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Neutron Radiography
Reading III-Level1Exercise
My ASNT Level III,
Pre-Exam Preparatory
Self Study Notes
3 July 2015
http://homework55.com/apphysicsb/ap5-28-08/
Nuclear Source-Reactors
Neutron Source-Cyclotron
3. Techniques/Calibrations
Micro-radiography
Multifilm technique
Laminography (tomography)
Stereoradiography
Panoramic exposures
Triangulation methods
Gaging
Autoradiography
Flash Radiography
In-motion radiography
Fluoroscopy
4. Interpretation/Evaluation
Image-object relationships
Material considerations
Codes, standards, and specifications
5. Procedures
Imaging considerations
Film processing
Viewing of radiographs
Judging radiographic quality
6. Safety and Health
Exposure hazards
Methods of controlling radiation exposure
Operation and emergency procedures
Reference Catalog Number
NDT Handbook, Third Edition: Volume 4,
Radiographic Testing 144
ASM Handbook Vol. 17, NDE and QC 105
Charlie Chong/ Fion Zhang
http://meilishouxihu.blog.163.com/
Greek
Alphabet
http://greekhouseoffonts.com/
http://minerals.usgs.gov/minerals/pubs/commodity/
Charlie Chong/ Fion Zhang
http://periodictable.com/Properties/A/NeutronCrossSection.html
Charlie Chong/ Fion Zhang
Screen Types-1
1. Transfer screen-indium or dysprosium, In, Dy.
2. Thermal neutron filter using Cadmium for epithermal neutron radiography,
Cd.
3. Converter screen uses gadolinium which emit beta particles, Gd.
4. the beta particles are caught by a fluorescing zinc sulfide material
5. Scintillator screen: Zinc sulfide, Lithium carbonate, plastid scintillator
6. Neutron Accelerator Target material: Beryllium, Be.
7. Boron used for neutron shields.
Screen Types-2
1.
2.
http://www.naturalreaders.com/
Reading III
Content
Reading One: ASNTHBVol4Chapter16
Reading Two: ASNTNRTMQ123
Reading Three:
Reading Four:
Reading-1
ASNTHBVol4Chapter16
FIGURE 1. Electric bridge wire squid: (a) drawing and (b) neutron radiograph
of part as aid to interpretation; (c) helium-3 gaseous penetrant applied to
serviceable unit; (d) penetrant applied to dysfunctional unit.
FIGURE 1. Electric bridge wire squid: (a) drawing and (b) neutron radiograph
of part as aid to interpretation; (c) helium-3 gaseous penetrant applied to
serviceable unit; (d) penetrant applied to dysfunctional unit.
(b)
FIGURE 1. Electric bridge wire squid: (a) drawing and (b) neutron radiograph
of part as aid to interpretation; (c) helium-3 gaseous penetrant applied to
serviceable unit; (d) penetrant applied to dysfunctional unit.
(c)
FIGURE 1. Electric bridge wire squid: (a) drawing and (b) neutron radiograph
of part as aid to interpretation; (c) helium-3 gaseous penetrant applied to
serviceable unit; (d) penetrant applied to dysfunctional unit.
(d)
Users Guide
Unlike many other forms of nondestructive testing, neutron radiography is not
a do-it-yourself technique. There have been neutron radiography service
centers in the United States since 1968. To try out neutron radiography on an
object of interest, it is simply necessary to locate the services currently
available and, if agreed, mail your item to them. Typically, the neutron
radiograph and your item will be mailed back within a day or two. The cost
could be less than 1 or 2 h of an engineers time. If assistance is required to
interpret the findings, this too may be requested on a service basis, as may
referrals to more specialized neutron radiographic techniques. The providers
of neutron radiography services use equipment and expertise that is highly
specialized. Even though one or more neutron radiography service centers
have been operating successfully for over 30 years, there has been no inhouse neutron radiography available at any general service, commercial
nondestructive testing center.
FIGURE 3. Radiographs of full size motorcycle: (a) neutron radiograph; (b) xradiograph.
Parallel & Divergent Collimator Fig. 2 Thermalization and collimation of beam in neutron radiography. Neutron collimators can be of the
parallel-wall (a) or divergent (b) type. The transformation of fast neutrons to slow neutrons is achieved by
moderator materials such as paraffin, water, graphite, heavy water, or beryllium. Boron is a typically used
neutron-absorbing layer. The L/D ratio, where L is the total length from the inlet aperture to the detector
(conversion screen) and D is the effective dimension of the inlet of the collimator, is a significant geometric
factor that determines the angular divergence of the beam and the neutron intensity at the inspection plane
Ug =D t/L
I = /16(L/D)2
I = Ioe nt
n = N
N = nuclei/cm2
N = N/A
N = Avogadro's number
n = N = [N/A]
For photons:
I = Ioe x t
Eq.1
For Neutron
I = Ioe Nt = Ioe n t
Eq.2
Where:
I is the transmitted beam;
Io is the incident beam;
x is the linear attenuation coefficient for photons;
t is the thickness of specimen in the beam path;
N is the number of atoms per cubic centimeter;
is the neutron cross section of the particular material or isotope
(a probability or effective area); and,
n is the linear attenuation coefficient for neutrons (n = N).
Where:
-is the linear attenuation coefficient of specific neutron (cm-1 ) ;
is the material density (g/cm3);
N is Avogadro's number (6.023 X 1023 atoms/gram-molecular weight) ;
is the total cross section in barns (cm2 ) ; and
A is the gram atomic weight of material.
Charlie Chong/ Fion Zhang
The established direct imaging technique uses thin gadolinium layer vapor
deposited on a solid converter screen, which is held flat against a single
emulsion film inside a vacuum cassette of thin aluminum construction. An
exposure of 109 neutrons per square centimeter (109 n/cm2) can give a high
resolution, high contrast radiograph if careful dust free film darkroom
procedures are used.
Neutron sensitive imaging plates consist of a thin phosphor layer containing a
mixture of storage phosphor, neutron converter and organic binder. Following
the neutron exposure stage is the information readout phase, in which the
plate is scanned by a thin laser beam stimulating the emission of a pattern of
light.
Merits of this neutron imaging technique include five decades of linearity (?) ,
wide dynamic range, direct availability of digital data for processing converter
efficiencies of 30 to 40 percent, and spatial resolution acceptable for some
applications.
(b)
(d)
(f)
http://www-llb.cea.fr/spectros/spectro/2t1.html
Another reactor that has provided neutron radiography services since 1968 is
illustrated in Fig. 6. It is above ground and the fuel of the 100 kW core is
arranged in an annulus with a moderator region in the center.
Two horizontal beams are extracted from the central moderator, one for direct
film neutron radiography of nonradioactive objects, the other for dysprosium
activation transfer neutron radiography of radioactive nuclear fuel.
Another service for static neutron radiography of radioactive nuclear fuel has
been provided by a 250 kW nuclear reactor installed in a hot cell complex (Fig.
7). Also several university reactors in the United States have been equipped
for neutron radiography. Worldwide, over fifty nuclear reactors have
contributed to development of this field.
Hot cell
Shielded nuclear radiation containment chambers are commonly referred to
as hot cells. The word "hot" refers to radioactivity. Hot cells are used in both
the nuclear-energy and the nuclear-medicines industries. They are required
to protect individuals from radioactive isotopes by providing a safe
containment box in which they can control and manipulate the equipment
required.
Hot cell
Shielded nuclear radiation containment chambers are commonly referred to
as hot cells. The word "hot" refers to radioactivity. Hot cells are used in both
the nuclear-energy and the nuclear-medicines industries. They are required
to protect individuals from radioactive isotopes by providing a safe
containment box in which they can control and manipulate the equipment
required.
https://en.wikipedia.org/wiki/Hot_cell
Hot cells at the Argonne National Laboratory. Each cell is equipped with a
viewing window and two remote manipulators.
https://en.wikipedia.org/wiki/Hot_cell
Applications:
Hot cells are used to inspect spent nuclear fuel rods and to work with other items which are high-energy
gamma ray emitters. For instance, the processing of medical isotopes, having been irradiated in a nuclear
reactor or particle accelerator, would be carried out in a hot cell. Hot cells are of nuclear proliferation concern,
as they can be used to carry out the chemical steps used to extract plutonium from reactor fuel. The cutting of
the used fuel, the dissolving of the fuel and the first extraction cycle of a nuclear reprocessing PUREX process
(highly active cycle) would need to be done in a hot cell. The second cycle of the PUREX process (medium
active cycle) could be done in gloveboxes.
Hot cells are commonly used in the nuclear medicines industry: - for the production of radiopharmaceuticals,
according to GMP guidelines (industry) - for the manipulation and dispense of radiopharmaceuticals (hospitals)
The user must never be subject to shine paths that are emitted from the radioactive isotopes and therefore
there generally is heavy shielding around the containment boxes, which can be made out of stainless steel 316
or other materials such as PVC or Corian. This shielding can be ensured by the use of lead (common) or
materials such as concrete (very large walls are therefore required) or even tungsten. The amount of
radioactivity present in the hot cell, the energy of the gamma photons emitted by the radioisotopes, and the
number of neutrons that are formed by the material will prescribe how thick the shielding must be. For instance
a 1 kilocurie (37 TBq) source of cobalt-60 will require thicker shielding than a 1 kilocurie (37 TBq) source of
iridium-192 to give the same dose rate at the outer surface of the hot cell.
Also if some actinide materials such as californium or spent nuclear fuel are used within the hot cell then a layer
of water or polyethylene may be needed to lower the neutron dose rate.
https://en.wikipedia.org/wiki/Hot_cell
Viewing windows:
In order to view what is in the hot cell, cameras can be used (but these require replacing on a regular basis) or
most commonly, lead glass is used. There are several densities for lead glass, but the most common is 5.2
g/cm3. A rough calculation for lead equivalence would be to multiply the Pb thickness by 2.5 (e.g. 10 mm Pb
would require a 25 mm thick lead glass window). Older hot cells used ZnBr2 solution in a glass tank to shield
against high-energy gamma rays. This shielded the radiation without darkening the glass (as happens to
leaded glass with exposure). This solution also "self-repairs" any damage caused by radiation interaction, but
leads to optical distortion due to the difference in optical indices of the solution and glass.
Manipulators:
Telemanipulators or tongs are used for the remote handling of equipment inside hot cells. These are incredibly
valuable as they do not require the user to place his/her arms inside the containment box and be subject to
heavy finger/hand doses. These need to be used in conjunction with a shielded sphere which can be made by
most lead engineering companies.
Gloves:
Lead loaded gloves are often used in conjunction with tongs as they offer better dexterity and can be used in
low radiation environments (such as hot cells used in hospital nuclear medicine labs). Some companies have
developed tungsten loaded gloves which offer greater dexterity than lead loaded gloves, with better shielding
than their counterparts. Gloves must be regularly replaced as the chemicals used for the cleaning/ sterilisation
process of the containments cause considerable wear and tear.
Clean rooms:
Hot cells are generally placed in clean rooms with an air classification ranging from D to B (C is the most
common). It is extremely rare to find a hot cell which is placed in a class A or unclassified clean room.
https://en.wikipedia.org/wiki/Hot_cell
Hot Cell
http://wwojnar.com/2012/10/research-nuclear-reactor-maria/
Hot Cell
Charlie Chong/ Fion Zhang
http://wwojnar.com/2012/10/research-nuclear-reactor-maria/
Hot Cell
http://wwojnar.com/2012/10/research-nuclear-reactor-maria/
http://wwojnar.com/2012/10/research-nuclear-reactor-maria/
Hot Cell
Hot Cell
http://wwojnar.com/2012/10/research-nuclear-reactor-maria/
Hot Cell
http://wwojnar.com/2012/10/research-nuclear-reactor-maria/
Hot Cell
Hot Cell
http://wwojnar.com/2012/10/research-nuclear-reactor-maria/
The system provided a peak thermal neutron flux of about 109 neutrons per
square centimeter second (109 ncm-1s-1), two orders of magnitude less than
the reactor systems described above but sufficient for low throughput work
using 2 h exposure times and a relatively low beam collimation ratio.
Cyclotrons and radio frequency quadrupole accelerators are other candidates
for a potential custom designed in-house neutron radiographic system.
Neutron radiographic performance data have been reported for designs with a
variety of sizes, neutron yields and costs. For transportable systems much of
the development work has used sealed tube acceleration of deuterium tritium
mixtures. This can consist of a source head that is maneuverable with long
high tension cable linking it to the high voltage power supply and control unit
as illustrated (Fig. 9). The particular type shown yields a peak thermal neutron
flux of about 108 neutrons per square centimeter second with a tube operation
half life of about 200 h.
http://www.orau.org/ptp/collection/Sources/cf-252.htm
Californium-252 Neutron
Source
Neutron Fluence
Particle fluence is defined as the number of particles
traversing a unit area in a certain point in space in a
unit period of time. Most frequently, it is measured in
ncm-2.
In particular, neutron fluence in high-energy physics
applications is of interest in the context of the
radiation environment around the interaction regions
of colliders; it serves as a measure for potential
radiation damage for the detector systems to be used
there. It is common practice to express charged and
neutral particle contributions to radiation in terms of
dose ( Radiation Measures and Units) and 1 MeV
neutron equivalent fluence ( also NIEL Scaling),
respectively.
The 1 MeV equivalent MeV equivalent neutron
fluence is the fluence of 1 MeV neutrons producing
the same damage in a detector material as induced
by an arbitrary particle fluence with a specific energy
distribution. The choice of this particular normalization
is partly due to historical reasons, as the standard
energy to scale to was considered first in damage
studies in the MeV range, in neutron physics;
however, there is also a physical background: the
neutron spectra expected in detectors at future
hadron colliders typically have a probability density
peaking in this energy region.
See also ASTM E261 - 10
Charlie Chong/ Fion Zhang
http://ikpe1101.ikp.kfa-juelich.de/briefbook_part_detectors/node123.html
FIGURE 12. Frames from real time studies of operating aircraft engine: (a)
first view; (b) second view.
FIGURE 14. Neutron radiographs of explosive bridge wire igniter: (a) thermal
neutron image; (b) cold neutron image.
Explosive charge
Charlie Chong/ Fion Zhang
3.6 Closing
Industry standards have been published on neutron radiographic testing.
End Of Reading 1
Reading-2
ASNTNRTMQA123
Level-I
Level 1 Questions
Neutron Radiographic Testing Method
Level 1 Answers
Neutron Radiographic Testing Method
Level 1 Answers
Neutron Radiographic Testing Method
Q6. Many of the absorption differences between neutrons and X-rays indicate
clearly that the two techniques:
a. cause radiation problems
b. complement each other
c. increase exposure speed
d. fog radiographic film
Q7. The neutron cross section is the term normally used to denote:
a. the danger in handling radioactive material
b. the absorbing power of a material for neutrons
c. the atomic number of neutron reactor material
d. radiation detection equipment
Q8. The sharpness of the outline in the image of the radiograph is a measure
of:
a. subject contrast
b. radiographic definition
c. radiographic contrast
d. film contrast
Charlie Chong/ Fion Zhang
Q9. The highest quality direct neutron radiographs obtainable today use:
a. imaging screens using lithium-zinc sulfide as the imaging materials
b. high-speed radiographic films
c. dysprosium as an imaging screen
d. gadolinium as an imaging screen (?)
Q10. When doing neutron radiography on radioactive materials, the materials
are best handled:
a. directly by personnel equipped with special protective clothing
b. by remote handling equipment
c. directly by personnel with special protective clothing except when
radiographs are being made
d. by the same methods used for nonradioactive materials
Q14. What has the highest thermal neutron absorption cross section?
a. gold
b. Indium
c. gadolinium
d. dysprosium
Q15. Conversion screens are used in neutron radiography:
a. to convert neutron energy into ionizing radiation
b. to increase the exposure time
c. both a and b are reasons for using conversion screens
d. neither a nor b is a reason for using conversion screens
Q16. A curie is the equivalent of:
a. 0.001 mCi
b. 1000 mCi
c. 1000 MCi
d. 100 MCi
The neutrons transmitted through a radioactive specimen will strike a metal detection
foil such as indium, dysprosium or gold, rather than a converter screen with film.
Q20. For inspection of radioactive objects or those that emit gamma radiation
when bombarded with neutrons, a preferable detection method is the:
a. direct exposure method
b. transfer method
c. isotopic reproduction method
d. electrostatic-belt generator method
Q24. A graph showing the relationship between film optical density and
exposure is called:
a. a bar chart
b. a characteristic curve
c. an exposure chart
d. a logarithmic chart
Q25. The three main steps in processing a radiograph are:
a. developing, frilling, and fixation
b. developing, fixation, and washing
c. exposure, developing, and fixation
d. developing, reticulation, and fixation
Q26. Radiographic contrast in a neutron radiograph is least affected by:
a. developer temperature
b. radiographic exposure time
c. radiographic beam collimation
d. radiographic film fog
Ug?
Q30. Which of the following materials is best for making identification labels
when using the neutron radiographic process?
a. aluminum
b. brass
c. cadmium or gadolinium
d. lead
Q34. Movement, geometry, and screen contact are three factors that affect
radiographic:
a. contrast
b. unsharpness
c. reticulation
d. density
Q35. The difference between the densities of two areas of a radiographic film
is called:
a. radiographic contrast
b. subject contrast
c. film contrast
d. definition
Q36. The selection of the proper type of film to be used for neutron
adiographic examination of a particular part depends on the:
a. thickness of the part
b. material of the specimen
c. neutron energy
d. none of the above (all the above?)
Q37. When radiographing a part that contains a large crack, the crack will
appear on the radiograph as:
a. a dark, intermittent, or continuous line
b. a light irregular line
c. either a dark or light line
d. a fogged area on the radiograph
Q38. Radiographic sensitivity, in the context of defining the minimum
detectable flaw, depends on:
a. the graininess of the film
b. the unsharpness of the flaw image in the film
c. the contrast of the flaw image on the film
d. all of the above
Charlie Chong/ Fion Zhang
Internal-conversion Electrons
http://wwwndc.jaea.go.jp/CN10/index.html
Reading- 2+
Booster
7. IMAGE RECORDERS
The neutron radiographic image recording on film is based upon two different
principles:
1) Silver Halide Based- A chemical process, caused by photons or
electrons ?e? in a photographic or Xray film: the image generation
occurs through a photon or electron triggered conversion of dispersed
minute grains of 0.1 to 3 m silverhalide crystals to metallic silver in a
gelatine coating on triacetate or polyester film base. During the film
development and fixation process, only the metallic silver is retained (black)
and fixed on the film, providing a high contrast image.
2) Trek etch Based- A physical process, caused by alpha particles (in
thermal NR) or recoil protons (in fast NR) in a nitrocellulose film: the
image generation is based on traces (defects) in the nitrocellulose film
produced by the alphas or protons . The alphaparticles originate from a
neutron/alpha reaction in a converter layer of boron or/and lithium in
contact with the film. The traces in the film are visualized and fixed by
etching in an alkaline solution.
Charlie Chong/ Fion Zhang
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Since most of the accepted screen materials can be used in one form or
another with each readout technique, the whole provides a wide range from
which to choose for the radiographic problem in hand. Even when expense
excludes the most sophisticated ones. A rational choice of image recorder
can only be made with a knowledge of the basic performance characteristics
of each screen readout system; signal buildup with exposure, neutron
registration efficiency, spatial resolution, and where relevant, half-life of the
secondary radiation. Data on the detectors and converters are given in
chapter 8.
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
However, the shape of the curves for films exposed to light, as in radiography
with fluorescent screens of photography, do not depend upon the type of film,
the color of the exposing light and the processing conditions used. All that
these films know is that they are being exposed to various intensities of light,
and their characteristic curves show graphically how they respond to these
intensities. The characteristic curve of a film exposed to X-rays or gammarays depends only on the film type and the processing conditions, not upon
the quality of the radiation nor the scattering characteristics of the subject.
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Film contrast refers to the slope (steepness) of the characteristic curve of the
film. It depends upon the:
(1) type of film,
(2) the processing it receives, and
(3) the film density.
It is this latter quantity, film contrast, with which this section is concerned.
Since the shape of the characteristic curve is independent of the major
radiographic variables, film contrast can be considered quite independently of
subject contrast, although, as pointed out above, both contribute equally to
the radiographic contrast that enables one area to be distinguished from
another when the finished radiograph is viewed on the illuminator. As can be
seen in Fig. 7.1, the slope, or steepness of the characteristic curve at first
increases with increasing film density (the toe); then, in the middle range of
densities becomes fairly straight; and finally, at higher densities the slope
decreases as density increases (the shoulder).
Practical.NR Chapter 7
Practical.NR Chapter 7
The shoulders of the curves for industrial X-ray films, and of the directexposure type of medical X-ray films, come at densities far above those that
can be viewed on available illuminators. Changes in the slope of the
characteristic curve have a definite relationship to the visibility of details in the
radiograph. For example, two slightly different thicknesses in the subject will
transmit slightly different exposure to the film. The exposures will have a
certain ration, i.e., will have a certain log exposure difference between them.
The difference in densities corresponding to the two exposures will depend
upon just where on the characteristic curve they fall; the steeper the curve,
the greater will be the density difference. This means that a certain log
exposure interval in the middle of the curve of Fig. 7.1 will correspond to a
greater density difference than the same interval at either end.
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
If the exposure is such that the densities fall on that part of the curve where
the gradient is 3.4, the 20% intensity difference results in a density difference
of 0.31 (or a difference in light transmission of 104%). In general then, if the
gradient of the characteristic curve is greater than 1.0, the intensity ratios, or
subject contrasts, of the radiation emerging from the subject are exaggerated
in the brightness ratios of the radiograph, and the higher the gradient, the
greater is the degree of exaggertion. Thus, at densities for which the gradient
is greater than 1.0, the film acts as a contrast amplifier. Similarly, if the
gradient is less than 1.0, the subject contrasts are less apparent in the
radiographic reproduction.
Practical.NR Chapter 7
Practical.NR Chapter 7
For example, if one film requires half the exposure to reach a certain density
as does a second film, and if the slower film is chosen as the standard, the
faster one will have a relative speed of 2.00. The choice of the film to which a
relative speed of 1.00 be assigned, is purely arbitrary, and may be made on
the basis of convenience alone. (See Table 7.3).
In a group of characteristic curves, those for the faster films will lie towards
the left of the diagram, in the region of smaller values of logarithm of relative
exposure, or, phrased differently, in the region where a smaller exposure is
needed to produce a certain film density. Conversely, the curves for the
slower films will lie towards the right side of the diagram in the region where
the relative exposure, or its logarithm, is larger. From such a diagram, relative
exposusres to produce a fixed density can be read, and the relative speeds
will be inversely proportional to these exposures (see Fig. 7.8). The speeds of
industrial X-ray films are usually determined at a density between 1.5 and 2.5
dependent on the manufacturer.
Practical.NR Chapter 7
Practical.NR Chapter 7
7.1.6. Use of the characteristic curve. The characteristic curve can be used in
the solution of quantitative problems arising in radiography, in the preparation
of technique charts and in radiographic research. Ideally characteristic curves
made under the actual radiographic conditions should be used in solving
practical problems. A range of screen-film signal exposure curves are shown
in Figs. 7.4 and 7.5. It must be observed immediately that in neutron
radiography exposure prediction to better than -25% should not be expected
from such curves, even when great care is taken to variations in beam energy
spectra between neutron radiographic facilities, used converter foil thickness,
type of film developer, manual or machine processing.
Practical.NR Chapter 7
Practical.NR Chapter 7
Figure 7.5. Typical signal-exposure characteristics for selected films used in conjunction with
charged particle (electron) emitting neutron intensifying screens of Gadolinium (25 m) and
Dysprosium (100 m)
Note: The exposure scale for Dysprosium is estimated for the transfer technique with a foil
exposure <1 half-life and a film exposure >3 half-lives
Charlie Chong/ Fion Zhang
Practical.NR Chapter 7
Close inspection of the gadolinium foil curves in Fig. 7.4 would show that it is
in fact close to exponential in shape. It is close to linear, therefore, when a
linear exposure scale is used (Fig. 7.5), as is the response of all films when
exposed directly to charged particles. Thus, sensitivity improves as exposure
is increased. Linear signal-exposure characteristics are, in fact, quite common
in neutron radiography, since they also apply to the track-etch technique and
to most electronic readout methods. So the less conventional style of
presentation used in Fig. 7.5 has advantages over that of Fig. 7.4.
Practical.NR Chapter 7
Unfortunately, these simple and helpful relations must now be qualified, since
only with a constant background signal is the full contrast of the recorder
realised. Generally, neutron radiography has to be carried out in the presence
of a background of both scattered neutrons and gamma radiation which
increases with exposure. Background due to gamma radiation can be readily
avoided by using Bi filters, track-etch technique, or an intensifying screen in
which the neutron produced reaction has a convenient half-life (Table 7.4). In
the latter case the screen alone is exposed to the neutron beam and the
stored image transferred to a film by autoradiography elsewhere; this is
known as the transfer technique. However, scattered neutron background
cannot be easily eliminated and generally increases with object thickness.
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical application. As the choice of an image recorder will depend upon the
need to obtain either good radiographic quality or high speed, it is only
possible to give general guidance as to their selection. When high quality is
required a fine grain film or track-etch material should be used; When speed
is the important parameter then fast X-radiographic type films should be used.
The image recorders given in Tables 7.5 to 7.7 and 7.9 are recommended,
based upon the practical experiences of radiographers. Detailed data on
some of the converter materials listed in Table 7.4 are given in chapter 10 in
Tables 10.5 to 10.9.
Practical.NR Chapter 7
TABLE 7.7. Effective thermal neutron absorption of lithium fluoride and boron
carbide screens
Practical.NR Chapter 7
7.1.8. Sensitometric standards. For X-ray films exposed to X- and gammarays ISO has issued a standard for the determination of speed and average
gradientt. No such international standard exists for X-ray films used in neutron
radiography. However, AFNOR has published a French standard for industrial
radiographic films used for neutron radiography with gadolinium converters.
In this standard the mode of irradiation and the method of determining the
sensitivity and average contrast of films used in industrial neutronography is
described. The spectrum of energy of the electrons emitted by the converter
during irradiation with neutrons is replaced by the spectrum emitted by carbon
14. A planar, non filtered carbon 14 source is used for the irradiation of films.
It is placed in close contact with the emulsion side of the film. The irradiation
ought to be such as to produce a characteristic curve including net density
between 1.5 and 3.5. The sensitivity S is determined from the formula:
Practical.NR Chapter 7
where E, and E2 are the exposures for net densities of 1.5. and 3.5.
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Provision of several images with different contrast from one film when
developed (etched) in steps and intermediately transferred to copying film.
Sharp image of objects containing low contrast materials.
Shorter or comparable imaging times to indirect method with X- ay
film/Dysprosium foil.
Practical.NR Chapter 7
At present two types of nitrocellulose film and converters are routinely used
by NRWG members:
1. A combined film, in form of sheets, where the nitrocellulose film is coated
on both film faces with in water soluble converters, e.g. Kodak CN 85 B,
and
2. as separate film and foils, in form of sheets and on rolls, e.g. Kodak CN 85
nitrocellulose film, and Kodak BN 1 converter foil with natural boron or
Kodak BE 10 converter foil with enriched boron. The roll-film is especially
suited for automatic NR-film cameras, e.g. For stepwise imaging of long
objects. The converter foils are re-usable.
The thickness of commercially available nitrocellulose film is approx. 100 m
and of the converters approx. 50 m. The films and foils are produced in
standard film sizes.
Practical.NR Chapter 7
7.2.2. Film handling and safety precautions. Nitrocellulose film handling and
storage requires in addition to cleanliness also special attention and
provisions due to:
1. The inflammablity.
2. The low auto-ignition temperature of approx. 180C (e.g. Kodak CN85).
3. The self-decomposition, causing release of nitrous gases, damaging the
film (leading to incidental spots, sticky surface or change of film color).
Film mountings and handling should avoid damage and processing artefacts
caused by:
1. Dust, attracted by static electricity, introduced by relative movements of
the plastic foils.
2. Moisture, destroying the converter layer of the combined film. Therefore,
nitrocellulose films and converter foils should be passed through a
decharging and cleaning device prior to mounting.
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
7.2.3. Exposure techniques and mounting. The exposure technique and film
processing form two closely-linked parameters and control the image
generation and its quality. As nitrocellulose film is an integrating image
recorder the exposure time is the main controlling factor in image generation
when considering a given NR-facility and image recording system. Typical
neutron fluences for a standard image on nitrocellulose film are summarized
in Table 7.10. It is common practice to optimize the exposure data for an
anticipated application by proof testing. Generally, under-exposure followed
by longer etching will provide a higher contrast image; whereas high- xposure
followed by short etching will deliver a low contrast, but sharper image. The
best radiographic image is obtained when the film is in contact with the object
or very closely positioned behind it.
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Practical.NR Chapter 7
Q60. Which elements are commonly used in the indirect transfer method?
a. gadolinium and cadmium
b. rhodium and samarium
c. dysprosium and indium
d. cadmium and dysprosium
75. White crescent-shaped marks on an exposed X-ray film are most likely
caused by:
a. crimping film after exposure
b. crimping film before exposure
c. sudden extreme temperature change while processing
d. a warm or exhausted fixer
76. Reticulation resulting in a puckered or netlike film surface is probably
caused by:
a. crimping film after exposure
b. sudden extreme temperature change while processmg
c. water or developer on unprocessed film
d. excessive object-film distance
77. Frilling , or loosening of the emulsion from the base of the film is
most likely caused by:
a. water or developer on unprocessed film
b. the low temperature of processing solutions
c. developer solution contamination
d. a warm or exhausted fixer solution
78. When the minute silver grains, on which the X-ray film image is formed,
group together in relatively large masses, they produce a visual impression
called:
a. air bells
b. graininess
c. reticulation
d. frilling
79. Static marks, which are black tree-like or circular marks on a radiograph,
are often caused by:
a. the film being bent when inserted in a cassette or holder
b. foreign material or dirt embedded in screens
c. scratches on lead foil screens
d. improper film handling techniques
80. The purpose of agitating an X-ray film during development is to:
a. protect the film from excessive pressure
b. renew the developer at the surface of the film
c. disperse unexposed silver grains on the film surface
d. prevent reticulation
81. When manually processing films, the purpose of tapping the hangers
sharply two or three times after the films have been lowered into the
developer is to:
a. disperse unexposed silver grains on the film surface
b. prevent frilling
c. dislodge any air bubbles clinging to the emulsion
d. all of the above
82. The decrease in activity of the developer solution is compensated by:
a. constant agitation
b. maintaining processing solutions within the recommended temperature
range
c. avoiding contamination from the wash bath
d. adding replenisher
87. The normal development time for manually processing X-ray film is:
a. 12 to 18 minutes in processing solutions at 75 F
b. 3 to 8 minutes in processing solutions at 75 F
c. 12 to 18 minutes in processing solutions at 68 C
d. 5 to 8 minutes in processing solutions at 68 F
88. A properly exposed radiograph that is developed in a solution at a
temperature of 58 F will be:
a. overdeveloped
b. underdeveloped
c. fogged
d. damaged by frilling
91. The average thermal neutron flux that gives a dose of 100 mrem in 40
hours is:
a. 700 n/cm2s
b. 70 n/cm2s
c. 7 n/cm2s
d. 0.7 n/cm2s
92. When working with a neutron radiography facility, the radiation expected
is:
a. gamma
b. beta
c. neutron
d. all of the above
93. The intensity of neutron radiation is usually measured m:
a. roentgens
b. ergs
c. neutrons/cm-s
d. neutrons/cm
Charlie Chong/ Fion Zhang
94. What does the term (R/h) refer to when speaking of intensity?
a. radiation limits for humans
b. roentgens per hour
c. X -rays per hour
d. radiation in hydrogen
95. Small amounts of exposure to neutrons or gamma rays:
a. may have a cumulative effect that must be considered when
monitoring for maximum permissible dose
b. will be beneficial since they build up an immunity to radiation poisoning.
c. will have no effect on human beings
d. will have only a short-term effect on human tissues
http://www.chemicalelements.com/elements/cf.html
The neutrons transmitted through a radioactive specimen will strike a metal detection
foil such as indium, dysprosium or gold, rather than a converter screen with film.
Q119. The term macroscopic cross section () " is synonymous with the:
a. linear attenuation coefficient () for neutrons
b. microscopic cross section () for neutrons
c. mass attenuation coefficient (/) for neutrons
d. cadmium ratio for neutrons
Comments:
= N/A, = microscopic cross section, = = macroscopic cross
section
MACROSCOPIC SCATTERING CROSS SECTIONS
The distinction between macroscopic and microscopic cross-section is that
the former is a property of a specific lump of material (with its density), while
the latter is an intrinsic property of a type of nuclei.
https://en.wikipedia.org/wiki/Nuclear_cross_section
Peach
Good Luck
Good Luck
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Charlie Chong/ Fion Zhang