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Feasibility Study On Iron Ore Mine Tailings

1.0 Introduction
India has large reserves of metal-bearing ore and occupies the sixth position in the
world for iron-ore reserves. Therefore, India is an important iron-ore producer and
exporter. However, approximately 1015% of the iron ore mined in India is unutilized,
even now, and is discarded as tailings. The tailing wastes that are called ultra fines or
slimes, mainly those ore solids having a diameter of less than 150 m, are not regarded to
be useful and hence are discarded. In India, approximately 1012 million tons of such
mined ore is lost as tailings. The safe disposal or utilization of such vast mineral wealth in
the form of ultra fines or slimes has remained as a major unsolved and challenging task
for the Indian iron-ore industry. Inevitably, the proportion of iron-ore wastes generated
will steadily increase, because the demand for iron ores will increase. Such a view is
confirmed by the number of steel plants that have been planned for future construction in
the state of Orissa and other parts of India. The total production of iron ore in India is
expected to exceed 400 million tons within the next decade. Therefore, dealing with the
environmental consequences of such enormous quantities of tailings will be a Herculean
task. It is therefore imperative that state-of-the-art iron-ore mining and processing
technologies be adopted to address and implement effective utilization of tailings.
Cementing materials have been used since thousands of years. Egyptians
employed calcined impure gypsum to grout the space between the huge blocks of stones
of the pyramids [1]. Greeks and Romans used calcined limestone as the building material.
In India powdered burnt clay and flat lime were mixed and wetground in the edgerunner
to get a plastic sticky mass to be used as mortar. Greek and Romans discovered that
certain volcanic deposits if finely ground and mixed with lime and sand yielded a mortar
as superior strength which was also resistant to actions of water.
In the eighteen century the most important advance in the field of cements leading
to the invention of modern Portland cement was made. John Semeaton carried out
investigations and discovered that mortars containing considerable clayey matter give the
best results. The investigations of L J Vicat on hydraulic lime led him to prepare an
artificial hydraulic lime by calcining an intimate mixture of limestone and clay, ground
together in a wet mill. In 1756 Joseph Parker burnt the nodules of argillaceous limestone
at a higher temperature than that used for burning lime. This was the beginning of cement
industry which later assumed great importance. The quality of cement varied considerably
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Feasibility Study On Iron Ore Mine Tailings


depending on the constituents of raw materials. Investigations soon began to experiment
with artificial mixtures of limestone and argillaceous rocks. Such a procedure had an
advantage that lime and clay could be mixed in the desired ratio and hence the properties
of the product could be kept under a more uniform and definite control. It was in 1824
that Joseph burnt the mixture of lime and clay at high temperatures and patented as
Portland Cement.
There were few problems and issues in cement production:
1. Shortage of Portland Cement
2. Scale of Production
3. The Utilisation of patterns of Cement
To overcome above mentioned difficulties Alternative Secondary Cements were
introduced, some of the better known alternatives are:
1. Portland-Pozzolona Cement
2. Portland-Blast furnace slag cements
3. Lime-Pozzolona cements.
Alternatives 1 and 2 are essentially variants of Portland cement and are dependent
on availability of Portland cement. Hence Lime-Pozzolona cement is considered as the
secondary alternative to Portland cement.
Surkhi or Burnt clay pozzolona have been used in India since ancient times to
produce a hydraulic cement by mixing it with lime. The term pozzolona has been used to
designate reactive siliceous and aluminous materials, which react with calcium
hydroxide in presence of moisture to form stable cementations compounds.
The following pozzolonic materials have been generally used:
1.

Waste Bricks

2.

Waste Tiles

3.

Burnt clay

4.

Flyash

5.

Rice husk ash

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Feasibility Study On Iron Ore Mine Tailings

2.0 History
2.1 Kudremukh Iron Tailings:
Kudremukh- meaning Horses Face in Kannada derives its name from the
shape of the highest peak obtaining in the Aroli- Gangamula range of the Western Ghats.
The deposits, principally Low grade Magnetite were discovered in 1913 by Late
Dr.P.Sampath Iyengar, a geologist of Mysore State. However the scientific Investigations
were carried out from 1965 to 1975 by NMDC & proved a mineable reserve of 430
Million Tons.
The Countrys prestigious 100% export oriented unit and Mini Rathna Company,
KIOCL Ltd was incorporated on 2nd April 1976. Headquartered at Bangalore with the
Company's mining and beneficiation facilities located at Kudremukh and was Asias
largest iron oxide pelletisation complex and Pig Iron unit at the well connected coastal
city of Mangalore in Karnataka. The 3.5 million-tonne capacity Pellet Plant complex
commissioned in1987, comprises of the Filter Plant, Wet grinding mills, mechanized
ship loading unit, 28-mw captive power plant, Roll Press, Pelletisation discs, Furnace
etc.,
The idea of beneficiating the ore deposits was first proposed when several Japanese
companies came together with the NMDC, a Government of India undertaking, evincing
an interest in such a project. Pilot studies suggested that the surface ore with 38% iron
could be enriched to a concentrate of 67% iron with available new technologies. The
concentrate could be transported to Mangalore, on the coast of the Arabian Sea, 110 kms
to the west of Kudremukh. But global steel industry went into decline in the late sixties
and the Japanese withdrew. Interest was revived in early 1970 when Iran drew up its
plans for an ambitious domestic steel industry and was looking for a reliable supplier of
iron ore. Kudremukh seemed ideal, abundant just across the sea and an agreement was
reached.
The 7.5 million tonnes annual capacity project at Kudremukh along with the 67 km
slurry pipeline and filtration units at Mangalore was to be completed in August 1980.
Soon after processing the ore, waste material called tailings were dumped in Lakya Dam
through pumping. Till now 184.15 Million metric tonnes were dumped over area of 21.5
sq.Km.

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Feasibility Study On Iron Ore Mine Tailings

Mining activities at the worksite at Kudremukh, 110 Kms from Mangalore came to
halt from the end of 2005 with the Supreme Court confirming the status of Kudremukh
National Park area over the present mines at Kudremukh. The Company's Mangalore
units of Pellet Plant and Blast Furnace Units are running with the outsourced hematite
iron ore to convert into iron oxide pellets.
2.2 Red Soil:
Red soils denote the second largest soil group of the country covering an area of
about 6.1 lakh sq. km (18.6% of the Country's area) over the Peninsula from Tamil Nadu
in the south to Bundelkhand in the north and Rajmahal hills in the east to Kachchh in the
west. They surround the black soils on their south, east and north.
These soils are found in large tracts of western Tamil Nadu, Karnataka, southern
Maharashtra, Chhattisgarh, Andhra Pradesh, Orissa and Chotanagpur plateau of
Jharkhand. Scattered patches are also seen in Birbhum (West Bengal), Mirzapur, Jhansi,
Banda, Hamirpur (Uttar Pradesh), Udaipur, Chittaurgarh, Dungarpur, Banswara and
Bhilwara districts (Rajasthan).
These soils, also known as the omnibus group, have been developed over
Archaean granite, gneiss and other crystalline rocks, the sedimentaries of the Cuddapah
and Vindhayan basins and mixed Dharwarian group of rocks. Their colour is mainly due
to ferric oxides occurring as thin coatings on the soil particles while the iron oxide occurs
as haematite or as hydrous ferric oxide, the colour is red and when it occurs in the hydrate
form as limonite the soil gets a yellow colour. Ordinarily the surface soils are red while
the horizon below gets yellowish colour.
The texture of red soils varies from sand to clay, the majority being loams. Their
other characteristics include porous and friable structure, absence of lime, kankar and free
carbonates, and small quantity of soluble salts. Their chemical composition include nonsoluble material 90.47%, iron 3.61 %, aluminium 2.92%, organic matter 1.01%, magnesium 0.70%, lime 0.56%, carbon-di-oxide 0.30%, potash 0.24%, soda 0.12%, phophorus
0.09% and nitrogen 0.08%. However significant regional differences are observed in the
chemical composition.

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Feasibility Study On Iron Ore Mine Tailings


In general these soils are deficient in lime, magnesia, phosphates, nitrogen, humus
and potash. Intense leaching is a menace to these soils. On the uplands, they are thin, poor
and gravelly, sandy, or stony and porous, light-coloured soils on which food crops like
bajra can be grown. But on the lower plains and valleys they are rich, deep, dark coloured
fertile loam on which, under irrigation, can be produced excellent crops like cotton,
wheat, pulses, tobacco, jowar, linseed, millets, potatoes and fruits. These are also
characterized by stunted forest growth and are suited to dry farming.
Ray Chaudhary (1941) Land Use Specialist, Planning commission, Govt. of India,
has morphologically grouped red soils into following two categories:
a) Red Loam Soil-these soils have been formed by the decomposition of granite,
gneiss charnocite and diorite rocks. It is cloddy porous and deficient in concretionary
materials. It is poorer in nitrogen, phosphorus and organic materials but rich in potash.
Leaching is dominant.
These soils have thin layers and are less fertile. These soils are mainly found in
Karnataka (Shimoga, Chikamagaluru and Hassan districts), Andhra Pradesh (Telangana),
eastern Tamil Nadu, Orissa, Jharkhand (Chotanagpur), Uttar Pradesh (Bundelkhand),
Madhya Pradesh (Balaghat and Chhindwara), Rajasthan (Banswara, Bhilwara, Bundi,
Chittaurgarh, Kota and Ajmer districts), Meghalaya, Mizoram, Manipur and Nagaland.
b) Sandy Red Soil-these soils have formed by the disintegration of granite, granigneiss, quartzite and sandstone. These are friable soil with high content of secondary
concentrations of sesquioxide clays.
Due to presence of haematite and limonite its colour ranges from red to yellow
These soils have been rightly leached occupying parts of former eastern Madhya Pradesh
(except Chhattisgarh region), neighbouring hills of Orissa Andhra Pradesh, and Tamil
Nadu (Eastern Ghats and Sahyadris.

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Feasibility Study On Iron Ore Mine Tailings

3.0 Literature review


3.1 Literature Review on Tailings:
Govt. of Karnataka (2013) [3] has set up the R&D Centre at National Institute
of Technology Karnataka to carryout research in the field of conversion of various
solid industrial wastes into value-added products. The centre has made successful
preliminary studies on the substitution of Iron Ore Waste Tailings for clay and other
raw materials used in the manufacture of various building products. Hammond(1998)
[4] in his study critically reviewed the usage of mining waste as building material. He
identified many mining wastes as concrete aggregates and pigments for paints.
Increase in mining may contribute in the future to local environmental damage or
health consequences of nearby residents. Such sites must be restored for sustainable
development, or, at least, secured to prevent off-site contaminant movement.
Mrs Mangalpady Aruna (2012) [2], studied the suitability and reliability of iron
ore tailings in manufacture of paving blocks. The results of the study show that the
compressive strength of tailing based mix was higher with 36.5 MPa for 28 days.
The outcome of study carried out by Gan et al.(2011) [15] shows that the burning
and steam curing free brick product (iron ore tailings, fly ash, sand, CaO, gypsum and
cement) has a comprehensive strength of 28.30 MPa and flexural strength of 5.63
MPa. Yongliang et al. (2011) [16] prepared eco-friendly bricks from hematite tailings.
Besides hematite tailings, the additives of clay and fly ash were also added to the raw
material to improve the brick quality. The results of the study indicated that the
mechanical strength and water absorption of the fired brick specimens are around
20.03 22.92 MPa and 16.54 17.93 %, respectively. The other physical properties
and durability were as per Chinese Fired Common Brick Standard (GB/T5101-2003).
The experiment carried out by Jian et al. (2011) [17] on sintered wall materials
reveals that the iron ore tailings and waste can be used very effectively as construction
material. The study also shown that due to higher iron content in iron ore tailings and
waste rock, the products reduce the sintering temperature and decreased energy
consumption.

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Feasibility Study On Iron Ore Mine Tailings


Niu and Chen (2011) [18] used several additives in their study to improve the
properties of concrete product. Further, a study carried out by Yongliang et al.(2011)
[19] on utilization of hematite tailings in production of non-fired bricks resulted that
the nonfired bricks with 78 % hematite tailings can be prepared in the optimal
conditions of forming water content and forming pressure of 15 % and 20 MPa,
respectively. The suitable curing condition is natural curing in room temperature for
28 days. It was also found that the comprehensive strength of products can be up to
15.9 MPa with other physical properties and durability, which is well confirmed to
non-fired gangue brick standard (JC/T422-2007).
Wang et al. (2011) [20] worked on development and application of intelligent
decision support system for comprehensive utilization of tailings and waste rocks. The
idea was implemented and the system was built by combining engineering practice of
comprehensive utilization of tailing and waste rocks with other subjects like artificial
intelligence, neural network, fuzzy mathematics and decision making technology.
Robert and Richard (2011) [21] performed experiments on mineral processing
wastes and made classifications of solid wastes based on physical and chemical
properties of each type of waste material. The need for research for utilization of
waste material is also documented in the investigation. In general, most of the
researchers felt that there is a large scope for R&D in developing alternative building
technologies. In the present study pavement blocks were prepared using iron ore
tailings and experiments were performed to understand the changes in behavior of
concrete with the replacement of sand by iron ore tailings. Tests have been carried out
to assess the physical properties of tailings like strength, bulk density, water
absorption etc.
Chao et al. (2010) [12] in their study on innovative methodology for
comprehensive utilization of iron ore tailings prepared cementitious material by
blending 30 % residues, 34 % blast furnace slag, 30 % clinker and 6 % gypsum. The
results of the study show that the mechanical properties of such bricks were well
comparable with those of 42.5 ordinary portland cement according to Chinese
GB175-2007 standard.

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Feasibility Study On Iron Ore Mine Tailings


A recent study by Jinhua et al.(2010) [13] reveals that it is quick and
economical to use GIS in tailing management and can provide a new way for the
decision analysis of utilizing tailing resource reasonably. Manufacture of building
bricks without burning of solid fuel is one of the options for utilization of mining and
industrial wastes, which also reduces CO2 emission. A considerable research has been
carried out to establish alternative methods by non firing processes in making building
materials.
Mr Ullas et al (2009)[1], in his study Kuduremukh iron ore tailings was
chosen for investigation of its stability as fine aggregates in mortors. He successfully
showed optimum replacement of sand with tailings is about 25%.
Ajaka E. O (2009) [6], selected, Nigeria presently produces a tail sometimes
containing up to 22% iron minerals mostly natural fines in the ore and fines produced
inevitably during comminution. He analyzed the existing circuit and undertook
specific recovery tests on the tailing material using simple hindered settling and
floatation process for the recovery of fine iron minerals in the tailings.
Roy et al. (2007) [11] used gold mill tailings for preparation of bricks. They
used ordinary portland cement, black cotton soils and red soils to increase the
plasticity of bricks. The results of the investigation indicated that bricks with 20 % of
cement and 14 days of curing are most suitable. The study also revealed that soil
tailing bricks are very economical.
Amit and Rao (2005) [9] in their paper highlighted the present status of waste
based building materials in India. Kumar et al. (2006) [10] demonstrated the usage of
fly ash, blast furnace slag and iron ore tailings in the preparation of floor and wall
tiles. Further, preparation of synthetic granite from fly ash as a value added products
was also investigated. These developed synthetic granite tiles were reported to have
very low porosity (<0.5 %), high bending strength (38 MPa) and dense
microstructure. It was concluded that partial addition of iron ore tailing, fly ash and
blast furnace slag in suitable combination in ceramic tiles will improve its scratch
hardness (>6 on Mohrs scale) and flexural strength (>25 MPa).
Monalisa Mohanty et al (2001) [5], in his study he addressed
phytoremediation and associated processes as they apply to iron-ore wastes and
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Feasibility Study On Iron Ore Mine Tailings


mining sites. He showed phytoremediation is cost-effective and feasible because
plants are able to slowly absorb toxins into their tissues and thereby help clean toxins
from waste sites.
Jaladi, S. K. (2001) [8], in his Studies mentioned that

pre-cast concrete

technology is becoming more and more popular in the practical field. The strength
and weight are the preliminary objectives to be considered for a good pre-cast
concrete construction.
In India approximately 10 15 % of the iron ore mined is unutilized, even
now, and is discarded as waste/tailings due to lack of cost effective technology in
extracting low grade ores. Because of this huge piles of mine wastes are found in and
around mine areas. However, some of these waste materials possess potential
characteristics, which can be tapped for various uses [2].
Innovative and sustainable processes such as mineral polymerization and mineral
cementation have been developed in the past for manufacture of cold setting building
bricks to utilize the mining and mineral wastes [14]. It was found that by adopting
mineral polymerization process and curing in atmosphere temperature ranging 20 35C
and hot air temperature below 100C, considerable binding strength is developed. The
results of the investigation also indicated that the bricks produced by polymerization
reaction using 95 % fly ash, 50 % beneficiated iron ore tailings and red mud attain 80150 kg/cm2 crushing strength under atmospheric curing condition.
3.2 Literature Review on Surkhi-Pozzolana:
Surkhi mortor has been used in India for buildings since ancient times. In case of
Mettur dam, in Tamilnadu portland cement was used in the constriction with a 20%
replacement by sukhi.[22]. Most of the research work in India has been on Brick and
Burnt clay pozzolanas. Studies have been done on effect of mortor proportions, effect of
grinding, duration of burning etc.
Karnataka Engineering Research Station [24] conducted compressive strength
tests on sandless lime surkhi mortors with different proportions of lime and surkhi.
Maximum strength is 123 kg/cm.sq was obtained at 28 days.

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Feasibility Study On Iron Ore Mine Tailings


R K Ghosh et al. (1964) [25], his studies reveal that compressive strength of lime
surkhi mortars cannot approach rich compressive strength of cement mortars like 1:3 or
1:4. But lime surkhi mortars are comparable with the cement mortars of mix 1:6 that are
commonly used in masonry works. Results also shows that the flexural and tensile
strength are appreciably higher than that of cement mortar 1:6.
Ram Lal et al. (1964) [26] in his study on pozzolona finds that ,With replacing
20% cement with surkhi in Plain cement concrete reveals that there are not any
appreciable changes in strength parameters in 28 days and there has been savings up to
10% by use of surkhi as partial replacement of cement. In his experiment, 45 tonnes of
cement was saved for everyone and half furlong stretch of pozzolona concrete pavement.
Ralph E Grim (1962), [27], in his research studies mentions that kaolinite would
perhaps be the optimum clay mineral constituent since it would contribute alumina and
silica. He also mentions that desirable to use kaolinite in the manufacture of white
portland cement. He investigated effect of clays of varying clay mineral composition on
the water retention and compressive strength of cement mortars. He also found that there
is a little difference when clays of various mineral compositions are added, except that
those composed of montmorillonite were relatively less desirable. This is because they
require large amount of water to give suitable working consistency which tends to result
in mortar of inferior strength.
N R Srinivasan et al(1956) [23], in his study showed that the optimum
temperature of burning for montmorillonite minerals lies in between 6000-8000C, and
for kaoline minerals it is 8000C and for illite it is around 10000C. He also concluded that
loamy soils which are generally used for bricks cannot yield surkhi of high reactivity.
Studies done by Srinivasan reveal that a morillonite type of clay belongingnto BeidelliteNontronite series, with a good amount of naturally occurring iron oxides and hydroxides
is eminently suited for high grade surkhis.

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Feasibility Study On Iron Ore Mine Tailings

4.0 Methodology:

METHODOLOGY
METHDOLOGY

Tailing Sample collection

Red Earth Sample collection

Preparation of sample

Preparation of sample

Physical properties

Physical properties

Engineering properties

Engineering properties

Analysis of results

Analysis of results

Cube casting

Cube casting

Comparison of results

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Feasibility Study On Iron Ore Mine Tailings

Methodology:

Iron ore tailing sample collection at Lakya Dam (Kudremukh) using plastic bags
such that site moisture is well maintained until tested for moisture content.

Soil is well prepared for testing Index and Engineering Properties.

Determination of Index Properties such as Liquid Limit, Plastic Limit and


Shrinkage Limit, Specific gravity, Sieve Analysis and in-situ Density.

Determination of Engineering Properties such as unconfined compressive


strength, Shear strength and Iron content determination.

Analysis of test result with both Engineering and Index Properties.

Results concluded that tailings are high density, Less cohesive, negligible
pozzolonic action.

Red soil samples are collected from Nursery near Nagarbhavi, Bangalore.

Soil is well prepared for testing Index and Engineering Properties.

Determination of Index Properties such as Liquid Limit, Plastic Limit and


Shrinkage Limit, Specific gravity, Sieve Analysis and in-situ Density.

Determination of Engineering Properties such as Shear strength and Iron content


determination.

Analysis of test result with both Engineering and Index Properties.

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Feasibility Study On Iron Ore Mine Tailings

5.0 Tests on iron ore tailings


5.1 Index properties of tailings:
5.1.1 Specific Gravity
Specific gravity of soil particles is defined as ratio of mass of given volume of soil
particles to mass of equivalent volume of distilled water at stated temperature. It is
also defined as the ratio of density of soil particles to density of distilled water at a
stated temperature. The test is conducted as per IS Code (29). The results obtained as
shown in table.
a) Test Temperature Tt c = 24c
b) Relative density of water at Tt c = 0.9973
c) Relative density of water at 27c = 0.9965

d) Correction factor due to temperature

e) Specific gravity,

Table 5.1 - Sample 1 (Iron ore tailings from pit 1)

Water used: Distilled water


1)

Density bottle No.

1.1

1.2

1.3

2)

Mass of density bottle


(W1) g

74.500

73.500

71.500

3)

Mass of density bottle


+ dry soil (W2) g

183.500 195.000 198.000

4)

Mass of density bottle


+ soil + water (W3) g

279.000 281.000 281.500

5)
6)
7)

Mass of density bottle


+ water (W4) g
Specific gravity at
Tt c
Specific gravity of soil
at 27c = (6) Ct

200.500 202.000 195.500


2.574

2.859

3.124

3.577

2.861

3.126

Average specific gravity = 3.188

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Feasibility Study On Iron Ore Mine Tailings

Table 5.2 - Sample 2 (Iron ore tailings from pit 2)

Water used: Distilled water


1)

Density bottle No.

2.1

2.2

2.3

2)

Mass of density bottle


(W1) g

72.000

75.000

73.500

3)

Mass of density bottle


+ dry soil (W2) g

161.500 175.500 166.000

4)

Mass of density bottle


+ soil + water (W3) g

261.500 270.500 258.500

5)
6)
7)

Mass of density bottle


+ water (W4) g
Specific gravity at
Tt c
Specific gravity of soil
at 27c = (6) Ct

200.500 202.000 195.500


3.140

3.141

3.136

3.143

3.143

3.138

Average specific gravity = 3.141

Table 5.3 - Sample 3 (Iron ore tailings from pit 3)

Water used: Distilled water


1)

Density bottle No.

3.1

3.2

3.3

2)

Mass of density bottle


(W1) g

72.000

75.000

73.500

3)

Mass of density bottle


+ dry soil (W2) g

190.500 199.500 164.500

4)

Mass of density bottle


+ soil + water (W3) g

278.500 285.000 257.000

5)
6)
7)

Mass of density bottle


+ water (W4) g
Specific gravity at
Tt c
Specific gravity of soil
at 27c = (6) Ct

200.500 202.000 195.500


2.926

3.000

3.084

2.928

3.002

3.087

Average specific gravity = 3.006

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Feasibility Study On Iron Ore Mine Tailings


Table 5.4 - Sample 4 (Iron ore tailings from pit 4)

Water used: Distilled water


1)

Density bottle No.

4.1

4.2

4.3

2)

Mass of density bottle


(W1) g

72.500

75.000

73.500

3)

Mass of density bottle


+ dry soil (W2) g

186.500 182.500 172.000

4)

Mass of density bottle


+ soil + water (W3) g

279.000 276.000 263.500

5)
6)
7)

Mass of density bottle


+ water (W4) g
Specific gravity at
Tt c
Specific gravity of soil
at 27c = (6) Ct

200.500 202.000 195.500


3.211

3.209

3.229

3.214

3.212

3.232

Average specific gravity = 3.219

Table 5.5 - Average specific gravity

Average specific gravity (using distilled water)


Sample 1

3.188

Sample 2

3.141

Sample 3

3.006

Sample 4

3.219

Table 5.6 - Comparison of specific gravity

Comparison of specific gravity


Distilled Water

Tap water

Sample 1

3.188

2.944

Sample 2

3.141

2.935

Sample 3

3.006

2.980

Sample 4

3.219

3.553

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5.1.2 Moisture content Determination
The natural water content also called the natural moisture content is the ratio
of the weight of water to the weight of the solids in a given mass of soil. This ratio
is usually expressed as percentage. The test is conducted as per IS Code (28).
The results obtained as shown in table.
Table 5.7 - Sample 1 (Iron ore tailings from pit 1)

1)

Container No.

2)

Mass of container + wet soil (W2) in g

60.500 64.500 59.000

3)

Mass of container + dry soil (W3) in g

59.595 62.614 57.860

4)

Mass of container (W1) in g

15.000 17.500 15.000

5)

Mass of dry soil (W3 W1) in g

45.595 45.114 42.860

6)

Mass of moisture (W2 W3) in g

0.905

1.886

1.140

1.980

4.180

2.650

7)

Water content

1.1

1.2

1.3

Average moisture content = 2.937%

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Table 5.8 - Sample 2 (Iron ore tailings from pit 2)

1)

Container No.

2)

Mass of container + wet soil (W2) in g

47.500 63.000 56.000

3)

Mass of container + dry soil (W3) in g

46.920 61.813 54.998

4)

Mass of container (W1) in g

12.000 14.500 15.000

5)

Mass of dry soil (W3 W1) in g

34.920 47.313 39.998

6)

Mass of moisture (W2 W3) in g

0.580

1.187

1.002

1.660

2.510

2.506

3.2

3.3

7)

Water content

2.1

2.2

2.3

Average moisture content = 2.225%

Table 5.9 - Sample 3 (Iron ore tailings from pit 3)

1)

Container No.

2)

Mass of container + wet soil (W2) in g

47.000 43.500 50.500

3)

Mass of container + dry soil (W3) in g

45.992 42.504 49.339

4)

Mass of container (W1) in g

12.000 13.500 13.000

5)

Mass of dry soil (W3 W1) in g

33.992 29.004 36.335

6)

Mass of moisture (W2 W3) in g

1.008

0.996

1.165

2.960

3.430

3.206

7)

Water content

3.1

Average moisture content = 3.199%

Civil Department, R V College of Engineering

Page 17

Feasibility Study On Iron Ore Mine Tailings


Table 5.10 - Sample 4 (Iron ore tailings from pit 4)

1)

Container No.

2)

Mass of container + wet soil (W2) in g

65.000 53.500 54.500

3)

Mass of container + dry soil (W3) in g

64.487 53.000 54.193

4)

Mass of container (W1) in g

18.000 14.500 14.500

5)

Mass of dry soil (W3 W1) in g

46.482 38.500 39.693

6)

Mass of moisture (W2 W3) in g

0.518

0.500

0.307

1.114

1.299

0.779

7)

Water content

4.1

4.2

4.3

Average moisture content = 1.064%

Table 5.11 - Average Moisture Content

Average Moisture Content ( % )


Sample1

2.937

Sample 2

2.225

Sample 3

3.199

Sample 4

1.064

5.1.3 Dry Sieve Analysis


The grain size analysis is widely used in classification of soils. The
data obtained from grain size distribution curves is used in the design of filters
for earth dams and to determine suitability of soil for road construction, air
field etc. Information obtained from grain size analysis can be used to predict
soil water movement although permeability tests are more generally used. The
test is conducted as per IS code (30).

Civil Department, R V College of Engineering

Page 18

Feasibility Study On Iron Ore Mine Tailings


Trial 1: Mass of sample taken for analysis = 500g
Water content = 2.937%
Table 5.12 - Sample 1 (Iron ore tailings from pit 1)

Mass of
I.S sieve
soil
Designation Retained
(g)
4.75
2.36
1.7
0.6
0.3
0.15
0.075
pan

Cumulative
mass
retained (g)

0.570
2.002
11.640
71.550
236.500
105.500
45.500
26.738

0.57
2.572
14.212
85.762
322.262
427.762
473.262
500.000

Percentage
of soil
retained
on each
sieve(g)
0.114
0.400
2.328
14.310
47.300
21.100
9.100
5.347

% finer

99.90
99.50
97.20
82.80
35.50
14.40
5.30
0.000

Sieve Analysis

Sample 1, Iron ore tailings


97.2 99.5

99.9

82.8

% Passing

D 60

35.5

D 30

D 10

14.4
5.3

0.01

0.1

Sieve Size (in mm)

10

Figure 5.1 Grain Size Distribution for Sample 1 (Iron ore tailings from pit 1)

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Page 19

Feasibility Study On Iron Ore Mine Tailings


From graph
a) D10 = 110
b) D30 = 260
c) D60 = 420
1) Coefficient of curvature

2) Uniform Coefficient

% of soil passing 75 IS sieve = 5.3

Trial 2: Mass of sample taken for analysis = 500g


Water content = 2.225%

Table 5.13 - Sample 2 (Iron ore tailings from pit 2)

Mass of
I.S sieve
soil
Designation Retained
(g)
4.75
2.36
1.7
0.6
0.3
0.15
0.075
pan

0.000
0.617
5.930
40.040
183.500
155.000
75.500
39.413

Cumulative
mass
retained (g)
0.000
0.617
6.547
46.587
230.087
385.087
460.58
500.000

Civil Department, R V College of Engineering

Percentage
of soil
retained
on each
sieve(g)
0.000
0.123
1.309
9.317
46.017
77.017
92.116
100.000

% finer

100
99.990
98.700
90.700
54.000
23.000
7.900
0.000

Page 20

Feasibility Study On Iron Ore Mine Tailings

Sieve Analysis

Sample 2, Iron ore tailings


98.7 99.99

100

90.7

% Passing

D 60
54

D 30
23

D 10
7.9
0.01

0.1

Sieve Size (in mm)

10

Figure 5.2 - Grain Size Distribution for Sample 2 (Iron ore tailings from pit 2)

From graph
a) D10 = 90
b) D30 = 185
c) D60 = 330
1) Coefficient of curvature

2) Uniform Coefficient

% of soil passing 75 IS sieve = 7.9

Civil Department, R V College of Engineering

Page 21

Feasibility Study On Iron Ore Mine Tailings


Trial 3: Mass of sample taken for analysis = 500g
Water content = 3.199%

Table 5.14 - Sample 3 (Iron ore tailings from pit 3)

Mass of
I.S sieve
soil
Designation Retained
(g)
4.750
2.360
1.700
0.600
0.300
0.150
0.075
pan

Cumulative
mass
retained (g)

0.000
3.890
17.905
76.500
212.500
97.500
57.000
34.705

0.000
3.890
21.795
98.295
310.795
408.295
465.295
500.000

Percentage
of soil
retained
on each
sieve(g)
0.000
0.778
4.360
19.660
62.160
81.660
93.060
100.000

Sieve Analysis

% finer

100.000
99.200
95.600
80.300
37.800
18.300
6.900
0.000

Sample 3, Iron ore tailings


95.6 99.2

100

80.3

% Passing

D 60
37.8

D 30
18.3

D 10

6.9

0.01

0.1

Sieve Size (in mm)1

10

Figure 5.3 - Grain Size Distribution for Sample 3 (Iron ore tailings from pit 3)

From graph
a) D10 = 110
b) D30 = 250
c) D60 = 410

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Page 22

Feasibility Study On Iron Ore Mine Tailings


1) Coefficient of curvature

2) Uniform Coefficient

% of soil passing 75 IS sieve = 6.9

Trial 4: Mass of sample taken for analysis = 500g


Water content = 1.064%

Table 5.15 - Sample 4 (Iron ore tailings from pit 4)

Mass of
Cumulative
I.S sieve
soil
mass retained
Designation Retained
(g)
(g)
4.750
2.360
1.700
0.600
0.300
0.150
0.075
pan

1.000
2.300
8.530
62.100
210.900
129.500
55.500
30.140

1.000
3.300
11.830
73.930
284.830
414.330
469.830
500.000

Civil Department, R V College of Engineering

Percentage
of soil
retained
on each
sieve(g)
0.200
0.660
2.366
14.786
56.966
82.866
93.966
100.000

% finer

99.800
99.300
97.600
85.200
43.000
17.100
6.000
0.000

Page 23

Feasibility Study On Iron Ore Mine Tailings

Sieve Analysis

Sample 4, Iron ore tailings


97.6 99.3

99.8

85.2

% Passing

D 60
43

D 30
17.1

D 10
6
0.01

0.1

Sieve Size (in mm)

10

Figure 5.4 - Grain Size Distribution for Sample 4 (Iron ore tailings from pit 4)

From graph
a) D10 = 120
b) D30 = 230
c) D60 = 395
1) Coefficient of curvature

2) Uniform Coefficient

% of soil passing 75 IS sieve = 6.0

Civil Department, R V College of Engineering

Page 24

Feasibility Study On Iron Ore Mine Tailings


5.1.4 Liquid limit:
The liquid limit of the soil corresponds to the water content of a paste
which would give 20mm penetration of the soil. Liquid limit is significant to
know the stress history and general properties of the soil met with
construction. The test is conducted as per IS code (31).
The test results as shown in below tables

Trial 1: Natural moisture content: 2.937%


Method adopted: Static Cone penetration method
Table 5.16 - Sample 1 (Iron ore tailing from pit 1)
Determination
Number
Penetration

13

14

25

20

1.1

1.2

1.3

1.4

13.676

16.434

17.981

15.757

36.831

38.962

66.996

61.180

32.911

35.060

58.037

53.145

Weight of water

3.920

3.907

8.959

8.035

Weight of dry soil


Moisture content
(%)

19.235

18.626

40.056

37.388

20.380

20.940

22.370

21.990

Container number
Weight of
container
Weight of
container + wet
soil
Weight of
container + dry
soil

Civil Department, R V College of Engineering

Page 25

Feasibility Study On Iron Ore Mine Tailings

Moisture Content (%)

Sample 1, Iron ore tailings


30
28
26
24
22
20
18
16
14
12
10
8
6
4
2
0

Scale: X-axis 1unit = 2mm


Y-axis 1unit = 2%

Cone Penetration

WL = 21.6%

10

12

14

16

22.37

21.99

20.94
20.38

18

20

22

24

26

28

30

Penetration value (mm)


Figure 5.5 - Liquid Limit for sample 1 (Iron ore tailings from pit 1)

Liquid Limit (WL) = 21.6%

Trial 2: Natural moisture content: 2.225%


Method adopted: Static Cone penetration method
Table 5.17 - Sample 2 (Iron ore tailing from pit 2)
Determination
Number
Penetration

16

22

24

27

2.1

2.2

2.3

2.4

15.219

18.143

14.098

15.041

38.039

32.014

31.490

38.471

35.061

29.514

28.346

33.822

Weight of water

2.978

2.500

3.144

4.649

Weight of dry soil


Moisture content
(%)

19.847

11.371

14.248

18.781

15.000

21.980

22.070

24.750

Container number
Weight of
container
Weight of
container + wet
soil
Weight of
container + dry
soil

Civil Department, R V College of Engineering

Page 26

Feasibility Study On Iron Ore Mine Tailings


Scale: X-axis 1unit = 2mm
Y-axis 1unit = 2%

Moisture Content (%)

Sample 2, Iron ore tailings Cone Penetration


30
28
26
24
22
20
18
16
14
12
10
8
6
4
2
0

21.98

WL = 18.0%

24.75

22.07

15

10

12

14

16

18

20

22

24

26

28

30

Penetration value (mm)


Figure 5.6 - Liquid Limit for sample 2 (Iron ore tailings from pit 2)

Liquid Limit (WL) = 18.0%

Trial 3: Natural moisture content: 3.199%


Method adopted: Static Cone penetration method
Table 5.18 - Sample 3 (Iron ore tailing from pit 3)
Determination
Number
Penetration

12

27

14

19

3.1

3.2

3.3

3.4

12.398

15.229

12.168

12.327

42.561

56.735

47.995

60.925

38.069

48.505

40.977

51.366

Weight of water

4.492

8.230

6.978

9.559

Weight of dry soil


Moisture content
(%)

25.671

38.276

28.809

39.039

17.490

24.730

24.020

24.480

Container number
Weight of
container
Weight of
container + wet
soil
Weight of
container + dry
soil

Civil Department, R V College of Engineering

Page 27

Feasibility Study On Iron Ore Mine Tailings

Moisture Content (%)

Sample 3, Iron ore tailings


30
28
26
24
22
20
18
16
14
12
10
8
6
4
2
0

Scale: X-axis 1unit = 2mm


Y-axis 1unit = 2%

Cone Penetration

24.73

24.02
24.48

WL = 25.6%
17.49

10

12

14

16

18

20

22

24

26

28

30

Penetration value (mm)


Figure 5.7 - Liquid Limit for sample 3 (Iron ore tailings from pit 3)

Liquid Limit (WL) = 25.6%

Trial 4: Natural moisture content: 1.064%


Method adopted: Static Cone penetration method
Table 5.19 - Sample 4 (Iron ore tailing from pit 4)
Determination
Number
Penetration

15

28

25

20

4.1

4.2

4.3

4.4

13.403

12.378

15.210

15.695

31.817

44.575

57.940

62.796

29.398

38.380

49.602

53.750

Weight of water

2.419

6.190

8.358

9.046

Weight of dry soil


Moisture content
(%)

15.995

26.002

34.392

38.055

15.120

23.800

24.300

23.770

Container number
Weight of
container
Weight of
container + wet
soil
Weight of
container + dry
soil

Civil Department, R V College of Engineering

Page 28

Feasibility Study On Iron Ore Mine Tailings

Scale: X-axis 1unit = 2mm


Y-axis 1unit = 2%

Moisture Content (%)

Sample 4, Iron ore tailings Cone Penetration


30
28
26
24
22
20
18
16
14
12
10
8
6
4
2
0

WL = 19.8%

24.3

23.77

23.8

15.12

10

12

14

16

18

20

22

24

26

28

30

Penetration value (mm)


Figure 5.8 - Liquid Limit for sample 4 (Iron ore tailings from pit 4)

5.1.5 Plastic limit:


Plastic limit is the water content at which the soil mass can be rolled into a thread
of 3mm diameter and the thread shows signs of cracking. The test is conducted as per
IS code (31). From the test it is found that the specimen is non plastic soil.
5.2 Engineering Properties:
5.2.1 Standard proctor compaction test:
As the water content is increased, dry density increase up to a certain maximum
value and thereafter decreases. The water content at which dry density attains
maximum value is called optimum moisture content. The test is conducted as per IS
code (32).
The results obtained as shown below
Details of the mould:
Diameter of mould: 10 cm
Height of mould: 12.7 cm
Volume of mould: 997.4557 cm3
Mass of mould: 2285 gm

Civil Department, R V College of Engineering

Page 29

Feasibility Study On Iron Ore Mine Tailings


Table 5.20 - Sample 1 (Iron ore tailing from pit 1)
Sl.
no

Determination No

Mass of mould with compacted soil (gm)

5299

5428

5512

5508

Mass of compacted soil (gm)

3014

3143

3227

3223

Wet Density (gm/cc)

3.021

3.151

3.235

3.231

Moisture cup No.

C1.1

C1.2

C1.3

C1.4

Mass of cup + wet soil (gm)

36.967

39.854

46.012

44.719

Mass of cup - dry soil (gm)

35.125

37.233

42.582

41.300

Mass of water (gm)

1.842

2.621

3.430

3.419

Mass of Cup (gm)

14.934

12.324

14.441

16.281

Mass of dry soil (gm)

20.191

24.909

28.141

25.019

10

Moisture content (%)

9.120

10.520

12.190

13.670

11

Dry Density (gm/cc)

2.780

2.850

2.880

2.840

12

Dry density at 100% saturation (gm/cc)

2.440

2.360

2.270

2.090

Dry Density (g/cc)

2.92
2.91
2.9
2.89
2.88
2.87
2.86
2.85
2.84
2.83
2.82
2.81
2.8
2.79
2.78
2.77
2.76
2.75

Scale: X-axis 1unit = 0.5%


Y-axis 1unit = 0.01g/cc

Compaction

Sample 1, Iron ore tailings


d max = 2.88g/cc

2.88

2.85
2.84

2.78

OMC = 12.1%
8

8.5

9.5

10

10.5

11

11.5

12

12.5

13

13.5

14

14.5

15

Moisture Content (%)


Figure 5.9 - Optimum moisture content for sample 1 (Iron ore tailings from pit 1)

Civil Department, R V College of Engineering

Page 30

Feasibility Study On Iron Ore Mine Tailings


Table 5.21 - Sample 2 (Iron ore tailing from pit 2)
Sl.
no

Determination No

Mass of mould with compacted soil (gm)

5123

5240

5304

5257

5241

Mass of compacted soil (gm)

2838

2955

3019

2972

2956

Wet Density (gm/cc)

2.845

2.962

3.026

2.980

2.963

Moisture cup No.

C2.1

C2.2

C2.3

C2.4

C2.5

Mass of cup + wet soil (gm)

44.383

33.933

32.462

46.291

53.098

Mass of cup - dry soil (gm)

42.177

32.127

30.478

42.199

47.893

Mass of water (gm)

2.206

1.806

1.984

4.092

5.205

Mass of Cup (gm)

19.158

14.160

13.958

15.223

15.269

Mass of dry soil (gm)

23.019

17.967

16.520

26.976

32.624

10

Moisture content (%)

9.580

10.050

12.010

15.180

15.950

11

Dry Density (gm/cc)

2.590

2.690

2.700

2.590

2.550

12

Dry density at 100% saturation (gm/cc)

2.440

2.410

2.310

2.150

2.110

Dry Density (g/cc)

Sample 2, Iron ore tailings


2.72
2.71
2.7
2.69
2.68
2.67
2.66
2.65
2.64
2.63
2.62
2.61
2.6
2.59
2.58
2.57
2.56
2.55
2.54
2.53
2.52
2.51
2.5

2.69

Compaction

Scale: X-axis 1unit = 0.5%


Y-axis 1unit = 0.01g/cc

2.7

d max = 2.71g/cc

2.59

2.59

2.55

OMC = 11%
8

8.5

9.5 10 10.5 11 11.5 12 12.5 13 13.5 14 14.5 15 15.5 16 16.5 17 17.5 18

Moisture Content (%)


Figure 5.10 - Optimum moisture content for sample 2 (Iron ore tailings from pit 2)

Civil Department, R V College of Engineering

Page 31

Feasibility Study On Iron Ore Mine Tailings


Table 5.22 - Sample 3 (Iron ore tailing from pit 3)
Sl.
no

Determination No

Mass of mould with compacted soil (gm)

5090

5170

5212

5197

500

Mass of compacted soil (gm)

2805

2885

2927

2912

2915

Wet Density (gm/cc)

2.812

2.892

2.934

2.919

2.922

Moisture cup No.

C3.1

C3.2

C3.3

C3.4

C3.5

Mass of cup + wet soil (gm)

19.917

35.489

25.332

36.124

30.269

Mass of cup - dry soil (gm)

19.107

33.581

24.107

33.462

27.777

Mass of water (gm)

0.810

1.908

1.225

2.660

2.472

Mass of Cup (gm)

11.335

18.334

14.974

16.122

11.482

Mass of dry soil (gm)

7.772

15.247

9.133

17.340

16.295

10

Moisture content (%)

10.420

12.510

13.410

15.350

15.290

11

Dry Density (gm/cc)

2.550

2.570

2.590

2.530

2.530

12

Dry density at 100% saturation (gm/cc)

2.290

2.180

2.140

2.050

2.060

Sample 3, Iron ore tailings

Scale: X-axis 1unit = 0.5%


Y-axis 1unit = 0.01g/cc

Compaction

2.62
2.61
2.6

Dry Density (g/cc)

2.59

2.59

2.58

d max = 2.592g/cc

2.57

2.57

2.56
2.55

2.55

2.54
2.53

2.53
2.53

2.52

OMC = 13.2%

2.51
2.5
8

8.5

9.5

10 10.5 11 11.5 12 12.5 13 13.5 14 14.5 15 15.5 16

Moisture Content (%)


Figure 5.11 - Optimum moisture content for sample 3 (Iron ore tailings from pit 3)

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Page 32

Feasibility Study On Iron Ore Mine Tailings


Table 5.23 Sample 4 (Iron ore tailing from pit 4)
Sl.
No

Determination No

Mass of mould with


compacted soil (gm)

5100

5191

5222

5295

5308

5325

5341

5328

2815

2906

2937

3010

3023

3040

3056

3043

2.822

2.913

2.944

3.017

3.030

3.047

3.063

3.050

C4.1

C4.2

C4.3

C4.4

C4.5

C4.6

C4.7

C4.8

40.800

32.734

26.185

46.909

35.733

40.480

36.604

53.710

39.169

31.105

24.857

43.978

33.759

37.240

33.918

49.574

2
3
4
5
6

Mass of compacted soil


(gm)
Wet Density (gm/cc)
Moisture cup No.
Mass of cup + wet soil
(gm)
Mass of cup - dry soil
(gm)

Mass of water (gm)

1.631

1.629

1.328

2.931

2.479

3.216

3.186

4.136

Mass of Cup (gm)

16.178

12.286

11.756

18.915

15.308

15.461

15.657

24.330

Mass of dry soil (gm)

22.910

18.819

13.101

25.063

18.271

21.803

18.261

25.244

10

Moisture content (%)

7.120

8.660

10.140

11.690

13.540

14.750

17.450

16.380

11

Dry Density (gm/cc)

2.630

2.680

2.670

2.700

2.670

2.660

2.610

2.620

12

Dry density at 100%


saturation (gm/cc)

2.620

2.520

2.430

2.340

2.240

2.180

2.060

2.100

Compaction

Sample 4, Iron ore tailings

Scale: X-axis 1unit = 0.5%


Y-axis 1unit = 0.01g/cc

2.72
2.71
2.7

2.7

Dry Density (g/cc)

2.69
2.68

d max = 2.70g/cc

2.68

2.67

2.67

2.66

2.66

2.65
2.64
2.63

2.63

2.62

OMC = 11.5%

2.61

2.61

2.6
5 5.5 6 6.5 7 7.5 8 8.5 9 9.5 1010.51111.51212.51313.51414.51515.51616.51717.51818.519

Moisture Content (%)


Figure 5.12 - Optimum moisture content for sample 4 (Iron ore tailings from pit 4)

Civil Department, R V College of Engineering

Page 33

Feasibility Study On Iron Ore Mine Tailings


5.2.2 Direct Shear:
A direct shear test is a laboratory or field test used by geotechnical
engineers to measure the shear strength properties of soil or rock material. Direct
shear tests can be performed under several conditions. The sample is normally
saturated before the test is run, but can be run at the in-situ moisture content. The rate
of strain can be varied to create a test of undrained or drained conditions, depending
whether the strain is applied slowly enough for water in the sample to prevent porewater pressure buildup. The test is conducted as per IS code (33).
Trial 1:
a) Proving Ring No.

= 71018

b) Dimension of specimen (cm) = 6 X 6 X 2.5


c) Weight of specimen (gm)

=158.5

d) Normal Load (N)

= 4.905

Table 5.24 - Sample 1 (Iron ore tailing from pit 1)

Sl.
No.

Load (KN)

Shear Displacement
(mm)
Dial Gauge
Value
readings
50
0.500

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

0.008

0.833

2.674

1)

Proving ring
readings
37

Load
Values
0.040

2)

53

0.057

100

1.000

0.017

1.667

3.830

3)

64

0.069

150

1.500

0.025

2.500

4.625

4)

71

0.077

200

2.000

0.033

3.333

5.131

5)

77

0.083

250

2.500

0.042

4.167

5.564

6)

81

0.088

300

3.000

0.050

5.000

5.853

7)

84

0.091

350

3.500

0.058

5.833

6.070

8)

87

0.094

400

4.000

0.067

6.667

6.287

9)

90

0.098

450

4.500

0.075

7.500

6.504

10)

93

0.101

500

5.000

0.083

8.333

6.721

11)

95

0.103

550

5.500

0.092

9.167

6.865

12)

95

0.103

600

6.000

0.100

10.000

6.865

13)

92

0.100

650

6.500

0.108

10.833

6.648

14)

90

0.098

700

7.000

0.117

11.667

6.504

Civil Department, R V College of Engineering

Page 34

Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Normal Load = 4.905kN

Y-axis 1unit = 1N/cm2

8
7

Shear Stress (N/cm2)

6
5.564
Shear stress at failure
5.131
qu = 6.8N/cm2

6.07

5.853

6.287

6.504

6.721 6.865 6.865 6.648


6.504

4.625
4

3.83

3
2.674
2

Shear strain at failure (9.2%)


1
0
0

Sample 1, Iron ore tailings

10

11

Shear Strain %

Figure 5.13 - Stress-Strain curve for sample 1 (Iron ore tailings from pit 1)

Civil Department, R V College of Engineering

Page 35

12

Feasibility Study On Iron Ore Mine Tailings


a) Dimension of specimen (cm)

= 6 X 6 X 2.5

b) Weight of specimen (gm)

= 149.5

c) Normal Load (N)

= 9.81

Table 5.25 Sample 1 (Iron ore tailing from pit 1)

Sl.
No.

Load (KN)

Shear Displacement
(mm)
Dial Gauge
Value
readings

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

Proving ring
readings

Load
Values

1)

110

0.119

50

0.500

0.008

0.833

7.949

2)

154

0.167

100

1.000

0.017

1.667

11.129

3)

195

0.211

150

1.500

0.025

2.500

14.092

4)

210

0.228

200

2.000

0.033

3.333

15.176

5)

220

0.238

250

2.500

0.042

4.167

15.898

6)

230

0.249

300

3.000

0.050

5.000

16.621

7)

233

0.253

350

3.500

0.058

5.833

16.838

238

0.258

400

4.000

0.067

6.667

17.199

9)

239

0.259

450

4.500

0.075

7.500

17.271

10)

240

0.260

500

5.000

0.083

8.333

17.344

11)

235

0.255

550

5.500

0.092

9.167

16.982

12)

232

0.251

600

6.000

0.100

10.000

16.766

13)

228

0.247

650

6.500

0.108

10.833

16.476

8)

Civil Department, R V College of Engineering

Page 36

Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Shear Stress (N/cm2)

Normal Load = 9.81kN


19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0

Y-axis 1unit = 1N/cm2

16.621 16.838

Shear stress at failure


15.176
qu = 17.2N/cm2

17.199 17.271 17.344 16.982

15.898

16.766 16.476

14.092

11.129

7.949

Shear strain at failure (8%)

Sample 1, Iron ore tailings

10

11

Shear Strain %

Figure 5.14 - Stress-Strain curve for sample 1 (Iron ore tailings from pit 1)

Civil Department, R V College of Engineering

Page 37

12

Feasibility Study On Iron Ore Mine Tailings


a) Dimension of specimen (cm)

= 6 X 6 X 2.5

b) Weight of specimen (gm)

= 154.5

c) Normal Load (N)

= 14.715

Table 5.26 Sample 1 (Iron ore tailing from pit 1)

Load (KN)
Sl.
No. Proving ring Load
readings
Values
1)
105
0.114

Shear Displacement
(mm)
Dial Gauge
Value
readings
50
0.500

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

0.008

0.833

7.588

2)

200

0.217

100

1.000

0.017

1.667

14.453

3)

255

0.276

150

1.500

0.025

2.500

18.428

4)

305

0.331

200

2.000

0.033

3.333

22.041

5)

338

0.366

250

2.500

0.042

4.167

24.426

6)

370

0.401

300

3.000

0.050

5.000

26.738

7)

395

0.428

350

3.500

0.058

5.833

28.545

414

0.449

400

4.000

0.067

6.667

29.918

9)

420

0.455

450

4.500

0.075

7.500

30.351

10)

419

0.454

500

5.000

0.083

8.333

30.279

11)

415

0.450

550

5.500

0.092

9.167

29.990

12)

393

0.426

600

6.000

0.100

10.000

28.400

8)

Civil Department, R V College of Engineering

Page 38

Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Shear Stress (N/cm2)

Normal Load = 14.715kN


32
31
30
29
28
27
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5

Y-axis 1unit = 1N/cm2

30.351

30.279
29.99

29.918
28.545

28.4

26.738

Shear stress at failure


qu = 30N/cm2

24.426
22.041

18.428

14.453

Shear strain at failure (7.4%)


7.588

Sample 1, Iron ore tailings

10

11

Shear Strain %

Figure 5.15 - Stress-Strain curve for sample 1 (Iron ore tailings from pit 1)

Civil Department, R V College of Engineering

Page 39

12

Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 2N/cm2

Sample 1, Iron ore tailings

Y-axis 1unit = 5N/cm2

35

Shear Stress at failure (N/cm2)

30

30

25

20
17.2
15

Angle of Internal friction = 67.067

10
6.8
5

0
0

10

12

14

16

18

20

Normal Stress (N/cm2)


Figure 5.16 Graph of Normal stress v/s Shear stress at failure

Civil Department, R V College of Engineering

Page 40

Feasibility Study On Iron Ore Mine Tailings


Trial 2:
a) Proving Ring No.

= 71018

b) Dimension of specimen (cm)

= 6 X 6 X 2.5

c) Weight of specimen (gm)

= 180.5

d) Normal Load (N)

= 4.905

Table 5.27 - Sample 2 (Iron ore tailing from pit 2)

Load (KN)

Sl.
No. Proving ring
readings
1)
65

Load
Values
0.070

Shear Displacement
(mm)
Dial Gauge
Value
readings
50
0.500

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

0.008

0.833

4.697

2)

82

0.089

100

1.000

0.017

1.667

5.926

3)

94

0.102

150

1.500

0.025

2.500

6.793

4)

102

0.111

200

2.000

0.033

3.333

7.371

5)

110

0.119

250

2.500

0.042

4.167

7.949

6)

116

0.126

300

3.000

0.050

5.000

8.383

7)

120

0.130

350

3.500

0.058

5.833

8.672

126

0.137

400

4.000

0.067

6.667

9.105

9)

130

0.141

450

4.500

0.075

7.500

9.394

10)

134

0.145

500

5.000

0.083

8.333

9.684

11)

135

0.146

550

5.500

0.092

9.167

9.756

12)

139

0.151

600

6.000

0.100

10.000

10.045

13)

141

0.153

650

6.500

0.108

10.833

10.189

14)

142

0.154

700

7.000

0.117

11.667

10.262

15)

143

0.155

750

7.500

0.125

12.500

10.334

16)

141

0.153

800

8.000

0.133

13.333

10.189

17)

141

0.153

850

8.500

0.142

14.167

10.189

18)

140

0.152

900

9.000

0.150

15.000

10.117

8)

Civil Department, R V College of Engineering

Page 41

Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Normal Load = 4.905kN

Y-axis 1unit = 1N/cm2

11

10.189
10
9

Shear Stress (N/cm2)

8
7
6

10.26210.334
10.189
10.189
10.045
9.6849.756
Shear stress at failure
9.394
9.105
qu = 10.3N/cm2
8.672
8.383
7.949
7.371
6.793

10.117

5.926

4.697

4
3
2

Shear strain at failure (12.5%)

1
0
0

Sample 2, Iron ore tailings

10

11

12

13

14

15

16

17

Shear Strain %

Figure 5.17 - Stress-Strain curve for sample 2 (Iron ore tailings from pit 2)

Civil Department, R V College of Engineering

Page 42

Feasibility Study On Iron Ore Mine Tailings


a) Dimension of specimen (cm)

= 6 X 6 X 2.5

b) Weight of specimen (gm)

= 151

c) Normal Load (N)

= 9.81

Table 5.28 - Sample 2 (Iron ore tailing from pit 2)

Sl.
No.

Load (KN)

Shear Displacement
(mm)
Dial Gauge
Value
readings

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

Proving ring
readings

Load
Values

1)

60

0.065

50

0.500

0.008

0.833

4.336

2)

130

0.141

100

1.000

0.017

1.667

9.394

3)

165

0.179

150

1.500

0.025

2.500

11.924

4)

193

0.209

200

2.000

0.033

3.333

13.947

5)

212

0.230

250

2.500

0.042

4.167

15.320

6)

222

0.241

300

3.000

0.050

5.000

16.043

7)

232

0.251

350

3.500

0.058

5.833

16.766

239

0.259

400

4.000

0.067

6.667

17.271

9)

246

0.267

450

4.500

0.075

7.500

17.777

10)

249

0.270

500

5.000

0.083

8.333

17.994

11)

253

0.274

550

5.500

0.092

9.167

18.283

12)

256

0.277

600

6.000

0.100

10.000

18.500

13)

256

0.277

650

6.500

0.108

10.833

18.500

14)

257

0.279

700

7.000

0.117

11.667

18.572

15)

256

0.277

750

7.500

0.125

12.500

18.500

16)

252

0.273

800

8.000

0.133

13.333

18.211

17)

247

0.268

850

8.500

0.142

14.167

17.850

8)

Civil Department, R V College of Engineering

Page 43

Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Shear Stress (N/cm2)

Normal Load = 9.81kN


20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0

Y-axis 1unit = 1N/cm2

18.283

Shear stress at failure


qu = 18.2N/cm2

17.271 17.777
17.994
16.766
16.043
15.32

18.5
18.5

18.5

18.572

18.211
17.85

13.947

11.924

9.394

4.336

Shear strain at failure (11.8%)

Sample 2, Iron ore tailings

10

11

12

13

14

15

16

Shear Strain %

Figure 5.18 - Stress-Strain curve for sample 2 (Iron ore tailings from pit 2)

Civil Department, R V College of Engineering

Page 44

Feasibility Study On Iron Ore Mine Tailings


a) Dimension of specimen (cm)

= 6 X 6 X 2.5

b) Weight of specimen (gm)

= 151

c) Normal Load (N)

= 14.715

Table 5.29 Sample 2 (Iron ore tailing from pit 2)

Sl.
No
.

Load (KN)

Shear Displacement
(mm)

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

Proving
ring
readings

Load
Values

Dial Gauge
readings

Value

1)

50

0.054

50

0.500

0.008

0.833

3.613

2)

165

0.179

100

1.000

0.017

1.667

11.924

3)

220

0.238

150

1.500

0.025

2.500

15.898

4)

260

0.282

200

2.000

0.033

3.333

18.789

5)

290

0.314

250

2.500

0.042

4.167

20.957

6)

317

0.344

300

3.000

0.050

5.000

22.908

7)

340

0.369

350

3.500

0.058

5.833

24.570

360

0.390

400

4.000

0.067

6.667

26.015

9)

378

0.410

450

4.500

0.075

7.500

27.316

10)

390

0.423

500

5.000

0.083

8.333

28.183

11)

400

0.434

550

5.500

0.092

9.167

28.906

12)

404

0.438

600

6.000

0.100

10.000

29.195

13)

409

0.443

650

6.500

0.108

10.833

29.556

14)

410

0.444

700

7.000

0.117

11.667

29.629

15)

407

0.441

750

7.500

0.125

12.500

29.412

16)

394

0.427

800

8.000

0.133

13.333

28.472

17)

380

0.412

850

8.500

0.142

14.167

27.461

8)

Civil Department, R V College of Engineering

Page 45

Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Shear Stress (N/cm2)

Normal Load = 14.715kN


32
31
30
29
28
27
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0

Y-axis 1unit = 1N/cm2

29.629
29.556
29.412
29.195
28.906
28.472
28.183
27.461
27.316
Shear stress at failure
26.015
qu = 29.2N/cm2
24.57
22.908
20.957
18.789
15.898
11.924

Shear strain at failure (11.4%)


3.613
0

Sample 2, Iron ore tailings

10

11

12

13

14

15

16

Shear Strain %

Figure 5.19 - Stress-Strain curve for sample 2 (Iron ore tailings from pit 2)

Civil Department, R V College of Engineering

Page 46

Feasibility Study On Iron Ore Mine Tailings

Sample 2, Iron ore tailings

Stress -Strain Curve Scale: X-axis 1unit = 2N/cm2

Y-axis 1unit = 5N/cm2

35

Shear Stress at failure (N/cm2)

30

29.2

25

20
18.2
15

Angle of Internal friction = 65.22

10.3

10

Cohesion C = 2N/cm2
0
0

10

Normal Stress

12

14

16

18

20

(N/cm2)

Figure 5.20 - Graph of Normal stress v/s Shear stress at failure

Civil Department, R V College of Engineering

Page 47

Feasibility Study On Iron Ore Mine Tailings


5.3 Chemical Properties:
Chemical Properties of Tailings: - (courtesy N.N. Sampath Kumar)
Omitted tailings generally consist of traces of silica, iron oxide, aluminium
oxide, titanium oxide etc. Constituents of the tailings are mentioned in the table
below.
Table 5.30 - Chemical Composition

Constituent

Percentage by weight
(per 100gm)

SiO2

68.61

TiO2

Traces

Al2O3

1.15

Fe2O3

25.88

MgO

0.34

CaO

0.63

Na2O

0.31

K2O

0.05

L.O.I.

2.92

Civil Department, R V College of Engineering

Page 48

Feasibility Study On Iron Ore Mine Tailings

6.0 Tests on red soil


6.1 Index properties:
6.1.1 Moisture content test on Iron ore tailings.
The test is conducted as per IS code (28).The results obtained as shown in
table.
Table 6.1 - Sample 1 (Red soil)

1)

Container No.

2)

Mass of container + wet soil (W2) in g

29.762 33.451

3)

Mass of container + dry soil (W3) in g

29.624 33.181

4)

Mass of container (W1) in g

5)

Mass of dry soil (W3 W1) in g

11.294 18.848

6)

Mass of moisture (W2 W3) in g

0.138

0.270

1.222

1.433

2.1

2.2

7)

Water content

1.1

18.330

1.2

14.33

Average moisture content = 1.328%


Table 6.2 - Sample 2 (Red soil)

1)

Container No.

2)

Mass of container + wet soil (W2) in g

29.340 29.608

3)

Mass of container + dry soil (W3) in g

29.089 29.325

4)

Mass of container (W1) in g

13.882 12.743

5)

Mass of dry soil (W3 W1) in g

14.825 16.182

6)

Mass of moisture (W2 W3) in g

0.251

0.283

1.693

1.749

7)

Water content

Average moisture content = 1.721%


Civil Department, R V College of Engineering

Page 49

Feasibility Study On Iron Ore Mine Tailings


6.1.2 Specific Gravity test on Red soil:
The test is conducted as per IS code (29).The results obtained as shown in table.
a) Test Temperature Tt c= 28.5c
b) Relative density of water at Tt c = 0.9962
c) Relative density of water at 27c = 0.9965

d) Correction factor due to temperature

e) Specific gravity,
Table 6.3 - Sample 1 (Red Soil)

Water used: Distilled water


1)

Density bottle No.

1.1

1.2

1.3

2)

Mass of density bottle


(W1) g

72.711

75.431

73.614

3)

Mass of density bottle


+ dry soil (W2) g

132.966 140.046 149.019

4)

Mass of density bottle


+ soil + water (W3) g

237.500 242.500 241.000

5)
6)
7)

Mass of density bottle


+ water (W4) g
Specific gravity at
Tt c
Specific gravity of soil
at 27c = (6) Ct

201.000 202.000 195.000


2.537

2.679

2.564

2.536

2.678

2.563

Average specific gravity = 2.592

Civil Department, R V College of Engineering

Page 50

Feasibility Study On Iron Ore Mine Tailings


Table 6.4 - Sample 2 (Red soil)

Water used: Distilled water


1)

Density bottle No.

2.1

2.2

2.3

2)

Mass of density bottle


(W1) g

72.711

75.431

73.614

3)

Mass of density bottle


+ dry soil (W2) g

134.193 149.561 144.394

4)

Mass of density bottle


+ soil + water (W3) g

237.000 247.000 239.000

5)
6)
7)

Mass of density bottle


+ water (W4) g
Specific gravity at
Tt c
Specific gravity of soil
at 27c = (6) Ct

201.000 202.000 195.000


2.413

2.545

2.643

2.412

2.544

2.642

Average specific gravity = 2.533

Table 6.5 - Average specific gravity

Average specific gravity (using distilled water)


Sample 1

2.592

Sample 2

2.533

Civil Department, R V College of Engineering

Page 51

Feasibility Study On Iron Ore Mine Tailings


6.1.3 Dry Sieve Analysis for Red Soil:
The test is conducted as per IS code (30).
Trial 1: Mass of sample taken for analysis = 500g
Water content =1.328%

Table 6.6 - Sieve analysis for sample 1 (Red soil)

Mass of
I.S sieve
Cumulative
soil
Designation
mass retained
Retained
(mm)
(gm)
(gm)
4.75
2.36
1.7
0.6
0.3
0.15
0.075
pan

4.500
14.500
38.500
46.000
155.000
166.000
38.500
37.000

4.500
19.000
57.500
103.500
258.500
424.500
463.000
500.000

Percentage
of soil
retained
on each
sieve(gm)
0.900
3.800
11.500
20.700
51.700
84.900
92.600
100.000

% finer

99.100
96.200
88.500
79.300
48.300
15.100
7.400
0.000

Sieve Analysis

Sample 1, Red soil


96.2

99.1

88.5

% Passing

79.3

D 60
48.3

D 30
15.1

D 10

7.4

0.01

0.1

Sieve Size (in mm)

10

Figure 6.1 - Grain Size Distribution for Sample 1 (Red soil)

From graph
a) D10 = 120
b) D30 = 205
c) D60 = 295

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Feasibility Study On Iron Ore Mine Tailings

1) Coefficient of curvature

2) Uniform Coefficient

% of soil passing 75 IS sieve = 7.4

Trial 2: Mass of sample taken for analysis = 500g


Water content = 1.721%
Table 6.7 - Sieve analysis for sample 2 (Red soil)

Mass of
Cumulative
I.S sieve
soil
mass retained
Designation Retained
(g)
(g)
4.75
2.36
1.7
0.6
0.3
0.15
0.075
pan

2.500
8.000
33.000
45.500
148.500
174.000
42.500
46.000

2.500
10.500
43.500
89.000
237.500
411.500
454.000
500.000

Civil Department, R V College of Engineering

Percentage
of soil
retained
on each
sieve(g)
2.500
2.100
8.700
17.800
47.500
82.300
90.800
100.000

% finer

97.900
97.900
91.300
82.200
52.500
17.700
9.200
0.000

Page 53

Feasibility Study On Iron Ore Mine Tailings

Sieve Analysis

Sample 2, Red soil


97.9

97.9

91.3

% Passing

82.2

D 60
52.5

D 30
17.7

D 10

9.2

0.01

0.1

Sieve Size (in mm)1

10

Figure 6.2 - Grain Size Distribution for Sample 2 (Red soil)

From graph
a) D10 = 90
b) D30 = 200
c) D60 = 350
1) Coefficient of curvature

2) Uniform Coefficient

% of soil passing 75 IS sieve = 9.2

6.1.4 Liquid Limit:


The liquid limit of the soil corresponds to the water content of a paste which
would give 20mm penetration of the soil. Liquid limit is significant to know the stress
history and general properties of the soil met with construction. The test is conducted
as per IS code (31).
The test results as shown in below tables

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Table 6.8 Sample 1 (Red soil)

Water used: Distilled water


Sl.
No.

Determination No.

34

27

L1.3

L1.4

24.689

27.713

26.696

21.555

21.729

24.694

23.002

18.876

1)

No of Blows

90

58

2)

Container No.

L1.1

L1.2

Mass of container & wet


29.989
soil(gm) w2
Mass of container &
26.621
dry soil(gm) w3

3)
4)

5
15
L1.5

5)

Mass of water

3.363

2.963

3.019

3.694

2.657

6)

Mass of container w1

14.940

12.296

15.415

12.064

11.414

7)

Mass of Dry soil

11.681

9.430

9.279

10.998

7.462

8)

Moisture Content

28.790

31.421

32.536

33.588

35.607

Sample 1, Red soil

Liquid Limit

Scale: Y-axis 1unit = 1%

35

Moisture Content (%)

34

33.588

33

32.536

WL = 34%

32

31.421

31
30
29

28.79

28
27

25 Blows

26

25.607

25
1

10

100

1000

No. of Blows
Figure 6.3 - Liquid limit for sample 1 (Red soil)

Liquid limit (WL) = 34%

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Table 6.9 Sample 1 (Red soil)

Water used: Distilled water


Sl.
No.

Determination No.

1)

No of Blows

2)

Container No.
Mass of container &
wet soil(gm) w2
Mass of container &
dry soil(gm) w3

3)
4)

37

97

27

42

26

L1.1

L1.2

L1.3

L1.4

34.356

35.787

38.973

44.225

49.573

29.772

31.869

33.501

37.481

41.431

L1.5

5)

Mass of water

4.584

3.918

5.472

6.737

8.142

6)

Mass of container w1

14.928

18.325

16.164

15.447

17.237

7)

Mass of Dry soil

14.844

13.544

17.337

22.014

24.194

8)

Moisture Content

30.881

28.928

31.563

30.566

33.653

Sample 2, Red soil

Liquid Limit

Scale: Y-axis 1unit = 1%

35

Moisture Content (%)

34

33.653

WL = 31.8%

33
32

31.563
30.881
30.556

31
30

29.928

29
28
27
26

25 Blows

25
1

10

100

1000

No. of Blows
Figure 6.4 - Liquid limit for sample 2 (Red soil)

Liquid limit (WL) = 31.8%


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Feasibility Study On Iron Ore Mine Tailings


6.1.5 Plastic Limit:
Plastic limit is the water content at which the soil mass can be rolled into a
thread of 3mm diameter and the thread shows signs of cracking. The test is
conducted as per IS code (31).
Table 6.10 Sample 1 (Red soil)

Sl.
No.

Determination No.

1)

Container No.

P1.1

P1.2

P1.3

2)

Mass of container &


wet soil(gm)

18.905

17.039

17.467

3)

Mass of container &


dry soil(gm)

18.407

16.347

16.726

4)

Mass of Moisture

0.498

0.692

0.741

5)

Mass of container

15.264

12.174

12.411

6)

Mass of Dry soil

3.143

4.173

4.315

7)

Plastic limit %

15.845

16.583

17.173

P2.1

P2.2

17.715

18.758

21.359

17.267

18.217

20.393

Average Plastic Limit = 16.534%


Table 6.11 Sample 1 (Red soil)

Sl.
No.
1)
2)
3)

Determination No.
Container No.
Mass of container &
wet soil(gm)
Mass of container &
dry soil(gm)

P2.3

4)

Mass of Moisture

0.448

0.541

0.966

5)

Mass of container

14.494

15.657

15.115

6)

Mass of Dry soil

2.773

2.560

5.278

7)

Plastic limit %

16.156

21.133

18.302

Average Plastic Limit = 18.530%


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6.2 Engineering Properties:


6.2.1 Standard proctor compaction test:
The test is conducted as per IS code (32).
Results are as shown in table:
a) Diameter of mould (cm), D = 10.6
b) Height of mould (cm),h

= 12.7

c) Volume of mould (cm3)

= 997.458

d) Mass of mould (gm)

= 2285

e) No. of Layers

=3

f) No. of Blows/ Layer

= 25

g) Specific Gravity

= 2.592

Dry density at 100% saturation (gm/cc) =

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Table 6.12 - Sample 1 (Red soil)
Sl.
No

Determination No

5162

5163

10

12

14

Mass Of mould with compacted soil (gm)

% water added

Mass Of compacted soil (gm)

2877

2878

2809

2772

Wet Density (gm/cc)

2.884

2.885

2.816

2.779

Moisture cup No.

C1.1

C1.2

C1.3

C1.4

Mass of Cup (gm)

13.674

15.085

16.208

14.931

Mass of cup + wet soil (gm)

26.847

36.025

41.267

37.801

Mass Of cup - dry soil (gm)

25.373

33.299

37.917

34.535

Mass of dry soil (gm)

11.699

18.214

21.709

19.604

10

Mass of water (gm)

1.474

2.726

3.350

3.266

11

Moisture content (%)

12.599

14.967

15.431

16.660

12

Dry Density (gm/cc)

2.561

2.509

2.440

2.382

13

Dry density at 100% saturation (gm/cc)

1.954

1.868

1.851

1.810

Dry Density (g/cc)

Sample , Red soil


2.6
2.59
2.58
2.57
2.56
2.55
2.54
2.53
2.52
2.51
2.5
2.49
2.48
2.47
2.46
2.45
2.44
2.43
2.42
2.41
2.4
2.39
2.38
2.37
2.36
2.35

Compaction

5094

4
5057

Scale: X-axis 1unit = 0.5%


Y-axis 1unit = 0.01g/cc

2.509

d max = 2.51g/cc

2.461
2.44

OMC = 15%

2.382

10 10.5 11 11.5 12 12.5 13 13.5 14 14.5 15 15.5 16 16.5 17 17.5 18 18.5 19

Moisture Content (%)


Figure 6.5 - Optimum moisture content for sample 1 (Red soil)

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Feasibility Study On Iron Ore Mine Tailings


Table 6.13 - Sample 2 (Red soil)
Sl.
No

Determination No

4881

5003

5173

5155

5120

10

12

14

16

Mass Of mould with compacted soil (gm)

% water added

Mass Of compacted soil (gm)

2596

2718

2768

2888

2870

2835

Wet Density (gm/cc)

2.603

2.725

2.775

2.895

2.877

2.842

Moisture cup No.

C2.1

C2.2

C2.3

C2.4

C2.5

C2.6

Mass of Cup (gm)

13.960

12.320

11.327

15.299

14.137

15.015

Mass of cup + wet soil (gm)

24.822

26.673

27.922

32.084

33.034

35.539

Mass Of cup - dry soil (gm)

24.095

25.516

26.519

30.365

30.766

32.902

Mass of dry soil (gm)

10.135

13.136

15.192

15.066

16.329

17.887

10

Mass of water (gm)

0.727

1.157

1.403

1.719

2.268

2.637

11

Moisture content (%)

7.137

8.768

9.25

11.410

13.889

14.743

12

Dry Density (gm/cc)

2.429

2.505

2.540

2.599

2.526

2.477

13

Dry density at 100% saturation (gm/cc)

2.144

2.073

2.053

1.965

1.874

1.844

Dry Density (g/cc)

Scale: X-axis 1unit = 0.5%


Y-axis 1unit = 0.01g/cc

Compaction

Sample 4, Iron ore tailings


2.62
2.61
2.6
2.59
2.58
2.57
2.56
2.55
2.54
2.53
2.52
2.51
2.5
2.49
2.48
2.47
2.46
2.45
2.44
2.43
2.42
2.41
2.4

5053

d max = 2.60g/cc

OMC = 11.4%

6.5

7.5

8.5

9.5 10 10.5 11 11.5 12 12.5 13 13.5 14 14.5 15 15.5 16

Moisture Content (%)


Figure 6.6 - Optimum moisture content for sample 2 (Red soil)

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Feasibility Study On Iron Ore Mine Tailings


6.2.2 Direct shear test:
The test is conducted as per IS code (32).The results are shown below
a) Proving Ring No.

= 71018

b) Dimension of specimen (cm)

= 6 X 6 X 2.5

c) Weight of specimen (gm)

= 197

d) Normal Load (N)

= 4.905

Table 6.14 Sample 1 (Red soil)

Load (KN)

Sl.
No. Proving ring
readings

Load
Values

Shear Displacement
(mm)
Dial Gauge
Value
readings

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

1)

40

0.043

50

0.500

0.008

0.833

2.891

2)

130

0.141

100

1.000

0.017

1.667

9.394

3)

210

0.228

150

1.500

0.025

2.500

15.176

4)

282

0.306

200

2.000

0.033

3.333

20.379

5)

327

0.354

250

2.500

0.042

4.167

23.631

6)

353

0.383

300

3.000

0.050

5.000

25.510

7)

364

0.395

350

3.500

0.058

5.833

26.305

343

0.372

400

4.000

0.067

6.667

24.787

9)

322

0.349

450

4.500

0.075

7.500

23.269

10)

301

0.326

500

5.000

0.083

8.333

21.752

8)

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Shear Stress (N/cm2)

Normal Load = 4.905kN


28
27
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0

Stress -Strain Curve Scale: X-axis 1unit = 1%

Y-axis 1unit = 1N/cm2

26.305

25.51

Shear stress at failure


qu = 26.1N/cm2

24.787

23.631

23.269
21.752

20.379

15.176

9.394

Shear strain at failure (5.8%)


2.891
0

Red soil

10

Shear Strain %
Figure 6.7 - Stress-Strain curve for sample 1 (Red soil)

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Feasibility Study On Iron Ore Mine Tailings


a) Dimension of specimen (cm) = 6 x 6 x 2.5
b) Weight of specimen (gm)

= 184.5

c) Normal Load (N)

= 9.81
Table 6.15 Sample 1 (Red soil)

Sl.
No.

Load (KN)

Shear Displacement
(mm)
Dial Gauge
Value
readings

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

Proving ring
readings

Load
Values

1)

0.001

50

0.500

0.008

0.833

0.072

2)

30

0.033

100

1.000

0.017

1.667

2.168

3)

133

0.144

150

1.500

0.025

2.500

9.611

4)

204

0.221

200

2.000

0.033

3.333

14.742

5)

290

0.314

250

2.500

0.042

4.167

20.957

6)

358

0.388

300

3.000

0.050

5.000

25.871

7)

425

0.461

350

3.500

0.058

5.833

30.713

466

0.505

400

4.000

0.067

6.667

33.676

9)

495

0.537

450

4.500

0.075

7.500

35.771

10)

508

0.551

500

5.000

0.083

8.333

36.711

11)

491

0.532

550

5.500

0.092

9.167

35.482

12)

460

0.499

600

6.000

0.100

10.000

33.242

13)

430

0.466

650

6.500

0.108

10.833

31.074

8)

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Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Shear Stress (N/cm2)

Normal Load = 9.81kN


39
38
37
36
35
34
33
32
31
30
29
28
27
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0

Y-axis 1unit = 1N/cm2

36.711
35.771
35.482
33.676
33.242
31.074
30.713

Shear stress at failure


qu = 36.5N/cm2

25.871
20.957

14.742
9.611

Shear strain at failure (8.2%)


2.168
0.072
0

Red soil

10

11

12

Shear Strain %
Figure 6.8 - Stress-Strain curve for sample 1 (Red soil)

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Feasibility Study On Iron Ore Mine Tailings


a) Dimension of specimen (cm) = 6 X 6 X 2.5
b) Weight of specimen (gm)

= 180

c) Normal Load (N)

= 14.715
Table 6.16 Sample 1 (Red soil)

Load (KN)
Sl.
No. Proving ring Load
readings
Values

Shear Displacement
(mm)
Dial Gauge
Value
readings

Shear
strain

Strain
(%)

Shear
Stress
N/cm2

1)

174

0.189

50

0.500

0.008

0.833

12.574

2)

293

0.318

100

1.000

0.017

1.667

21.174

3)

380

0.412

150

1.500

0.025

2.500

27.461

4)

452

0.490

200

2.000

0.033

3.333

32.664

5)

514

0.557

250

2.500

0.042

4.167

37.144

6)

561

0.608

300

3.000

0.050

5.000

40.541

7)

588

0.637

350

3.500

0.058

5.833

42.492

575

0.623

400

4.000

0.067

6.667

41.552

9)

554

0.601

450

4.500

0.075

7.500

40.035

10)

526

0.570

500

5.000

0.083

8.333

38.011

8)

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Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 1%

Shear Stress (N/cm2)

Normal Load = 14.715kN


45
44
43
42
41
40
39
38
37
36
35
34
33
32
31
30
29
28
27
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10

Y-axis 1unit = 1N/cm2

42.492
40.541

Shear stress at failure


qu = 42.5N/cm2

41.552
40.035
38.011

37.144
32.664

27.461

21.174

Shear strain at failure (6%)


12.574
0

Red soil

10

Shear Strain %
Figure 6.9 - Stress-Strain curve for sample 1 (Red soil)

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Feasibility Study On Iron Ore Mine Tailings

Stress -Strain Curve Scale: X-axis 1unit = 2N/cm2

Red soil

Y-axis 1unit = 5N/cm2

45

42.5

Shear Stress at failure (N/cm2)

40
36.5

35
30
26.1

25

Angle of Internal friction = 56.3


20
15

Cohesion C = 21N/cm2

10
5
0
0

10

Normal Stress

12

14

16

18

(N/cm2)

Figure 6.10 - Graph of normal stress v/s Shear stress at failure for sample 1(Red soil)

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Page 67

20

Feasibility Study On Iron Ore Mine Tailings

7.0 Properties of Mixture:


Two combinations of mixes were used in the present study, such as Burnt Clay
Mortar Mix and Burnt Iron Ore Tailings Mix. We all know that when clay is burnt at
higher temperatures for certain duration it turns into pozzolona. Therefore, both the
samples, namely red soil and iron ore Tailings were wet sieved under 75 micron sieve.
Quantity obtained after wet sieving the sample through 75 IS sieve were collected
and dried in sun light till the moisture evaporates and then it is kept for burning in
muffle furnace for four hours after attaining 6000C.
Below table gives the proportion of mix by weight.

Table 7.1 Constituents used for different types of mixes

Burnt Clay
Mortar mix
Iron ore tailing
mortar mix

1
Lime
1
Lime

Burnt Clay
Mortar mix
Burnt Iron ore
tailing mortar mix

1
Lime
1
Lime

Types of mixes
2
Burnt Clay
2
Iron ore
tailing
Types
of mixes
2
Burnt Clay
2
Iron ore
tailing

Civil Department, R V College of Engineering

6
Standard Sand(1:1:1)
6
Standard Sand(1:1:1)
9
Standard Sand(1:1:1)
9
Standard Sand(1:1:1)

Page 68

Feasibility Study On Iron Ore Mine Tailings

8.0 Experimental Investigations


Two Mixes with different ratio of constituents were prepared from each type of
mixtures (i.e. burnt clay Mortar mix as lime surkhi and Burnt Iron ore tailing mortar
mix). Six samples were prepared from each mix with proportions of 1:2:6 and 1:2:9
for both Burnt Clay and Iron Ore Tailings and were tested for 7 and 21 days. The
mixture is prepared as per weight batching and it is dried properly under sunlight. The
ingredients were mixed by adding known amount of water and immediately used for
moulding. Three specimens (Blocks 5x5x5cm) from each type of mix proportions,
cured for 7 days and 21 days were tested for compressive strength. The test method
followed was as per IS Specification.

Table 8.1 - Compressive strength of specimens of different mix proportions

Burnt Clay Mortar mix

Mix

1:2:6
1:2:9

Compressive
strength (MPa)
7 days
28
curing
days
curing
1.4308
3.208
2.038
3.252
2.038
3.252
1.171
2.950
1.084
2.818
1.127
2.862

Civil Department, R V College of Engineering

Burnt Iron ore tailing


mortar mix
Compressive
Mix
strength (MPa)
7 days
28
days
curing
curing
1:2:6
0.1734
0.2168
1:2:9
0.1794

Page 69

Feasibility Study On Iron Ore Mine Tailings

9.0 Results and Overall Discussion


9.1 Compressive strength
The compressive strength of mix was compared according to the leanness of
the mix proportion and also with its respective mix proportions (i.e. with burnt clay
and burnt tailings mixes). But, in our study, blocks casted of burnt iron ore tailings
yielded negligible strength an shown in the table (7.1). Therefore our study narrow
downs to the comparison of burnt clay mix only. As shown in the below chart 8.1,
when we compare 7 days and 21 days strength, there is considerable increase in the

Avg. compressive
strength (Mpa)

strength for both 1:2:6 and 1:2:9 mixes.


4

3.2373

2.877

3
2

1.8356
1.1273

7 days

21 days

0
1

1:2:6

1:2:9

mixes
Figure 9.1 - Comparison of compressive strengths of burnt clay mix cured for 7 days and 28 days

Avg. compressive strength (Mpa)

Below figure shows the comparison according to the leanness of mixes. We


can observe that there is decrease in 7 days strength of 1:2:9 burnt clay mixes when
compared to 1:2:6 burnt clay mix. This compares 21 days strength also.

3.2373

3.5

2.877

3
2.5
2

1.8356

1.5

7 days

1.1273

21 days

1
0.5
0

1:2:6

1:2:9

1 1:2:6

1:2:9

mixes
Figure 9.2 Comparison of compressive strengths of burnt clay mixes, (1;2:4) with (1:2:9)

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Page 70

Feasibility Study On Iron Ore Mine Tailings

10. Conclusion
Lime-Pozzolona cement is considered as the secondary alternative to Portland
cement. Surkhi or Burnt clay pozzolona has been used in India since ancient times to
produce hydraulic cement by mixing it with lime. The term pozzolona has been used
to designate reactive siliceous and aluminous materials, which react with calcium
hydroxide in presence of moisture to form stable cementations compounds.
Following conclusions were made from results obtained by conducting tests.
From tests it is revealed that iron Ore Tailings bought from Kudremukh, do not posses
or have negligible pozzolonic action, though they contain ferruginous material.
However, tests show that red soil as a surkhi produces 21 day compressive strength of
3.2373 MPa for 1:2:6 mix. According to IS 1905, cement mortar should posses the
strength of 3 MPa in 28 days. Our study yielded required strength for 21 days only.
Since, it matches Indian Standards specifications for 21 days only; it is expected to
more strength in 90 days and 180 days.
Red soils denote the second largest soil group of the country covering an area
of about 6.1 lakh sq. Km, this red clay pozzolona can be used as an alternative
material for building construction as replacement to cement.
In our study, stabilisation of red soil was studied by adding, lime to the virgin
red soil in the proportions (lime: virgin soil) 1:10 and 1:12. Soil did not attain much
strength, therefore our study suggests to carryout tests in this aspect by increasing
lime content.
Further studies should be carried out on this burnt clay pozzolona at different
temperatures, different burning duration and also for different proportions like (lime:
pozzolona) 1:1, 1:1.5 and many other combinations to yield better strength.

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11.0 References
1. Ullas S N and Venkatarama Reddy IISc, 2009, Proceedings of the International
Seminar On Waste To Wealth, November , New Delhi, India. Iron Ore tailings as
substitutenfor sand in masonry mortor, [P.No 151-155]
2. Mangalpady Aruna, 2012 Utilization of Iron Ore Tailings in Manufacturing of
Paving Blocks for Eco-friendly Mining March [P.No. 1-12].
3. Shri N.N. Sampath Kumar, 2013, Article On 'SAVE THE EARTH' - Eco friendly
solutions to iron ore tailings, [P.No. 1-3].
4. Hammond, A. A., 1998, Mining and Quarrying Wastes A Critical Review,
Engineering Geaology, [P.No. 17-31].
5. Monalisa Mohanty, Nabin Kumar Dhal, Parikshitha Patra, Bisweswar Das and Palli
Sita Rama Reddy., 2001, A Novel Approach for Utilization of Iron Ore Wastes,
Reviews of Environmental Contamination and Toxicology, [P.No. 29-35].
6. Ajaka E. O., vol. 4, No. 9, NOVEMBER 2009, ARPN Journal of Engineering and
Applied Sciences, Recovering Fine Minerals From ITAKPE Iron Ore Process
Tailing, [P.No. 1-6]
7. Venkateshwarlu, J., Strength Characteristics of Concrete Hollow Bricks With
Replacement of Sand by Iron Ore Tailings, MS Thesis, Civil Engineering Department,
Mangalore University, India, 2000.
8. Jaladi, S. K. (2001) Studies on Concrete Hollow Bricks With Iron Ore Tailings as
Fine Aggregate, MS Thesis, Mangalore University at Karnataka.
9. Amit, R., Rao, D. B. N. 2005., Utilization Potentials of Industrial/Mining Rejects and
Tailing as Building Materials, Management of Environmental Quality: An
International Journal, Name of Journal,16, 605-614,
10. Kumar, S., Kumar, R., Amitava, B. 2006., Innovative Methodologies for the
Utilization Waste from Metallurgical and Allied Industries, Resources, Conservation
and Recycling, 48(4), 301-314.
11. Roy, S., Adhikari, G. R., Gupta, R. N., 2007, Use of Gold Mill Tailings in Making
Bricks: A Feasibility Study, Waste Management and Research, 25, 474-482.
12. Chao, L., Hengu, S., Zhongalai, Y., Longtu, L., 2010, Innovative Methodology for
Comprehensive Utilization of Iron Ore Tailings: Part 2 The Residues After Iron
Recovery From Iron Ore Tailings to Prepare Cementitious Material, Journal of
Hazardous Material,174(1-3), 7883.

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13. Jinhua, W., Fuping, L., Jain,, W., Lijie, S., Rong,, J. , 2010, Spatial query and
Analysis of Tailings Management Based on GIS, Information Science and
Engineering (ICISE), in Second International Conference, 4, pp. 4033-4035.
14. Muduli, S. D., Raut, P. K., Pany, S., Mustakim, S. M., Nayak, B. D., Mishra, B. K.,
Innovative Process in Manufacture of Cold Setting Building Brick from Mining and
Industrial Wastes, The Indian Mining and Engineering Journal, 49(8), 127- 130, 2010.
15. Gan, D., Chen, C., Zhang, J. , 2011, Test Research on Preparation of New Wall
Material with Iron Tailings in Tangshan Area, Advanced Material Research, 295-297,
535-538.
16. Yongliang, C., Yamin, Z., Tiejun, C., Yunliang, Z., Senxu, B , 2011, Preparation of
Ecofriendly Contruction Bricks from Hematite Talings, 25(4), 2107-2111.
17. Jian, S., Yuan, L., Yang, L., Tan, H., Xiang-guo, L., Bao-guo, M. , 2011, Study on
Sintered Wall Materials Made Use of Iron Tailings and Waste Rock, Advanced
Material Research, 243-249, 7036-7040.
18. Niu, X., Chen, J (2011)., Effect of Additives on the Properties of Concrete Products
Made from Iron Ore Tailings, in Proceedings of International Symposium on Water
Resource and Environmental Protection (ISWREP), 3, pp. 1670-1673.
19. Yongliang, C., Yimin, Z., Tiezun, C., Tao, l., Yunliang, Z., Xiangke, J, 2011,
Utilization of Hematite Tailings in Non-fired Bricks Production, Bioinformatics and
Biomedical Engineering (ICBBE), 1-4.
20. Keqing Wang, L., Chen, H., Sanxia, 2011, Development and Application of
Intelligent Decision Support System for Comprehensive Utilization of Tailings and
Waste Rocks, in International Conference on E-Business and E-Government (ICEE),
PP. 1-4.
21. Robert, J. C., Richard, H. M. , 2011, Utilization of Mining and Mineral Processing
Wastes in the United States, Earth and Environmental Science, 1(1), 8-19.
22. M R Yogananda (1983) A Thesis on Surkhi and Rice husk ash pozzolona dept of
Civil Engineering, IISc, Bangalore, 11-14.
23. N R Srinivasan, (1956), Surkhi as a pozzolona, CRRI- Central Road Research
Institute, New Delhi, 55-60.
24. Karnataka Engineering Research Station (KERS), National Conference on Emerging
Trends of Energy Conservations in Buildings, a CBRI, 6-10.

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25. R K Ghosh, N R Srinivasan, M L Bhatia and S G Banerjee, (1964), Road Research
Sprecial ReportPozzolonic Clays of India, Their industrial Exploitation and use in
Engineering works, A Study on Reactive Surkhi Mortars. 235-238.
26. Ram Lal, R K Ghosh and N R Srinivasan, (1964),

Road Research Sprecial

ReportPozzolonic Clays of India, Their industrial Exploitation and use in


Engineering works, Construction of an Experimental Pozzolona concrete Road
Stretch on the National Highway-2, 226-230.
27. Ralph E Grim, (1962), Applied Clay Mineralogy, Mcgraw-hill inc., New York
Toronto London, 348-351.
28. IS: 2720 (Part 2) 1973, (Reaffirmed 2002), Edition 3.1 (1982-08). Indian Standard
methods of test for soils part 2, determination of water content (second revision).
29. IS 2720 ( Part 3/Sec I ) 1980 Indian standard methods of test for soils part 3,
determination of specific gravity, Section 1 Fine Grained Soils.
30. IS: 2720 (Part 4) - 1985(Reaffirmed 1995), Indian standard methods of test for soils
part 4, grain size analysis (Second Revision).
31. IS: 2720 (Part 5) - 1985(Reaffirmed 1995), Indian standard methods of test for soils
part 5, determination of liquid limit and plastic limit (Second Revision).
32. IS : 2720 (Part 7) 1980 (Reaffirmed 2002), Edition 3.2 (1984-07) Indian Standard
methods of test for soils part 7, determination of water content-dry density relation
using light compaction (Second Revision).
33. IS : 2720 ( Part 13 ) - 1986 ( Reaffirmed 1997 ) Indian Standard methods of test for
soils part 13, direct shear test (Second Revision)

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