DGHT-3-01

Bioseparaciones Fludo Fludo

INSTITUTO POLITCNICO NACIONAL

Unidad Profesional Interdisciplinaria de Biotecnologa

Bioseparaciones Fludo- Fludo

Group: 6LM2
Homework: 3-01
Professor: Dr. Edgar Salgado Manjarrez
Team:
Del Ro Trujillo Mara Fernanda
Galaviz Hernndez Stephania
Herrera Hurtado Paola Lucero
Trejo Vzquez Jessica Angelina

Date. 27/11/15

DGHT-3-01
Bioseparaciones Fludo Fludo

Exercise
100 mol/s of an aqueous flow contains 0.2 mol fraction of ethanol, will be distillated till a concentration of 0.8 mol fraction
also its obtained in the distillated 0.02 mol fraction in the bottoms.
We have the following data from the last problem:

F=100 mol/s
= 0.2
= 0.8
= 0.02
f=0.6

We need to find
a)
b)
c)
d)

Determinate
With a = 2.47, determinate the number of theoretical stages
Determinate the real stages with a efficiency = 0.7 for liquid phase
Specify the system

a) We have to locate the following points = 0.02 (interpolate with liquid line, it will give us . Also
we obtain 1 , interpolating with steam line), = 0.2, = 0.8 (interpolate with liquid line, it will give us
value)

Figure 1.1 Determination of enthalpies

DGHT-3-01
Bioseparaciones Fludo Fludo
= 1 + (1 ) = 0.6 (21

) + 0.4 (3
) = 13.8

With = 13.8 14 value, we will extend it until this line intercepts with line (Figure 1.2), we obtain value.

Figure 1.2 hF and hD values

DGHT-3-01
Bioseparaciones Fludo Fludo
With these values, we can determinate the minimum proportion.

( )

1
1

54 21
= 1.92
21 3.9

b) With( ) = 2.74, we will determinate the theoretical stages

From

1
1

We can obtain

= ( ) (1 ) + 1

= (2.74)*(21

- 3.9

) +21

= 67.85

DGHT-3-01
Bioseparaciones Fludo Fludo

Figure 1.3 New hD and hB values

We have to begin to draw the stages, beginning with 1 point

DGHT-3-01
Bioseparaciones Fludo Fludo

Figure 1.4 Theoretical stages=8

Graphically we obtained 8 stages and we can say that we can feed in seventh stage, due to H7 line is over from line.

DGHT-3-01
Bioseparaciones Fludo Fludo
c) To know the number of real stages the line of operation must be traced and then the efficiency, but before of
this we have to pass the points to distribution diagram.
First= We have to locate 0 point and point
Then= We have to draw the operation line with points from previous diagram (Hs and hs points).

x
0.8
0.76
0.71
0.63
0.49
0.26
0.1
0.02

y
0.8
0.77
0.73
0.67
0.58
0.41
0.29
0.24

Figure 1.5 Real stages=11

DGHT-3-01
Bioseparaciones Fludo Fludo
The real stages =11, drawn with efficiency line (blue line, Figure 1.5).
d) Specify system

So now, we need to determine the values of flows D, B, the heat qc and qR and the temperatures of each flow as well.

qc= 1475.33

D= 27.07
XD=0.8
TD=78.5C

F= 100
ZF=0.2
TF=90C

B= 76.93
XB=0.02

qR= 461.58

TB=93C

Afterwards, we need to know the value of distillates (D) and funds (B). To calculate them, we appeal to mass balance.
F= D + B

DGHT-3-01
Bioseparaciones Fludo Fludo

The respective fractions are added to each flow

F ZF =D XD + B XB
We substitute de B for F-D
F ZF =D XD + (F-D) XB
We group the terms with F and the terms with D
F (ZF - XB) = D (XD - XB)
Later, we solve the equation for D
(Z X )
X )

D= (X

And substituting in the equation we get the value for D

(0.2 0.02)

D= 100 (0.8

0.02)

= 23.07

= = 100 23.07 = 76.93

Finally, we need to know the value of and . To calculate them, we appeal to heat balance.

= +

=(
)=(67.85

)=(3
=(

3.9
)23.07
= 1475.33

= 67.85

=3

(3
))76.93
= 461.58

In addition, to get the temperatures of TF , TD an TB , we look to the diagram and with the values of ZF, XD
and XB, respectively, we determine the approximate value of the isotherm located at each point on the xaxis