SAMPLE DESCRIPTION BASICS

The wellsite geologist is responsible for inspection of rock samples as they are gathered
and preparation of the sample log. He may delegate this to the mud loggers if they are on
site. The wellsite geologist also is responsible for a myriad of other tasks, including ordering
geological supplies, picking the location of cores and tests, packing and shipping recovered
cores and fluid samples, calling for and supervising wireline logging operations, velocity
surveys, mud logging crews, and other survey personnel, liaison with drilling crews and
home office, and above all, must be a good cribbage or gin rummy player.
The sample log, often called the stratigraphic log, strat log, or geology log, is a record of the
rock samples retrieved from the drilling mud, and is one of the primary sources of rock and
fluid descriptions for the well. It consists of a verbal description of the rock type as well as
qualitative or interpretive data concerning evidence of the fluid content of the rock. Sample
description is sometimes called formation evaluation, but this term usually covers a broader
scope, including drill stem test a and log analysis.

Cuttings are collected, washed, and described at 5 to 20 foot (2 to 5 meter) intervals unless
extremely rapid penetration rate makes this impractical. In such cases, they would then be
collected as often as possible, but no less than once for each time drilling is resumed after a
pipe connection. A constant sampling rate is chosen, depending on the lithology expected.

Sample chips are quite small, so large scale features such as fractures, bedding planes, and
fossils often cannot be seen. Samples can be contaminated by rock sloughing from above,
or may be lost due to lost circulation, pulverization, or careless well site procedures.

Washed sample of a siltstone magnified 20 times
Washed rock chips are observed under a microscope (10 to 20 power) and described as to
mineralogy, colour, texture, rounding, sorting, grain size, cementing minerals, porosity,
porosity type, permeability, macro fossils, and fractures. These are qualitative descriptions.
Quantitative values usually come from core analysis and log data, but semi-quantitative
lithology analysis is possible under the microscope. Obvious formation tops, marker beds,
and lithology changes are listed. Drill stem test recoveries, coring intervals and coring
times, logs run, bit changes, and other logistical data which might influence the
understanding of the sample log are given.

Obvious formation tops, marker beds, and lithology changes are listed. Drill stem test
recoveries, coring intervals and coring times, logs run, bit changes, and other logistical data
which might influence the understanding of the sample log are given.

Sample descriptions will include an
estimate of visual porosity, porosity
type, grain size, sorting, roundness,
and colour, as well as shale
distribution, brittleness, laminations,
and colour.
Primary porosity is the porosity
developed by the original
sedimentation process by which the
rock was created. In reports, it is
often referred to in terms of
percentages, while in calculations it
is always a decimal fraction.

Secondary porosity is created by
processes other than primary
cementation and compaction of the
sediments. An example of secondary
porosity can be found in the solution
of limestone or dolomite by ground
waters, a process which creates
vugs or caverns. Fracturing also
creates secondary porosity.
Dolomitization results in the
shrinking of solid rock volume as
the material transforms from calcite
to dolomite, giving a corresponding
increase in porosity.
Porosity Types: a. intergranulas, b.
Sucrosic,
c. Moldic or Oolitic, d. Matrix or
Chalky,
e. Moldic or Vuggy, e. Fracture
porosity.
Intergranular porosity is primary, the
balance are secondary.
For details,See Also:
Shale Basics
Porosity Basics

Oil show indicators are found by examination of the rock samples for oil stain, bleeding,
fluorescence, or cut. Stain is the trace of asphaltic material left behind on drill cuttings after
the oil has been washed off during drilling. Stain left by high quality oil has a typical
iridescent sheen, visible in normal light. Bleeding is the exudation of oil from the pores due
to pressure release as the sample is brought to the surface.

Fluorescence represents oil's distinctive ability of emitting light in the visible range when
exposed to ultraviolet light. Unfortunately, quite a number of minerals and many refined
products are fluorescent, so there is a certain amount of technique involved in
distinguishing between primary hydrocarbons and refined products or fluorescent minerals.

A simple chemical test may be carried out to determine whether fluorescence in drill
cuttings is a result of oil or some fluorescing mineral. This is easily and quickly established
by immersing some of the drill cuttings in a petroleum solvent (chlorothene, trichlorothene,
ether, or acetone). If the fluorescence is derived from mineral sources, the minerals will not
dissolve in the solvent and the solvent will remain colorless under ultraviolet light.

However, if hydrocarbons are present in the rock, they will disseminate into the solvent,
giving the entire solvent a distinctive color under ultraviolet light. This sheen under UV light
is called cut and the colour of the cut indicates the quality of the oil. Pale blue-white is high
gravity (light) oil, yellow is medium gravity, and orange-brown for low gravity (heavy) oil.


Lightly washed wet samples should also be examined, and not dried, because light oils and
condensates may evaporate. Under UV light, a differentiation should be made between
mineral fluorescence, natural hydrocarbon fluorescence, and fluorescence from introduced
oils and grease. Natural hydrocarbon fluorescence will usually be lithology specific, while
introduced hydrocarbon fluorescence will be associated with all lithologies. A note of
percentage of cuttings exhibiting natural hydrocarbon fluorescence and the color and
intensity should be made. Mineral fluorescence is determined by the test for cut.

Under ordinary light, the oil stain or oil bleeding from the sample may be visible. It should be
noted for its volume and its intensity, and efforts made to distinguish introduced oil.
Bleeding often indicates low permeability. Light oils are more prone to exhibit irridescence,
while dark stains tend to indicate heavier crudes.

To test for hydrocarbon cut, a small sample is placed in a spot plate, the solvent is
introduced, and the color, intensity, and rate of cut are observed in ordinary and ultraviolet
light. The sample is crushed and the test is repeated. If there is no cut at this stage, any
fluorescence is probably mineral derived. Generally, the heavier the oil, the greater the cut;
however, asphaltic oils show a greater cut than paraffinic oils of the same gravity.

The chromatography of the oil should be noted. A drop sample of hydrocarbon
contaminated solvent should be placed on filter paper and observed under ordinary and
ultraviolet light. The characteristics of any separation should be noted, including the number
of rings formed.

Larger samples, or a number of smaller samples, may be placed in a test tube and examined
in a similar manner as in a spot plate; the sample should be crushed and the solvent
introduced. A standard method should be employed so comparisons can be made with
nearby wells, ie., 1 cc of crushed cuttings in 2 cc of solvent in a standard 10 cc test tube.

A control test tube of 3 cc solvent should also be set up, and a comparison against white
paper is then observed. Again, a drop of hydrocarbon contaminated solvent should be
tested for chromatography as before.

To test for gas in the cuttings, place an unwashed sample in a blender or food processor,
add water, and analyze the resulting gas. This is done by running a sample of the headspace
gas into the gas chromatograph operated by the mud logging crew.

Sample containing carbonates, either as a main constituent or as a cement, can be tested
further for oil by adding a small amount of hydrochloric acid. Hydrocarbons present in a
sample, either natural or introduced, will cause carbon dioxide bubbles, released by the
action of hydrochloric acid on carbonates, to enlarge by forming an oil film around the
bubbles. Thus, the reaction is more prone to frothing. This test is very sensitive, but it does
not differentiate between natural and introduced hydrocarbons.

The sample log can take many forms: a written narrative, a graph versus depth with a
schematic drawing (along with abbreviated verbal descriptions), or a mud log, which
describes the rock samples, as well as fluids, recovered in the mud. Drilling data such as
penetration rate may also be included.

Example of a sample description log
Below is a a sample of the colours and symbols in use for lithology descriptions on modern
sample description logs.


Colour codes and symbols used to plot lithology and accessory features on a sample
description log
All sample log results are reported daily by telephone, FAX, or email and recorded on a
standard report form for distribution within the oil company. Hydrocarbon shows are
especially desirable; a show is defined as any indication of hydrocarbons, ie., stain,
fluorescence, or cut, or any increase in drilling mud gas of reasonable percentage above
background.


LAG TIME
Depth information is obtained from the driller's log, which records depth versus the time of
day. However, these depths cannot be used directly. We wish the mud log data to be
presented at the depth of the drill bit, but the mud log measurements are made at the
surface. The time it takes for the mud to move from the bit to the surface must be accounted
for in positioning samples and gas kick data on the log. This time is called the lag time and
depends on the velocity of the mud in the annulus between the drill pipe and the rock. This
in turn depends on the mud pump speed and displacement, which are usually constant for
reasonable periods of time.
The lag time can vary from a few minutes in an air drilled hole, to hours in a deep mud filled
hole. If lag time is much shorter than expected or multiple lags are found, it usually means a
leak in the drill pipe which must be repaired immediately. The most reliable method of
establishing the lag time is to use a tracing material such as oats, corn, paint, or calcium
carbide. Carbide will produce a bubble of acetylene gas. Typically, a sample of tracing
material is introduced into the drill pipe during a connection and circulated down through
the bit jets and back up the annulus. The use of calcium carbide as a lag tracer has a
secondary benefit. It permits verification that the entire gas detection system is functioning.
Since it is necessary for the gas detector to extract, pump to the logging unit, and sense the
acetylene gas, it verifies the integrity of the entire system.

This is only part of the story, as the time it takes the tracer to go down the inside of the drill
pipe must first be calculated from the pump displacement, pump speed, pipe diameter, and
pipe length. The calculated downward time is deducted from the total measured time to find
the lag time.

SAMPLE DESCRIPTION LOG EXAMPLES
Below are examples of sample description logs from various eras.

One of the first well logs in Western Canada from Proceedings and Transactions of the
Royal
Society of Canada for the Year 1886 Volume IV. Glenbow Archives

A hand drawn sample log typical of the 1940 to 1970 era.

A computer drawn sample log of the 1980's. Hand drafted logs could be drawn as neatly as
this using lettering guides.


Modern sample log using colour and computer graphics symbols.