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Nirma University.
M.Tech CASAD Semester I
CL1105 Advanced materials 2014-2015
Assignment I
Revision of Concrete Technology
Tejas M. Patil
M. Tech. 1st Year
14MCLC22
Due date - 11th August 2014
Question 1.2
Discuss in brief the equipments used, the procedure for the evaluation of following properties of cement along with their significance.
Fineness, Standard consistency, Setting time, Compressive strength.
Answer,1. Fineness test- The fineness of cement has an important bearing on
the rate of hydration and hence on the rate of gain of strength and also
on the rate of evolution of heat. Finer cement offers a greater surface
area for hydration and hence faster the development of strength. Different cements are ground to different fineness. The disadvantages of
fine grinding is that it is susceptible to air-set and early deterioration.
Hence optimum grinding should be chosen.
Sieve Test- Weigh correctly 100 grams of cement and take it on
a standard IS Sieve No. 9 (90 microns). Break down the air-set
lumps in the sample with fingers. Continuously sieve the sample
giving circular and vertical motion for a period of 15 minutes.
Weigh the residue left on the sieve. This weight shall not exceed
10% for ordinary cement.
Air Permeability Method- This method of test covers the
procedure for determining the fineness of cement as represented
by specific surface expressed as total surface area in sq. cm/gm.
of cement. The principle is based on the relation between the flow
of air through the cement bed and the surface area of the particles
comprising the cement bed.From this the surface area per unit
weight of the body material can be related to the permeability of
a bed of a given porosity.
2. Standard Consistency- The standard consistency of a cement paste
is defined as that consistency which will permit a Vicat plunger having
10 mm diameter and 50 mm length to penetrate to a depth of 33-35
mm from the top of the mould shown in Vicat Apparatus.
For finding out initial setting time, final setting time and soundness of
cement, and strength a parameter known as standard consistency has
to be used.
Procedure Take about 400 gms of cement and prepare a paste with a weighed
quantity of water for the first trial. The paste must be prepared
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Take 500 gm. of cement sample and guage it with 0.85 times the
water required to produce cement paste of standard consistency
(0.85 P).
The paste shall be guaged and filled into the Vicat mould in
specified manner within 3-5 minutes.
Start the stop watch the moment water is added to the cement.
The period elapsing between the time when water is added to
the cement and the time at which the needle penetrates the test
block to a depth equal to 33-35 mm from the top is taken as
initial setting time.
Replace the needle of the Vicat apparatus by a circular attachment. The cement shall be considered as finally set when, upon,
lowering the attachment gently cover the surface of the test block,
the centre needle makes an impression, while the circular cutting
edge of the attachment fails to do so.
4. Soundness test- The testing of soundness of cement, is done to ensure
that the cement does not show any appreciable subsequent expansion
is of prime importance.
procedure-
Question 1.3
Discuss in detail the phenomenon of Hydration of cement.
Answer, Hydration of cement- The chemical reactions that take place between cement and water is called Hydration of Cement. By the process of hydration, Portland cement when mixed with sand gravel and
water produces the synthetic rock we call concrete. The reaction with
water is termed hydration. This involves many different reactions,
often occurring at the same time. As the reactions proceed, the products of the hydration process gradually bond together the individual
sand and gravel particles, and other components of the concrete, to
form a solid mass. These products are important because they have
cementing or adhesive values. The hydration of cement can be explained in two ways namely, through solution and solid state mechanisms. In through solution mechanism, compounds dissolve to produce supersaturated solution from which different hydrated products
get precipitated. During solid state mechanism, water attacks cement compounds to produce hydrated products starting from surface
and proceeding to interior of compounds with time. It is likely that,
both mechanisms may occur during the course of hydration reaction
depending upon availability of water.
Heat of Hydration- When water is added, the reactions which occur
are mostly exothermic, that is, the reactions generate heat. We can
get an indication of the rate at which the minerals are reacting by
monitoring the rate at which heat is evolved using a technique called
conduction calorimetry. On mixing cement with water, the rapid heat
evolution occurs. It is mainly due to Aluminates and Sulphates and
ceases quickly due to Gypsum. The next heat evolution is because
of ettrignite and partly due to reaction of C3 S. Different compounds
hydrate at different rates to produce different amount of heat. Fig
shows rate of hydration of different compounds. It is noticeable that
Aluminate have very high rate of hydration but retarders, like Gypsum control their solubility. So, heat of hydration is mainly due to
hydration of C3 S.
Hydration of silicates-
Question 1.8
Discuss in detail the various stages in manufacturing of concrete.
Answer,Bad concrete and good concrete, are both made of essentially the same
materials or ingredients. The only thing most often separates them is, the
care taken during at each stage of manufacturing of concrete. The various
stages of manufacturing of concrete are as follows.
1. batching
batching of concrete is nothing but the measurement of concrete.
Volume batching(a) In this method, measurement is done in volume.
(b) Since it is very difficult to measure granular material in terms
of volume,this method is not preffered for batching.
(c) Gauge boxes are used for measuring the fine and coarse aggregates. Usually, The volume of the box is made equal to
the volume of one bag of cement. i.e., 35 liters.
(d) in India volume batching is adopted even for large concreting
operations.
(e) Correction to the effect of bulking should be made to cater
for bulking of fine aggregate, when the fine aggregate is moist
and volume batching is adopted.
Weigh batching(a) Measurement is done by weight.
(b) Since measurement of weight provides accuracy, flexibility
and simplicity to operation, Weigh batching is the more precise and correct method of measuring than Volume batching.
(c) in smaller works, the weighing arrangement consists of two
weighing buckets, each connected through a system of levers
to spring-loaded dials which indicate the load. On large work
sites, the weigh bucket type of weighing equipments are used.
The weighing is done through a lever-arm system and two
interlinked beams and jockey weights the materials.
(d) Addition of water by graduated bucket in terms of liters will
not be accurate enough for the reason of spillage of water etc.
It is usual to have the water measured in a horizontal tank
or vertical tank fitted to the mixer.
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2. Mixing- Mixing is essential to ensure that the mass becomes homogeneous, uniform in colour and consistency. There are two methods of
mixing.
Hand Mixing(a) Hand mixing is practiced for small scale unimportant concrete works.
(b) The measured quantity of coarse aggregate and fine aggregate are spread in alternate layers. The cement is poured on
the top of it, and mixed dry by shovel, turning the mixture
over and over again until uniformity of colour is achieved.
Water is taken in a water-can fitted with a rose-head and
sprinkled over the mixture and simultaneously turned over.
This operation is continued till such time a good uniform,
homogeneous concrete is obtained.
Machine Mixing(a) Mixing of concrete is carried out by machine, for reinforced
concrete work and for medium or large scale mass concrete
work.
(b) Many types of mixers are available for mixing concrete. They
can be classified as batch-mixers and continuous mixers.
(c) Machine mixing is efficient and economical, especially in large
plants.
(d) As per I.S. 17911985, concrete mixers are designated by a
number representing its nominal mixed batch capacity in
liters. The following are the standardized sizes of three types:
Tilting( 85 T, 100 T, 140 T, 200 T), Non-Tilting( 200 NT,
280 NT, 375 NT, 500 NT, 1000 NT), Reversing( 200 R, 280
R, 375 R, 500 R and 1000 R). The letters T, NT, R denote
tilting, non-tilting and reversing respectively.
3. Transporting Concrete- Main objective of transporting concrete is
that homogeneity obtained at the time of mixing should be maintained
while being transported to the final place of deposition.
(a) Motar Pan. Use of mortar pan for transportation of concrete
is labour intensive, and one of the common methods adopted in
India.
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Miscellaneous
(a) Calcium chloride is used either as a surface coating or as an
admixture. It can be used as curing medium since it absorbs
moisture from atmoshpere and retains at surface.
(b) Formwork prevents escaping of moisture from the concrete,
particularly, in the case of beams and columns. Keeping the
formwork intact and sealing the joint with wax or any other
sealing compound prevents the evaporation of moisture from
the concrete. This can also be seen as method of curing.
7. Finishing- Concrete is often dubbed as a drab material, incapable of
offering pleasant architectural appearance and finish. This shortcoming of concrete is being rectified and concretes these days are made to
exhibit pleasant surface by process of finishing. Surface finishes may
be grouped as under:
Formwork Finishes. Concrete obeys the shape of formwork
i.e., centering work. By judiciously assembling the formwork,
pleasant finishing can be achieved.
Surface Treatment. This is one of the methods of giving good
look to the concrete surface.
Applied Finishes. The term applied finish is used to denote the
application of rendering to the exteriors of concrete structures.
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Question 1.9
Explain in detail the what you mean by Shrinkage, Creep and Modulus of
Elasticity of concrete.
Answer,1. Shrinkage is a reduction in volume, and in concrete, it is mainly
caused by the loss of water. In most cases, shrinkage is measured by
monitoring longitudinal strain. When tensile stresses due to restrained
volume contraction exceed the tensile strength of concrete, the shrinkage leads to cracking, which is called shrinkage cracking. Shrinkage
is classified based on the causes of volume change and the state of
concrete.
Plastic shrinkage is the shrinkage that occurs due to loss of
moisture from fresh concrete. This loss may in be in form of surface evaporation or moisture loss to the subgrade, for slabs on the
ground. The loss of moisture leads to the formation of menisci.
These menisci generate negative capillary pressures, which cause
a volume reduction in the cement paste (Mindess, Young, and
Darwin 2003). Because the loss of moisture is concentrated at the
exposed surfaces, the volume contraction is uneven. Differential
volume changes produce tensile stresses in concrete, which may
result in the formation of cracks in the plastic concrete. This type
of cracking generally appears in random patterns and is shallow.
Autogenous Shrinkage (also known as chemical shrinkage) is
a volume change that occurs without moisture loss to the surrounding environment. It occurs when water in cement paste is
consumed by the hydration reactions, and results due to self desiccation of the concrete. This type of shrinkage mainly occurs
in the mixes with low water-cement (w/c) ratios and may be increased by the use of reactive pozzolans. For the concretes with
w/c ratios of 0.42 and greater, autogenous shrinkage is normally
small and can be considered as a part of drying shrinkage.
Drying shrinkage occurs due to the loss of moisture from hardened concrete. Among the different types of shrinkage, drying
shrinkage usually results in the largest volume change. Moisture
loss causes volume changes based on three mechanisms that result
in changes in capillary stress, disjoining pressure, and surface free
energy. Capillary stress occurs between relative humidity of 45
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Carbonation shrinkage occurs as the result of chemical reactions between hardened cement paste and carbon dioxide. It is
believed that CO2 reacts with calcium silicate hydrate (C-S-H)
inducing a decrease in its calcium-silica (C/S) ratio with a concomitant water loss. Carbonation shrinkage is a function of relative humidity and is greatest around 50 percent relative humidity.
Carbonation shrinkage, although not very significant itself, can
add to the effect of drying shrinkage and thereby lead to cracking.
2. Creep- The degree of curvature of the stress-strain relationship depends upon many factors amongst which the intensity of stress and
time for which the load is acting are of significant interest. Therefore,
it clearly shows that the relation between stress and strain for concrete
is a function of time. The gradual increase in strain, without increase
in stress, with the time is due to creep. Creep can also be defined as
the increase in strain under sustained stress.
One of the explanations given to the mechanics of creeps is based
on the theory that the colloidal particles slide against each other to
re-adjust their position displacing the water held in gel pores and capillary cavities. This flow of gel and the consequent displacement of
water is responsible for complex deformation behaviour and creep of
concrete.
Measurement of Creep- it is generally assumed that the creep
continues to assume a limiting value after an infinite time under
load. It is estimated that 26 per cent of the 20 year creep occurs
in 2 weeks. 55 per cent of 20 year creep occurs in 3 months and
76 per cent of 20 year creep occurs in one year. If creep after one
year is taken as unity, then the average value of creep at later
ages are:
1.14 after 2 years
1.20 after 5 years
1.26 after 10 years
1.33 after 20 years and
1.36 after 30 years
There are many expressions to give the magnitude of ultimate
creep in concrete member. Ross suggested the relation between
specific creep (creep strain per unit stress)c and time under load
t in the form c=
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t
a+bt
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