Documenti di Didattica
Documenti di Professioni
Documenti di Cultura
3
4
Course
Engineering
Chemistry-II (IS-1)
Engineering
Mathematics-III
(IS-2)
Solid Mechanics (IS3)
Chemical Engineering
Materials
(CS-1)
Unit Processes (CS-2)
TOTAL
Code
Credits
Examination Scheme
CY 201
Theory
Sess
Hr
ional
2
50
MH 210
50
25
50
---
---
125
AM 203
50
---
50
20
30
150
CH 201
50
25
50
---
---
125
CH 203
3
22
3
17
0
3
0
4
50
250
--75
50
250
--40
--60
100
675
Tu
Pr
25
End
Sem
50
Practicals
Sess
End
ional
Sem
20
30
Tota
l
Mar
ks
Tu
Total Credit = 22
175
Course
Electrical
Technology
(IS-1)
Engineering
Chemistry-III
(IS-2)
Theory of Machines
and Machine Design
(IS-3)
General Chemical
Technology
(CS-1)
Process Calculations
(CS-2)
TOTAL
Code
Credits
Theory
Tu
Pr
Hr
Total
Marks
---
End
Sem
50
Practicals
Sess End
ional Sem
20
30
150
EE 214
Sess
ional
50
CY 202
50
25
50
20
30
175
ME 214
50
25
50
20
30
175
CH 202
50
25
50
20
30
175
CH 204
50
25
50
---
---
125
23
15
250
100
250
80
120
800
Total Credit = 23
Tu
SEPARATION METHODS
(06 Hours)
Concepts of precipitation, fractional distillation, fractional crystallization, electrodeposition, electrodialysis, reverse osmosis, distribution (partition co
efficient), Chromatography Basic concepts; paper
chromatography and thin layer chromatography with suitable examples.
CHEMICAL ANALYSIS OF WATER
(04 Hours)
Specifications of water; cooling water (Langelier Index and its treatment); tertiary waste water treatment;
introduction to heavy water and rain water harvesting.
ORGANIC CHEMISTRY
(11Hours)
Preparation, properties and uses of alcohols (ethanol, ethylene glycol, glycerol).Carbohydrates
structures, stereochemistry and reactions of monosaccharides (glucose and fructose), disaccharides
(sucrose and maltose), polysaccharides (starch and cellulose). Peptides and proteins - general methods of
protein structure determination with suitable examples; introduction to enzymes. Basic concepts of drug
design; some drug types (antimalarials, antibiotics, antiseptic), structure and synthesis; antimalarials (4 and
8 anthraquinolines), antiseptics, antibiotics (chloramphenicol, peniclillin). Newer concepts of dyes
development/high-tech dyes (Liquid crystalline,fluorescent, biomedicinal dyes), natural and photochromic
dyes.
INSTRUMENTAL METHODS OF CHEMICAL ANALYSIS
(06 Hours)
Instrumental methods of chemical analysis (Basic concepts and relevant applications); Spectroscopic
methods IR, UV- Visible, and fluorescence spectroscopy. TGA, DTA, DC polarography. Significant
figures and expression of data.
POLYMERS
(06 Hours)
Engineering polymers, plastics, composites and their characterization. Novel functional polymersprocessing and applications.
NEW APPROACH IN CHEMISTRY
(06 Hours)
Green chemical technology with few examples. Photochemical reactions: basic concepts and relevant
Examples. Some aspects of supramolecular chemistry
REACTIONS AND MECHANISMS
(06 Hours)
Organic reactions and mechanisms: types of organic reactions; general methods of getting mechanisms,
mechanism of ionic, free radical and isopolar reactions
(Total Contact Hours: 45)
PRACTICALS:
1. Separation of SO42- from NO3- by BaSO4 precipitation.
2. Determination of total dissolved solids in a given water sample by Conductometric method.
3. Separation of Cu2+ from Ni2+ by Electrodeposition.
4. Spectrophotometric analysis of any two important impurities of water like Ca2+, Mg2+, Fe2+, NO3- ,
NO2-, PO4-3, CO3-2, Cl-, SO4-2
5. Organic spotting of Salicylic acid, Naphthalene, Aniline, Glycerol etc.
6. Electrogravimetric analysis of Cu in Non-ferrous alloys like brass.
7. Estimation of HCl and HAc using Conductometric acid base titration.
8. Coulometric titration of As2O3 by Internal generation of I2.
9. Separation of Amino acids by Paper Chromatography.
10. To determine the specific rotation of given substance using different concentration of sucrose.
BOOKS RECOMMENDED:
1.
2.
3.
4.
5.
6.
Chawla S., Text Book of Engineering Chemistry, Dhanpat Rai & Co. Pvt. Ltd., Delhi, 2003.
Sharma B. K., Engineering Chemistry, Krishna Prakashan Media (P) Ltd, Meerut.,2001
Ewing G. W., Instrumental Methods of Chemical Analysis, Tata-McGraw Hill., New Delhi, 2001.
Khopkar S. M., Basis Concept of Analytical Chemistry, New Age International Publishers, 1998.
Vogel A. I., A Text Book of Quantitative Chemical Analysis, ELBS UK, 5th Edition, 1996.
Billmeyer F. W., A Text Book of Polymer Science, Wiley Interscience, New York, 3rd ed., 1984.
FOURIER SERIES
(06 Hours)
Definition, Fourier series with arbitrary period, in particular periodic function with period 2 . Fourier series
of even and odd function, Half range Fourier series.
COMPLEX VARIABLES
(08 Hours)
Basic mathematical concept, Analytic function, C R equations, Harmonic functions, its applications,
Linear transformation of complex domain, some special transformation, bilinear transformations, conformal
mapping and its application, complex integration including contour integration.
BOOKS RECOMMENDED :
1.
2.
3.
4.
5.
Kreyszing E., Advanced Engineering Mathematics, John Wiley & Sons, Singapore, Int. Student Ed. 1995.
Wiley C. R., Advanced Engineering Mathematics, McGraw Hill Inc., New York Ed. 1993.
ONeel Peter., Advanced Engg. Mathematics, Thompson, Singapore, Ind. Ed. 2002.
Greenbar Michael D., Advanced Engg. Mathematics, Pearson, Singapore, Ind. Ed. 2007.
Ramana D. V., Higher Engg. Mathematics, The MaGraw-Hill Inc., New Delhi, 2007.
PRACTICALS
1. Tension Test on MS and CI specimens
2. Torsion Test on MS Specimen
3. Charpy Impact Test
4. Transverse Test on Wooden beam
5. Spring Test
6. Compression test on CI Columns
7. Shear Strength Test
8. Hardness Test
BOOKS RECOMMENDED:
1. Timoshenko S & Young D H Elements of Strength of Materials, Tata Mc Graw Hill, New Delhi, 2006.
2. Ryder G H, Strength of Material, English Language Book Society, New Delhi,2006
3. Bhavikatti S S Strength of Materials, Vikas Publication House, New Delhi,2007
nd
4. Egar P. Popov & Toader A . Balan Engineering Mechanics of Solids 2 Edition, Prentice Hall of India
Pvt Ltd, New Delhi,2002
5. Beer F. P. & Johnston S J, Strength of Materials Tata Mc Graw Hill Publication, New Delhi,2004
(06 Hours)
(04 Hours)
(07 Hours)
Crystalline and non-crystalline ceramic systems, Glass and porcelain enamels, Cement refractories, Ceramics.
CORROSION AND ITS PREVENTION
(08 Hours)
Protective coatings, chemical principles involved. Factors determining the choice of materials of construction in
chemical industries.
(Total Contact Hours:
45)
BOOKS RECOMMENDED:
1. ZasterZebski D., Nature and Properties of Engineering Materials, John Wiely & Sons, 2nd Edition, 1976.
2. Rumford F., Chemical Engineering Materials, Constable and Company Limited, 2nd Edition, 1987.
3. Vlack V., Elements of Material Science & Engineering Structures, Properties and Performance, Wesley
Publishing Company, 2nd Edition, 1964.
4. Chaudhry H., Chemical Engineering Materials Indian Book Distributing Company, 2nd Edition, Delhi, 1982.
5. Lee and Evans, Selecting Engineering Materials for Chemical and Process Plants, Business Works, 1978.
NITRATION
(5 Hours)
Definition & scope of nitration reactions, Nitrating agents, Aromatic Nitration (schimid and Biazz;
nitrators)mixed acid for nitration, D.V.S. value and nitric reaction, Comparison of batch Vs. Cont. nitration,
Mfg. of Nitrobenzene, Dinitrobenzene, O-and P-Chloronitrobenzene.
AMINATION BY REDUCTION
(6 Hours)
Definition & scope of Amination reactions, various methods of reductions and factors affecting it, Batch
and Cont. process for manufacture of Aniline from Nitrobenzene, Cont. process for Mfg. of Aniline from
nitrobenzene using catalytic fluidized bed reactor, M/c. in such processes.
HALOGENATION
(6 Hours)
Definition and scope of various halogenation reactions, Halogenating agents Industrial halogenation with
types of equipments and its materials M/c. MFG. of Chlorobenzene, Benzene hexa-chloride and vinyl
chloride from Ethylene and Acetylene.
AMINATION BY AMMONOLYSIS
(3 Hours)
Definition & types of reactions, Aminating agents, Physical and Chemical factors affecting it. Catalyst used
in Ammonolysis, Mfg. of Aniline from chlorobenzene and Nitroaniline from Dichloro Nitro Aniline.
OXIDATION
(5 Hours)
Definition and Types, Oxidizing agents, Liquid phase oxidation with oxidizing agents and oxygen. Oxidation
of toluene with MnO2. Mfg. of Acetaldehyde from Acetic acid and mfg. of Acetic acid from Ethanol. Vapor
phase oxidation of Methanol, Benzene and Naphthalene, Apparatus and its M/s. for oxidation reactions.
HYDROGENATION
(5 Hours)
Definition and its scope, properties of hydrogen and sources of hydrogen, gas catalytic hydrogenation and
hydrogenolysis, factors affecting it, Apparatus and M/c., Industrial hydrogenation of fat & oil, Mfg. of
Methanol from CO2 & H2.
HYDROLYSIS
(3 Hours)
Definition and types of hydrolysis, Hydrolyzing agents, equipments of hydrolysis, Industrial Hydrolysis of
fat, hydrolysis of carbohydrates, starch to dextrose, Mfg. of ethanol from ethylene (shell process) Mfg. of
phenol from benzene sulfonic.
POLYMERIZATION
(5 Hours)
Introduction & chemistry of polymerization reactions, classifications of polymers methods of polymerization.
(Total contact time : 45 Hours)
BOOKS RECOMMENDED:
1. Groggins P. H., Unit Processing of Organic Synthesis, 5th edition, Tata-McGraw Hill, New Delhi, 2001.
2. Gopalarao. M. & Sitting M., Drydens Outlines of Chemical Tech., 2nd Ed., East-West Pub., New Delhi,
1997.
3. Austin G. T., Shreves Chemical Process Industries, 5th Ed. McGraw-Hill Pub., 1994.
4. Felder R.M., Rousseau R.W., "Elementary Principles of Chemical Processes", 3rd ed., John Wiley, New
York, 2000.
5. Kent J.A., Riggels Handbook of Industrial Chemistry, Van Nostrant Reinhold, 1974.
D.C. MACHINES
( 08 Hours)
Construction, windings, EMF, torque and power equations, circuit model, Generating and Motoring modes,
introduction to armature reaction, Types of generators and motors and their characteristics, Efficiency and
Losses, Speed control of D C motors
TRANSFORMERS
(07 Hours)
Review of equivalent circuit, no load and short circuit tests, per unit system, voltage regulation, Efficiency,
Auto-transformer, three phase transformers, star and delta connection.
INDUCTION MACHINE
( 06 Hours)
Review of equivalent circuit, torque speed characteristics, No load and blocked rotor tests, load test,
efficiency and losses , starting, Braking & speed control.
SYNCHRONOUS-MACHINE
(07Hours)
Construction and basic principals, EMF equation, Synchronous speed, armature reaction, synchronous
reactance, voltage regulation, vector diagram for generating and motoring modes, synchronous motor
starting, Synchronous condensers.
SPECIAL MACHINE
Hours)
applications of Servo motors, Stepper motors.
(06
Theory, performance and
PRACTICALS:
1.
Speed control of D.C. shunt motor.
2.
Speed Torque Characteristics of D.C. Shunt motor.
3.
D.C. Series motor N.T. characteristics.
4.
D.C. Generator Characteristics.
5.
Efficiency and regulation of 1 phase Transformer from O.C. and S.C. test .
6.
Load test on Induction motor.
7.
Circle diagram.
8.
Regulation of an alternator by synchronous impedance method.
9.
V and inverted V curve .
10.
Calibration of single phase energy meter.
BOOKS RECOMMENDED:
1
Mehta, V.K.,Principles of Power System S. Chand & Co., New Delhi, 2005
2
Husain A., Fundamentals of Electrical Engineering, Dhanpat Rai & Co., Delhi, 2001
3.
Bimbhra P.S., Electrical machinery ,Khanna Pub.,Delhi,1998
4.
Mukherjee P.K., Chakravorti S. ,Electrical Machines Dhanpat Rai & Co., Delhi, 2001
5.
Thereja B.L., & Thereja A.K., A Text Book of Electrical Technology, S. Chand & Co., New Delhi, 2005
CHEMICAL KINETICS
(04 Hours)
Chemical equilibrium, determination of rate and order of reaction, ultra fast processes, kinetics of enzyme
catalysis
THERMODYNAMICS
Laws of thermodynamics, Clapeyron clausius equation, carnot cycle
SURFACE CHEMISTRY
(05 Hours)
Roughness and friction lubricants, absorption adsorption isotherms, catalysis, surface characterization,
organic assemblies; synthesis, structure, property and application of nanoparticles
A.FUELS
(10 Hours)
Classification, characteristics, combustion, calorific value and its determination by Bomb and Bouys
calorimeters, theoretical calculations by Dulong formula, analysis of coal and fuel gases, fuel cells, H2 as
fuel and biofuels
B.NUCLEAR CHEMISTRY
Nuclear fission and fusion, nuclear energy, nuclear reactors, disposal of nuclear waste, radiation
measurement and contentment
(10 Hours)
(04 Hours)
PRACTICALS:
1. Rate determination of chemical reactions.
2. Conductometric rate determination of esterification reaction.
3. Potentiometric estimation of Cu+2 by titration with EDTA.
4. Photometric estimation of Ti.
5. Estimation of Cu+2 by iodimetric titration.
6. Viscosity measurement.
7. Study of Corrosion of Steel at different concentration of Sulfuric Acid OR
Study of effect of inhibitors on corrosion of steel in sulphuric acid.
8. Demo: 1. Effects of removal of DO on corrosion.
9. Demo: 2. Anodic protection of steel in sulphuric acid.
BOOKS RECOMMENDED:
1.
2.
3.
4.
5.
Atkins P. & de Paula J., Physical chemistry, Oxford University Press, UK, 2002.
Chawla S., Text Book of Engineering Chemistry, Dhanpat Rai & Co., Delhi, 2003.
Dara S. S., A Text Book of Enginering Chemistry, S Chand & Sons., New Delhi, 2004.
Fontana M. G., Corrosion Engineering., Tata-McGraw Hill, New Delhi,1988.
Skoog, West & Holler,Analytical Chemistry: An Introduction, 6th edition, Saunders College Publishing,
1994.
THEORY OF MACHINES:
CAMS
(06 Hours)
Introduction, Types of Cams, Types of Followers, Cam Terminology, Displacement Diagrams, Motions of
the Follower, Drawing of Cam Profile.
GEARS
(05Hours)
Different Types of Motion Transmitting Elements, Advantages and Disadvantages, Types of Gears and
Gear trains, Gear Terminology and classification.
FRICTION
(05 Hours)
Introduction to Friction, Significance of Friction, its Merits and Demerits, Application of Friction to Screw
Jack, Bearings, Breaks, Clutches etc.
MACHINE DESIGN:
DESIGN PROCESS, MATERIAL SELECTION, FACTOR OF SAFETY, FAILURES & THEIR CAUSES
(07 Hours)
Introduction, Types of Load, Design Process, Material Selection, Factor of Safety, Failure and Their
Causes, Introduction to Corrosion (Design Aspect).
DESIGN OF JOINTS
(07 Hours)
Introduction, Different types of Joints and Their Applications, Design of Bolts and Rivets joints, Design of
Screw Joint, Design of Welded Joints (Efficiency & Strength).
PRACTICALS:
Design and Drawing of various machine elements using conventional methods and few drawing sheets will
be prepared using CAD software.
BOOKS RECOMMENDED:
1.
2.
3.
4.
5.
Rattan, S.S.: Theory of Machines, Tata McGraw-Hill Publishing Co. Ltd., New Delhi, 1984.
Rao, J.S., and Dukkipati, R.V.: Mechanism and Machine Theory, Wiley Eastern Ltd., 1992.
Green, W.G.: Theory of Machines, 2nd Ed., Balckie, London, 1992.
Bhandari, V.B.: Design of Machine Elements, Tata McGraw-Hill Publishing Co. Ltd., 1984.
Shigley, J.: Mechanical Engineering Design, McGraw Hill Book Co., 1989.
CHLOR-ALKALI INDUSTRY
( 4 Hours)
Manufacture of soda ash, Caustic Soda, Chlorine, hydrogen and Hydrochloric acid.
CEMENT & GLASS MANUFACTURE
(4 Hours)
Portland cements, other cements, Methods and manufacture of special Glasses
SULFURIC ACID MANUFACTURE
(2 Hours)
PULP & PAPER INDUSTRY
(3 Hours)
Cellulose derivatives, pulp , paper & board.
SUGAR & STARCH INDUSTRY
(3 Hours)
Sugar, starches and related products
(3 Hours)
OIL, FATS, SOAPS AND DETERGENTS
Vegetable Oils, animal fats, their nature, analysis& extracted methods, Hydrogenations oil,
Fatty acids and alcohol, waxes, soap, synthetic detergent.
POLYMER INDUSTRY:
(4 Hours)
Manufacture of Phenol and Urea Formaldehyde resin, PVC, Polyethylene, Synthetic rubber etc.
SYNTHETIC FIBER INDUSTRY:
(4 Hours)
Nylon, Polyester, Acrylics, and Rayons.
FINE CHEMICALS AND DRUGS
(5 Hours)
Classifications of pharmaceuticals, manufacture of important drugs and pharmaceuticals,
salicylic acid, Methyl salicylate, Aspirin, Anti-biotics, Vitamins.
(3 Hours)
INTRODUCTION TO N & P FERTILIZERS.
INTRODUCTION TO PETROLEUM REFINING & PETROCHEMICAL INDUSTRY
(10 Hours)
(Total Contact Hours: 45)
PRACTICALS
1. Preparation of Boric acid by acidified solution of Borax (Na2B4O7).
2. Preparation of CaCl2 from HCl and lime (CaCO3).
3. Preparation of detergent.
4. Preparation of nitro naphthalene from given chemicals.
5. Preparation of polystyrene from styrene monomer.
6. Preparation of Potash alum from Aluminium Sulphate and Potassium sulphate.
7. Preparation of soap from KOH and coconut oil
8. Determination of the kinematic viscosity of given oil sample using Engler viscometer& Red Wood
Viscometer.
9. Determination of the aniline point of diesel using proper instruments.
10. Determination of the smoke point of kerosene and diesel.
11. Measurement of the softening point of grease sample.
12. Determination of the penetration index using pentrometer.
13. Determination of flash point and fire point of kerosene using Pensky Martin apparatus.
14. ASTM Distillation of gasoline.
BOOKS RECOMMENDED:
1. Austin G. T., Shreves Chemical Process Industries, 5th Ed. McGraw-Hill Pub., 1994.
2. Gopalarao M. & Sitting M., Drydens Outlines of Chemical Tech., 2nd Ed., East-West Pub., New
Delhi,1997
3. Rao B.K.B., Modern Petroleum Refining Processes, 4th ed.,Oxford & IBH Publishing Co. Pvt. Ltd., New
Delhi, 2002.
4. Nelson, W.L., Petroleum Refinry Engineering, 4th ed. (International student edition), McGraw-Hill
Kogakusha, Ltd., Tokyo, 1958.
5. Mall I.D., Petrochemicals Process Technology, Macmillan India Ltd, New Delhi, 2006.
10
INTRODUCTION
(4 Hours)
Dimension and Units, Fundamental and derived quantities, Mathematical techniques in chemical
engineering.
(6 Hours)
COMBUSTION
(8 Hours)
MATERIAL BALANCE
(9 Hours)
THERMOPHYSICS
(8 Hours)
Heat capacity calculations. Enthalpy changes of reactions, dissolution and laws of thermochemistry. Effect
(10 Hours)
Combined material and energy balances for single stage processes. Material and energy balance calculations for
industrial processes.
(Total Contact Hours: 45)
BOOKS RECOMMENDED:
1. Bhatt B.I. & Vora S.M., "Stoichiometry, 4th Ed., Tata-McGraw-Hill, New Delhi, 2004
2. Hougen O.A., Watson K.M. & Ragatz R.A., Chemical Process Principals: Part-I, 2nd Ed., CBS Publishers and
Distributors, New Delhi, 1995.
3. Himmelblau D.M., Basics Principles and Calculations in Chemical Engineering 6th Ed., Prentice-Hall India,1996.
4. Whitwell J.C. & Jone R.K., Conservation of Mass and Energy, McGraw-Hill, Singapore, 1973.
5. Process Calculation for Chemical Engineering, Second Revised Edition, Chemical Engineering Education
Development Centre, I.I.T., Madras, 1981.
11
Sr.
No.
1
2
(CS-1)
Heat Transfer
Operations
(CS-2)
Mass Transfer
Operations-I
(CS-3)
Mechanical
Operations
(CS-4)
EIS-1*
CH 301
50
25
50
---
---
125
CH 303
50
25
50
20
30
175
CH 305
50
25
50
20
30
175
CH 307
50
25
50
20
30
175
50
---
50
---
---
100
22
15
250
100
250
60
90
750
TOTAL
Total contact hours per week = 25
Sr.
No.
1
2
Total Credit = 22
(CS-1)
Chemical Reaction
Engineering -I
(CS-2)
Fluid Flow
Operations
(CS-3)
Mass Transfer
Operations-II
(CS-4)
EIS-2*
Total
Marks
Total
Marks
CH 302
50
25
50
---
---
125
CH 304
50
25
50
20
30
175
CH 306
50
25
50
20
30
175
CH 308
50
25
50
20
30
175
50
---
50
---
---
100
22
15
4
6
Total Credit = 22
250
100
250
60
90
Total marks = 750
750
TOTAL
Total contact hours per week = 25
* Students have to opt for one subject from each Elective Interdisciplinary Subject Group-1 & 2 as listed below:
EIS: Elective Interdisciplinary Subjects (Group-2)#
EIS: Elective Interdisciplinary Subjects (Group-1)#
CH 309: Bioprocess Engineering
CH 312: Bioseparations
CH 311: Energy Technology
CH 314: Cleaner Technologies in Chemical Process
CH 313: Fertilizer Technology
Industries
CH 315: Fuels and Combustion
CH 316: Introduction to Industrial Biotechnology
CH 317: Polymer Science and Engineering
CH 318 Petrochemical Technology
CH 322: Petroleum Refinery Engineering
Sr.
No.
1
2
3
4
5
6
7
8
Course
Code
Chemical Reaction
Engineering-II
(CS-1)
Instrumentation and
Process Control
(CS-2)
Process Equipment Design
and Drawing
(CS-3)
Transport Phenomena
(CS-4)
ES-1**
Seminar
Project Preliminaries
Training
Teaching
Scheme
Hours per
Week
Credits
Examination Scheme
Theory
Total
Marks
Practicals
Tu
Pr
Hr
Sess
ional
Tu
End
Sem
Sess
ional
End
Sem
CH 401
50
---
50
---
---
100
CH 403
50
25
50
20
30
175
CH 405
50
25
50
20
30
175
CH 407
50
25
50
---
---
125
CH 409
3
1
3
0
0
0
0
2
2
---
50
---
-----
50
---
--20
--30
100
50
CH 411
---
---
---
---
40
60
100
CH 413
---
---
---
---
---
50
50
24
15
10
250
75
250
100
200
875
TOTAL
Total contact hours per week = 28
Total Credit = 24
2
3
Course
Code
Credits
Teaching Scheme
Hours per Week
L
Chemical Engineering
Plant Design and
Economics
(CS-1)
Chemical Systems
Modeling
(CS-2)
Computer Aided Design in
Chemical Engineering
(CS-3)
Tu
Pr
Examination Scheme
Theory
Sess
Hr
Tu
ional
End
Sem
Practicals
Sess
End
ional
Sem
Total
Marks
CH 402
50
---
50
---
---
100
CH 404
50
---
50
---
---
100
CH 406
50
25
50
20
30
175
50
---
50
20
30
150
0
0
0
8
12
2
---
50
--250
----25
50
------80
120
250
120
180
Total marks = 825
100
200
825
4
3
CH 408
Process Industries (CS-4)
5
ES-2**
3
3
6
Project
CH 412
4
0
TOTAL
22
15
Total contact hours per week = 28
Total Credit = 22
** Students have to opt for one subject from each Elective Subjects Group-1 & 2 as listed below:
ES: Elective Subjects (Group-1)#
INTRODUCTION
( 6 Hours)
Conservation of energy and first law of thermodynamics, application to steady state flow
process,
enthalpy, internal energy, equilibrium state, phase rule, reversible and irreversible processes, heat capacity
specific heat.
PROPERTIES OF PURE SUBSTANCES
P-V-T behavior, ideal and non-ideal gases, different equations of state for real gases.
( 8 Hours)
HEAT EFFECTS
( 5 Hours)
Heat capacities of gases as a function of temperature of liquids and solids, heat of vaporization, heat of
fusion, heat of sublimation, etc.
SECOND AND THIRD LAW OF THERMODYNAMICS
( 7 Hours)
Thermodynamic temperature scale, ideal gas temperature scale, concept of entropy, entropy change and
irreversibility, third law of thermodynamics.
THERMODYNAMIC PROPERTIES OF FLUID
( 8 Hours)
Mathematical relation among thermodynamic functions, Mexwells relations, Interrelation between H, S,
U, G, Cp, Cv, properties of single and two phase system. Types of thermodynamic diagrams.
( 6 Hours)
THERMODYNAMICS OF FLOW PROCESS
Fundamental relation for flow in pipes, maximum velocity in pipe flow, throttling process, flow through
nozzles, single stage and multi stage compressors.
REFRIGERATION AND LIQUEFACTION:
( 5 Hours)
Carnot refrigeration cycle, air refrigeration cycle, absorption refrigeration, heat pump, choice of
refrigeration, liquefaction processes.
(Total contact time: 45 hours)
BOOKS RECOMMENDED:
1. Smith J. M., Van Ness H. C., M.M. Abbott, Introduction to Chemical Engineering Thermodynamics, 6th
Ed., McGraw-Hill, New York, 2001
2. Dodge B. F., Chemical Engineering Thermodynamics, McGraw-Hill Book Co., New York, 1960.
3. Rao Y. V. C., Chemical Engineering Thermodynamics, Universities Press Limited, Heydrabad, 1997.
4. Kyle, B.G., "Chemical and Process Thermodynamics, 2nd Ed., Prentice-Hall of India, New Delhi,1990.
5. Sandler, S.I., "Chemical and Engineering Thermodynamics", 2nd Ed., Wiley, New York, 1989.
INTRODUCTION
(02 Hours)
Modes of Heat Transfer: Conduction, Convection and Radiation
CONDUCTION
(05 Hours)
Fourier conduction equation, General conduction equation in Cartesian, Cylindrical and Spherical coordinates, Steady state and transient conduction equation.
FORCED CONVECTION
(10 Hours)
Heat transfer in fluids without phase change, Forced convection, Dimensional analysis, Heat transfer
in laminar and turbulent flows inside and outside tubes. Concept of thermal boundary layer, Overall
heat transfer coefficient, LMTD, Fouling factors, Transfer units, Flow over flat plates with heat
transfer, Empirical correlations.
NATURAL CONVECTION
(04 Hours)
Qualitative description of free convection flows, Hear transfer correlations for free convection.
BOILING AND CONDENSATION
(04 Hours)
Boiling phenomena: Regimes of boiling etc, Condensation: Film and drop condensation etc.
EVAPORATION AND CRYSTALIZATION
(06 Hours)
Single effect and Multi-effect evaporation, Forward and backward feed system.
Equilibrium in crystallization, operation and equipment.
HEAT EXCHANGERS
(06 Hours)
Double pipe heat exchanger and Shell-and-tube heat exchanger, its applications and design
RADIATION HEAT TRANSFER
(04 Hours)
Basic concepts of radiation heat transfer, Radiative heat exchange between surfaces, Radiation shield.
EXTENDED SURFACES
(04 Hours)
Heat transfer from extended surfaces, fin efficiency
(Total contact time: 45 hours)
PRACTICALS:
1. Experiment on Heat transfer through composite wall at different temperature
2. Experiment on Thermal conductivity of insulating powder (Asbestos powder)
3. Experiment on Heat transfer in double pipe heat exchanger in laminar flow
4. Experiment on Heat transfer in turbulent flow
5. Experiment on Heat transfer by forced convection
6. Experiment on Heat transfer coefficient in natural convection
7. Experiment on Extended surface heat transfer
8. Experiment on Shell and tube heat exchanger
9. Experiment on Heat transfer by radiation: Stefan-Boltzmann Law
BOOKS RECOMMENDED:
1. McCabe W.L., Smith J.C., Harrott P., Unit Operations of Chemical Engineering, 6th & 7th Eds. McGrawHill, New York, 2001 & 2005.
2. Kern D. Q., Process Heat Transfer, McGraw-Hill, New York, 1950.
3. Hollman J. P., Heat Transfer Basic approach, McGraw-Hill, New York, 1985.
4. Gebhart B. U., Heat Transfer, Tata McGraw-Hill, New York, 1961.
5. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. Chemical Engineering Vol. 1. 6th Ed.
Elservier, New Delhi, 2004.
INTRODUCTION
Introduction to Mass Transfer Operation: classification & method.
DIFFUSION AND MASS TRANSFER
Molecular diffusion in fluids, steady state diffusion
(both gases & liquids), diffusivity of liquids & gases.
( 02 Hours)
( 08 Hours)
( 03 Hours)
DIFFUSION IN SOLIDS
Introduction to diffusion in solids, Ficks law, types of solid diffusion
( 06 Hours)
( 04 Hours)
DISTILLATION
VLE data, flash, differential and continuous distillation,
McCabe-Thiele and Ponchon-Savarit method, Azeotropic,
Extractive, Reactive, Molecular and Multicomponent distillation,
Equipment for gas-liquid operation
( 16 Hours)
HUMIDIFICATION
( 06 Hours)
Vapor-gas mixtures, vapor-liquid equilibrium,gas-liquid contact operations,
adiabatic & non-adiabatic operations.
(Total contact time: 45 hours)
PRACTICALS
1. Humidification and dehumidification
2. Mass transfer coefficient
3. Crystallization
4. Azeotropic distillation
5. Diffusion coefficient
6. Latent heat of vaporization
7. Cooling tower
8. Packed distillation
BOOKS RECOMMENDED:
1. Treybal R.E., Mass-Transfer Operations, 3rd Ed., McGraw-Hill, New York, 1981.
2. McCabe W.L, Smith J.C., Harriott P., Unit Operations in Chemical Engineering, 6th & 7th Eds., McGrawHill, New York,2001 & 2005.
3. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. Chemical Engineering Vol. 1. 6th Ed.
Elservier, New Delhi, 2004.
4. Sherwood, T.K., Pigford, R.L., Wilke, C.R., Mass Transfer, McGraw-Hill, New York, 1976.
5. Cussler E.L.,Diffusion: Mass Transfer in Fluid Systems, 2nd Ed., Cambridge University Press, Cambridge,
1997.
INTRODUCTION
(03 Hours)
Solids, Storage, Transportation and Handling of Solis, Liquid and Gases, characteristics of solid particles
SIZE REDUCTION
(05 Hours)
Size reduction and enlargement, crushers, grinders, disintegrates for coarse & intermediate & fine grinding,
energy and power requirements, law of crushers, work index, etc.
SEDIMENTATION
Sedimentation, Settling velocity, flocculation, Thickener, Sedimentation zones.
FILTRATION
(10 Hours)
Filtration, filter media, filter aids, batch & cont. filtration, filtration equipment, filter press, leaf, cartridge,
vacuum filter, rotary drum filters.
CONVEYERS
Mechanical and Pneumatic conveying, elevators, Bins, silos etc.
(05 Hours)
(03Hours)
(Total contact time: 45 hours)
PRACTICALS:
1. Determination of the optimum speed and critical speed of a ball mill.
2. Calculation of the overall effectiveness of screen.
3. Analysis of solid powder sample.
4. Study of Roll crusher
5. Finding characteristic constants of Jaw crusher
6. Obtaining the collection efficiency of cyclone
7. Obtaining settling rates of slurry as function of solid concentration
8. Study of pressure drop as function of superficial velocity
BOOKS RECOMMENDED:
1. McCabe W.L., Smith J.C., Harriott P., Unit Operations of Chemical Engineering, 6th & 7th Eds., McGrawHill, New York, 2001 & 2005.
2. Foust A.S., Wenzel L.A., Clump C.W., Maus L., Anderson L.B. Principles of Unit Operations, John
Wiley & Sons, New York, 1980.
3. Brown G.G., Unit Operations, John Wiley & Sons, New York, 1953.
4. Badger W.L., Banchero J.T., Introduction to Chemical Engineering, McGraw Hill, New York, 1997.
5. Coulson J.M., Richardson J.F., Chemical Engineering, Vol. 2, 5th Ed., Elservier, New Delhi, 2002.
PHASE EQUILIBRIUM
(15 Hours)
Phase rule, Duhem theory, miscible system, immiscible system, partially immiscible system, testing of
vapor-liquid equilibrium data, Gibbs-Duhem equation, Van Laar equation. Margules equation,
Redlich-Kister equation, P-X-Y, T-X-Y, & X-Y Diagram, vapor-liquid equilibrium of ideal and nonideal solution, Roults law & Henrys law.
CHEMICAL EQUILIBRIUM
(10 Hours)
Criteria, equilibrium conversion (X), constant (K), effect of Temp. & Pressure on K, evaluation of K,
evaluation of equilibrium conversion for gas phase reaction.
( 8Hours)
INTRODUCTION TO STATISTICAL THERMODYNAMICS
Stefen-Boltzman, Bose-Einstein and Fermi-Dirac distributions, corrected boltzman statistics, partition
function etc.
(Total contact time: 45 hours)
BOOKS RECOMMENDED:
1. Smith J. M. Van Ness H. C., Abbott M.M., Introduction to Chemical Engineering Thermodynamics, 6th &
7th Eds., McGraw-Hill, New York, 2001 & 2005.
2. Dodge B. F., Chemical Engineering Thermodynamics, McGraw-Hill, New York, 1960.
3. Rao Y. V. C., Chemical Engineering Thermodynamics, Universities Press Limited, Heydrabad, 1997.
4. Sonntag R.E., Van Wylen G.J., Fundamentals of Statistical Thermodynamics, John Wiley & Sons,
Singapore, 1991.
5. Sandler, S.I., Chemical and Engineering Thermodynamics, 2nd Ed., Wiley, New York, 1989.
INTRODUCTION
(01 Hour)
Chemical kinetics, Classification of reactions, Variables affecting the rate of reaction, Reaction rate
KINETICS OF HOMOGENEOUS REACTIONS
(06 Hours)
Concentration dependent term and temperature dependent terms of rate equation, Single and multiple
reactions, Elementary and non-elementary reactions, Molecularity and order of reaction, Rate
constant, Representation of reaction rate, Kinetic models, Temperature dependency from Arrhenius
law, thermodynamics, various theories, Activation energy, Searching for the reaction mechanism
INTERPRETATION OF BATCH REACTOR DATA
(08 Hours)
Constant volume batch reactor, Variable volume batch reactor, Integral method and differential
method of analysis of kinetic data, Temperature and reaction rate
INTRODUCTION TO REACTOR DESIGN
(03 Hours)
Types of reactors, PFR, CSTR etc., Material & energy balances single ideal reactor, Space-time and
space-velocity, Holding time, Introduction of non-ideal flow
DESIGN FOR SINGLE REACTIONS
(08 Hours)
Size comparison of single reactors, General graphical comparison, Multiple reactor system, Recycle
reactor, Autocatalytic reactions
DESIGN FOR MULTIPLE REACTIONS SYSTEMS
(08 Hours)
Reaction in parallel, Reaction in series, Series-parallel reaction and applications
TEMPERATURE & PRESSURE EFFECTS
(04 Hours)
Single & multiple reactions, Heats of reaction from thermodynamics, Product distribution
INDUSTRIAL APPLICATIONS
(04 Hours)
Types of reactors used in industries, Advanced chemical reactors.
INTRODUCTION TO BIOCHEMICAL REACTION ENGINEERING
(03 Hours)
Types of bio-reactors, Design, scale-up, operation and control of bio-reactors, Kinetics of biochemical
reactions
(Total contact time: 45 hours)
PRACTICALS:
1. Integral method of analysis of kinetic data
2. Differential method of analysis of kinetic data
3. Activation energy and frequency factor
4. Half-life method
5. Pseudo first order reaction
6. Study of kinetics of the reaction in presence of DC current
7. Study of membrane reactor
8. Study of spiral coiled reactor
9. Study of annulus flow reactor
10. Study of specific reaction/reactor system
BOOKS RECOMMENDED:
1. Levenspiel O., Chemical Reaction Engineering, 3rd Ed., John Wiley & Sons, Singapore, 1998.
2. Fogler H.S., Elements of Chemical Reaction Engineering, 4th Ed., Prentice-Hall, NJ, 2006.
3. Smith J. M., Chemical Engineering Kinetics, 3rd Ed., McGraw-Hill, New York, 1981.
4. Froment G.F., Bischoff K.B., Chemical Reactor Analysis and Design, 2nd Ed., John Wiley & Sons,
Singapore, 1990.
5. Inamdar S.T.A., Biochemical Engineering Principles and Concepts, Prentice-Hall of India, New Delhi,
2007.
6. Shuler M.L., Kargi F., Bioprocess Engineering Basic Concepts, 2nd Ed., Prentice-Hall of India, New
Delhi, 2006.
INTRODUCTION
(4 hours)
Definitions of Unit operations, Basic concepts of fluids and its application area, Properties of fluids,
Unit systems, Standards, Conversion on units, Units and equations, Dimension analysis, Dimension
and units, Dimensional homogeneity, Dimensionless equations, Buckingham theorem, Common
groups, examples.
(8 hours)
PRACTICALS
1. Experiment on Viscosity by Stokes law
2. Experiment on Reynolds number
3. Experiment on Friction in circular pipe
4. Experiment on Friction in annulus
5. Experiment on Calibration of venturimeter
6. Experiment on Orifice meter
7. Experiment on Characteristics of centrifugal pump
8. Experiment on Equivalent length of pipe fittings
BOOKS RECOMMENDED
1. McCabe W.L., Smith J.C., Harriott P., Unit Operations of Chemical Engineering, 6th & 7th Eds., McGrawHill, New York, 2001 & 2005.
2. Coulson & Richardsons Chemical Engineering, Vol. 2, 5th Ed., Elesevier, New Delhi, 2005.
3. Coulson & Richardsons Chemical Engineering, Vol. 4, 2nd Ed., Elesevier, New Delhi, 2001.
4. Coulson & Richardsons Chemical Engineering, Vol. 6, 4th Ed., Elesevier, New Delhi, 2006.
5. de Nevers N., Fluid Mechanics for Chemical Engineers, 2nd Ed., McGraw-Hill, New York, 1991.
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ABSORPTION
( 10 Hours)
Equilibrium, material balance for single component transfer, multi-stage & packed tower
operation, multicomponent system, non-isothermal operation, absorption with chemical
reaction
LIQUID EXTRACTION
( 08 Hours)
Liquid equilibria, stage wise extraction, stage type extractor, differential extractor
( 06 Hours)
DRYING
Equilibrium, batch drying, mechanism, continuous
( 06 Hours)
LEACHING
Steady state & unsteady state operations, methods of calculation
( 04 Hours)
CRYSTALLIZATION
Equilibrium, operations and equipment
( 03 Hours)
( 08 Hours)
PRACTICALS
1. Leaching
2. Liquid-liquid extraction
3. Freundlich isotherm
4. Ternary diagram
5. Drying
6. Fluidization apparatus
7. Cooling tower
8. Fluid bed dryer
9. Evaporator
BOOKS RECOMMENDED:
1. Treybal R.E., Mass-Transfer Operations, 3rd Ed., McGraw-Hill, Singapore, 1981.
2. McCabe W.L, Smith J.C., Harriott P., Unit Operations in Chemical Engineering, 6th &7th Eds.,
McGraw-Hill, New York, 2001 & 2005.
3. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. Coulson & Richardson's Chemical
Engineering, Vol. 1, 6th Ed., Elservier, New Delhi, 2004.
4. Chopey N.P., Handbook of Chemical Engineering Calculations, 3rd Ed., McGraw-Hill, New
York, 2004.
5. Suryanarayana A., Mass Transfer Operations, New Age International, New Delhi, 2002.
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INTRODUCTION TO RTD
(03 Hours)
Non ideal flow in reactors, RTD of fluid in reactors, Age distribution, F curve, C curve and E curve,
Intensity Function, Effects of RTD on performance of Chemical Process Equipment
CATALYTIC REACTORS
(06 Hours)
ion kinetics, External and Internal Diffusional Resistances, Effects of Heat Generation/Absorption,
Effectiveness Factors, Fixed Bed, Fluid Bed, Trickle bed, Slurry Reactors,
CATALYSIS
(05 Hours)
Typical Catalysts used in chemical processes, Catalyst Characterizations, Catalyst Deactivation and
Regeneration, Metal recovery from the Spent Catalysts
ZEOLITE CATALYSTS
Applications, Rise of Acidity, Modifications, Shape Selectivity
(05 Hours)
ENVIRONMENTAL CATALYSIS
Importance, Applications
(03 Hours)
MONOLITHIC REACTORS
(03 Hours)
Configurations, Preparation, Hydrodynamics and Applications, Accelerated Deactivation of catalysts,
Laboratory reactors, Oscillatory motion of reactants in catalyst pores, Microreactors.
BOOKS RECOMMENDED:
1. Fogler H.S., Elements of Chemical Reaction Engineering, 4th Ed., Prentice Hall, NJ, 2006.
2. Levenspiel O., Chemical Reaction Engineering, 3rd Ed., John Wiley & Sons, Singapore, 1998.
3. Smith J. M., Chemical Engineering Kinetics, 3rd Edition, McGraw Hill, N Y, 1981.
4. Davis M.E., Davis R.J., Fundamentals of Chemical Reaction Engineering, McGraw-Hill, New York,2003.
5. Froment G.F., Bischoff K.B., Chemical Reactor Analysis and Design, 2nd Ed., John Wiley & Sons,
Singapore, 1990.
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INTRODUCTION
(02 Hours)
Steady and unsteady state design equation for an agitated heated tank. Introduction to P, PI, PID
controls.
ADVANCED CONTROL
(05 Hours)
Cascade Control, Feed forward Control, Ratio control, Split Range Control, Auctioneering Control and
Multivariable Control.
(02 Hours)
(02 Hours)
(03 Hours)
(02 Hours)
(03 Hours)
(03 Hours)
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PRACTICALS:
1. Dynamics of First Order Liquid Level System.
2. Dynamics of Non Interacting Tanks.
3. Simulation of Heat Exchanger
4. Simulation of Catalytic Reformer
5. Simulation of Binary Distillation
6. Study of Temperature Control Trainer
7. Study of Pressure Control Trainer
8. Study of Flow Control Trainer
9. Study of Level Control Trainer
10. Dissolved Oxygen Meter
11. Thermocouple Calibration
BOOKS RECOMMENDED:
1. Coughanowr D.R., Process Systems Analysis and Control, 2nd Ed., McGraw-Hill, New York, 1991.
2. Stephanopoulos G., Chemical Process Control, Prentice-Hall of India, New Delhi, 2001.
3. Luben W.L., Luben M.L., Essentials of Process Control, McGraw-Hill, New York, 1997.
4. Kopell L.B., Coughanowr D.R., Process Systems Analysis and Control, McGraw-Hill, New York, 1986.
5. Eckman D.P., Industrial Instrumentation, Dhanpat Rai and Sons, New Delhi, 1999.
6. Morris M. M., Kime C.R., Logic and Computer Design Fundamentals, Prentice-all, PLACE2000.
7. Considine D.M., Process Industrial Instruments and Control Handbook, McGraw-Hill, New York, 2001.
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INTRODUCTION
(02 Hours)
Introduction to Chemical Engineering Design, Process design, Mechanical aspects of process
equipment design, General design procedure, Equipment classifications, Design codes and standards
(IS, ASTM and BS)
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BOOKS RECOMMENDED:
1. Joshi M.V., Mahajani V.V., Process Equipment Design, 3rd Ed., MacMillan, Delhi, 1996.
2. IS Code: 2825 (1969).
3. Bhattacharyya B.C., Introduction to Chemical Equipment Design: Mechanical Aspects, 5th Ed., CBS
Publishers, New Delhi, 2008.
4. Soares C., Process Engineering Equipment Handbook, McGraw-Hill, New York, 2002.
5. Cheremisinoff N.P., Handbook of Chemical Processing Equipment, Butterworth Heinemann, Oxford,
2000.
6. Coulson & Richardsons Chemical Engineering, Vol. 6, 4th Ed., Elesevier, New Delhi, 2006.
7. Kern D.Q., Process Heat Transfer, McGraw-Hill, New York, 1965.
8. Brownell L.E., Young E.H., Process Equipment Design, Wiley Eastern, Delhi, 1977.
9. Branan C.R., Rules of Thumb for Chemical Engineers, 4th Ed., Elsevier, Oxford, 2005.
16
INTRODUCTION
(6 Hours)
(1 Hour)
(04 Hours)
(02 Hours)
(01 Hour)
17
INTRODUCTION
( 02 Hours)
Basic consideration in chem. Engg. plant design, project identification, preliminary technoeconomic feasibility.
.
PROCESS DESIGN ASPECTS
( 04 Hours)
Selection of process, factors affecting process selection, types of flow diagrams.
PROCESS AUXILIARIES
( 04 Hours)
Piping design, layout, support for piping insulation, types of valves, process control &
instrumentation control system design.
PROCESS UTILITIES
( 06 Hours)
Process water, boiler feed water, water treatment & disposal, steam, oil heating system,
chilling plant, compressed air and vacuum system.
COST ESTIMATION
( 06 Hours)
Factors involved in project cost estimation, total fixed & working capital, types & methods of
estimation of total capital investment, estimation of total product cost, factors involved.
DEPRECIATION
Types and methods of determination, evaluation.
PROFITABILITY
( 04 Hours)
Alternative investment & replacement methods for profitability evaluation, economic
consideration in process and equipment design, inventory control.
OPTIMUM DESIGN
General products rates in plant operation, optimum conditions etc.
( 04 Hours)
( 03 Hours)
( 02 Hours)
BOOKS RECOMMENDED:
1. Peters M.S., Timmerhaus, K.D., Plant Design and Economics for Chemical Engineers, 4th Ed., McGrawHill, Singapore, 1991.
2. Vilbrant F.C., Dryden, C.E., Chemical Engineering and Plant Design, 4th Ed., McGraw-Hill, New York,
1959.
3. Pant J.C. CPM and PERT with Linear Programming, Jain Brothers, New Delhi, 1986.
4. Davis, G.S, "Chemical Engineering Economics and Decision Analysis", CENDC, I.I.T., Madras, 1981.
5. Holland, F.A., Watson, F.A and Wilkinson, J.K., "Introduction to Process Economics", Wiley, New
York, 1974.
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INTRODUCTION
(3 hours)
Physical and mathematical modeling, Principles of similarity, Independent variables, Dependent
variables, Parameters and boundary conditions.
(3 hours)
INDUSTRIAL SIMULATORS
Introduction and applications
(4 hours)
19
INTRODUCTION
(3 hours)
Introduction to Computer aided design in chemical engineering, Mathematical modeling, Steady state
and dynamic Simulation, Process simulation program (ASPEN PLUS).
PRACTICALS
1. Simulation by ASPEN PLUS
2. Simulation by ASPEN PLUS
3. Simulation by ASPEN PLUS
4. Simulation by ASPEN PLUS
5. Simulation by ASPEN PLUS
6. Simulation by ASPEN PLUS
7. Simulation by ASPEN PLUS
8. Simulation by ASPEN PLUS
(8 hours)
BOOKS RECOMMENDED
1. Sinnott R. K., Coulson & Richardsons Chemical Engineering, Vol. 6, 4th Ed., Elsevier, 2005.
2. Edgar T. F., Himmelblau D. M., Lasdon L. S., Optimization of Chemical Processes, 2nd Ed., McGrawHill, New York, 2001.
3. Smith R., Chemical Process Design, McGraw-Hill, New York, 2000.
4. Biegler L. T., Grossmann E. I., Westerberg A. W., Systematic Methods of Chemical Process Design,
Prentice-Hall , New Jersey, 1997.
5. Douglas J., Conceptual Design of Chemical Processes, McGraw-Hill, New York, 1989.
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