography where
we combine the techniques of X-rays tomography and
those of displacement of fluids.
Physically, the characteristics of these three regions are
separated by the characteristics peculiar of porosity of
conduction of fluids and of the porosity of stagnation for
each case of study. In the same way, had processed of
image, a special study of the analysis of the isolated
porosity would be taken to deduce if it is important or not
to take it into account, mainly in limestone and dolomite
cores that come from fields with information of a strong
dolomitization influence.
Next each one of the three
regions will be described (Wompe,2000):
The region I is defined for smallest porosities that the
porosity of percolation where the porous space is not
connected by nets of conduction of fluids, that is to say,
in this region the porosity of conduction of fluids it is very
low or zero, con=0, therefore, the permeability also is
zero. Here, it is considered that the total porosity is very
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3 D Quantification of Vugs and Fractures Networks in Limestone Cores
5
low nevertheless it will be associated to the porosity of
Relationship between porosity of conduction con
stagnation tot = est , inside this region, the fluids cannot
and total porosity tot.
be transported inside the porous media, because the
As it was discussed in the previous section, the region II
total porosity is too small to the required minimum value
is limited by the porosity of percolation and the critical
so that percolation of fluids needs. In this region, the
porosity, this region is the correct one that more interests
value of the factor of electric resistivity is infinite and that
has for the petroleum engineer, since in his work where
of the hydraulic permeability is zero, kw=0.
the porosities of conduction of fluids and that of
stagnation coexist.
The region II is defined by the porosities that are located
Considering the exposed ideas, the relationship between
inside the limits of porosity of percolation and critical
conduction porosity and total porosity, proposed by
porosity, where the total porosity is, partly,
Prez -Rosales, would modify in the following way:
interconnected and it is a growing function. It has been
con = A(tot per ) m ,..., per tot cri
(19)
observed in some cases, mainly in granular clastics
(breccias, sandstones and shales) that the stagnation
per
A=
,..., per tot cri
(20)
porosity exists and it has high values, since values have
tot per
been reported until of 70% of the total porosity. Because
not the whole porosity is available for the flow of fluids in
where
this region, the value of porosity of conduction of fluids
A is numerically a parameter that depends on the
should be considered accurately and as a consequence,
petrophysics of the formation, it is a factor that climbs
that of total porosity and of stagnation for a core in study.
the porosity values inside the limits of percolation
The permeability of the porous media will depend on the
porosity and critical porosity.
It depends strongly on
quantities of porosity of conduction of fluids regarding
measured properties by the petrophysics (forms and
the stagnation porosity, that is to say, of others
distribution of blocks sizes, cementation, dolomitization,
petrophysical parameters of the porous media such as:
compaction,...), of the rock.
clay content, cementation, dolomitization, compaction,
This way, in some authors they show graphic of several
fracturing, deposit of asphaltenes and; sorting (forms
values of the exponent m using the modified expression,
and distribution of pore sizes and matrix blocks).
respecting the initial conditions of the regions I and III in
The region III is defined for higher porosities that the
terms of conduction porosity, stagnation porosity, of
critical porosity, in which, the grains or matrix blocks
permeabilities and of resistivity factors. Also, it is
begins to be in suspension and the whole porous space
demonstrated at same time that the empiric relationship
is not only connected, but rather it participates in the
of Gal et all is a peculiar case of the proposed
conduction of fluids. The above mentioned is translated
relationship, with the following quantities: porosity of
in that the stagnation porosity is very low or zero est =0,
percolation per =0.021: critical porosity cri=0.54: and
the conduction porosity grows lineally from the value
m=1.38. In this same order of ideas the Equation of
Prez.Rosales (Eq. 11), it is conserved in their original
reached in cri up to 1, in this case: m = 1, tot =con, the
terms except that we were put the porosity limits, so the
permeability in this region is infinite and the factor of
electric resistivity only depends on the conduction
modified equation is
porosity of fluids and not of the other parameters of the
For region II
porous space like sorting (forms and distribution of grain
m
size), clay content, dolomitization, fracturing and
FR = 1 + G con 1
per=tot =cri(21)
asphaltenes deposition.
2
In the table 3 it is shown the main characteristics of the
FR = 1 + G A m ( tot per ) m 1
per=tot =cri (22)
three regions of flow of fluids schematically.
where
Taking into account the porosity concepts described
per
above, these model could only be applied to any
A=
,..., per tot cri
(23)
sedimentary rock, for what the modified relationship for
tot per
the estimate of the total porosity tot as the sum of the
porosity of conduction of fluids, the porosity of stagnation
and the isolated porosity, but subject to three porosity
For region I
domains, as it is the region of interest. This relationship
is the following: (Figures 27 and 28).
0=tot =per
(24)
FR =
FR = ( A(con per ))
cri=tot =1 (25)
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tot =
CTosatob CTdryob
CToil CTair
(26)
where CT denotes the CT value for each voxel, crosssection or core and the subscripts osatob, dryob, oil, air
and tot refer to the oil-saturated core, air-saturated core
or dry core, oil CT number, air CT number and, total
porosity, respectively, (Figure 4).
Partial oil saturation profiles during forced imbibition may
be constructed from raw CT data according to equation
S oil =
CTpsatob CTdryob
CToil CTair
(27)
where CT denotes the CT value for each voxel, crosssection or core and the subscripts posatc, dryob, oil and
air refer to the partially oil-saturated core, air-saturated
core or dry core, oil CT number and air CT number,
respectively. Oil and air CT numbers are calibrated as
0 and 1000, respectively, (Figure 5).
Unidirectional forced displacement of oil by water
experiment
The core is taken as described above when the first step
finished.
For counter-current forced imbibition, pure
water is introduced to the core through the end cap by
pumping water through this end cap at a rate of 10
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3 D Quantification of Vugs and Fractures Networks in Limestone Cores
7
cm3/minute, forcing a unidirectional displacement of oil
by means of the injection of solvents during two days
by water with the core completely saturated with crude
and then it was dried in oven at 70C during one day,
oil (as nonwetting phase). Later, after 73 hours, the
until achieving a version of core denominated dry core.
saturated core is scanned every 2mm in same positions
We were carried out a tomographic plan and we
as the dry and oil saturated core versions and in
proceeded to scan each preset distance interval, the
agreement with the scans plan. Finally, the conduction
usual sampling interval is of an image every 2 mm of
porosity is estimated, and then the stagnation porosity
distance, for simplification in the Figure 3, is shown a set
(or saturation of residual oil) is estimated.
of only 10 images, 1 every cm is presented for the dry
As future work, we will collect images periodically
core data. Later on, we proceeded to saturate the core
throughout the duration of the second experiment.
with a reference fluid, in this case, crude oil of the field
was chosen, because in a second saturation experiment
Because values of 100% water and oil filled core are
we proceeded to carry out a displacement of this crude
available from calibration, two images of conduction and
oil by distilled water, until achieving a version of core
stagnation porosity for each voxel, cross-section or core
denominated core saturated with oil to 100%. Then, we
can be estimated from the next equation
proceeded to scan every distance interval preset
according to the tomographic plan and, the sampling
wsatob
osatob
interval was of an image every 2 mm of distance, for
con
(28)
simplification in Figure 4 .the same set of 10 X-rays
water
oil
images of saturated core is presented, one for each cm.
As a following step of the developed methodology,
the distribution of total porosity of each digital image was
(29)
est
tot
con
ro
calculated, this way in the Figure 5 the same set of 10
where CT denotes the CT value for each voxel, crossimages of total porosity is presented, which was
section or core and the subscripts wsatob, osatob,
obtained by means of the arithmetic difference, pixel to
water, oil, con , est and Sro refer to the water-saturated
pixel, between the dry and oil saturated images, (Figures
core, oil-saturated core, water CT number, oil CT
3 and 4), the Figure 5 was the image-result of applying a
number, conduction porosity, stagnation porosity and
porosity equation, it ranges from 0 untol 100 units.
residual oil saturation, respectively.
Then, by means of image processing tools, we
segmented this set of porosity images in three regions
Partial water saturation profiles during forced imbibition
corresponding to different porosity: vugs region, micro
may be constructed from raw CT data according to
fractures zones and unsat urated regions. In Figure 6
equation
the set of 10-segmented images is presented starting
from the set of images of dry core of the Figure 3. The
CT pwsat CT posat
segmentation approach was the way of separating the
S water =
(30)
zero density population because of the contained air
CTwater CToil
3
inside the vugs of dimensions greater than 1x1x2 mm .
where CT denotes the CT value for each voxel, crossWith this resolution, the X-rays scanner is an excellent
section or core and the subscripts pwsat, posat, water
equipment to map vugs population directly. In this way,
and oil refer to the partially water-saturated core,
the vugs cartography is achieved, for what comes off a
partially oil -saturated core, water CT number and oil CT
vugs definition to differentiate it of the micro fractures
number, respectively. Oil and water CT numbers are
population that we establish that a vug is that internal
calibrated as 0 and 3000, respectively.
structure of a calcareous sedimentary rock whose value
The CT scanner is a Picker IQ Premier X-rays scanner,
density is zero and whose dimensions are bigger than
3
with 1200 detectors.
The voxel dimension is
2mm , both parameters are determined in the X-rays
0,4x0,4x2mm3.
The tube current is 120 mA.
The
tomography laboratory.
average level of radiation is 140 keV. The acquisition
In the Figure 7 the set of 10-segmented images is
time of one digital image is 2 seconds while the
presented starting from the set of 10 images of oil
reconstruction time for an image is 22 seconds.
saturated core of the Figure 4.
The segmentation
approach was the one of separating the saturation of
Results on limestone cores
100% of crude oil, associated to the containe d fluids
The analyzed base data for the conclusions it was
inside the vugs micro fractures from of unsaturated
1600 X-rays digital images corresponding to 16 different
areas related with matrix blocks of variable dimensions,
cores.
that is to say, in this Figure 7 the division is presented of
In this section the main results of the exposed
the rock-fluids system in areas of flow of fluids and
theoretical ideas are presented.
As entrance fact we
unsaturated areas.
dispose of rock core like the one shown in the Figure 2,
The two previous results represent the most
whose longitude is 10 cm and its diameter is 5,4 cm.
important conclusions in our investigation, since the
Firstly, we proceeded to carry out a cleaning of the core,
population of areas of flow of fluids can be directly
CT
CT
CT
CT
=S
p=
l
c/ 2
(31)
g=
1
p
(32)
The mean pore width and the mean grain thickness can be
expressed in terms of the porosity and the specific surface.
p=
4
Ss
(33)
C
C3
3
2
k= p = 2 =
g
16
(1 ) 2
Ss
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p and g ,
(34)
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3 D Quantification of Vugs and Fractures Networks in Limestone Cores
9
of we have worked with dry core data. This implies that
performed by an examination of gray level variations
more than 4/5 of the vug networks were composed of
according to the method suggested. We have shown how the
only one independent path between any two points
method for region or contour extraction provides attributes
within the vug space (Figs. 24 and 26). However, when
which allow to distinguish the pixels liable to belong the vugewe worked with oil saturated core data, for the same
grain contact from the rest of the image information.
core, it was found that 90% of the vug networks had
some hydraulic connectivity among them (Figure 25).
Nomenclature
This implied that more than 9/10 of the vug networks
L = total length of the grid lines
were transformed in effective porosity as it was
m =cementation exponent
experimentally previewed.
n =number of grid nodes within pore areas
N =total number of grid nodes or pixels
Conclusions
tot =total porosity
In this paper some results about static and dynamic
con =Porosity od conduction of fluids
characterization
of
vuggy-fractured
calcareous
est =Stagnation porosity
sedimentary rocks were presented, using X-rays
ais =Isolated porosity
tomography and displacement of fluids in laboratory.
per =Percolation porosity
cri =Crirical porosity
The distribution of total porosity of each X-rays digital
Ss =specific surface
image was calculated.
Then, we segmented this
p =average pore width
porosity image in three regions of interest with different
porosity meaning: vugs, microfractures and unsaturated
g =average grain thickness
blocks.
A following process led to the calculation of
k =absolute permeability
specific surface of vugs and flow areas, of average
c =number of intersections between grid lines and
thickness of vugs, flow areas and microfracture areas;
the perimeter of the pores
as a last calculation we carried out estimates of absolute
C
=constant
of proportionality in Koseny equation
permeability.
In a second stage we were carried out unidirectional
displacements of crude oil by pure water in a field core
to estimate the relationship of porous space that
participates in the flow of fluids regarding stagnation
areas, with that which was corroborated and the theory
developed by Prez-Rosales and now adapted to ours
objectives. We arrived to a quantitative estimate of the
saturation of residual oil.
In the part of results, several segmented images
were presented, where it is observed the enormous
influence of the vugs population as oil stocking part and
microfractures system as a fluid conductive part of
matrix-vug-microfracture of calcareous rocks of mexican
offshore productive formations.
The most important
conclusion in this study is that the original volume of
such reservoirs could be increased due to the increment
of the vug porosity from 8 to 25% and of the permeability
magnitude that we report and it represents an
opportunity area for the enhanced oil recovery methods.
The segmentation procedure is very simple. The data required
to calculate the various geometrical characteristics can be
easily measured. The results can be made as precise as
desired. Precision depends upon the resolution of the digital
image. The formulas presented here offer a variety of
functional relationships that can be used to develop other
experimental procedures for analyzing fractured porous media.
The notion of mean pore width, and mean grain thickness, as
defined in the paper, are important because they lead to
correlations of experimental interest. The segmentation into
consistent regions and the contours extraction can be
Acknowledgements
The authors wish to express his appreciation to the
management of the Mexican Petroleum Institute for
permission to publish this paper.
References
1.-
10
SPE77780
SI Metric Conversion
cp
X
ft
X
ft 2
X
ft 3
x
in
X
md
X
psi
X
factors
1.0000*
2.0480*
9.2903*
2.8317*
2.5400*
9.8602*
6.8948*
E-03= Pa s
E-01= m
E-02= m2
E-02= m3
E 00= cm
E-04= m2
E 00= kPa
Figure 1b
Result of the second step of the
experiment, the unidirectional (from up to down) forced
displacement of crude oil by pure water. Presentation
of a ternary image where white color represents
unsaturated areas, black color represents crude oil
stagnation areas (saturation of residual crude oil), while
the blue color represents water flow areas. The white
regions are considered as unsaturated regions, since
SPE 77780
3 D Quantification of Vugs and Fractures Networks in Limestone Cores
11
any fluid (crude oil or water) didn't penetrate after two
the union of both, vugs and microfractures regions.
sessions of saturation laboratory procedures with crude
oil and pure water. The regions marked as blue color
represent the porosity of conduction of fluids.
Figure 5
Set of the 10 images of total porosity,
which was obtained by means of the arithmetic
difference between the dry and saturated images from
the figures 3 and 4, this is called porosity image in gray
(arbitrary colors) levels.
12
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SECONDARY POROSITY
60
POROSITY (%)
Figure 8
Set of 10 segmented binary images
starting from difference between the segmented sets of
Figures 6 and 7.
The segmentation approach was the
one of separating the population of microfractures areas
(black color) from vugs and unsaturated blocks (white
color).
Figure 10
Set of 10 segmented binary images,
representing the specific surface of the flow zones from
Figure 7. The segmentation approach was the one of
separating the contact (lack color) between the
population of unsaturated areas of the permeable ones.
The contour length of fl ow regions Cflow could be
estimated in cm, so the specific surface of the flowing
population is Ss=Cflow/Vu, where Vu=18.323cm3.
50
40
flow zones
30
vugs
20
microfractures
10
0
1
10
vugs
microfractures
11
matrix block
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13
SPECIFIC SURFACE
POROSITY DISTRIBUtION IN
TOTAL CORE VOLUME
0.4
0.3
Ss
1
2
3
flow Ss
0.2
vugs Ss
0.1
microfractures
Ss
100%
microfractures
11
matrix-blocks
12
10
8
6
4
2
0
flow zones
vugs
microfractures
vugs
0%
MEAN THICKNESS cm
MEAN THICKNESS
50%
1
2
3
3.5
3
2.5
2
1.5
1
0.5
0
flow zones
K vugs
microfractures
Permeability
milliDarcy
PERMEABILITY
14
SPE77780
3.
250
200
150
length vug
100
50
72
45
35
27
22
17
13
mm
Rango 5
180
160
140
Frecuencia
120
100
Rango 4
80
60
40
20
0
0.83
6.60
12.37
18.13
23.90
29.67
35.44
41.20
46.97
52.74
58.51
Rango Volumen
vugs
reconstruction
from
60
Frecuencia
Rango 6
10
9
8
7
6
5
4
3
2
1
0
Rango 6
0.83
0.89
0.95
1.00
1.06
1.12
1.18
1.23
1.29
1.35
1.41
Rango Volumen
551
501
451
401
351
301
251
201
151
101
51
80000
60000
40000
20000
0
1
mm3
(b)
Figure 26. (a) A second example of 3-D reconstruction
from 100 consecutive segmented images with vug zones
in the limestone core. In this case we found 355 vug
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3 D Quantification of Vugs and Fractures Networks in Limestone Cores
15
networks (b) the biggest segmented vug.
limestone
1
51
50
dolomite
1
51
50
Table 3 Description of the characteristics of the three
regions of flow of fluids.
R
I
tot
0=tot<per
con
0
est K, FR
?0
0, 8
II
per=tot =cri
?0
?0
f (tot ),
f (,m,G)
III
cri <tot=1
?0
8 , f(con )
Porous medium
Tie homogeneous
Sedimentary rock
Clastic sedimentary
rock
Vuggy -fractured rock
Some Sediments
Sediments
16
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