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BS 1016-104.3:
1998
ISO 562:1998
BS 1016-104.3:1998
National foreword
This British Standard is the UK implementation of ISO 562:1998. It
supersedes BS 1016-104.3:1991 which is withdrawn.
The UK participation in its preparation was entrusted to Technical Committee
SFI/3, Analysis and testing of coal and coke, which has the responsibility to:
aid enquirers to understand the text;
present to the responsible international/European committee any
enquiries on the interpretation, or proposals for change, and keep the UK
interests informed;
monitor related international and European developments and
promulgate them in the UK.
A list of organizations represented on this committee can be obtained on
request to its secretary.
Cross-references
The British Standards which implement international or European
publications referred to in this document may be found in the BSI Standards
Catalogue under the section entitled International Standards Correspondence
Index, or by using the Find facility of the BSI Standards Electronic
Catalogue.
A British Standard does not purport to include all the necessary provisions of
a contract. Users of British Standards are responsible for their correct
application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.
Summary of pages
This document comprises a front cover, an inside front cover, pages i and ii,
the ISO title page, page ii, pages 1 to 6 and a back cover.
This standard has been updated (see copyright date) and may have had
amendments incorporated. This will be indicated in the amendment table on
the inside front cover.
Date
Comments
BS 1016-104.3:1998
Contents
National foreword
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagent
5 Apparatus
6 Preparation of the test sample
7 Procedure
8 Expression of results
9 Precision
10 Test report
Annex A (informative) Bibliography
Figure 1 Example of suitable furnace
Figure 2 Silica crucible and lid
Figure 3 Crucible stands
Table 1
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Inside front cover
iii
1
1
1
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4
5
5
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2
3
4
5
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BS 1016-104.3:1998
Foreword
ISO (the International Organization for Standardization) is a worldwide
federation of national standards bodies (ISO member bodies). The work of
preparing International Standards is normally carried out through ISO technical
committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee.
International organizations, governmental and non-governmental, in liaison with
ISO, also take part in the work. ISO collaborates closely with the International
Electrotechnical Commission (IEC) on all matters of electrotechnical
standardization.
Draft International Standards adopted by the technical committees are circulated
to the member bodies for voting. Publication as an International Standard requires
approval by at least 75 % of the member bodies casting a vote.
International Standard ISO 562 was prepared by Technical Committee
ISO/TC 27, Solid mineral fuels, Subcommittee SC 5, Methods of analysis.
This second edition cancels and replaces the first edition (ISO 562:1981), which
has been technically revised.
Annex A of this International Standard is for information only.
Descriptors: Solid fuels, fossil fuels, coal, pit-coal, coke, tests, determination of content, volatile
matter, gravimetric analysis, test equipment.
ii
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BS 1016-104.3:1998
Introduction
3 Principle
1 Scope
This International Standard specifies a method of
determining the volatile matter of hard coal and of
coke. It is not applicable to brown coals and lignites.
2 Normative references
The following standards contain provisions which,
through reference in this text, constitute provisions
of this International Standard. At the time of
publication, the editions indicated were valid. All
standards are subject to revision, and parties to
agreements based on this International Standard
are encouraged to investigate the possibility of
applying the most recent editions of the standards
indicated below. Members of IEC and ISO maintain
registers of currently valid International Standards.
ISO 331:1983, Coal Determination of moisture in
the analysis sample Direct gravimetric method.
ISO 687:1974, Coke Determination of moisture in
the analysis sample.
ISO 11722:1), Solid mineral fuels Hard coal
Determination of moisture in the analysis sample by
drying in nitrogen.
1) To
4 Reagent
Cyclohexane of recognized analytical grade.
5 Apparatus
5.1 Furnace, heated by electricity, in which a zone of
uniform temperature of 900 C 5 C can be
maintained. It may be of the stop-ended type or
fitted at the back with a flue approximately 25 mm
diameter and 150 mm long (see Figure 1).
NOTE It is important for furnaces with flues that the furnace
door seal well. The flue should not reach far out of the oven and
should be fitted with a butterfly valve to restrict airflow through
the furnace.
be published.
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7 Procedure
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8 Expression of results
The volatile matter V in the sample as analysed,
expressed as a percentage by mass, is given by the
equation:
100 ( m 2 m 3 )
V = -------------------------------------M
( m2 m1 )
9 Precision
Table 1
Volatile matter
Reproducibility
critical difference
Hard coal of
volatile
matter < 10 %
Hard coal of
volatile
matter >10 %
3 % of the
mean result
Coke
0,5 % absolute
or 4 % of the
mean result,
whichever is
greater
10 Test report
where
m1
m2
m3
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BS 1016-104.3:1998
Annex A (informative)
Bibliography
[1] ISO 1170:1977, Coal and coke Calculation of analyses to different bases.
[2] ISO 1213-2:1992, Solid mineral fuels Vocabulary Part 2: Terms relating to sampling testing and
analysis.
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BS 1016-104.3:
1998
ISO 562:1998
BSI
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