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Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
1 +, 1 +
01 ' 5
Jawaharlal Nehru
! $ ' +-
Satyanarayan Gangaram Pitroda
! > 0 B
BharthariNtiatakam
IS I 1676. 1960
xxxx
2009
Indian Standard
SPECIFICATION FOR
OLEIC ACID, TECHNICAL
FO\Irin Reprint JANUARY 1998
( Incorporating Amendment No.1)
UDe 665.127.42
C Copyright
BUREAU
OF
1968
INDIAN
STANDARDS
Gr4
Nounnb" 1960
Indian Standard
SPECIFICATION FOR
OLEIC ACID, TECHNICAL
DaJ. S.
BADAMI
M",*"
Da S. L. BAJfMuJu
S.... N. BHOWllUt
or
Directorate Sugar
AJricuhure )
a:
Direetonte GeaeraJ of Suppliel &: DiJpcu1J (Miniatry of Worlu, Houainl &: Supply)
Development WioI, MlDiatry of Commerce &:
Industry
~emic:a.l Worb,
Delhi
SHUJ. B. DAVIU
HiDdustan Lever Ltd, Bombay
DR G. S. HA'l'TlAJIlODt ( AlJmuIU)
5lftt N. DamAClIIAa
The Tata Oil Mi11a Co Lad, Bombay
DR B. G. GUJms ( .4ltmJiIU)
S.... S. B. DtrI'rA
The Te&tile Auociation ( India) Regd, Bombay
SHIU SA'l'tIK DIIAJ ( .flllrru* )
SHIUS. C. GHOIS
IDdiaD Soap ad Toiletrin MUm' AIIociation,
Calc:utta
SHal P. R. Artu ( A.~)
SHU R. K. MALm
Direc:tOnteof Marketinl
Impection (Miniatry
Food Acriculture)
SHIUB. S. MODI
The Vaaupad ManuCacturen' AIIociation or India,
Bombay
SHU K. G. MATRtJa (~)
SKat 011 hAKAaB
Harcourt Butler TecbDolocical Imtitute, Kanpur
SHU H.ll. R.A.JA
Bombay Oibced. aDd OiJa &chancc Lid, Bombay
a:
a:
or
(A""""')
DR H. G. RAllAltaJlll1fA 1laooY
GovenlilleDt Soap Factory, BaoCalore
S.... K. A. N. RAG (A""")
( ContWft OIIIGI' 2 )
18 I 1676 1960
( eolllittMMlfrom N' I )
M"u,,1
n. M. L. au GUPJ'A
Da M.
Bombay
CouDdI oI8clmtiBc I: IDdUItrial Reteareb
Da M. SWAMDCATIIAIC ( .u",.,..,,)
D. Y. K. S~RARlWfYAil
Directorate GeDerai of Health Servicea (M1D1Itry Of
Health )
8DJ S. a GAIfOVLY (.4/",.,..,,)
s... L. R. StID
MbUatry oIDefeDce (R I: D)
DR LAs. O. VUIWC ( ~ )
Director, lSI
S.,,1arlu
DR SAIlQO'AL
S... S. SWaAJDWn'AIf
DR G. S. HATTlAIfODI
MlIII1IIn
81m G. M. Jou.u ( A"",.,. to
Dr G. S. Hattiaqdi)
Da K. J. B.u.AuDHlCAif
M1DJItry or Defence ( R I: D)
SID! K. J(. GAlfOVLY ( AltIrMtI)
SHaI N.1bIowMm
DeveIoPmeDt Wine. Miniltry or Commerce I:
IDClUItry
8HaI N. DumAClRAa
The Ta.. 011 MilIa 00 Ltd, Bombay
Da D. G. GUM" ( ..clImtc,,)
SBasS. C. GBoa
IDdiaD bp and Toiletria Maken' A.odatiOD,
Calcutta
SBaJ R. It. M.wz
Dlrectonte of Marketillf I: IaapectiOD (Minlatry of
food I: ARriculture)
S.... B. S. MODI
The Vuupati MaDuCacturen' AIIoc:IatioD of IDdia,
Bombay
BRa. 011 Pa.u.uH
Harcourt Butler TechDo1ollcailmtitute, KaDpur
D. S. P. PATJLu:
8eDaru Hindu University, VaraDUi
s H. R. R.A,JA
Bombay Oilleedll: Olla ExchaDlC Ltd, Bomba,
SID! ClwtAIfDAI V. MAanvALA
(.411mtM1 )
AMENDMENT NO. 2
FEBRUARY 1976
TO
Alteration
[Pa.~e 4 (jJoge 5 of the reprint), Table I, clause rrfn ence under the title oj
the table J- Substitute ' ( Clauses 4.3 and 5.1 )' for' ( Clauses 4.2 and :1.1 ) '.
Addenda
I Page 3 (page 4 of the reJlrint), clause 4.1.1] - Add the following new
clause after 4.1.1 and re-number the existing clause' 4.2' as ' 4.3 ':
'4.2 Fluxing Property - The material, when intended for Defence use,
shall also pass the test prescribed in Appendix C. '
(I'age 12, clause
after B-3.2.3:
APPENDIX C
( Clause 4.2 )
TEST FOR FLUXING PROPERTY
c-r.
C-2. MATERIALS
C-2.1 Tin Plates-two of 10
c-3.1 Take the tin plates and polish them with emery paper. De-grease
them with a suitable solvent and finally clean with dry cloth.
C-3.2 Apply oleic acid by brush on the part of the surface of the plates
to be soldered. Put the soldering material Oll the portion to be soldered
and spray it by red hot solder gun. Put the plates one over the other and
allow the soldered plates to cool for 2 to 3 minutes. The soldered portion
shall not get detached under normal stress.
C-3.3 The test shall be taken as satisfactory if the plates do not get
separated easily when tried to break off the soldered joint.
(CAFDC 5)
2
Reprography Unit. 815, New Delhi, India
18 I 1676 1960
Indian Standard
SPECIFICATION FOR
OLEIC ACID, TECHNICAL
o.
FOR E W 0 R D
0.1 This Indian Standard was adopted by the Indian Standards Institution
on 4 July 1960, after the draft finalized by the Oils, Fats and Soaps
Sectional Committee had been approved by the Chemical Division
Council and the Agricultural and Food Products Division Council.
0.2 Oleic acid is used in India in the manufacture of various products,
such as lubricants, carbon paper, stencil paper, paints, cosmetics, liquid
soaps, disinfectants, textile finishing preparations, printing inks, pharmaceuticals, metal polishes, etc. Although there are many commercial
specifications drawn up by individual manufacturers which relate to
different grades of oleic acid, these have no official recognition and no
standard has yet been formulated for this material by any country. In
preparing this standard, due consideration has been given to the different
grades of oleic acid being used at present for various purposes.
0.3 Taking into consideration the views of producers, consumers and
technologists, the Sectional Committee responsible for the preparation of
this standard felt that it should be related to the manufacturing, trade
and technological procedures followed in the country in this field.
0.4 In the preparation of this standard, substantial aasistance has been
derived from the valuable data made available by various organizations
in this country, notably Calcutta Chemical Co Ltd, Calcutta; Godrej
Soaps Private Ltd, Bombay; Hindustan Lever Ltd, Bombay; Modi
Vana.tpati Manufacturing Co Ltd, Modinagarj Navsari Oil Products Ltd,
Naveari; and Standard-Vacuum Oil Compan~ Ltd, Bombay. The
following publications were also referred to:
British Pharmacopoeia, 1958
United States Pharmacopoeia, 1955
0.5 Indian Standard Methods of Sampling and Test for Vegetable Oils
and Fag (IS: 548-1954-) is a necessary adjunct to this standard. Besides,
thiJ .tandard requires reference to IS: l07{).1960 Specification for Water,
Distilled Quality ( Rlvisld).
0.5.1 Wherever a reference to apy Indian Standard mentioned in 0.5 or
otherwise appean in this standard, it shall be taken as a reference to the
latest venion of the standard
SiDce reviled.
IS I 1676 1960
I. SCOPE
1.1 This standard prescribes the requirements and the methods of test for
oleic acid, "technical.
2. GRADES
2.1 The material shall be of three grades, namely, Grade 1, Grade 2 and
Grade 3.
2.1.1 Grade 1 is recommended for UK in the manufacture of COIrneticl.
3. SAMPLING
3.1 Representative lam pies of the material Ihall be drawn as prescribed in
Appendix A.
f. REQ.UIREMENTS
f.2 The material shall also comply with the requirements given in Table I.
5. TESTS
5.1 Testl shall be carried out by methods prescribed in col 6 and 7 of
Table 1.
6. PACKING AND MAltKlNG
6.1 The material Ihall be lupplied in suitable containers, u
between the purchaser and the lupplier.
agreed
11116781_
T4IIL& I
~ ~
I)
i)
(2)
Grade 1
Grade 2
Grade 5
(2)
(of)
(5)
M.
M ..
025
025
Ii) R,pooificadOll value,
197
IlK
W) Acid value .hall DOt differ
fromaaponjficadOll value by
..
6
8
more thaD
90 to 95 85 to 95 85 to 95
Iv) Iodine value
NU
NU
Nil
v) NiDeral acidity
01
01
025
vi) Aih, percent by welsht, M.
YO) U...ponliable . .tter, per10
15
loS
ceIl& by welPt, M.
Mel
15
20
21
vW) Poq, point
Is) Colour I'I~ CIQ .... Loft 1500 Y+ 10'0Y1;.
15R.1D 200R.
boDcI""lI..
ro),
MaTaoD cw TIlT,
..
14
6
IS
Bol
Bo2
7
12
tSlace,......
a) Maautae:turer'. name;
b) RecopiIed trad~mark, if any;
c) Name and ....de of the material.
d) Wdaht of the material in the containeri
e) Month and year otthe manufacture; and
r) Batch Dumber In code or otberwile to enable the lot of manufaet\11'e to be need back &om recorda.
'.2.1 The COGtalaen may alto be marked with StaD~.rd mark.
1.1.2 TIle UIC of tbe StiDdard Mlrk I. 80vered by 1be provisions of tbe
Burtlll of laelllD Stladuds Act. 1986 lad tbe Rules Ind Regulilions made
lberea.r. ne detans of conditlona under wbicb Ibe licence for Ibe.use of
Sliadard Mark may be pRIed to mlnuflcturera or produced may be obtained
flOa die Ba... of IDdlia StiDd,...
117.1_
lam'" -
A-3.~ t .....
The third set of the teat aamplea, bearinl the
seals 0( the purchuer and the IUpplier, aball constitute the rd'eree umple
and lhall be used in cue or dispute between the purchaser and the luppher.
It shall be kept at a place IIreed to between the purcbuer and the lupplier.
A-.5.2 The teat reaultl (or sapoDifieation value. acid value and pour point
shall be recorded u abown In Table III. The mean andthc range ahall
be c:aJculated u foUows ud ahaU be recorded in col aad 5 reapecdveJr
otTable III:
ThN:tr
8..
No.
(J)
ClaAuoruIma
(2)
I) Sapoalficadoa value
iI) Add value
W) Pourpobac
(t)
il
il
it
(5)
(6)
R. il-46RI
Its
Cam_lOlI
00IIf0ugry
(7)
=ed
Corrected mean~
=
f::l8ed
valuela
able I (it)
Corrected
mean
~
ir-46Ra
valuela
able I (Ill)
s::
valueiD
able I (vW)
18 I 1676. 1960
A-5.3 The composite sample when tested for the remaining characteristics
not tested in A-5.2 shall satisfy the corresponding requirements for them
al specified in Table I.
APPENDIX B
( Table I)
TEITS FOR MINEIlAL ACIDITY. ASH AND POUR
POINT
8-1. TEST FOR MINElUL ACIDITY
8-1.1 ~aUty of R,ent. - Unless specified otherwise, pure chemicalt
and distilled water (s" IS: 1070.1960) shall be employed In telts.
Non - Pure chemicals' shall mean chemicals that do not contain impurities which
affect the resultl or analysil.
.1
fuaed
U I 1676.1960
contents gently. Incinerate the residue in a muffle furnace at 550 100e
until free from carbon. Cool the crucible in a desiccator and weigh.
Repeat the above procedure of heatin$" cooling and weighing until the
difference between two successive weighmgs does not exceed I mg.
"2.3 CaleuladoD
-w
.
100 w
Ash, percent by weight where
- 38e to + 500
1C
108 mm
225 10 mm
5'5 to 8'0 mm
Cylindrical
7 to 11) mm
Not greater than stem
65 to 805 rom
l20mm
5C from -35e
100e from _30C
To allQw heating to
Plain
0'5Q
o,
""
10
11,16711_
Fro. 1
Pou.
PODn'
11
IS I 1676 1960
8-3.1.5 Bath G - of any size and shape convenient for obtaining the
required temperature, and equipped with a support which will hold
jacket D firmly in a vertical position.
8-3.1.5.1 It is convenient to have two or more baths available when
determining pour points below 10C.
8-3.1.5.2 The bath liquid may be maintained at the required
temperature by refrigeration, if available, taking care to avoid disturbance
of the bath liquid and also avoiding direct contact of any immersed cooling
coil. with the jacket. Alternatively, one of the following freezing mixtures
may be used in the bath;
For Temperature Down to
JOOC
Crushed ice and water
-12C
Crushed ice and sodium chloride
-25C
Crushed ice and calcium chloride crystals
-55C
Solid carbon dioxide and acetone
Free,ting Mixture
8-3.2 Procedure
8-3.2.1 Pour the material, heated in a water-bath, if necessary, into the
jar to a height of 51 to 57 mm (see 8-3.2.1.1). Close the jar with the cork
carrying the thermometer so that the thermometer bulb is immersed vertically in the material with the beginning of the capillary 3 mm below the
surface. Heat the material, without stirring, to a temperature of 4Goe in
a bath maintained at a temperature not higher than 48C. Cool the sample
to 32C in air or in a water-bath at approximately 25C. Fit the gasket
on to the jar 25 mm from the bottom and insert the jar into the jacket.
The disc, the gasket and the jacket shall be kept clean and dry.
8-3.2.1.1 The jar may be marked to indicate the proper level of the
sample.
8-3.2.2 Once the material has cooled enough to allow the formation of
wax crystals, take great care not to disturb the mass of sample nor to permit
the thermometer to shift in the sample. Any disturbance of the spongy
network of crystals will lead to false results.
8-3.2.3 Maintain the bath temperature of the cooling bath at minus
1 to plus 12C. Support the jacket and jar in a vertical position in the
bath 110 that not more than 25 rom projects from the cooling medium.
Beginning at a temperature 12C before the expected pour point, at each
thermometer reading which is a multiple of 3C, remove the jar from the
jacket carefully and tilt it just enough to ascertain whether there is a movement of the material, and replace it; this complete operation, removal and
replacement should take not more than three seconds. Take care not to
disturb the mass of the liquid nor to permit the thermometer to shift in
12
IS I 1676- 1960
the liquid. If the material has not ceased to flow when it has been cooled
to goe, place the jar and jacket in another bath maintained at a temperature of minus 15 to minus 18C. If the material has not ceased to Bow
when it has been cooled to 6C, place the jacket and jar in another bath
maintained at a temperature of minus 32 to minus 350. As soon as the
material ceases to flow when the jar is tilted, hold the jar in a horizontal
position for exactly 5 seconds. If the sample shows any movement, replace
the jar in the jacket and cool the material another 3C. If the material
shows no movement during the 5 seconds, record the reading of the
thermometer. Take the pour point as the temperature 3C above this
temperature.
13
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