Chemicals Used For Frac

Amasra CBM 2
07.01.2011

Main Frac
12/20 Sand
16/30 Sand
70/140 Sand
16/20 FT ISP

16/30 Optiprop
20/40 Sand
0

BioClear
WGA 20
OC DE-11
TRS CS-1
OC TEA
TRS APS
TRS CL-1
GB-102 100%
OC TS 11

0
32,000
0
0
0
0
0
7.2
440.0
235.0

15.0
180.0
47.5

Minifrac

kg

kg

kg

kg

kg

kg

kg

kg

kg

kg

kg

kg

kg

kg

liters

liters

kg

kg

liters

liters

liters

liters

liters

liters

kg

kg

liters

liters

liters

kg

kg

kg

Total
0.0
32000.0
0.0
0.0
0.0
0.0
0.0
7.2
440.0
235.0
0.0
0.0
15.0
180.0
47.5
0.0
0.0
0.0
0.0
0.0

kg
kg
kg
kg
kg
kg
kg
liters
kg
liters
liters
liters
kg
liters
kg
kg
Input any
new chemicals
here

TACROM Job Summary Sheet (Step)

Well Name:

Turkey - 1200 m

Date

07/01/2011

Mixed Volume

180.0

Max Pressure

500

Bar

16/30 Sand

Pumped Volume

Extra

Pumping Rate

Bulk Density

Tank Mixed Chemicals

157.4

OC DE-11
1.5 l/m

2650

TRS CS-1

Tank
#1
#2
#3
#4
#5
#6
#7

l/m

Stage 1

Stage 2

Stage 3

Stage 4

Stage 5

0.9

1.1

1.2

1.2

APS

0.10

0.10

0.10

0.10

0.10

CL-20

1.50

1.00

1.00

1.00

1.00

GB-102 (25%)

Stage

Stage 1
Stage 2
Stage 3
Stage 4
Stage 5
Stage 6
Stage 7
Stage 8
Stage 9

CL Stage

40
10
15
30
61
0
0
0
0

Clean Vol Slurry Vol

m
m
0
40.0
50.0
65.0
95.0
156.0
156.0
156.0
156.0
156.0

0
40.0
50.2
65.8
98.4
167.6
167.6
167.6
167.6
167.6

Sand Slug

50-100
100-150

Abs Density

Bioclear
0.02 l/m

Breaker/Stage

4.8 m/min

1650

WGA 20
2.5 kg/m

22.6

Stage 6

Stage 7

Stage 8

WGA 20
kg
75
75
75
75
75
75
0
450

m
30.0
30.0
30.0
30.0
30.0
30.0
0.0
180.0

1.3
0.00

Rate
m/min

Conc
kg/m

CFR
m/min

GB-102
L/min

OC CL rate
g/l

APS rate
kg/min

4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8

0
50
100
230
360
0
0
0
0
0

4.8
4.71
4.63
4.42
4.23
4.80
4.80
4.80
4.80
4.80

4.3
4.7
5.1
5.3
5.1
0.0
0.0
0.0
0.0
6.2

7.2
4.7
4.6
4.4
4.2
0.0
0.0
0.0
0.0
0.0

0.48
0.47
0.46
0.44
0.42
0.00
0.00
0.00
0.00
0.00

OC DE-11
liter
45
45
45
45
45
45
0
270

BioClear
kg
0.6
0.6
0.6
0.6
0.6
0.6
0
3.6

Totals

Stage 9 Flush
1.3

TRS CS-1
liter
0
0
0
0
0
0
0
0

Sand Rate
kg/min
0
236
463
1016
1521
0
0
0
0
0

173.5 liters
15.6 kg
176.0 liters
Total Sand
kg/stage

500
1500
6900
21960
0
0
0
0

Cumm Prop Stage Time

Pumped
min
kg

500
2000
8900
30860
30860
30860
30860

8.33
2.08
3.13
6.25
12.71
0.00
0.00
0.00
0.00

End Stg Flush

1.4

157.4

169.0

4.8

END

4.80

6.2

0.0

0.00

30860

0.29

S.C. Tacrom S.R.L.

7 Str. Sinaii
1000389 Ploiesti, Romania

Company Hema Energy

Contract
0
Location Turkey
Field
Hema
Well Depth/PBTD (m)
/ 393.5
Tubing Size (mm)
2.4
Packer Type
0

JOB TICKET

Date
Company Rep.
Contractor Rep.
Well Number

07.01.2011
Selcuk Gurpinar
George Stavarache
Amasra CBM 2
Casing Size(mm) 4.5
Tubing Depth (m) 351
Packer set at (m) 351

Work Plan Main Frac

Function

Time
Date
Off Location
08:00
07.01.2011
Personnel on Site, Contractor
Name
First Name
On Site

Chief Frac Engineer

Koskamp

Ralph

Frac Engineer

Gunn

Matthew

Frac Engineer

Calota

C-tin

Frac Engineer

Angheloiu

Ioan

Frac Supervisor

Stavarache

George

Frac Supervisor

Lache

Adrian

Driver/Operator

Voica

Sorin

Driver/Operator

Carabus

Mihai

Driver/Operator

Istrate

Liviu

Driver/Operator

Ionita

Teodor

Driver/Operator

Stan

Bogdan Cat

Crew Supervisor

Aldea

Daniel

Driver/Operator

Barbu

Gheorghe

Driver/Operator

Finichiu

Alexandru

Driver/Operator

Malaescu

Iulian

Driver/Operator

Stanciu

Ioan

Driver/Operator

Cristu

Augustin

Driver/Operator

Constantin

Marian

Driver/Operator

Iancu

Ionel

Driver/Operator

Ionita

Vasile

CNCAN Licienced Operator

Ionita

Remus

Driver/Operator

David

Vasile

Driver/Operator

Enache

Florin

Driver/Operator

Ionita

George

Driver/Operator

Nazaru

Valentin

Driver/Operator

Manea

Neculai

Operator

Buzatoiu

Bogdan

On Location

File: 297225721.xls

Date
07.01.2011

5 / 45

Time
16:30
Off

x
x
x
x
x
x
x
x

x
x

S.C. Tacrom S.R.L.

7 Str. Sinaii
1000389 Ploiesti, Romania

JOB TICKET

Equipment on Site, Contractor Supply

Qty.
Hours
Description
Qty.
1
3
Manifold Truck
1
1
3
HP Manifold
1
1
3" HP Piping PN 15,000 PSI
1 set
1
4" LP Hoses
1 set
2 " Annulus relief valve
1
3
1.5
Volume heated
180
Volume filtered
Nuclear densitometer
Crane (40 tonne) with trailer
1
7
Tractor w/Crane & Trailer
Mileage to Location
Frac Fleet (Qty/km)
Tanks (Qty/km)
Propp(Qty(t)/km)
Tanks (Qty/km)
Chems.(Qty(t)/km)
Tanks (Qty/km)
Equipment on Site, Company Supply
Acid Pump
Annulus Pump Truck
1
Steam Generator w/ Piping
2" HP Piping
1 set
Flat Bed Truck
Crane
Proppant & Chemicals Used
Quantity mixed
168
m3
Quantity Pumped
168
m3
Tank mixed
On the fly
168
WGA 20
440
kg
OC TEA
0
l
BioClear
7.2
l
TRS APS
15
kg
OC DE-11
235
l
TRS CL-1
180
l
TRS CS-1
0
l
GB-102 100%
47.5
kg
OC TS 11
0
kg
0
16/20 FT ISP
0
12/20 Sand
kg
kg
32,000
16/30 Optiprop
0
16/30 Sand
kg
kg
0
20/40 Sand
0
70/140 Sand
kg
kg
Work Program
Re-Fill Fluid Tanks
Mix Frac Fluid
Safety Meeting
Pressure Test
Run Main Frac
Rig Down Frac Equipment
Comments
On the date of 06.01.2011, we tried to frac the well CBM 2, lower intervall.After 50 m3 of gel and s1.5 tonnes
of pumped sand, screen out in the wellbore occurred. We decided to repeat the operation next day with
crosslinked gel and redesign the entire job.
Name
Function
Name
Function
Company Representative
Contractor Representative
Selcuk Gurpinar
George Stavarache
Description
Data Van / h
Blender / h
Sand Truck
Pick-up Truck Ford/KIA
Crew transporter
Frac Pump Truck (TacRom) / h
Flat Bed Truck
Filteration / Heating Unit
Fluid Tanks(days/Qty)
Hydration Unit

Signature

File: 297225721.xls

Signature

6 / 45

S.C. Tacrom S.R.L.

7 Str. Sinaii
1000389 Ploiesti, Romania

File: 297225721.xls

JOB TICKET

7 / 45

Treatment Summary
General Info

Wellbore Data
Type
Wellbore Configuration
Size
Wall thick Grade
Tubing:
2.4
0
Casing: 1

4.5

Job Date:
07.01.2011
Job Type: Slick water - Cross-linked Water Frac

Capacity Max Pres

(m/m)
(bar)
0.0038

5.2

0.0187

TVD Top Perf

Midperf
Packer (m)

George Stavarache

TacRom Rep
Hema Energy
Turkey
Amasra CBM 2
Selcuk Gurpinar

Customer
Location
Well name
Customer Rep

Depth
(m)
351.0

Volume
(m)
1.34

393.5

0.21

Flush
(m)
1.55

Perforations
Top
Bottom
(m)
(m)
362.0

SPM

366.0

362
364
351.0

PBTD (m)

393.5

Treating Mode

Fluid in Tanks Minifrac

Pre-Job
m
Post-Job
0.0
m
Pumped
m
Fluid in Tanks Mainfrac
Pre-Job
180.0
m
Post-Job
23.1
m
Pumped
156.9
m

255.0
350.0
60.0
50.0

Bar
Bar
Bar
Bar

Avg Treating Press

Minifrac Results
Surface ISIP
BH ISIP
Surface closure
BH Closure

118.0
135.0
102.4
137.8

Bar
Bar
Bar
Bar

Closure time
Fluid effic.
Net Pressure
Frac Gradient

Minifrac
Rate
m
m
m
m
m
kg

Formation Treated

Proppant Data
Proppant Type
Mesh Size
Pumped Minifrac
Pumped Mainfrac
In Formation
Sand Plug sand slug
Final Conc @ Perfs

Treatment Data
Max Treating Pressure
Max Allowable Press
Annular Relief Set
Annulus Pressure

Pumping Summary
Stage
Volume
Hole fill
Step rate
Calibration
Flush
Total
Sand

Tubing

m/min
m/min
m/min
m/min

4.4
38
17.5
37.3

Pumping Summary
Stage
Volume
Pad
Sand stg
Flush
Total

min
%
Bar
kPa/m

Badger
16/30
0
32,000
32,000

0
0
0

ISIP Press mainfrac

ISIP Press minifrac
Net Pressure gain

118.0

Bar
Bar
Bar

Mainfrac
Rate
m
m
m
m

m/min
m/min
m/min

kg

Design vs Actual ***(Main frac only)***

Design
Fluid + sand design
169.0453 m
Sand designed
kg

Actual
Fluid + sand pumped
Sand pumped

0.0
32,000

m
kg in formation

Totals
Water mixed
Gelled Water pumped
Total Gel + sand
Sand pumped

WGA 20
Bioclear
OC DE 11
OC CS 11

440
7.2
235
0

118.0

Calc perfs open

32000.0

m
m
m
kg

kg
kg
kg
kg
kg/m

360

Sand pumped

180.0
156.9
0.0
32,000

50-100 kg/m3

230 Bar

sandstone

kg
l
l
l

Sand in formation

OC CL 20
OC TEA
OC APS
GB-102 10

180
0
15
47.5

32,000

l
l
kg

Hema Energy

Company
Contract number
Date
Contractor Rep
Customer rep
Location

January 7, 2011

George Stavarache
Selcuk Gurpinar
Turkey

Field
Well Name
Well Depth
Plug back depth
Casing Size
Tubing Size
Tubing Depth
Packer type
PSD
Perfs (from:to)
TVD Top Perf
On Loc Minifrac
Finish Minifrac
Start Main frac
Off Loc Mainfrac

Type of sand used

Hema
Amasra CBM 2
393.5
4 1/2
2.4
351

Zone

Coal

Thickness

5.2

Time
Time
Time
Time

08:00
16:30

351
362

366
362

Date
Date
Date
Date

07.01.2011
07.01.2011

Sand
Sand
Sand
Carbolite
Optiporop
Sand

Mini Frac
12/20 Sand
16/30 Sand
70/140 Sand
16/20 FT ISP
16/30 Optiprop
20/40 Sand

Sand
Sand
Sand
Carbolite
Optiporop
Sand

Main Frac
12/20 Sand
16/30 Sand
70/140 Sand
16/20 FT ISP
16/30 Optiprop
20/40 Sand
0

kg
kg
kg
kg
kg
kg
q

kg
32,000 kg
kg
kg
kg
kg
kg

Version 1.5
Revised October 5, 2010

mm
mm

Fluid Quality Test

Amasra CBM 2
1.) Minifrac

07/01/2011

Procedure:
1. Watersamples taken from each tank, tested volume 200 [ml]
2. Temperature measurement
3. pH measurement
4. add 0.3 ml OC CS 11 + OC DE 11 0.3 ml + 0,84 [g] of WGA-20 (4.2 kg/m3)
5. 5 min mixing time + 20 minutes hydration time
6. viscosity measurement
7. add 0,3 [ml] of OC CL 20 cross linker (1.5l/m3)
8. check fluid flow
9. add 0,04 g of DRB-HT Breaker (0.1 kg/m3)
10. wait 1 hour at reservoir temperature
11. check fluid flow
.
Results:
Reservoir Temperature:
T [C]

pH [-]

[cp]

Tank 1
Tank 2
Tank 3
Tank 4
Tank 5
Tank 6
Tank 7
Tank 8

2.) Mainfrac
Proceedure before Treatment:
1. Pad sample taken from each mixed tank, tested volume 200 [ml]
2. Temperature measurement
3. viscosity measurement

Minifrac Design

Amasra CBM 2
1/7/2011
Chemicals /Tank
5.0 kg/m WGA20
1.5 l/m3 OC DE 11
1.5 l/m3 OC CS 11
0.05 kg/m DRB-HT
2.0 L/m OC CL20

1. Circulate pumps to blender

2. Press ure test to
600
3. Open well
4. Pump
2.1 m3 linear gel
Pump rate
3 m3/min
5. Step down with linear gel
Volume
0
6. Reset counters
Pump rate
3
7. Pump Job
0
Flush
2.1
8. Wait until closure

m3
m3/min
m3 x linked gel

12-17 m3 100-200 kg/m3

m3 linear gel

Total; Volume Pumped

4.3 m3

Minifrac Calculation
Casing
0.018721 [m3/m]
Tubing
0.003826 [m3/m]
BH
393.5 [m]
Tubing Depth
351 [m]
TOP
362 [m]
BOP
366 [m]
Hole Fill
2.1 [m3]
Step up
0 [m3]
Step down
0 [m3]
Minfrac Volu
0 [m3]
Flush
2.1 [m3]
Total Pumped
4.3 [m3]

Casing volumes
OD inches Wall mm
5 1/4
7.7
5 1/2
6.2
5 1/2
6.9
5 1/2
7.7
5 3/4
9
6 3/4
8.05
7
10.36

0.011
0.0127
0.0124
0.0121
0.0128
0.0189
0.0193

Tbg volumes
OD inches Wall mm
2 7/8
C90
2 7/8
J55

0.0025
0.003

WELL #

Amasra CBM 2

Description

UM

WGA 20

kg

Minifrac
-

Bioclear

TRS DE-1

TRS CS-1

OC TS 11

kg

OC TEA

OC APS

kg

kg

Sand

12/20 Sand

Sand

16/30 Sand

Sand

70/140 Sand

Carbolight

16/20 FT ISP

16/30 Optiprop

OC CL 20
DRB HT

Optiprop
Description

UM

WGA 20

kg

Mainfrac

Bioclear

7.20

TRS DE-1

235.00

440.00

TRS CS-1

OC TS 11

kg

OC TEA

OC APS

kg

15.00

180.00

kg

47.50

OC CL 20
DRB HT
Sand

12/20 Sand

Sand

16/30 Sand

32,000.00

Sand

70/140 Sand

Carbolight

16/20 FT ISP

16/30 Optiprop

Optiprop

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

FRACTURE GEOMETRY

PREJOB DESIGN

FRACTURE CONDUCTIVITY

PREJOB DESIGN

Slurry Volume
Liquid Volume

m
m

Proppant Mass

kg

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

PRODUCTION DATA

PREJOB DESIGN

STIMULATED VERSUS UNSTIMULATED

PREJOB DESIGN

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

SCHEDULE

PREJOB DESIGN

NPV

PREJOB DESIGN

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

FRACTURE PROPAGATION SOLUTION

PREJOB DESIGN

PROPPANT DESIGN SUMMARY

PREJOB DESIGN

PREJOB DESIGN

PREJOB DESIGN

PREJOB DESIGN

PREJOB DESIGN

PREJOB DESIGN

PREJOB DESIGN

PREJOB DESIGN

PREJOB DESIGN

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

FRACTURE GEOMETRY

POST JOB DESIGN

FRACTURE CONDUCTIVITY

POST JOB DESIGN

Slurry Volume
Liquid Volume

m
m

Proppant Mass

kg

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

FRACTURE PROPAGATION SOLUTION

POST JOB DESIGN

PROPPANT DESIGN SUMMARY

POST JOB DESIGN

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

NET PRESSURE MATCH

POST JOB DESIGN

PRESSURE MATCH

POST JOB DESIGN

Amasra CBM 2 / Coal

Perforations:362 to 366m / Date: 7 January, 11y

CHEMICALS

HYDRATION UNIT CHEMICALS

POST JOB DESIGN

POST JOB DESIGN

POST JOB DESIGN

POST JOB DESIGN

POST JOB DESIGN

POST JOB DESIGN

POST JOB DESIGN

POST JOB DESIGN