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Why
Phase identification
Chapter 9
NaCl
Anatase TiO2
The powder pattern for the spinel MgAl2O4 looks different from the
powder pattern of a MgO, Al2O3 mixture
KCl
Phase identification
Rutile TiO2
A PDF card
There
Each entry is associated with a card number, the name and composition of
the phase, the conditions for the data collection, a reference to the source
of the information, crystallographic data, physical data, sample preparation
information, a quality mark, and a list of d-spacings and intensities
Hanawalt index
Search procedure
The
Locate
NaCl example
If
Plot-replot method
When
Plot-replot method
Make
If
Make
Problems
Try multiple packings of sample. If you see intensity variations consider using a
different sample preparation method or grinding the sample.
Phase identification
Illustrate
Collect your data with an internal standard present so that you can correct any
angular errors