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Sulfur and Chlorine by Wickbold Apparatus
ASTM D 2384, ASTM D 2784, ISO 4260, IP 243, JIS K2240, JIS K2541-1, FD M07-008
Product group(s): Fuel
User group(s): Biodiesel, Chemicals, Fuel, Gas Oil, Gasoline, Jet Fuel, Liquefied Petroleum Gases, Power Generation
Scope:
These test methods cover the determination of the total volatile organic chlorides in concentrations from 10 to
100 ppm in butane-butene mixtures.
DIN 51408 describes a special procedure for the determination of chlorine content in the range of 0.5 to
10 mg/kg.
automatic ignition
automatic control of cooling water
flame arresters
Wickbold Test Equipment
to be composed of:
- Wickbold-Combustion-Apparatus Type V 5
- Water-Ring Vacuum Pump
- Circulation Cooler
Technical Data
Dimension (W x D x H): 910 x 420 x 820 mm
Main Unit
13-0670 Wickbold-Combustion-Apparatus Type V 5
improved for safety reasons, in analogy to
ASTM D 2384 - ASTM D 2784 - DIN 51 408-1 - EN 24 260 -
FD M07-008 - IP 243 - ISO 4260 - JIS K2240 - JIS K2541-1
Measuring sulfur (1... 50,000 ppm) and chlorine (1...10 ppm).
Consisting of:
Instrument frame:
Consisting of:
control console; all holders and clamps for mounting the glassware; connections for supply of vacuum,
cooling water, hydrogen, nitrogen and oxygen.
Glass-equipment:
Consisting of:
1 combustion chamber with condenser (13-0673)
2 measuring flasks 100 ml (13-0657)
1 absorption vessel (13-0676) with rinsing device (13-0677)
1 gas-washing bottle with insert (13-0688)
1 ignition tube (13-0674)
1 suction burner, quartz-glass for liquids (13-0652)
Note: Vacuum pump is not included!
The included burner is only for liquids.
For solids order 13-1398 and for gases 13-0641.
Power supply: 230 V, 50/60 Hz
13-0671 Wickbold-Combustion-Apparatus Type V 5
Power supply: 115 V, 50/60 Hz
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Options & Accessories
13-1390 Water-Ring Vacuum Pump regulated by Wickbold-unit
Power supply: 230 V, 50/60 Hz
13-1391 Water-Ring Vacuum Pump regulated by Wickbold-unit
Power supply: 115 V, 50/60 Hz
13-1392 Circulation Cooler adjusted for Wickbold-unit
As a substitution of cooling the safety devices of the Wickbold-Apparatus with tap water or in warm
environment, there is recommended the use of this specially designed coolant circulator.
Technical Data:
Cooling: 2900 Watt / 20C
Pump: 600 l/h / 22 mWS
Pressure: max 38 mWS (3,8 bar)
Bath volumne: 50 Liter
Dimensions (WxHxD): 560 x 1100 x 560 mm
Power supply: 230 V, 50 Hz
13-1393 Circulation Cooler adjusted for Wickbold-unit
Like 13-1392 but:
Power supply: 115 V, 50 Hz
13-1394 Pre-Combustion Unit VE for solids & suspensions
Temperature range: up to 1100 C within 7-8 min.
Power supply: 230 V, 50/60 Hz
13-1395 Pre-Combustion Unit VE for solids & suspensions
Like 13-1394 but:
Power supply: 115 V, 50/60 Hz
13-1398 Burner BITC VE for solids
13-0641 Burner F1 for gases with low sulfur content
13-1355 Ground Joint VE
13-1357 Boat VE
Spare Parts
13-0652 Burner SB5 for liquids
13-0664 Taper with rim
13-0675 Micro-Switch with quartz-rod
13-0657 Flask, glass with ground neck, 100 ml
13-0673 Combustion Chamber with condenser
13-0674 Ignition Tube of quartz glass
13-0676 Absorption Vessel
13-0677 Rinsing Device
13-0688 Gas-Washing Bottle DIN 12 596 - A 500
13-0967 Sampling Vessel with Single-Valve, 100 ml
ASTM D 1265, ISO 4257, NF M41-001, BS 5309-2+3
670 psi (46 bar) max. working pressure
cylinder & valve made of stainless steel
straight-through valve with 1/8 in. BSP connection
pressure tested and with UKAS certifikate
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13-0968 Sampling Vessel with Single-Valve, 50 ml
ASTM D 1265, ISO 4257, NF M41-001, BS 5309-2+3
670 psi (46 bar) max. working pressure
cylinder & valve made of stainless steel
straight-through valve with 1/8 in. BSP connection
pressure tested and with UKAS certifikate
Order Guideline
Minimum equipment: 1x 13-0670, 1x 13-1390, 1x 13-1392
Spares (approx. 1 year): 13-0657, 13-0674, 13-0688
Additional requirements: H2 = 1 bar, tube ID 10 mm, 20 l / min
O2 = 2 bar, tube ID 6 mm, 20 l / min
N2 = 1 bar, tube ID 6 mm, 2 l / min
Cooling H2O = 1 bar, tube ID 3 mm, 3,5 l / min