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pressure drop, the pattern of the pressure is increasing up until power at 1.00 kW
and decreasing at pressure 1.25 kW to 1.50 kW. Finally, a graph of overall top
and bottom pressure drop versus boiling up rate is plotted. The overall top and
bottom pressure drop is the value of difference between top pressure drop and
bottom pressure drop. From the graph, it shows that, at low boiling up rates the
pressure drop remains fairly constant until foaming occurs when the pressure
drop would be expected to rise sharply for unit in boil up rate but there is sudden
decrease of pressure drop at boil up rate 64.80 mL/s and 54.00 mL/s. This is
because the degree of forming occurs at these times which are foaming violently
over whole tray and liquid flooding in column effect the pressure drop.
In the second experiment, the refractive index of methylcyclohexane and
toluene is measured by using refractometer for different concentration of
methylcyclohexane which is 100% , 75 % , 50 % , 25 % and 0 % . First, the
calculation of volume methylcyclohexane and volume of toluene needed for each
different concentration is made.
The calculation is made by using the formula :
Concentration =
CONCLUSION
Based on the experiment A, Determining Column Pressure Drop, students
are able to determine the pressure drop over the distillation column for various
boil up rates in batch distillation. From the results obtained, it shows that when
the power input increase, the boil-up rates and the pressure drop also increase
but decrease at power 1.50 kW. By plotting the graph of pressure drop versus
boil up rate, it is clearly shows that at low boil-up rate the pressure drop will
remain fairly constant until foaming occurs when the pressure drop would be
expected to rise sharply with the increases in boil up rate but there is sudden
decrease of pressure drop at boil up rate 64.80 mL/s and 54.00 mL/s. Based on
the result obtained in the experiment B, the Determining Mixture Composition,
the composition of the mixtures of Methylcyclohexane and Toluene is determine
by using refractometer . After plotting the graph of refractive index versus mole
fraction methylcyclohexane, the graph shows that when the concentration of
methylcyclohexane increases, the refractive index is decrease. The refractive
index is higher when the concentration of methylcyclohexane is 0%.
RECOMMENDATION:
There are some recommendations that can help to improve the performance of
these two experiment :
1. In both experiment, the accuracy of taking the reading is really required to
make sure the good result. Thus, each of the experiment need to be
repeated at least three times to obtain an accurate result.
2. In the experiment A, it is recommended that when taking the sample,
ensure that the liquid remains in the flexible connecting tube to prevent
vapour from escaping by partially open the valve V3 and drain the
condensate from the reflux system until a steady flow is obtained.
3. It is need to make sure that when taking the reading of pressure drop for
top and bottom of the column, the valve V6 and V7 must be always open
to prevent vapour from the column entering the manometer.
4. It
is
highly
advised
to
allow
10
minutes
between
each
set
of
measurements before starting the next set in order to let the system reach
equilibrium again.
5. For experiment B, it is highly recommended to rinse the refractormeter
and dropper with distilled water before used it. This is done to removed
impurities that maybe disturb the reading of refractive index.