Valco Instruments Co. Inc.

HP2w.p65
Rev. 1/11
Printed in USA
Helium Purifier and
Nitrogen Purifier
Instruction Manual
For item numbers:
HP2
HP2-220
NP2
NP2-220
I-23572HP2
I-23572NP2
Valco Instruments Co. Inc.
800 367 8424 sales
713 688 9345 tech
713 688 8106 fax
valco@vici.com
VICI International
Schenkon, Switzerland
Int + 41 41 925 6200 phone
Int + 41 41 925 6201 fax
info@vici.ch
Introduction
Specifications ................................................................................................ 1
Theory of Operation ...................................................................................... 2
Power Supply Requirements ......................................................................... 2
Installation and Operation
Installation ..................................................................................................... 3
Activation ....................................................................................................... 3
Operation....................................................................................................... 3
Removing the HP2 or NP2 from the System ................................................. 4
Routine Maintenance
Replacing the Getter Cartridge ....................................................................... 5
Disposing of Spent Getter Cartridges ............................................................. 5
Technical Drawings ............................................................................................... 6
Warranty ............................................................................................................. 10
1
Introduction
The Valco Helium Purifier (HP2) and Nitrogen Purifier (NP2) provide point-
of-use carrier gas purification to sub-ppm levels of gaseous impurities.
Designed originally for the Valco Trace Gas Analysis system with its Helium
Ionization Detectors, the Helium Purifier provides point-of-use ultrahigh-
purity helium for use in any chromatographic application requiring high-
quality helium or other noble gas (Ar, Ne, Kr, Xe). The Nitrogen Purifier was
developed for use with our Electron Capture Detector.
Specifications
Gases purified
Max. operating pressure
Max. operating temperature
Max. flow rate
Impurities removed
Impurities not removed
He, Ne, Ar, Kr, Xe, Rn
1000 psig
400C
1 liter/min
Outlet impurities less than 10 ppb
H
2
O, H
2
, O
2
, N
2
, NO, NH
3
, CO, and
CO
2
, based on 10 ppm total inlet
impurities. Other impurities
removed include CF
4
, CCl
4
, SiH
4
,
and hydrocarbons such as CH
4
He, Ne, Ar, Kr, Xe, and Rn
He, Ne, Ar, Kr, Xe, Rn, N
2
1000 psig
400C
1 liter/min
Outlet impurities less than 10 ppb
H
2
O, H
2
, O
2
, NO, NH
3
, CO, and CO
2
,
based on 10 ppm total inlet impurities.
Other impurities removed include
CF
4
, CCl
4
, SiH
4
, and hydrocarbons
He, Ne, Ar, Kr, Xe, Rn, CH
4
, and N
2
Helium Purifier
(HP2)
Nitrogen Purifier
(NP2)
WARNING!
This product is not for use with oxygen either pure
oxygen or gases with a significant proportion of
oxygen. The purifiers gettering alloy is pyrophoric
at operating temperature. Use with significant
amounts of oxygen can result in combustion of the
material, potential damage to the surrounding area,
and possible injury.
In no event shall Valco Instruments Co. Inc. be liable
for any direct, indirect, special, incidental, or con-
sequential damage, whether based on contract, tort,
or any other legal theory and whether advised of the
possibility of such damages.
2
Introduction
Theory of Operation
The purification substrate in the Valco purifiers is a non-evaporable
gettering alloy, with a nominal composition of zirconium, vanadium, and
iron. This alloy must be heated so that the oxide layers on the particle
surface are eliminated. This process must be performed under a vacuum or
in at atmosphere of helium (for the HP2) or nitrogen (for the NP2).
Although the gettering alloy will purify even at ambient temperatures, raising
the temperature vastly improves the life span and efficiency of the alloy.
However, the elevated temperature causes hydrogen generation, which is
trapped only at temperatures below 250C. Therefore the Valco purifiers
have been designed to operate at a fixed temperature gradient which yields
a long life span and high efficiency and insures that any hydrogen gener-
ated will be trapped.
Accurate temperatures at the inlet (380-400C) and at the outlet (170-
190C) are maintained with the use of a precision 24 VDC power supply.
Power Supply Requirements
As stated on the purifier, the power supply must conform to EN 61010-1:
Section F.2.1 Limited circuit. This section mandates that the power source
must be limited to 42.4 VDC or less (open circuit). In addition, the energy
must be limited by one of the following means:
the current under any condition of load, including short circuit, is not
more than 8A measured after 1 minute of operation
the source is rated or set to limit its power to 150 VA under any
condition of load
an overload protector or circuit component opens to interrupt the
power output at a lower value than 150 VA under any condition
including short circuit
The power supply is critical for safe and proper opera-
tion of this unit. It is therefore recommended that the
purifer be used only with the power supply received
with it.
3
Installation and Operation
This procedure describes a chromatographic installation. Although that is not
the only possible application, it is the most common. It is up to the user to
determine whether the purifier is suitable for a particular application based
upon the specifications of the purifier.
Installation
The Valco HP2 and NP2 are two part systems comprised of the purifier and
the power supply. The purifier must be installed in a vertical position to
eliminate the possibility of channeling. For best results, do not modify the
fittings or tubing lengths; small particles which might be generated by such
modifications are difficult to remove and can restrict the flow.
1. Connect the input line (tagged INLET) to a carrier gas cylinder with a
high purity regulator. (Save the caps to seal the purifier whenever you
remove it from the system.)
2. Purge the system for 15 to 30 minutes at 20 to 30 mL/min to eliminate
air from the getter material.
CAUTION: The getter material should never be heated
when air is present.
3. Connect the barrel connector of the power supply to the purifier.
4. Connect the power supply to mains (115/230 VAC). The LED on the
power supply should come on to confirm power output.
5. Connect the purifier output line to the chromatographic systems carrier
gas input line using a 1/16" union (Valco Product Number ZU1).
Activation
When the purifier reaches operating temperature (usually in about 2
hours) the getter will be activated. Once the getter is activated, active
gaseous impurities such as H
2
, O
2
, H
2
O, CO, and CO
2
(plus N
2
for the HP2)
are captured and chemisorbed on the getter surface. Only noble gas atoms
are not affected. Once adsorbed, oxygen, carbon, and nitrogen atoms
cannot be released by the getter material even at its melting point (1400C),
due to the formation of strong chemical bonds with the alloy atoms.
Hydrogen atoms behave quite differently, diffusing into the getter material
bulk more quickly than the other atoms and becoming almost uniformly
distributed within the bulk. However, hydrogen sorption occurs below 250C,
achieved through the temperature gradient of the trap assembly.
4
Installation and Operation
Operation
In normal operation the outside temperature of the purifier is warm, but
should not be uncomfortable to the touch. The 24 VDC power supply main-
tains the purifier trap at a constant temperature, and should be located so
that the illuminated LED can serve as a visual indicator of purifier operation.
Removing the HP2 or NP2 from the System
To remove the purifier from the carrier gas line:
1. Disconnect the power supply. Disconnect the output line from the
instrument while maintaining carrier flow.
2. Allow several hours for the the getter oven to cool. After the oven
reaches ambient temperature, cap the output line and allow the
purifier to be pressurized for several minutes.
3. Remove the input line and immediately cap it. This maintains a carrier
gas atmosphere on the gettering substrate, increasing its lifetime.
To reinstall, follow the instructions in the Installation section at the top of
page 3.
5
Routine Maintenance
Do not open or modify the trap assembly.
In normal usage there is no maintenance required on the purifier or power
supply. If the purifier shows signs of saturation it will need replacement.
Replacement cartridges can be ordered from Valco using the product
numbers below.
For an HP2: I-23572HP2
For an NP2: I-23572NP2
Replacing the Getter Cartridge
1. Disconnect the power supply from the purifier, but leave the helium
flow on.
2. Allow at least two hours for the purifier to cool.
3. Using a thin-edged screwdriver or knife, remove the two hole plugs
from the side of the unit and one from the top.
4. The side holes allow access to the two screws which secure the trap.
With a 5/32" allen wrench, turn each screw counterclockwise one to
two rotations.
5. If the trap is still too hot to the touch, allow more cooling time. If it can
be handled, pull it out through the hole in the top of the unit.
6. Disconnect the output line at the fitting, and cap it to allow the trap to
pressurize.
7. Have a second cap at the ready. Disconnect the input line at the
fitting, and cap it immediately.
8. Insert the new trap, making sure the insulation and feed-through hole
plug are snug against the top of the trap. Push the trap assembly
down until the feed-through hole plug is resting on the top of the unit.
9. Tighten both allen screws, making sure the trap does not move.
10. Snap in the feed-through hole plug, and both the side hole plugs.
11. Refer to the Installation section at the top of page 3 to get the
system back in operation.
Disposing of Spent Getter Cartridges
Obtain a return authorization number from VICI by emailing tga@vici.com or
calling 800-367-8424. The packaged getter cartridge should be clearly
marked Traps for Disposal.
6
Technical Drawings
Enclosure Assembly................................................ Drawing 23575 Page 7
Secondary Assembly .............................................. Drawing 23579 Page 8
Final Assembly HP2/NP2 ........................................ Drawing 23580 Page 9
7
Technical Drawings
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S
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10
Warranty
This Limited Warranty gives the Buyer specific legal rights, and a Buyer
may also have other rights that vary from state to state. For a period of 365
calendar days from the date of shipment, Valco Instruments Company, Inc.
(hereinafter Seller) warrants the goods to be free from defect in material
and workmanship to the original purchaser. During the warranty period,
Seller agrees to repair or replace defective and/or nonconforming goods or
parts without charge for material or labor, or, at the Sellers option, demand
return of the goods and tender repayment of the price. Buyers exclusive
remedy is repair or replacement of defective and nonconforming goods, or,
at Sellers option, the repayment of the price.
Seller excludes and disclaims any liability for lost profits, personal
injury, interruption of service, or for consequential incidental or
special damages arising out of, resuiting from, or relating in any
manner to these goods
This Limited Warranty does not cover defects, damage, or nonconformity
resulting from abuse, misuse, neglect, lack of reasonable care, modification,
or the attachment of improper devices to the goods. This Limited Warranty
does not cover expendable items. This warranty is VOID when repairs are
performed by a nonauthorized service center or representative. For infor-
mation about authorized service centers or representatives, write Customer
Repairs, Valco Instruments Company, Inc, P.O. Box 55603, Houston, Texas
77255, or phone (713) 688-9345. At Sellers option, repairs or replace-
ments will be made on site or at the factory. If repairs or replacements are
to be made at the factory, Buyer shall return the goods prepaid and bear all
the risks of loss until delivered to the factory. If Seller returns the goods,
they will be delivered prepaid and Seller will bear all risks of loss until
delivery to Buyer. Buyer and Seller agree that this Limited Warranty shall
be governed by and construed in accordance with the laws of the State of
Texas.
The warranties contained in this agreement are in lieu of all
other warranties expressed or implied, including the warranties
of merchantability and fitness for a particular purpose.
This Limited Warranty supercedes all prior proposals or representations oral
or written and constitutes the entire understanding regarding the warranties
made by Seller to Buyer. This Limited Warranty may not be expanded or
modified except in writing signed by the parties hereto.