High-Pressure Uid-Phase Equilibria: Experimental Methods and Systems Investigated (2000-2004)

Fluid Phase Equilibria 288 (2010) 154
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Fluid Phase Equilibria

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High-pressure uid-phase equilibria: Experimental methods and systems investigated (20002004)

Ralf Dohrn a, , Stephanie Peper b , Jos M.S. Fonseca c
a b c
Bayer Technology Services GmbH, Fluid Properties & Thermodynamics, Geb. B310, D 51368 Leverkusen, Germany Helmut-Schmidt-University/University of the Federal Armed Forces Hamburg, Institute of Thermodynamics, D 22043 Hamburg, Germany Technical University of Denmark, Department of Chemical and Biochemical Engineering, DK-2800 Kgs. Lyngby, Denmark
a r t i c l e
i n f o
a b s t r a c t
As a part of a series of reviews, a compilation of systems for which high-pressure phase-equilibrium data were published between 2000 and 2004 is given. Vaporliquid equilibria, liquidliquid equilibria, vaporliquidliquid equilibria, solidliquid equilibria, solidvapor equilibria, solidvaporliquid equilibria, critical points, the solubility of high-boiling substances in supercritical uids, the solubility of gases in liquids and the solubility (sorption) of volatile components in polymers are included. For the systems investigated, the reference, the temperature and pressure range of the data, and the experimental method used for the measurements are given in 54 tables. Most of experimental data in the literature have been given for binary systems. Of the 1204 binary systems, 681 (57%) have carbon dioxide as one of the components. Information on 156 pure components, 451 ternary systems of which 267 (62%) contain carbon dioxide, 150 multicomponent and complex systems, and 129 systems with hydrates is given. Experimental methods for the investigation of high-pressure phase equilibria are classied and described. Work on the continuation of the review series is under way, covering the period between 2005 and 2008, and will be published in 2010. 2009 Elsevier B.V. All rights reserved.
Article history: Received 26 June 2009 Received in revised form 12 August 2009 Accepted 13 August 2009 Available online 20 August 2009 Keywords: Experiment Data Method VLE high pressure Hydrocarbons Non-hydrocarbons
1. Introduction For the design and optimization of high-pressure chemical processes and separation operations, information on high-pressure phase equilibria and solubilities is essential. The simulation of petroleum reservoirs, enhanced oil recovery, carbon capture and storage, the transportation and storage of natural gas, refrigeration and heat-pump cycles, and the study of geological processes are other examples for the need of high-pressure phase-equilibrium data. The interest in old and new applications of supercritical uids [13], like extraction, particle formation, impregnation and dyeing, cleaning, reaction, chromatography, injection molding and extrusion, and electronic chip manufacturing, as well as the interest in ionic liquids and green solvents, led to a continuation of the increase in the number of publications concerning high-pressure phase-equilibrium data. There are many ways to obtain information about the phase behavior of uid mixtures, but the direct measurement of phaseequilibrium data remains an important source of information, though it is difcult and expensive to take precise experimental data. On the other hand, for a company, it is very often more expen-
Corresponding author. Fax: +49 214 30 81554. E-mail address: ralf.dohrn@bayertechnology.com (R. Dohrn). 0378-3812/$ see front matter 2009 Elsevier B.V. All rights reserved. doi:10.1016/j.uid.2009.08.008
sive to use imprecise data or to estimate data a couple of times over the years, if experimental data are not available. There are several review articles about techniques for experimental investigations [414]. Information about experimental equilibrium data is important, even when thermodynamic models are used to calculate the phase behavior of a mixture. Thermodynamic models can help to reduce the number of experimental data points needed for a special design problem, but very often, at least some experimental data points are needed to adjust interaction parameters of the model [15]. Reviews of high-pressure phase-equilibrium data in the literature have been published by several authors [8,10,13,14,1624]. Some reviews cover a specic topic, like the solubility of certain substances in supercritical carbon dioxide, e.g., Bartle et al. [14] for solids and liquids, Gcli-stndag and Temelli [19,23,24] for lipids, and Higashi et al. [21] for high-boiling compounds, or for a specic binary system, like Diamond and Akenev [22] on carbon dioxide + water. Other reviews cover high-pressure uid-phase-equilibria data that have been published in a specic periods, e.g., Knapp et al. [17] covering 19001980, Fornari et al. [8] covering 19781987, Dohrn and Brunner [10] covering 19881993, and Christov and Dohrn [13] covering 19941999. This work gives an overview about systems for which high-pressure phase-equilibrium data have been published from 2000 to 2004, including vaporliquid equilibria (VLE), liquidliquid equilibria
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154
(LLE), vaporliquidliquid equilibria (VLLE), the solubility of highboiling substances in supercritical uids, and the solubility of gases in liquids (GLE). Work on the continuation of the review series is under way, covering the period between 2005 and 2008, and will be published in 2010. 2. Literature search and evaluation This survey covers the most important journals in the eld of high-pressure phase equilibria, as listed in Table 1; abbreviation of journal titles were used according to ISO 4 [25]. To nd candidates for articles that are of interest for this review we used a three-stage search strategy. In Stage 1 we systematically searched the table of contents of all volumes that appeared between 2000 and 2004 of the journals of Table 1, checked in cases of doubt the abstracts and downloaded the article. Stage 1 yielded more than 95% of the articles of interest. In Stage 2 we used the online search function of the journals to search for certain keywords, like highpressure, phase equilibrium or gas solubility. Stage 3 was only started after the evaluation process of the articles of interest was almost nished. We identied important authors in the eld of high-pressure phase-equilibrium measurements and searched for other papers of these authors that might have been overlooked in Stages 1 and 2. During the evaluation process of more than 700 articles of interest, about 10% of the papers were found to be irrelevant for this review, since they contain neither new experimental data nor the description of a new experimental apparatus, or the measured data were not high pressure. Of course, the expression high pressure is relative; we chose 1 MPa as the lower limit: a paper was considered to contain high-pressure data if at least one data point was measured at a pressure of 1 MPa or higher. The increase of interest in high-pressure phase equilibria continues. Fig. 1 shows an almost linear increase of articles published per year during the last 25 years. While in the early 1980s about 20 articles on high-pressure phase equilibria were published each year, this number increases by 67 each year, so that in 2004 more than 7 times as many articles appeared as in 1982. In Table 1, the
Table 1 Bibliographic information. Journal Number of articles 19781987a J. Chem. Eng. Data Fluid Phase Equilibr. J. Supercrit. Fluidse Ind. Eng. Chem. Res. J. Chem. Thermodyn. Int. J. Thermophys. Phys. Chem. Chem. Phys.f AIChE J. J. Phys. Chem. B Chem. Eng. Sci. Can. J. Chem. Eng. Green Chemistryg J. Chem. Eng. Jpn. Other journals Total 92 69 0 15 10 5 3 2 3 0 199 19881993b 115 158 43 18 8 5 5 1 13 0 14 380 19941999c 214 182 73 30 30 6 1 1 4 8 0 4 16 569 20002004d 231 206 115 58 26 23 13 10 4 4 1 1 0 5 697
Fig. 1. Increase in the number of articles published per year during the last 25 years.
number of papers published in different journals from 1978 to 1987 [8] is compared with the number published from 1988 to 1993 [10], from 1994 to 1999 [13], and from 2000 to 2004 (this work). Authors tend to submit their publications on high-pressure phaseequilibrium data to a rather limited number of mostly specialized journals. More than 80% of the information was published in the three major journals of high-pressure phase equilibria: the Journal of Chemical Engineering Data, Fluid-Phase Equilibria, and The Journal of Supercritical Fluids. As compared to our previous reviews [10,13], we no longer cover Zeitschrift fr Physikalische Chemie since no relevant articles were found in this journal for the period between 2000 and 2004, and ELDATA (International Electronic Journal of PhysicoChemical Data), which had 13 relevant articles in the previous period (19941999), but ceased to appear in 1999. We included International Journal of Thermophysics as a new journal. And we also included Green Chemistry, which rst appeared in 1999 and shows rising coverage of high-pressure phase equilibria due to increasing interest in the solubility of volatile components in ionic liquids, particularly in the period of the coming review that will cover 2005 and 2008. 3. Experimental methods Particularly at high pressures, the measurement of phase equilibria is the most suitable method to determine the phase behavior, which often is far more complex than at ambient and moderate pressures. Due to large deviations from ideal behavior, the prediction of high-pressure phase equilibria is less accurate than at lower pressures. Another difculty of using predictive methods is the fact that molecules of interest for high-pressure applications, particularly supercritical uid extraction, can be large and contain several functional groups. Many different methods are used to measure high-pressure phase equilibria. The reason is that not a single method is suitable to determine all different phenomena. To the reader the variety of experimental methods is even more confusing since different authors use different names for the same experimental method. Expressions like static or dynamic are used in connection with many different methods. Therefore, an overview and a classication of experimental methods for the determination of high-pressure phase equilibria are given in this chapter. The classication includes a unique name and an abbreviation of the name for each method. In Tables 356, listing the investigated systems, information on the experimental method used to determine the data is included.
Abbreviation of journal titles according to ISO 4 [25]. (): not covered in the review of the period. a Fornari et al. [8]. b Dohrn and Brunner [10]. c Christov and Dohrn [13]. d This work. e The rst issue of The Journal of Supercritical Fluids appeared in 1988. f Before 1999: Berichte der Bunsengesellschaft fr Physikalische Chemie and J. Chem./Faraday Trans. g The rst issue of The Green Chemistry appeared in 1999.
Fig. 2. Classication of experimental methods for high-pressure phase equilibria.
The classication of experimental methods for the investigation of high-pressure phase equilibria that has been used in the previous reviews [10,13] has been further rened for this work (Fig. 2). There are two main classes, depending on how the compositions of the equilibrium phases are determined (analytically or not) and whether the mixture to be investigated has been prepared (synthesized) with precisely known composition or not: analytical methods and synthetic methods.
3.1. Analytical methods (An) Analytical methods (designated with An) involve the analytical determination of the compositions of the coexisting phases. When the equilibrium cell is lled with the components at the beginning of the experiment, the overall composition of the mixture is not precisely known, only so far that the mixture under desired conditions (P and T) separates into two or more phases that are to be investigated, e.g., into a liquid and a vapor phase when VLE is to be measured. The composition of the phases is analyzed either with sampling and analysis under ambient pressure or without sampling by using physicochemical methods of analysis inside the equilibrium cell under pressure. Analytical methods with sampling can be classied, depending on the attainment of equilibrium, into isothermal methods (AnT), isobaricisothermal methods (AnPT) and isobaric methods (AnP). Withdrawing a large sample from an autoclave causes a considerable pressure drop, which disturbs the phase equilibrium signicantly. This pressure drop can be avoided by a variablevolume cell (Var) [26], by using a buffer autoclave in combination with a syringe pump [27], or by blocking off (Blo) the sampling volume from the remaining content of the equilibrium cell before pressure reduction [2830]. Sane et al. [31] use an electronic syringe pump to keep the pressure in a variable-volume cell constant during sampling. If only a small sample is withdrawn or if a relatively large equilibrium cell is used, the slight pressure drop does not affect the phase compositions signicantly. The largest equilibrium cell (volume of 9 dm3 ) used in the articles of this review was used by the late Danesh and co-workers [32] to measure phase equilibria in gas condensate systems.
Small samples can be withdrawn using capillaries (Cap) [33] or special sampling valves (Val), e.g., using HPLC-valves [34] or fastacting pneumatic valves, like the rapid on-line sampler-injector of Richon [35]. Often sampling valves are directly coupled to analytical equipment, e.g., to a gas chromatograph [36], a high-performance liquid chromatograph [37], or a supercritical uid chromatograph [34]. For sampling from multiphase systems (e.g., VLLE) a movable sampling needle [38] can be used. The smallest equilibrium cell of all articles from this review using an analytical method with sampling was used by Bahramifar et al. [39]: only 0.5 cm3 volume with a sampling loop of 23 mm3 . The largest relative sample (14%) from a constant volume cell was taken by Garmroodi et al. [40]: a 143 mm3 sample from a 1 cm3 equilibrium cell. Sometimes, equilibrium cells used for analytical methods are equipped with one or more windows for visual observation of the cell content (Vis). Secuianu et al. [41] use a variable-volume cell with two sapphire windows where one of the windows acts as a piston. Analytical methods without sampling use a physicochemical method of analysis inside the equilibrium cell under pressure. These are mainly spectroscopic methods (AnSpec), e.g., Andersen et al. [42], gravimetric methods (AnGrav), e.g., Sato et al. [43], or other methods (AnOth), e.g., Boudouris et al. [44]. These methods avoid the problems related to sampling from a high-pressure cell. The main advantage of analytical methods is that they can be used for systems with more than 2 components without signicant complications. When the compositions of all phases are analyzed, each experiment yields complete information on the tie-line(s). 3.1.1. Analytical isothermal methods (AnT) Characteristic for isothermal methods is that the temperature of the system stays constant during the equilibration process, e.g., when the system is in contact with a heat reservoir. The other equilibrium properties, like the pressure and the composition of the phases, reach equilibrium values, depending on other variables, like mole numbers and volume. At the beginning of an experiment, an equilibrium cell is charged with the substances of interest. The pressure is adjusted above or below the desired equilibrium value, depending on how equilibration will change the pressure. After
the desired temperature has been reached, the mixture is kept at a constant temperature. By stirring the mixture or by rocking the autoclave or by recirculating one or more phases, time for equilibration of the phases is reduced. After some time, the pressure reaches a plateau. The pressure can be readjusted, by adding or withdrawing material or by changing the volume of the equilibrium cell. Usually, the equilibration is continued for at least 30 min after the pressure plateau is sufciently close to the desired value. Before taking samples from the coexisting phases, the mixture is given sufcient time without stirring, rocking or recirculation for the separation of the phases [41]. Otherwise the sample might not be homogeneous but contain material from another phase, e.g., droplets, bubbles or solid particles. For the measurement of solidliquid equilibria in wax systems, Pauly et al. [45] used an isobaric and isothermal ltration step to ensure that the liquid phase to be sampled is free of solid particles. This was performed in an equilibrium cell with two variable-volume chambers connected via a ltration system (a disc of sintered steel with 3 m of porosity). Isothermal methods that use stirring or rocking to ensure a rapid approach to equilibrium are often called analytical-static methods. As opposed to recirculating methods, the mixture does not leave the equilibrium cell during the experiment. But, since the expressions static cell and static method are used by some authors for other experimental methods (e.g., for a synthetic method in a view cell or for a synthetic method using the material balance to determine solubilities of gases in liquids), we avoid the expression static in our classication. Sampling through capillaries can lead to differential vaporization and scattering results, especially for mixtures containing light and heavy components when no precautions have been taken to prevent a pressure drop all along the capillary [46]. Differential vaporization can be avoided with an experimental design that ensures that most of the pressure drop occurs at the end of the capillary close to the chromatographic circuit, e.g., Richon and coworkers [47] used a micro-stem ending with a nose entering inside the capillary to reduce the cross-sectional area at the end of the capillary. Another possibility to reduce sampling problems is the recirculation of one or more phases, having the advantage that the sampling volume (e.g., the loop of a six-port valve) is lled isobarically. Disadvantages of a recirculation are the need for a wellworking pump with only little pressure drop and the need for a uniform temperature eld to avoid partial condensation or vaporization in the recirculation line. Therefore, recirculation methods are not suitable in the region close to the critical point where small changes in temperature and pressure have a strong inuence on the phase behavior [11]. When only the vapor phase is recirculated (Vcir), it is withdrawn continually and passed back into the equilibrium cell through the liquid phase by the action of a pump, e.g., Mather and co-worker [48]. Samples can be withdrawn by placing a sampling valve in the recirculation loop [37] or by blocking off a volume between two valves in the recirculation loop [49]. The liquid phase is usually analyzed by taking samples through capillaries. Laursen et al. [50] proposed a simple VLE equipment with vapor-phase recirculation that allows liquid phase sampling to measure the gas solubility in substances with high stickiness and viscosity, like wood resins. Recirculation of both the vapor and the liquid phase (VLcir) has the advantage that sampling from both phases is possible without using capillaries [51,52]. If a vibrating-tube densimeter is installed in a recirculation loop, the density of the circulated phase can be determined easily. The pump should be turned off during density measurement to avoid errors due to pulsation [52]. Sometimes only the liquid phase is circulated (Lcir), e.g., for mixing, for blocking off a large liquid phase volume from the equilibrium cell before pressure reduction [53], for the measurement of liquidliquid equi-
libria or for the measurement of solubilities of gases in liquids [54]. In a special kind of blocking off a part of the equilibrium cell the sampling volume is within the equilibrium cell. We call this method in situ sampling (AnTIns). It can be used for the measurement of the solubility of solids in supercritical uids. Sherman et al. [55] put an excess amount of solute in a glass vial, capped with coarse lter paper, in the equilibrium cell. After equilibration and careful depressurization, the vial is removed and weighed. The solubility can be calculated from the difference of the initial and nal mass of the solute in the vial and the difference of the volume of the equilibrium cell and the vial. As modication, Galia et al. [56] used three vials, of which only one was initially lled with the solute. Nikitin et al. [57,58] used an alternative technique which avoids sampling from a high-pressure cell, for sorption measurements of carbon dioxide in polystyrene. Equilibration, the absorption of volatile component in the polymer, might take several hours. Then, a fast depressurization procedure (<10 s) followed by a quick transport of the sample to an analytical balance (<5 s) is performed. The mass decrease of the polymer sample due to desorption of carbon dioxide is recorded and analyzed. The initial value of sorbate mass can be determined by extrapolation of the desorption curve to the beginning of depressurization. We designate this sampling and analytical method with material loss analysis (AnTMla). As compared to analytical isobaricisothermal methods, isothermal methods have the advantage that time for equilibration can be easily extended. If carried out carefully they can produce very reliable results. 27.6% of all systems investigated of this review have been measured with an analytical isothermal method. 3.1.2. Analytical isobaricisothermal methods (AnPT) In isobaricisothermal methods, often called dynamic methods, one or more uid streams are pumped continuously into a thermostated equilibrium cell. The pressure is kept constant during the experiment by controlling an efuent stream, usually of the vapor phase. 3.1.2.1. Continuous-ow methods (AnPTCon). In a typical design of a continuous-ow method, high-pressure metering pumps feed the preheated components into a mixer, where the desired temperature and phase equilibrium is attained. Often, static mixers are used [59,60]. The feed stream from the mixer is separated in an equilibrium cell into a vapor and a liquid phase. To facilitate phase separation, a cyclone separator was used by Fonseca et al. [59]. Efuents from both phases are withdrawn continually, depressurized, accumulated and analyzed, usually after the experiment. The pressure is adjusted by controlling the efuent stream of the top phase. The interface level between the uid phases in the equilibrium cell can be adjusted with the bottom-phase expansion valve, whereby the interface level is usually determined visually [61]. Continuous-ow methods have the advantage that sampling does not disturb the equilibrium. If larger samples are needed for analyses, the run time of the experiment can be extended to accumulate more material. Measurements at higher temperatures are possible without thermal decomposition or polymerization reactions due to the short residence time of the components in the apparatus [62]. Using a continuous-ow method, Haruki et al. [63] measured phase equilibria for water + hydrocarbon systems near the critical point of water. Hurst et al. [64] describe a continuous-ow cell with large diameter optical ports suitable for visual observation and Raman spectroscopic studies of aqueous solutions at temperatures up to 500 C. The cell was instrumented with a heated cylindrical insert (hot nger) that was employed for salt solubility, salt deposition
and salt nucleation studies in near-critical aqueous solutions. The crystalline phases were observed using Raman spectroscopy. Continuous-ow methods can be used only for systems where the time needed to attain phase equilibrium is sufciently short. 3.1.2.2. Semi-ow methods (AnPTSem). In semi-ow methods, only one phase is owing while the other phase stays in an equilibrium cell. Semi-ow methods are sometimes called single-pass ow methods, gas-saturation methods or pure-gas circulation methods. A gas stream from a high-pressure cylinder is passed through two cells in series containing the liquid. The rst cell serves as a presaturator and the second cell as equilibrium cell. Upon equilibration, the efuent of the vapor phase is reduced in pressure and directed to a trap where the condensed liquid is collected. The quantity of the gas coming out of the trap can be determined volumetrically, e.g., with a wet test meter. Most often, only the composition of the vapor phase is analyzed (AnPTSemY), for example to determine the solubility of a low-boiling (liquid or solid) substance in a supercritical gas [65]. The composition of the vapor-phase efuent can be determined in many different ways, e.g., by using a spectroscopic method [66], by using a multi-port sampling valve and subsequent HPLC analysis or after expansion to atmospheric pressure using cold traps, an absorption bath, or a chromatography column lled with an appropriate adsorbent for the solute studied [67]. For these kinds of measurements (AnPTSemY), no samples from the condensed phase are taken. When a semi-ow method is used for the measurement of vaporliquid equilibria AnPTSemXY, the composition of the liquid phase needs to be determined. Therefore, a sample from the liquid phase is withdrawn through tubing, depressurized, and analyzed [68]. Semi-ow methods can also be used to measure the solubility of a gas in a liquid, e.g., Tan et al. [69]. The experimental procedure (AnPTSemX) is similar to the one for measuring vaporliquid equilibria, but there is no need to determine the composition of the efuent from the vapor phase. Tuma et al. [70] used a modied supercritical uid chromatograph (SFC) to measure the solubility of dyes in carbon dioxide. The column was lled with nely pulverized dyestuff. Analysis of the vapor-phase stream is done by VIS-spectroscopy (AnPTSemYSpec). The major uncertainty of all ow methods is the possible lack of attainment of equilibrium. Sauceau et al. [71] used an equilibrium cell with three compartments, which is equivalent to three cells in series. Another difculty is the partial condensation of the solute from the saturated vapor stream in the tubing, particularly in and after the expansion valve. This undesired variable hold-up of the solute can lead to scattering results in the order of 10% [72]. To collect precipitated solute at the end of an experiment from the tubing and from the expansion valve, Takeshita and Sato [73] use a stream of carbon dioxide after having blocked off the equilibrium cell. Ferri et al. [74] describe an experimental technique that allows to measure high concentrations of dyestuff in a supercritical uid. They use a second pump to stabilize the ow rate of the uid in the extractor, damping the pulses of the rst pump. Glass wool before and after the packed bed guarantees a uniform ow distribution and prevents particle entrainment. A line by-passing the extractor allows solubility measurements at high concentrations. It dilutes the saturated uid stream with clean carbon dioxide and reduces the risk of valve clogging and ow rate instability. To overcome the problems connected to depressurization, Pauchon et al. [75] developed a semi-ow method that works without pressure reduction. The efuent vapor-phase ows into the top part of an autoclave which is lled with mercury. The use of mercury, acting as a piston, allows obtaining a precise adjustment of the vapor ow and avoids pressure changes that
produce solute precipitation. Sampling at isobaric conditions is performed with a six-port valve. Special attention must be taken into account during the regeneration of mercury and cleaning of the apparatus. 3.1.2.3. Chromatographic methods (AnPTChro). Chromatographic methods measure solute retention in a chromatographic column and connect it with the Gibbs energy of solute transfer between the stationary and the mobile phase. Roth [76] gives a review on applications of SFC for the determination of the relative values of solute solubilities in supercritical uids, and on the determination of solute partition coefcients between a supercritical uid and the stationary phase. In SFC, the thermodynamic analysis of solute retention is more difcult than in GC because the uptake of the mobile phase uid by the stationary phase is no longer negligible. Chromatographic methods have as advantage the possibility to determine equilibrium properties and diffusion coefcients in one experiment [77]. Sato et al. [78] used a chromatographic method (AnPTChro) to measure the vaporliquid equilibrium ratio of n-hexane at innite dilution in propylene + impact polypropylene copolymer, while to determine the solubility of propylene in the polymer they used the synthetic isothermal method (SynT). Chester [79] reviewed a chromatographic technique, which he calls ow injection peak-shape method that allows to determine the pT coordinates of the vaporliquid critical locus of binary systems. It can be implemented using open-tubular SFC instrumentation by replacing the SFC column with several meters of fused-silica tube. This tube may be deactivated but is not coated with a stationary phase. The procedure to map a critical locus involves selecting a temperature, then making injections at various pressures while looking for the pressure where the peaks change from their rectangular appearance ( = liquid + vapor phase in the column) to distorted Gaussian (= homogeneous phase in the column). This transition pressure provides an estimate of the mixture critical pressure corresponding to the oven temperature. 3.1.3. Analytical isobaric methods (AnP) The boiling temperature of a mixture is measured at isobaric conditions and phase compositions are determined after sampling and analysis. Typically, isobaric experiments are performed in an ebulliometer (from latin ebullio to boil, to bubble up), which is a one-stage total-reux boiler equipped with a vapor-lift pump to spray slugs of equilibrated liquid and vapor onto a thermometer well. As opposed to the more frequently used synthetic isobaric method (SynP), vapor and liquid streams are separated, collected and can be sampled and analyzed. The compositions of the liquid and the vapor phase change with time and reach a steady state which should differ insignicantly from the true equilibrium value. Usually, the analytical isobaric method is used to measure lowpressure data. Then, it is often called the dynamic VLE method. 3.1.4. Analytical spectroscopic methods (AnSpec) Spectroscopic methods allow analyzing the composition of the phases at high pressures without having to take samples, e.g., by using near infrared spectroscopy [42]. Cruz Francisco et al. [80] investigated the phase behavior of lecithin + water + hydrocarbon + carbon dioxide mixtures using a 2 H NMR technique in combination with light microscopy. Aizawa et al. [81] developed a high-pressure optical cell for the investigation of absorption and uorescence phenomena using a totsu (denoting the shape) type window. The protruding part of the window acts as a light-guide and enhances the laser power imparted onto the sample in the monitoring light. Shieh et al. [82] studied the effect of carbon dioxide on the morphological structure of compatible crystalline/amorphous polymer
blends by means of small angle X-ray scattering (SAXS) with the measurement of absolute scattering intensity. The advantage of avoiding the trouble with taking samples is often overcompensated by the need of time consuming calibrations at high pressures. Only 1.5% of all systems covered in this review have been investigated with a spectroscopic method. 3.1.5. Analytical gravimetric methods (AnGrav) With gravimetric methods the mass of a condensed phase (e.g., a polymer [43] or an ionic liquid [83]) in phase equilibrium with a uid phase is measured. Using additional information, like the phase densities, the phase compositions can be determined. Palamara et al. [84] placed the entire high-pressure cell on a balance and performed the equilibration under isobaric conditions. The weight of the cell and attached valve is critical because commercially available analytical balances sensitive enough to perform these measurements have low maximum load capacities. In the study of Palamara et al. [84] the cell and attached valve weighed approximately 190 g. Cutugno et al. [85] placed a quartz spring balance and Moore and Wanke [86] placed an electro microbalance within a highpressure cell to measure sorption of gases in polymers. Kleinrahm and Wagner [87] developed a unique balance, so-called a magnetic suspension balance, for accurate measurements of uid densities. It has the main advantage that the sample and the balance are isolated. An electronically controlled magnetic suspension coupling is used to transmit the measured force from the sample enclosed in a pressure vessel to a microbalance. The suspension magnet, which is used for transmitting the force, consists of a permanent magnet, a sensor core and a device for decoupling the measuring-load. An electromagnet, which is attached at the underoor weighing hook of a balance, maintains the freely suspended state of the suspension magnet via an electronic control unit. Using this magnetic suspension coupling, the measuring force is transmitted contactlessly from the measuring chamber to the microbalance, which is located outside the chamber under ambient atmospheric conditions. Several investigators used a magnetic suspension balance to measure the solubility and diffusivity of volatile components in polymers, e.g., Sato et al. [88]. Gravimetric methods need corrections for buoyancy. Therefore, particularly at high pressures, exact information on the density of the uid phase and on the density and volume of the condensed phase is essential. 3.1.6. Other analytical methods (AnOth) Like in gravimetric methods, quartz crystal microbalances can be used to determine the solubility of a gas in a polymer by measuring the mass of the polymer in equilibrium with the gas. From the basic principle, it is not a gravimetric measurement, so that buoyancy effects play a different role. Quartz crystal microbalances are based on the piezoelectric effect observed in a AT-cut quartz crystal. The crystal under the inuence of an applied alternating electric voltage undergoes a shear deformation which becomes maximum at a certain frequency called the resonance frequency [44]. This resonance frequency depends on the mass, and thus any mass change will result in a respective frequency shift. The sorption experiment involves measurement of the resonance frequency of the bare (clean) crystal, of the same crystal coated with polymer, and of the coated crystal after the polymer reaches equilibrium with a gas, all at the same controlled temperature. Concurrently, the resonance frequency of a reference crystal is also measured under the same conditions in order to compensate any temperature or pressure effects. Park et al. [89] examined the effect of temperature deviation and pressure change on the frequency shift by measuring the frequency change of an uncoated crystal under high-pressure carbon dioxide.
Guigard et al. [90] further developed the quartz crystal technique to measure low solubilities of metal chelates in supercritical uids. A small mass of solute was deposited on the crystal and solubility was measured by observing the crystals frequency change as this solute dissolves in the supercritical uid. Mohammadi et al. [91] used a quartz crystal balance as an extremely sensitive detector for the appearance of hydrates. 1 ng mass change results in a 1 Hz frequency change. Concerning the classication of methods this is not an analytical method (AnOth), but a non-visual synthetic method (SynNon). As compared to conventional methods, such as gravimetric (AnGrav) or pressure decay (SynT), a much higher sensitivity for the determination of mass changes can be achieved with a quartz microbalance. Therefore, smaller samples are needed and phase equilibrium is attained much faster [92], since equilibration time is inversely proportional to the square of the lm thickness. Errors rise with temperature and pressure, due to dampening and viscous dissipation [89]. Another analytical method was used by Morris et al. [93] to measure low gas solubilities, e.g., of hydrogen in water. A palladium/hydrogen electrical resistance sensor was used to determine the hydrogen content in the liquid phase. Abbott et al. [94] proposed a capacitative method (dielectric constant method) to measure the solubility of low-volatile substances in supercritical gases. They used a 25 cm3 high-pressure cell, lined with a layer of Teon. A capacitor consisting of two parallel rectangular stainless steel plates (area of 6.6 cm2 , held 1 mm apart by Teon spacers) was placed in the vapor phase. The dielectric constant of the saturated vapor phase was measured at different pressures. To calculate the concentration of the solute in the vapor phase from the dielectric constant, information on the permanent dipole moments and the molecular polarizabilites of the components of the mixture needs to be known. 3.2. Synthetic methods (Syn) The idea of synthetic methods is to prepare a mixture of precisely known composition and then observe the phase behavior in an equilibrium cell and measure properties in the equilibrium state, like pressure and temperature. No sampling is necessary. The problem of analyzing uid mixtures is replaced by the problem of synthesizing them [7]. Synthetic methods can be applied with or without a phase transition. In both cases, rst a mixture of precisely known composition is prepared. In synthetic methods with a phase transition values of temperature and pressure are adjusted so that the mixture is homogeneous, a single phase exists. Then the temperature or pressure is varied until the beginning of the formation of a new, a second phase is observed. The composition of the rst, large phase can be set to the known overall composition. The composition of the second, small phase is not known. Each experiment yields one point of the pTx phase envelope. Instead of a variation of temperature or pressure to cause a phase transition the overall concentration can be changed. Wubbolts et al. [95] use this approach, designated with vanishing-point method or clear-point method, for SLE measurements. A clear solution of a given solute concentration is added to a known amount of antisolvent until the last crystal disappears. The composition of the mixture at this vanishing point equals the solubility of the mixture. When the procedure is repeated with a solution of a different concentration another point of the curve is found. Depending on how the phase transition is detected, synthetic methods with a phase transitions can be divided into visual (SynVis) and non-visual synthetic methods (SynNon). In synthetic methods without a phase transition, equilibrium properties like pressure, temperature, phase volumes and densi-
ties are measured and phase compositions are calculated using the material balance. Synthetic methods without a phase transition can be divided into isothermal (SynT), isobaric (SynP) and other (SynOth) synthetic methods. During the period covered in this review (20002004) synthetic methods with a phase transition have been used about 5 times more often than synthetic methods without a phase transition. Synthetic methods can be used where analytical methods fail, i.e., when phase separation is difcult due to similar densities of the coexisting phases, e.g., near or even at critical points and in barotropic systems, where at certain conditions the coexisting phases have the same density. Often, the experimental procedure is easy and quick [5]. Because no sampling is necessary the experimental equipment can concentrate on few components and the volume of the equilibrium cell can be small. Therefore, the apparatus can be rather inexpensive. On the other hand, it can be designed for extreme conditions concerning temperatures and pressures [96]. Cohen-Adad [97] describes a diamond anvil cell that can be used for pressures up to 135 GPa. The experimental data at the highest pressures of all articles covered in this review were taken by Fang et al. [98], also with a diamond anvil cell, at pressures up to 2.6 GPa. For multicomponent systems, experiments with synthetic methods yield less information than with analytical methods, because the tie-lines cannot be determined without additional experiments. Therefore, synthetic methods are less often used for systems containing more than 2 components. 3.2.1. Visual synthetic methods (SynVis) The appearance of a new phase is usually detected by visual observation of the resulting turbidity or meniscus in a view cell. For isooptic systems where the coexisting phases have approximately the same refractive index, visual observation is impossible. The visual synthetic method can be used not only for the determination of simple vaporliquid equilibria, but also to study complicated phase behavior, e.g., multiphase equilibria [99], solidliquid equilibria [100], critical curves of mixtures [101], gas hydrate formation [102], cloud-point determination [103] and phase equilibria in polymersolvent systems [104]. The Cailletet apparatus of TU Delft [105] is the most frequently used type of apparatus according to the synthetic visual method. It consists of a thick-walled Pyrex glass tube (50 cm long, 3 mm inner diameter) with the open end placed in an autoclave and immersed in mercury. The mercury connes the sample in the Cailletet tube. A stainless steel ball driven by reciprocating magnets stirs the sample. Daridon et al. [106] used a very small cell with a volume of 0.03 cm3 for the visual observation of synthetic waxes at high pressures. The cell is placed within a polarizing microscope. The apparatus allows the visual observation of crystals of 2 m. When only small quantities of a sample shall be used in the experiment, e.g., to observe solidliquidgas equilibria, a glass capillary can be placed inside the high-pressure view cell [107,108]. To improve the detection of phase transitions, some authors use laser light scattering techniques [103,109]. Jager and Sloan [110] use Raman spectroscopy to detect hydrates. Dong et al. [111] use additional SAXS measurements to determine the median micelle size of the water-in-carbon dioxide microemulsions. Veiga et al. [112] used glass capillary helixes not only to investigate the high pressure behavior of pure compounds but also at negative pressures as far down as 20.8 MPa. With 36.4% of all systems investigated in this review, synthetic visual methods were the most frequently used type of method. 3.2.2. Non-visual synthetic methods (SynNon) As an alternative to visual observation, other physical properties can be monitored to detect phase transitions. Minicucci et al. [113] made use of transmitted X-rays instead of visible light, as
the basis of phase detection, while Drozd-Rzoska et al. [114] used measurements of the relative dielectric permittivity for LLE measurements at high, low and negative pressures. If the total volume of a variable-volume cell can be measured accurately, the appearance of a new phase can be obtained from the abrupt change in slope on the pressurevolume plot more accurately than by visual observation [115,116]. As an alternative pVT measurements can be performed and the intersection of isochors can be used to determine points on the coexistence curve. A sharp change in the slope (dp/dT), occurs at the phase boundary. May et al. [117] used a microwave re-entrant resonator to detect the appearance of dew and bubble points in hydrocarbon systems. Takagi et al. [118] measured bubble point pressures using an ultrasonic speed apparatus. Since the acoustic wave excited in the sample for the speed of sound measurement was strongly absorbed in the gas phase as compared to the absorption in the liquid phase, the appearance of the gas phase was detected by the change of the acoustic echo signal. For searching critical points of pure uids, acoustic methods have the advantage that even for temperatures several degrees above the critical point, the sound velocity exhibits a minimum when measured isothermally as a function of pressure [119]. To measure the critical temperature of thermally unstable substance, the pulse-heating method, as described by Nikitin et al. [120], can be used. It is based on measuring the pressure dependence of the temperature of the attainable superheat (spontaneous boiling-up) of a liquid with the help of a thin wire probe heated by pulses of electric current. When the pressure in the liquid approaches the critical pressure, the temperature of the attainable superheat approaches the critical temperature. A synthetic non-visual method that looks at rst sight like an analytical continuous-ow method (AnPTCon) was used by VonNiederhausern et al. [121] to determine the critical points of thermally unstable or reactive components. To achieve very short residence times, a sample of precisely known composition is continuously displaced and heated in a capillary tube. No analysis of the samples takes place. To determine the critical point, several temperature scans must be made in the vicinity of the critical point. Below the critical point, the temperature scan will show a at, horizontal region indicative of isothermal boiling. Above the critical point, the transition region is no longer at and horizontal. The critical point is inferred by the temperature and pressure where isothermal boiling is no longer observed. Valyashko et al. [122] used jumps of the isochoric heat capacity to detect the appearance of a vapor phase or a second liquid phase. Wuringer and Urban [123] studied the phase behavior of liquid crystals with high-pressure differential thermal analysis (DTA). The experiments at the highest temperatures of all articles covered in this review were performed by Manara et al. [96]. They investigated the melting point of uranium dioxide at high pressures. Temperatures of almost 3200 K were needed. Such high temperatures can be measured optically by pyrometry. Two pulsed NdYAG laser beams were mixed through a suitable optical system in the same ber and then focused onto the sample surface. The pulse with the higher power peak was used to heat the sample above the melting point; the other one, less powerful, but of longer duration, was used to control the cooling rate on the sample surface. This lead to a much better denition of the freezing plateau. Pressure was applied by using helium. Diamond anvil cells are particularly suitable for non-visual measurements at very high pressures [97]. The selective transparency of diamond for IR to X-ray and gamma-ray radiations permits in situ measurements during experiments. Ngo et al. [124] used the synthetic non-visual method to measure the solubility of solids in carbon dioxide. First the cell was charged with the solid. Then it was pressurized with carbon diox-
ide and stirred constantly. Equilibrium of the mixture was observed in situ by periodically taking spectra (UV absorbance) of the solution. The pressure was raised stepwise until no further signicant increase in the peak absorbance was observed. This meant that all solids had been dissolved in the uid phase. Randzio [125] used a new transitiometric method for investigation of the solid phase behavior in asymmetric binary systems. Transitiometry is based on a simultaneous recording of both mechanical and thermal variables of a thermodynamic transition induced by scanning one independent variable (p, T or V) while the other independent variable is being kept constant. Taking the (tetracosane + methane) binary system as a test example, the three-phase curve (solid + liquid + vapor) has been determined. The apparatus (transitiometer) consists of a calorimeter equipped with high-pressure vessels, and a pVT system. During the isobaric temperature scans both the heat ux and the volume variations were recorded. For measurements of solidliquid equilibria at high pressures, the dead-volume of the apparatus can have a very negative inuence [97]. The volatility of constituents changes the nominal composition of a sample and can induce an incorrect apparent retrograde solubility curve. To investigate the phase behavior in porous media, non-visual methods are particularly advantageous. Zatsepina and Buffett [126] used electrical resistance measurements to monitor the appearance and growth of CO2 hydrate crystals in the pore uid. Omi et al. [127] used a high-pressure NMR probe to investigate the pressure and pore size dependence of the critical behavior of xenon in mesopores. Ivanic et al. [128] monitored the pressure and temperature in a hydrate-bearing system and identied equilibrium at the conditions where the last hydrate crystal in the system dissociates at the cross-point of the pT curves from cooling and from heating. Oag et al. [119] describe an apparatus where the determination of phase transitions and critical points can be carried out with different methods: visually, by measuring the laser reectance of the uid, which is at its maximum at the critical point, the sound velocity and by using vibrating shear mode sensors. 3.2.3. Synthetic isothermal methods (SynT) Synthetic isothermal methods are performed without a phase transition, where the pressure of a synthesized multiphase mixture is measured at isothermal conditions and phase compositions are calculated using the material balance. At the beginning of an experiment, an equilibrium cell is charged with a known amount of the rst component, evacuated and thermostated to a given temperature. Then a known amount of the second component is added whereby the pressure increases. The second component dissolves into the liquid phase, which leads to a decay of the pressure in the equilibrium cell. Therefore, this method is also called pressure-decay method, especially when a polymer is used as the rst component. After equilibration pressure and temperature are registered. No samples are taken. The composition of the vapor phase is calculated using a phase equilibrium model or assumed as just containing the pure gas, if we consider solubility in polymers for example, or other compounds with negligible volatility. The composition of the liquid phase is calculated using the material balance from the known total composition, the composition of the vapor phase and the phase densities and volumes [129]. By repeating the addition of the second component into the cell, several points along the boiling point line can be measured. At lower pressures, were they are often designated as static method or isothermal pTx method, synthetic isothermal methods are very commonly used [130,131]. Examples for the use of the synthetic isothermal methods at high pressures are the determination of the solubility of low-boiling substances in polymers
[132] or the solubility of gases in ionic liquids [133] or in electrolyte solutions, e.g., by Gmehling and co-workers [134]. When used for a pure component, the synthetic isothermal method delivers the vapor pressure, e.g., Funke et al. [135]. Then, it is often called the static vapor-pressure method. Often in synthetic isothermal methods, a view cell is used as equilibrium cell. This has the advantages that unusual behavior, like foaming, can be seen, that the volumes of the liquid and the vapor phase can be determined visually and that the cell can be used also according to the synthetic visual method. For example, FuknKokot et al. [107] measured solidliquidgas equilibria using the synthetic isothermal method to determine the CO2 content in the liquid phase and the synthetic visual method to detect solid formation. Krger et al. [136] compared results of the isothermal method for VLE of the n-pentane + poly(dimethylsiloxane) system with results of the gravimetric sorption method (AnGrav) and with inverse gas chromatography. These methods differ in the underlying experimental principles as well as in the complexity of data analysis. Despite of these differences, the agreement of the measured VLE data is excellent. 3.2.4. Synthetic isobaric methods (SynP) The boiling temperature of a synthesized mixture is measured at isobaric conditions and phase compositions are calculated using the material balance. As opposed to analytical isobaric methods (AnP), no sampling or analysis is performed. Just as synthetic isothermal methods (SynT), synthetic isobaric methods (SynP) are performed without a phase transition. When used for a pure component the composition is given anyway the synthetic isobaric method delivers the vapor pressure, e.g., Weber et al. [137]. Then, it is often called the dynamic vapor-pressure method. Typically, isobaric experiments are performed in an ebulliometer as described in Section 3.1.3 (AnP). An ebulliometer was rst used to determine the molecular weights of substances, by measuring the changes of the boiling point of water caused by the presence of the unknown substance. Twin ebulliometry can be used to determine the activity coefcient at innite dilution. The temperature difference between an ebulliometer lled with the rst (pure) component and a second ebulliometer (under the same pressure) lled with the rst component and with a small amount of a second component (diluted solution) is measured. From the difference of the boiling temperatures, the activity coefcient at innite dilution can be calculated. Usually synthetic isobaric methods are used to measure low-pressure data. Ewing and Ochoa [138] used comparative ebulliometry to precisely determine the vapor pressure of pure components at high pressures. The sample and a reference uid are boiled in separate ebulliometers under a common pressure of gas such as helium or nitrogen, and the condensation temperatures of the sample and of the reference uid are measured. The common pressure is calculated from the known vapor pressure of the reference uid. The method has many advantages: direct measurement of pressure is avoided, the uids are degassed by boiling, and the ebulliometers act as heat pipes to provide high-performance thermostats. The corresponding disadvantages are the considerable demands on thermometry, the solubility of the buffer gas at high pressures, and thermal gradients due to pressure heads. But the greatest advantage is speed of measurement; typically, a pressuretemperature point can be obtained in an hour. 3.2.5. Other synthetic methods (SynOth) Properties measured in the homogenous or heterogeneous region are used to calculate the phase boundaries. Abdulagatov et al. [139] used two-phase isochoric heat capacity measurements to determine the values of the critical pressure and
slope of the vapor-pressure curve at the critical point of 18 pure components. For systems with two degrees of freedom (e.g., binary two-phase equilibria or ternary three-phase equilibria), the compositions are xed when temperature and pressure are given. Luks and co-worker [140] took phase volume and overall composition raw data for a set of three experimental runs at the same temperature and pressure; in each run a different phase is caused to be volumetrically dominant relative to the other two phases. With the use of mass balance, the compositions and molar volumes of the three phases were determined from the three conjugate measurements [141]. Di Nicola et al. [142] used isochoric pvTx measurements in the single phase region (remark: otherwise it would be SynT) to t the binary interaction parameters of an equation of state. Then, the compositions of the coexisting phases are calculated using the equation of state model.
4. Systems investigated Almost 700 articles with experimental data on high-pressure phase equilibria were found [143745]. More than 2000 systems have been investigated, from pure components, binary systems up to complex mixtures with many components. In Tables 356, the following information about the systems investigated is given: the reference, the temperature and pressure range of the data and the experimental method used for the measurements. The abbreviations used to designate the experimental method have been explained in the text above or are explained in Table 2.
Table 2 Experimental methods: abbreviations and frequency of use in review period. 46.7%
Because the size of the equilibrium cell can be of importance, e.g., for the pressure drop during sampling or for the amount of substances needed, the volume of the equilibrium cell is also given in the tables. Information on pure-component systems is given in Table 3. Most of experimental phase equilibrium data were on binary systems: 1204 systems investigated have been divided into 28 tables (Tables 431), with Table 4 (carbon dioxide + X) containing 681 binary system being by far the largest one. Many data have been measured for binary systems containing water, propane, diuoromethane (HFC-32), and methane. Information on the tables and their order can be found in the list of tables. The additional components X are listed in alphabetic sequence. The results of 434 ternary systems are given in 17 tables (Tables 3248), e.g., 76 ternary systems of the type CO2 + water + X. The order of the tables is analog to the order of the binary systems. Information on 134 multicomponent systems (410 components) is listed in Tables 4952. Results for complex systems with many components, like gas condensate reservoirs, are listed in Table 53. Special tables have been generated for systems containing hydrates (Tables 5456). Overall, 129 systems with hydrates were found. To provide the reader with information on articles with corrections and discussions on published experimental high-pressure data, we prepared a compilation (Table 57). We give the original article and the articles with corrigenda, comments or rebuttals to comments when at least one of them falls in the period of the review. Work on the continuation of the review series is under way, covering the period between 2005 and 2008, and will be published in 2010.
Analytical methods, total composition is not exactly known, analysis of phases in equilibrium Analytical methods with sampling: 27.6% AnT Analytical method: isothermal method Blo Blocking off a large sampling volume from the equilibrium cell Cap Sampling through capillaries Ins In situ sampling: a sampling vial is in the equilibrium cell, careful depressurization, removal of vial Lcir Liquid-phase recirculation Mla Material loss analysis: sampling after depressurization, weight loss of sample due to desorption is investigated Val Sampling using a special valve Var Variable-volume cell Vcir Vapor-phase recirculation VLcir Recirculation of the vapor and the liquid phase 0.0% AnP Analytical isobaric method, ebulliometry with phase analysis 15.4% AnPT Analytical isobaric-isothermal method Con Continuous-ow method SemX Semi-ow method used to measure the solubility of a gas in a liquid SemY Semi-ow method used to measure the solubility of substance in a gas (or supercritical uid) Chro Chromatographic method, e.g. inverse SFC, inverse HPLC Analytical methods without sampling: 1.5% AnSpec Spectroscopic analysis 1.1% AnGrav Gravimetric determination of phase composition: suspension balance or microbalance or quartz spring balance 1.1% AnOth Other determination of phase composition, e.g. by resonance in a Quartz Crystal Microbalance Synthetic methods, total composition is exactly known, no analysis of phases in equilibrium Synthetic methods with a phase transition: 36.4% SynVis Visual detection of phase transitions 8.4% SynNon Non-visual detection of phase transitions Synthetic methods without a phase transition: 6.1% SynT Isothermal, at least 2 phases, total pressure measured, often for pure-component vapor pressures; mixtures: y calculated 0.2% SynP Isobaric, at least two phases, ebulliometry, often for pure-component vapor pressures, mixtures: differential ebulliometry 2.2% SynOth Measured properties in the homogenous or heterogenous region are used to calculate the phase boundaries
53.3%
Additional remarks for all methods: Var, variable-volume cell; Vis, view cell, visual observation; Spec, spectroscopic method to get information; Pc, the critical pressure has been measured; Tc, the critical temperature has been measured; X, only the composition of the liquid phase is determined; Y, only the composition of the vapor phase is determined.
10 Table 3 Pure-component systems: X. X
Reference Otake et al. [553] Otake et al. [553] Yasumoto et al. [731] Sako et al. [596] Sako et al. [597] Lee et al. [439] Lim et al. [463] Pitschmann and Straub [564] Otake et al. [553] Di Nicola [264] Gruzdev et al. [342] Hu et al. [363] Lee et al. [439] Park et al. [555] Valtz et al. [685] Valtz et al. [689] Wang and Duan [701] Yasumoto et al. [731] Yasumoto et al. [731] Yasumoto et al. [731] Di Nicola and Giuliani [260] Sako et al. [596] Sako et al. [597] Sako et al. [596] Sako et al. [597] Sako et al. [596] Sako et al. [597] Ho et al. [353] Lim et al. [466] Park et al. [555] Yasumoto et al. [731] Duan et al. [274] Wang and Duan [701] Yasumoto et al. [731] Duan et al. [274] Lim et al. [462] Lim et al. [465] Lim et al. [466] Pitschmann and Straub [564] Widiatmo et al. [705] Yasumoto et al. [731] Yasumoto et al. [731] Yasumoto et al. [731] Otake et al. [553] Lim et al. [463] Lim et al. [465] Lim et al. [466] Park et al. [555] Takagi et al. [661] VonNiederhausern et al. [693] VonNiederhausern et al. [693] VonNiederhausern et al. [693] Wilson et al. [708] Wilson et al. [708] Abdulagatov et al. [139] Yasumoto et al. [731] Nikitin et al. [537] Nikitin et al. [538] Nikitin et al. [537] Nikitin et al. [538] Nikitin et al. [537] Nikitin et al. [538] Nikitin et al. [537] Nikitin et al. [538] VonNiederhausern et al. [693] VonNiederhausern et al. [693] Nikitin et al. [537] Nikitin et al. [538] Yang et al. [100] Yang et al. [728] Nikitin et al. [537] Nikitin et al. [538] VonNiederhausern et al. [693] Abdulagatov et al. [139] Nikitin et al. [537] Nikitin et al. [538]
T (K) 332498 302476 299473 453453 453453 293313 283293 303339 299475 235365 272373 233375 303323 283323 293353 276375 253373 302475 312486 285516 255363 447447 447447 449449 449449 467467 467467 273313 273313 303323 374374 253396 255393 293476 251343 323333 283293 273313 316345 300345 297463 300501 322510 297500 293293 283293 273313 283303 243333 719719 676676 722722 718718 723723 530563 410410 827827 827827 808808 808808 780780 780780 770770 770770 624624 605605 790790 790790 263293 263293 757757 757757 699699 403536 743743 743743
P (MPa) 02.2 02.5 02.2 2.92.9 2.92.9 1.22 0.91.2 1.53.6 02.6 02.4 0.12.8 02.9 0.50.9 0.20.9 0.31.8 0.22.9 02.8 02.2 01.9 02.1 01.2 2.12.1 2.12.1 2.42.4 2.42.4 2.52.5 2.52.5 0.21 0.61.8 0.71.3 44 03 01.9 02.7 0.23.5 2.32.8 0.81.1 0.21 23.7 1.33.7 02.7 03.1 02.5 03.6 0.50.5 0.30.5 0.20.9 0.30.6 01.4 8.28.2 5.95.9 6.36.3 6.56.5 5.55.5 4.84.8 44 11 11 1.11.1 1.11.1 1.31.3 1.31.3 1.41.4 1.41.4 2.72.7 33 1.21.2 1.21.2 24.8183.6 24.8183.6 1.61.6 1.61.6 3.73.7 10.110.1 1.61.6 1.61.6
V (cm3 ) 16 16 16 5.3 5.3 80 85 n.a. 16 254.8 439 13 80 85 n.a. n.a. 200 16 16 16 254.8 5.3 5.3 5.3 5.3 5.3 5.3 85 85 85 16 200 200 16 200 85 85 85 n.a. 139 16 16 16 16 85 85 85 85 60 n.a. n.a. n.a. n.a. n.a. n.a. 16 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a.
Method SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisPcTc SynVisPcTc SynT SynVis SynVisPcTc SynVisVarPcTc SynT SynT SynVis SynT SynVis SynVis SynVis SynT SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynT SynVisPcTc SynVisPcTc SynVisPcTc SynVisPcTc SynVisPcTc SynVisPcTc SynVis SynVis SynVis SynVisVarPcTc SynT SynT SynVisVarPcTc SynT SynT SynT SynVis SynVisPcTc SynT SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVis SynT SynVis SynVis SynNon SynNonConPcTc SynNonConPcTc SynNonConPcTc SynNonConPcTc SynNonConPcTc SynOthPcTc SynVisVarPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonConPcTc SynNonConPcTc SynNonPcTc SynNonPcTc SynVis SynVis SynNonPcTc SynNonPcTc SynNonConPcTc SynOthPcTc SynNonPcTc SynNonPcTc
1,1,1,2,2,3,3,4,4-Nonauorohexan-5-one 1,1,1,2,2,3,3-Heptauoropentan-4-one 1,1,1,2,2-Pentauoro-3-(1,1,2,2-tetrauoroethoxy)-propane 1,1,1,2,2-Pentauoro-3-butanone 1,1,1,2,2-Pentauoroethane (HFC-125)
1,1,1,2,2-Pentauoropentan-3-one 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea)
1,1,1,2,3,3-Hexauoro-3-(2,2,2-triuoroethoxy)propane 1,1,1,2,3,3-Hexauoro-3-(2,2,3,3,3-pentauoropropoxy)-propane 1,1,1,2,3,3-Hexauoro-3-(2,2,3,3-tetrauoropropoxy)-propane 1,1,1,2,3,3-Hexauoropropane (HFC-236ea) 1,1,1,2,4,4,4-Heptauoroisobutyl triuoromethyl ether 1,1,1,2-Tetrauoro-2-diuoro-methoxyethyl diuoromethyl ether 1,1,1,2-Tetrauoro-2-triuoromethyl-3butanone 1,1,1,2-Tetrauoroethane (HFC-134a)
1,1,1,3,3,3-Hexauoropropane (HFC-236fa) 1,1,1,3,3-Pentauoropropane (HFC-245fa) 1,1,1-Triuoro-2-(2,2,2-triuoroethoxy)ethane 1,1,1-Triuoroethane (HFC-143a)
1,1,2,2-Tetrauoro-1-(2,2,2-triuoroethoxy)ethane 1,1,2,2-Tetrauoro-2-(2,2-diuoroethoxy)ethane 1,1,2,2-Tetrauoro-3-(1,1,2,2-tetrauoroethoxy)propane 1,1,2,2-Tetrauorobutan-3-one 1,1-Diuoroethane (HFC-152a)
1,2-Ethanediol 1,2-Propanediol 1,3-Propanediol 1,4-Butanediol 1-Butanol 1-Chloro-1,1-diuoroethane 1-Docosanol 1-Eicosanol 1-Heptadecanol 1-Hexadecanol 1-n-Butoxy-2-propanol 1-n-Propoxy-2-propanol 1-Octadecanol 1-Octanol 1-Pentadecanol 1-Phenylethanol 1-Propanol 1-Tetradecanol
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 3 (Continued ) X 1-Tridecanol 2-(2-Aminoethylamino)ethanol 2-(2-Butoxyethoxy)ethyl acetate 2-(2-Ethoxyethoxy)ethyl acetate 2,2-Diuoroethylbis(triuoromethyl)amine 2,3,3,5,5,6,6-Heptauoro-1,4-dioxane 2-Butanol 2-Diuoromethoxy-1,1,1-triuoroethane 2-Methyl-1,3-propanediol 2-Methylpropane (isobutane) Reference Nikitin et al. [537] Nikitin et al. [538] Wilson et al. [708] Wilson et al. [708] Wilson et al. [708] Otake et al. [553] Sako et al. [596] Sako et al. [597] Abdulagatov et al. [139] Yasumoto et al. [731] Wilson et al. [708] Galicia-Luna et al. [47] Glos et al. [331] Glos et al. [332] Lee et al. [439] Miyamoto et al. [517] Abdulagatov et al. [139] Sako et al. [596] Sako et al. [597] Yasumoto et al. [731] Yasumoto et al. [731] Yasumoto et al. [731] Yasumoto et al. [731] Yasumoto et al. [731] Yasumoto et al. [731] Yasumoto et al. [731] Wueringer and Urban [123] Wueringer and Urban [123] Wueringer and Urban [123] Ewing and Ochoa [138] VonNiederhausern et al. [693] Poot et al. [565] Brandt et al. [187] Abdulagatov et al. [139] Wang et al. [698] VonNiederhausern et al. [693] Wilson et al. [708] Nikitin et al. [541] Nikitin et al. [120] Nikitin et al. [540] Abdulagatov et al. [139] Horstmann et al. [358] May et al. [117] Stuart et al. [654] He et al. [351] Magee et al. [491] Wang et al. [698] Domanska and Morawski [269] Ewing and Ochoa [287] Nikitin et al. [540] Nikitin et al. [541] Abdulagatov et al. [139] Veiga et al. [112] Poot et al. [565] VonNiederhausern et al. [693] Coquelet et al. [26] Lee et al. [440] Lim et al. [463] Park et al. [555] Pitschmann and Straub [564] Wu et al. [710] Nikitin et al. [539] Nikitin et al. [541] Nikitin et al. [539] Domanska and Morawski [269] Nikitin et al. [539] Funke et al. [311] Horstmann et al. [358] Nikitin et al. [539] Nikitin et al. [120] VonNiederhausern et al. [121] Nikitin et al. [540] Veiga et al. [112] Nikitin et al. [539] Nikitin et al. [541] Nikitin et al. [539] Kao and Miller [405] Nikitin et al. [541] T (K) 732732 732732 739739 693693 673673 293460 452452 452452 519546 294444 708708 317406 115340 115340 293323 310407 473508 435435 435435 298455 301487 342505 309482 473482 291481 301546 317395 308395 319395 277535 545545 546639 342405 83149 562562 709709 709709 851851 660660 650650 278304 304304 295295 299300 310345 250301 631631 293353 281552 551551 845845 605643 258333 523655 557557 283343 268318 283293 283303 318351 233400 837837 859859 743743 313353 820820 91305 305305 590590 614614 492618 604604 302303 792792 842842 785785 177291 841841 P (MPa) 1.71.7 1.71.7 4.64.6 2.12.1 2.52.5 02.6 2.82.8 2.82.8 4.64.6 03.4 5.35.3 0.53.5 01 01 0.30.6 0.53.6 5.15.1 2.62.6 2.62.6 02.7 03.1 03.2 01.9 1.71.9 02.3 02.5 0.1200 0.1200 0.1200 04.1 4.84.8 3.467.2 3.211.3 4.84.8 4.84.8 4.34.3 4.34.3 6.46.4 2.92.9 2.52.5 7.37.3 7.37.3 66 6.67 1.43.1 13.8 3.33.3 23.3153.1 04 44 2.52.5 21.621.6 -20.88.2 4.1115.2 3.83.8 1.14.8 0.62.7 1.11.4 1.11.9 2.85.7 05.3 1.11.1 2.12.1 1.91.9 16.2225 1.21.2 04.8 4.84.8 5.85.8 3.63.6 0.63.6 3.23.2 -818 1.31.3 3.23.2 1.41.4 02.9 3.83.8 V (cm3 ) n.a. n.a. n.a. n.a. n.a. 16 5.3 5.3 n.a. 16 n.a. 40 n.a. n.a. 80 1125 n.a. 5.3 5.3 16 16 16 16 16 16 16 n.a. n.a. n.a. 605 n.a. n.a. n.a. n.a. 18 n.a. n.a. n.a. n.a. n.a. n.a. 10 185 28 25 28.8 18 n.a. 605 n.a. n.a. n.a. 0.004 n.a. n.a. n.a. 85 85 85 n.a. 11.3 n.a. n.a. n.a. n.a. n.a. n.a. 10 n.a. n.a. 0.1 n.a. 0.004 n.a. n.a. n.a. 30 n.a. Method
11
2-Propanol (isopropanol) 2-Triuoromethyl-4,4,5,5-tetrauoro-1,3dioxolane 3-Diuoromethoxy-1,1,1,2,2-pentauoropropane 3-Methoxy-1,1,2,2,3,3-hexauoropropane 3-Methoxy-1,1,2,2-tetrauoropropane 4-Ethoxy-1,1,1,2,2,3,3,4,4-nonauorobutane 4-Methoxy-1,1,1,2,2,3,3-heptauorobutane 5-Methoxy-1,1,2,2,3,3,4,4-octauoropentane 5-n-Decyl-2-(4 -isothiocyanato-phenyl)-1,3-dioxane 5-n-Hexyl-2-(4 -isothiocyanato-phenyl)-1,3-dioxane 5-n-Octyl-2-(4 -isothiocyanato-phenyl)-1,3-dioxane Acetonitrile (ethanenitrile) Adamantane Ammonia Argon Benzene Bis(2-aminoethyl)amine Butanedioic acid Butylbenzene Butylcyclohexane Carbon dioxide
Chlorodiuoromethane (HCFC-22) Chlorotriuoromethane (CFC-13) Cumene Cyclohexane
Decanedioic acid Deuterium oxide Diamantane Diethyl sulde Diuoromethane (HFC-32)
Dimethyl ether Docosanoic acid Dodecanedioic acid Dodecanoic acid Eicosane Eicosanoic acid Ethane Ethanoic acid Ethylbenzene Ethylcyclohexane Gallium Heptadecanoic acid Heptanedioic acid Hexadecanoic acid Hexauoroethane (pfc-116) Hexanedioic acid
SynNonPcTc SynNonPcTc SynNonConPcTc SynNonConPcTc SynNonConPcTc SynVisVarPcTc SynVisPcTc SynVisPcTc SynOthPcTc SynVisVarPcTc SynNonConPcTc SynT SynT SynT SynT SynTVar SynOthPcTc SynVisPcTc SynVisPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynNon SynNon SynNon SynPVcir SynNonConPcTc SynVis SynVisVar SynOthPcTc SynVisPcTc SynNonConPcTc SynNonConPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynOthPcTc SynVisTc SynNonVcirVar SynVisVar SynT SynT SynVisPcTc SynNonVar SynPVcir SynNonPcTc SynNonPcTc SynOthPcTc SynVis SynVis SynNonConPcTc SynVis SynVis SynVis SynVis SynVisPcTc SynTVis SynNonPcTc SynNonPcTc SynNonPcTc SynNonVar SynNonPcTc SynTPcTc SynVisTc SynNonPcTc SynNonPcTc SynNonConPcTc SynNonPcTc SynVis SynNonPcTc SynNonPcTc SynNonPcTc SynT SynNonPcTc
12 Table 3 (Continued ) X Hexanoic acid Hexylbenzene Methane Methanol Methylbenzene Methylcyclohexane Mobil eal arctic 22 oil n-Butane n-Decane n-Dodecane n-Heptane n-Hexadecane
Reference Nikitin et al. [539] Nikitin et al. [120] Abdulagatov et al. [139] Veiga et al. [112] Nikitin et al. [120] Nikitin et al. [540] Skripov et al. [645] Glos et al. [331] Glos et al. [332] Abdulagatov et al. [139] Yang et al. [728] Abdulagatov et al. [139] Weber [137] Domanska and Morawski [269] Skripov et al. [645] Yang et al. [100] Abdulagatov et al. [139] Abdulagatov et al. [139] Di Nicola et al. [265] Abdulagatov et al. [139] Domanska and Morawski [269] Abdulagatov et al. [139] Ewing and Ochoa [288] Nikitin et al. [541] Abdulagatov et al. [139] Pfohl et al. [132] Yang et al. [100] Daridon et al. [106] Domanska and Morawski [269] Nikitin et al. [539] Kao and Miller [405] Nikitin et al. [541] Nikitin et al. [539] Nikitin et al. [539] Kayukawa et al. [409] Widiatmo et al. [705] Nikitin et al. [541] Nikitin et al. [120] Wilson et al. [708] Nikitin et al. [120] Nikitin et al. [120] Nikitin et al. [120] Nikitin et al. [120] Nikitin et al. [120] Grolier et al. [341] Abdulagatov et al. [139] Coquelet et al. [26] Glos et al. [331] Glos et al. [332] Horstmann et al. [358] Lee et al. [440] Glos et al. [331] Glos et al. [332] Ho et al. [353] Wang et al. [698] Nikitin et al. [540] Wilson et al. [708] VonNiederhausern et al. [121] Valtz et al. [35] Valtz et al. [689] Horstmann et al. [358] Hurly et al. [368] Funke et al. [135] Jarne et al. [380] Sako et al. [596] Sako et al. [597] Nikitin et al. [541] Nikitin et al. [539] Abdulagatov et al. [139] Bazaev et al. [164] VonNiederhausern et al. [121] Lim et al. [462] Lim et al. [463] Lim et al. [465] Kayukawa et al. [409] Nikitin et al. [539] Manara et al. [96] Manara et al. [496]
T (K) 652652 695695 105190 298329 588588 569569 825825 135340 135340 453617 268293 373540 335479 293353 720720 293323 343507 313431 219273 383594 303353 373569 323563 844844 313470 308423 283318 267287 293353 803803 234387 843843 690690 777777 240380 310406 840840 675675 685685 752752 708708 725725 790790 763763 380460 292369 277353 90340 90340 369369 268318 95340 95340 273313 364364 624624 762762 473635 288403 288403 318318 278313 224318 213261 462462 462462 862862 763763 562593 591673 586591 283293 283293 283293 300375 728728 31353180 24003150
P (MPa) 3.33.3 2.32.3 4.64.6 3.823.8 44 3.43.4 0.60.6 00.7 00.7 2.12.1 27.4160.3 2.72.7 01 9.2309.7 1.41.4 8.1144.6 33 4.44.4 0.53.1 2.22.2 11.2259.9 2.42.4 02.3 2.72.7 3.43.4 01.5 16183.1 0.198.3 134.3582 1.31.3 02.6 2.92.9 2.82.8 1.51.5 01.7 0.32.8 4.24.2 2.52.5 3.53.5 1.71.7 2.12.1 1.91.9 1.51.5 1.61.6 50200 4.24.2 0.53.1 02.4 02.4 4.24.2 0.41.5 02.9 02.9 0.51.6 4.64.6 2.82.8 4.14.1 0.33.8 0.24.9 0.23.3 3.73.7 1.43.3 0.23.7 0.18.1 2.32.3 2.32.3 1.91.9 1.61.6 4.24.2 435.5 3.94.1 3.24.2 3.24.1 3.24.2 0.63.4 2.12.1 10250 100100
V (cm3 ) n.a. n.a. n.a. 0.004 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. 273.5 n.a. n.a. n.a. 605 n.a. n.a. 345 n.a. 0.03 n.a. n.a. 85 n.a. n.a. n.a. n.a. 139 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. 36.3 n.a. n.a. n.a. n.a. 10 85 n.a. n.a. 85 18 n.a. n.a. 0.1 n.a. n.a. 10 27 n.a. n.a. 5.3 5.3 n.a. n.a. n.a. n.a. 0.1 85 85 85 n.a. n.a. n.a. n.a.
Method SynNonPcTc SynNonPcTc SynOthPcTc SynVis SynNonPcTc SynNonPcTc SynNonPcTc SynT SynT SynOthPcTc SynVis SynOthPcTc SynPVcir SynNonVar SynNonPcTc SynVis SynOthPcTc SynOthPcTc SynOth SynOthPcTc SynNonVar SynOthPcTc SynPVcir SynNonPcTc SynOthPcTc SynTVis SynVis SynVis SynNonVar SynNonPcTc SynT SynNonPcTc SynNonPcTc SynNonPcTc SynT SynT SynNonPcTc SynNonPcTc SynNonConPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNonPcTc SynNon SynOthPcTc SynVis SynT SynT SynVisTc SynVis SynT SynT SynVis SynVisPcTc SynNonPcTc SynNonConPcTc SynNonConPcTc SynVis SynVis SynVisTc SynT SynTPcTc SynVis SynVisPcTc SynVisPcTc SynNonPcTc SynNonPcTc SynOthPcTc SynOthPcTc SynNonConPcTc SynT SynVis SynT SynNon SynNonPcTc SynNonVis SynNonVis
n-Hexane Nitrogen tetraoxide Nitrous oxide n-Nonane n-Octadecane n-Octane Nonanedioic acid n-Pentane n-Tetradecane n-Tridecane Octadecanoic acid Octauorocyclobutane Octanedioic acid Octanoic acid Pentadecanoic acid Pentauoroethyl methyl ether (HFC245mc) Pentanedioic acid Pentylbenzene Phenyl acetate Phenyldecane Phenylheptane Phenyloctane Phenyltridecane Phenylundecane Poly(ethylene) (MDPE) Propane
Propene
Propylcyclohexane Propylene carbonate Styrene Sulfur dioxide Sulfur hexauoride Sulphur hexauoride Synthethic natural gas Tert-peruorobutyl methyl ether Tetradecanedioic acid Tetradecanoic acid Toluene
Triuoromethane (HFC-23)
Triuoromethyl methyl ether Undecanoic acid Uranium dioxide Uranium dioxide (non-stoichiometric)
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 3 (Continued ) X Water Xenon XMPA refrigeration oil Table 4 Binary systems: carbon dioxide + X. X (S)-Boc-piperazine 1-((4-Nitrophenyl)azo)-2-naphthalenol (Para Red) 1,1,1,2,2-Pentauoroethane (HFC-125) 1,1,1,2,3,3,3-heptauoropropane (HFC-227ea) 1,1,1,2,3,4,4,5,5,5-Decauoropentane 1,1,1,2-Tetrauoroethane (HFC-134a) 1,10-Phenanthroline 1,2-Limoneneoxide 1,4-Bis-(1-methylethylamino)-9,10-anthraquinone (AQiso03) 1,4-Bis-(butylamino)-9,10-anthraquinone (AQ04) 1,4-Bis-(ethylamino)-9,10-anthraquinone (AQ02) 1,4-Bis-(methylamino)-9,10-anthraquinone (AQ01) 1,4-Bis-(octadecylamino)-9,10-anthraquinone (AQ18) 1,4-Bis-(octylamino)-9,10-anthraquinone (AQ08) 1,4-Bis-(pentylamino)-9,10-anthraquinone (AQ05) 1,4-Bis-(propylamino)-9,10-anthraquinone (AQ03) 1,4-Diamino-2-methoxy-9,10-anthraquinone (C.I. Disperse Red 11) 1,4-Dihydroxy-3-methylthioxanthone 1,4-Dimethoxybenzene 1,4-Naphthoquinone 1,8-Cineole 1,8-Dihydroxy-2-(prop-2-enyl)-9-anthrone 1,8-Dihydroxy-9-anthrone 1,8-Dihydroxyanthraquinone 1-Amino-2,3-dimethyl-9,10-anthraquinone 1-Amino-2,4-dimethyl-9,10-anthraquinone 1-Amino-2-ethyl-9,10-nthraquinone 1-Amino-2-methyl-9,10-anthraquinone 1-Amino-4-hydroxy-2-phenoxy-9,10-anthraquinone (C.I. Disperse Red 60) 1-Butanol Reference Uchida et al. [679] Fasihi et al. [290] Di Nicola et al. [263] Valtz et al. [687] Kho et al. [413] Duran-Valencia et al. [276] Silva-Oliver et al. [641] Shamsipur et al. [621] Corazza et al. [236] Tuma et al. [70] Tuma et al. [70] Tuma et al. [70] Tuma et al. [70] Tuma et al. [678] Kraska et al. [430] Tuma et al. [70] Tuma et al. [70] Kraska et al. [430] Tuma et al. [70] Tuma et al. [678] Shamsipur et al. [619] Lee et al. [447] Ngo et al. [124] Cruz Francisco and Sivik [239] Karami et al. [406] Karami et al. [406] Galia et al. [56] Shamsipur et al. [618] Shamsipur et al. [618] Shamsipur et al. [618] Shamsipur et al. [618] Kraska et al. [430] Tuma et al. [678] Chen et al. [224] Secuianu et al. [607] Silva-Oliver and Galicia-Luna [640] Yeo et al. [732] Wu et al. [711] Wu et al. [711] Bardas et al. [163] Scheidgen and Schneider [601] Lee et al. [441] Blanchard et al. [133] Shariati and Peters [624] Mesiano et al. [512] Elizalde-Solis et al. [283] Scheidgen and Schneider [601] Scheidgen and Schneider [601] Beier et al. [168] Elizalde-Solis et al. [283] Shariati and Peters [623] Shamsipur et al. [620] Shamsipur et al. [620] Shamsipur et al. [620] Shamsipur et al. [620] Shamsipur et al. [620] Karami et al. [406] Karami et al. [406] Shamsipur et al. [620] Karami et al. [406] Shamsipur et al. [619] Shamsipur et al. [620] Shamsipur et al. [619] Lee et al. [441] Gutirrez and Luks [346] Kamps et al. [403] Kumelan et al. [433] Anthony et al. [83] T (K) 308328 308348 284304 276367 298298 252292 329354 308348 313343 299346 299346 299346 299346 330400 310340 299346 299346 305340 299346 300340 308348 313328 313313 313333 308348 308348 327357 308358 308358 308358 308358 303322 310310 333353 293324 324426 303428 313313 313313 303333 393393 313393 313333 308366 323323 293431 393393 393393 303313 324432 298363 308348 308348 308348 308348 308348 308348 308348 308348 308348 308348 308348 308348 318398 219308 293393 293395 283323 P (MPa) 920.5 12.235.5 1.63.3 0.27.1 0.76.3 0.12 1.97.3 10.135.5 8.213.8 720 720 720 720 17180 919.9 720 720 7.818.9 720 10140 12.135.4 2028 8.412.3 825 10.132.9 10.135.5 6.920.1 12.235.5 12.235.5 12.235.5 12.235.5 7.297.6 7130 512 0.510 9.617 717.4 1515 1515 0.28.4 01000 1.723.1 09.4 1.497.1 3035 421.5 01000 01000 0.59.8 2.220.1 0.694.6 12.235.5 12.235.5 12.235.5 12.235.5 12.235.5 10.135.5 10.135.5 12.235.5 10.135.5 12.135.4 12.235.5 12.135.4 4.824.9 0.57.9 0.19.6 0.19.6 01.3 V (cm3 ) Method 240 1 254.8 n.a. 130 50 40 1 25 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. 1 50 n.a. 30 1 1 85.3 1 1 1 1 n.a. n.a. 100 2560 40 26.71 55 55 200 80 28 10 3.5 n.a. 100 80 80 50 100 3.5 1 1 1 1 1 1 1 1 1 1 1 1 28 79 30 29.2 n.a. Reference Abdulagatov et al. [139] Veiga et al. [112] Omi et al. [127] Skripov et al. [645] T (K) 573646 253333 291323 890890 P (MPa) 2222 15.519.5 010 2.52.5 V (cm3 ) n.a. 0.004 n.a. n.a. Method
13
SynOthPcTc SynVis SynNonTc SynNonPcTc
1-Butyl-3-methylimidazolium hexauorophosphate ([bmim][PF6]) 1-Butyl-3-methylimidazolium tetrauoroborate ([bmim][BF4]) 1-Butyne 1-Decanol 1-Ethyl-2-pyrrolidinone 1-Ethyl-3-methylimidazolium ethyl sulfate [emim][EtSO4] 1-Ethyl-3-methylimidazolium hexauorophosphate 1H,1H,9H,9H-peruoro-1,9-nonanediol 1-Heptanol
1-Hexanol 1-Hexyl-3-methylimidazolium hexauorophosphate 1-Hydroxy-2-(1-propoxymethyl)-9,10-anthraquinone 1-Hydroxy-2-(butoxymethyl)-9,10-anthraquinone 1-Hydroxy-2-(ethoxymethyl)-9,10-anthraquinone 1-Hydroxy-2-(methoxymethyl)-9,10-anthraquinone 1-Hydroxy-2-(n-amyloxymethyl)-9,10-anthraquinone 1-Hydroxy-2,4-dimethyl-9-anthrone 1-Hydroxy-2-ethyl-9-anthrone 1-Hydroxy-2-methyl-9,10-anthraquinone 1-Hydroxy-2-methyl-9-anthrone 1-Hydroxy-3-methylthioxanthone 1-Hydroxy-9,10-anthraquinone 1-Hydroxythioxanthane 1-Methyl-2-pyrrolidinone 1-Methylnaphthalene 1-N-Butyl-3-methylimidazolium hexauorophosphate ([bmim][PF6]) 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6]
AnPTSemY AnTValY SynT AnTValVis AnTVisVar AnTVal AnTValVis AnTValY SynVisVar AnPTSemYSpec AnPTSemYSpec AnPTSemYSpec AnPTSemYSpec SynVisSpec AnPTSemYSpec AnPTSemYSpec AnPTSemYSpec AnPTSemYSpec AnPTSemYSpec SynVisSpec AnTValY AnPTSemY SynNonSpec AnPTSemY AnTValY AnTValY AnTIns AnTValY AnTValY AnTValY AnTValY AnSpecVis SynVisSpec AnTVcirVis AnTVisVar AnTValVisPc SynVisVar AnPTSemYVis AnPTSemYVis AnTVLcirVis AnT SynVisVarPc SynT SynVisVar SynVisVar AnTValVisPc AnT AnT AnTVLcirVis AnTValVisPc SynVisVar AnTValY AnTValY AnTValY AnTValY AnTValY AnTValY AnTValY AnTValY AnTValY AnTValY AnTValY AnTValY SynVisVarPc SynOthVis SynVis SynVis AnGrav
14 Table 4 (Continued ) X
Reference Blanchard et al. [133] Blanchard et al. [133] Kumean et al. [433] Blanchard et al. [133] Blanchard et al. [133] Blanchard et al. [133] Feng et al. [291] Hwu et al. [369] Scheidgen and Schneider [601] Laursen et al. [50] Silva-Oliver and Galicia-Luna [642] Gamse and Marr [317] Laursen and Andersen [435] Yeo et al. [732] Mesiano et al. [512] Mesiano et al. [512] Medina and Bueno [511] Lee et al. [448] Shamsipur et al. [617] Shamsipur et al. [617] Shen et al. [627] Chen et al. [225] Silva-Oliver sand Galicia-Luna [640] Garach-Domech et al. [321] Joung et al. [394] Ghaziaskar et al. [329] Ghaziaskar et al. [329] Ghasziaskar and Daneshfar [327] Joung et al. [394] Chen et al. [225] da Silva and Barbosa [247] Heo et al. [352] Heo et al. [352] Yamini et al. [725] Petrova et al. [562] Li et al. [459] Ngo et al. [124] Medina and Bueno [509] Gamse and Marr [317] Silva-Oliver and Galicia-Luna [642] Medina and Bueno [509] Lopes et al. [484] Bamberger and Maurer [160] Galicia-Luna et al. [47] Secuianu et al. [41] Mesiano et al. [512] Matsuyama et al. [506] Bristow et al. [189] da Silva and Barbosa [247] Lee et al. [442] Lopes et al. [484] Lee et al. [442] Medina and Bueno [511] Fasihi et al. [290] Fasihi et al. [290] Bristow et al. [189] Lee and McHugh [451] Leeke et al. [453] Powell et al. [572] Sane et al. [31] Sato et al. [598] Guney and Akgerman [344] Matsuyama et al. [506] Shamsipur et al. [621] Yamini et al. [725] Chen et al. [228] Yamini and Bahramifar [722] Bristow et al. [189] Bamberger et al. [61] Byun et al. [195] Powell et al. [572] Powell et al. [572] Bamberger and Maurer [160]
T (K) 313313 313333 293413 313333 313333 313333 328328 328328 393393 313343 333426 303323 308318 298425 323323 323323 313333 318328 308348 308348 294377 331351 335431 308348 323344 313323 313323 313353 322343 331351 288313 313353 313353 308348 313333 308328 313313 313333 303323 332431 313333 313323 293333 324348 293323 323323 308318 343363 288313 313313 313323 313313 313333 308348 308348 343363 308367 353383 273333 313373 313333 308328 308318 308338 308348 308322 308348 313353 313353 313393 273333 293293 303333
P (MPa) 13.713.7 09.5 0.99.8 09.3 09.2 09.3 313.3 313.3 01000 1.910.3 3.518.6 3.59 0.48.3 6.216 2335 3035 820 1224 12.448.6 12.448.6 2.317.6 4.912 8.514.5 1.913.5 7.312.4 6.818 6.818 1325.3 5.212.4 512 1.58.2 3.612.9 4.612.1 12.235.5 3.216 1030 8.818 820 2.27.2 2.115.7 820 8.224.4 1.18.1 110.4 0.68.6 918 10.125.3 912 1.28.1 28.3 5.29.4 28.2 820 12.235.5 12.235.5 914 13.489.2 9.430.7 1025.6 10.332.4 10.325.2 1121 9.125.3 10.135.5 12.235.5 918 12.135.4 825 1.111.1 2.716.5 7.231.7 9.511 1.18.1
V (cm3 ) n.a. 10 29.2 10 10 10 300 300 80 90 40 140 570 26.71 n.a. n.a. 15.7 50 1 1 30 n.a. 40 30 50 10 10 10 50 n.a. 23 33 33 0.5 4.014.0 377 n.a. 20 140 40 20 35 38 40 2560 n.a. 210 n.a. 23 n.a. 35 n.a. 15.7 1 1 n.a. n.a. 25 n.a. 45 40 n.a. 210 1 0.5 1500 1 n.a. 38 28 n.a. n.a. 38
Method AnPTSemY SynT SynVis SynT SynT SynT AnPTSemXY AnPTSemXY AnT AnTVcirX AnTValVisPc AnTVcirVal AnTVis SynVisVar SynVisVar SynVisVar AnPTSemY AnPTSemY AnTValY AnTValY SynVis AnTVcirVisVar AnTValVisPc SynVisVar AnTVLcirValVisPc AnPTSemY AnPTSemY AnPTSemY AnTVLcirValVisPc AnTVcirVisVar AnTVis SynVisVar SynVisVar AnTValY SynVisVar AnPTSemY SynNonSpec AnPTSemY AnTVcirVal AnTValVisPc AnPTSemY AnTValVis AnPTConVis AnTCapValVis AnTVisVar SynVisVar AnPTSemY AnPTSemYSpec AnTVis AnTVLcirValPc AnTValVis AnTVLcirValPc AnPTSemY AnTValY AnTValY AnPTSemYSpec SynVisVar SynVis SynVisVar AnTVisVarVal AnTVcirSpec AnPTSemY AnPTSemY AnTValY AnTValY AnPTSemY AnTValY AnPTSemYSpec AnPTCon SynVisVar SynVisVar SynVisVar AnPTConVis
1-n-Butyl-3-methylimidazolium methyl sulfate ([bmim][CH3SO4]) 1-n-Butyl-3-methylimidazolium nitrate [bmim][NO3] 1-n-Octyl-3-methylimidazolium hexauorophosphate [C8mim][PF6] 1-n-Octyl-3-methylimidazolium tetrauoroborate [C8mim][BF4] 1-Octanol
1-Pentanol 1-Phenylethanol 1-Propanol 2,2,3,3,4,4-Hexauoro-1,5-pentanediol 2,2,3,3-Tetrauoro-1,4-butanediol 2,3-Dimethylanilin 2,3-Dimethylhexane 2,4-Dinitrophenol 2,5-Dinitrophenol 2,Chloroethyl sulde 2-Butanol 2-Chloroethyl methyl sulde 2-Ethoxyethanol 2-Ethyl hexanoic acid 2-Ethyl-1-hexanol 2-Ethyl-hexyl-2-ethyl hexanoate 2-Methoxyethanol 2-Methyl-1-propanol (isobutanol) 2-Methyl-2-butanol 2-Methyl-2-propanol 2-Methylanthracene 2-Methylpentan-2,4-diol 2-Naphthol 2-Nitroanisole 2-Octanol 2-Pentanol 2-Phenyl-1-propanol 2-Phenylethanol 2-Propanol (isopropanol)
3,3,4,4,5,5,6,6-Octauorooctan-1,8-diol 3,3 ,4 ,5,7-Pentahydroxyavone (quercetin) 3-Methoxybenzamide 3-Methyl-1-butanol (isopentanol)
3-Methyl-2-butanol 3-Nitrotoluol 4-(N,N-Diethylamino)-4 -nitroazobenzene 4-(N,N-Dimethylamino)-4 -nitroazobenzene 4-Methoxybenzamide 4-Methoxyphenylacetic acid 4-Phenyl-toluene 4-Vinylbenzyl acetylacetone 5,10,15,20Tetrakis(3,5bis(triuoromethyl)phenyl)porphyrin 5,10,15,20-Tetrakis(pentauorophenyl)porphyrin 5-Fluorouracil 7,8-Dihydroxyavone 8-Hydroxyquinoline 9-nitroanthracene -Asarone Acenaphthene Acetaminophen Acetic acid (ethanoic acid) Acetoacetate Acetoacetate uoroacrylate polymer Acetone
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 4 (Continued ) X Reference Chen et al. [226] Wu et al. [709] Corazza et al. [236] Potluri et al. [569] Phiong and Lucien [563] Sahle-Demessie et al. [595] Abaroudi et al. [143] Goodarznia and Esmaeilzadeh [334] Li et al. [459] Ngo et al. [124] Shinoda and Tamura [635] Mishima et al. [516] Chouchi et al. [232] Cruz Francisco and Sivik [239] Xing et al. [720] Huang et al. [365] Borg et al. [185] Chen et al. [222] Fang et al. [289] Skerget et al. [644] Skerget et al. [644] Yamini et al. [724] Maeda et al. [489] Mishima et al. [516] Hansen et al. [348] Sovova et al. [649] Potluri et al. [569] Garmroodi et al. [40] Weinstein et al. [704] Fukn-Kokot et al. [107] Fukn-Kokot et al. [304] Galia et al. [56] Jin et al. [385] Lee et al. [448] Cheng et al. [231] Franceschi et al. [99] Guney and Akgerman [344] Fischer et al. [297] Fukn-Kokot et al. [107] Fukn-Kokot et al. [107] Fukn-Kokot et al. [304] Guigard et al. [90] Guigard et al. [90] Asghari-Khiavi and Yamini [153] Sovova et al. [650] Abaroudi et al. [143] Gaspar et al. [325] Leeke et al. [453] Shen et al. [628] Ghaziaskar and Nikravesh [328] Byun and McHugh [104] Byun et al. [195] Tamura and Shinoda [662] Gordillo et al. [335] Lee et al. [445] Lee et al. [446] Shinoda and Tamura [635] T (K) 323336 322363 313343 298298 308323 318338 308318 308308 308328 313313 323323 308333 323323 313333 310338 308328 303333 313333 313353 313353 303353 308348 308318 333333 313343 313333 298298 308348 298318 373395 373393 318318 328328 318328 308328 313343 308328 322342 321342 321341 321341 313318 313318 308348 313333 308328 283328 353383 293379 313353 308383 313393 323383 313353 323413 323413 323383 P (MPa) 8.99.9 9.211 4.811.7 2047 2.99.1 1030 10.616.2 10.218.1 1030 720.8 1030 15.225.3 9.39.3 825 1027 1225 12.525.8 9.824.1 5.629.6 8.430.3 1.611.2 12.235.5 9.125.3 10.125.3 6.834.2 1228 2047 12.235.5 8.425.1 0.116.6 2.316.6 923 823 1227 11.124.4 2.216.4 10.522 0.130 0.119.8 0.114.7 0.114.7 1010.3 9.610.3 12.235.5 1228 9.915.2 630 9.820.1 6.228.5 818 216 318.9 1025 1035 10.532.9 10.532.9 1030 V (cm3 ) 2050 14 25 100 70 43.92 n.a. n.a. 377 n.a. 2.3 210 50 30 0.83 10 1.712.4 n.a. 170 120 120 1 210 210 n.a. 12 100 1 5.530 20 20 85.3 377 50 300 27 n.a. n.a. 14 20 20 2 2 1 8 n.a. 334 25 30 63 28 28 n.a. 25.5 n.a. n.a. 2.3 Method
15
Acetonitrile (ethanenitrile) -Cyclodextrin octadecaacetate -Methylstyrene Amical-48 (diiodomethyl p-tolyl sulfone) -Naphthol Anthracene
Anthraquinone -Pinene Artemisinin (artemisia annua L,) Aspirin -Tetralol (1,2,3,4-tetrahydro-1-naphtol) -Tocopherol
Atropine Azobenzene -Carotene -Cyclodextrin heneiicosaacetate Benzocaine Benzoic acid
Benzoin Bergamot peel oilCitrus bergamia -Estradiol Biphenyl
Bis(acetylacetonato)copper(II) (Cu(acac)2) Bis(thenoyltriuoroacetonato)copper(II) (Cu(tta)2) Bisacodyl Black currant seed oil -Naphthol Borage oil Bromobenzene Butyl 2,5-dichlorobenzoate Butyl acetate Butyl methacrylate Butyric acid C.I. Disperse Blue 134 C.I. Disperse Blue 14 C.I. Disperse Blue 3 C.I. Disperse Blue 354 ([2-[[4-(dihexylamino)-2methylphenyl]methylene]-1,1dioxidobenzo[b]thien-3(2H)ylidene]propanedinitrile) C.I. Disperse Blue 79
SynVisVarPcTc SynVis SynVisVar SynVisVar AnTLcirVis AnPTSemYVis AnPTSemY AnPTSemY AnPTSemY SynNonSpec AnPTSemY AnPTSemY SynVis AnPTSemY AnPTSemYSpec AnPTSemY SynVisVar SynOthVLcirVis AnTVLcirBlo AnT AnT AnTValY AnPTSemY AnPTSemY AnSpecY AnPTSemY SynVisVar AnTValY SynVisVar SynTVis SynTVis AnTIns AnPTSemY AnPTSemY AnPTSemY SynVisVar AnPTSemY SynNon SynVis SynTVis SynTVis AnOth AnOth AnTValY AnPTSemY AnPTSemY AnPTSemY SynVis SynVisVar AnPTSemY SynVisVar SynVisVar AnPTSemY AnPTSemY AnPTSemYSpec AnPTSemYSpec AnPTSemY
C.I. Disperse Blue 79:1 C.I. Disperse modied Yellow 119 C.I. Disperse Orange 25 (3-[N-ethyl-4-(4nitrophenylazo)phenylamino]propionitrile) C.I. Disperse Orange 3 C.I. Disperse Red 1 C.I. Disperse Red 13 C.I. Disperse Red 153 C.I. Disperse Red 324 C.I. Disperse Red 82 C.I. Disperse Yellow 119 C.I. Disperse Yellow 16
Ferri et al. [74] Lee et al. [445] Lee et al. [446] Lin et al. [470] Lin et al. [472] Lin et al. [472] Ngo et al. [535] Shinoda and Tamura [635] Ferri et al. [74] Shinoda and Tamura [636] Shinoda and Tamura [636] Lin et al. [470] Ferri et al. [74] Lin et al. [472] Lin et al. [470] Tamura and Shinoda [662]
353393 323383 323383 353393 353393 353393 313313 323383 353393 323383 323383 353393 353393 353393 353393 323383
1830 9.930.5 9.930.5 1530 1530 1530 9.718.1 1030 1628 1030 1030 1530 1830 1530 1530 1025
32 n.a. n.a. 16.6 16.6 16.6 n.a. 2.3 32 2.3 2.3 16.6 32 16.6 16.6 n.a.
AnPTSemY AnPTSemYSpec AnPTSemYSpec AnPTSemY AnPTSemY AnPTSemY SynNonSpec AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTSemY
16 Table 4 (Continued ) X Caffeic acid Caffeine Caproic acid Caprylic acid Capsaicin Carbamazepine Carbazole Carbobenzoxy aspartic acid Carbobenzoxy proline Carbobenzoxy valine Carbon monoxide Carvacrol Carvone (p-mentha-6,8-dien-2-one) Cerium(2,2,6,6-tetramethyl-3,5-octanedionate) chelate Cerium(2,2,7-trimethyl-3,5-octanedionate) chelate Chloramphenicol Chlorothalonil (tetrachloroisophthalonitrile) Cholesterol Cholesteryl acetate Cholesteryl benzoate Cholesteryl butyrate Citral Codeine Coenzyme Q10 (ubiquinone) CuHAsO4 Cumene Cyclobutanone Cyclohexyl acetate Cyproterone acetate Decanal Decanoic acid Decyl 2,5-dichlorobenzoate Diazepam Dibenzo-24-crown-8 (DB24C8) Dibenzo-27-crown-9 (DB27C9) Dibenzo-30-crown-10 (DB30C10) Dibenzoylmethane Dibutyl phthalate Dicarbonyl(h5-cyclopentadienyl)-cobalt Dichloromethane (HCC-30)
Reference Murga et al. [528] Burgos-Solrzano et al. [194] Byun et al. [195] Byun et al. [195] Hansen et al. [348] Yamini et al. [724] Goodarznia and Esmaeilzadeh [334] Vedaraman et al. [691] Vedaraman et al. [691] Vedaraman et al. [691] Ke et al. [411] Leeke et al. [452] Gamse et al. [316] Corazza et al. [236] Andersen et al. [42] Andersen et al. [42] Li et al. [460] Sahle-Demessie et al. [595] Huang et al. [366] Huang et al. [366] Huang et al. [366] Huang et al. [366] Benvenuti and Gironi [170] Fonseca et al. [59] Yamini et al. [724] Matias et al. [503] Takeshita and Sato [73] Phiong and Lucien [563] Cruz Duarte et al. [238] Lee et al. [450] Asghari-Khiavi et al. [154] da Silva et al. [245] Heo et al. [352] Scheidgen and Schneider [603] Shen et al. [628] Yamini et al. [724] Shamispur et al. [616] Shamispur et al. [616] Shamispur et al. [616] Shamsipur et al. [621] Cheng et al. [230] Casimiro et al. [203] Casimiro et al. [203] Corazza et al. [236] Tsivintzelis et al. [676] Vega-Gonzalez et al. [692] Im et al. [372] Hwu et al. [370] Hwu et al. [370] Garach-Domech et al. [321] Hwu et al. [370] Cheng et al. [230] Cheng et al. [68] Feng et al. [291] Jou et al. [388] Lin et al. [471] Lin et al. [471] Lin et al. [471] Lin et al. [471] Di Nicola et al. [263] Diefenbacher and Trk [101] Diefenbacher and Trk [268] Rivollet et al. [587] Bahramifar et al. [39] Bahramifar et al. [39] Camy et al. [202] Im et al. [372] Laursen et al. [38] Vega-Gonzalez et al. [692] Bahramifar et al. [39] Rajasingam et al. [581] Fischer et al. [297] Fischer et al. [297] Margon et al. [498]
T (K) 313333 313313 308373 308373 308328 308348 308308 323343 323343 313333 280298 313323 303324 313343 313333 313333 313333 318338 313333 308328 308328 308328 315315 323323 308348 305323 308308 323323 277368 333413 308348 288313 313353 273393 293375 308348 308338 308348 318348 308338 308328 313363 313363 313343 308328 311326 320340 308328 308328 308348 308328 308328 308328 308328 298398 333413 333413 333413 333413 287294 304351 280318 283343 308348 308348 322373 310340 298320 309328 308348 298318 375413 418438 343453
P (MPa) 1550 1030 2.520.4 2.324 12.924.9 12.235.5 10.320.1 2026 1826 2028 8.19.9 0.230.8 1.810 7.715.6 10.135 9.824.3 1446.3 1030 1025 924 1227 1024 4.710 8.79.4 12.235.5 9.226.2 9.824.5 39.1 0.413.6 28 12.235.5 1.68.2 2.223.7 0100 6.239 12.235.5 12.244.6 12.248.6 12.248.6 10.135.5 1.412.5 1.814.8 1.814.8 4.610.1 1.98.8 4.19 0.79 1.48.3 1.48.3 1.413.1 1.48.3 1.410.1 1.512.5 1.410.1 021.1 220 117.5 216 120 1.33.5 5.77.4 1.67.5 1.17.4 12.235.5 12.235.5 1.312.7 0.89.9 0.67.3 412.5 12.235.5 19 0.130 0.229.1 113
V (cm3 ) 4.4 32 28 28 n.a. 1 n.a. 7.9 7.9 7.9 n.a. 500 140 25 2.8 2.8 n.a. 43.9 20 20 20 20 200 3.4 1 42.5 n.a. 70 3.5 600 1 23 33 80 30 1 1 1 1 1 300 36 3.5 25 202.1 9 320 300 300 30 300 300 300 300 n.a. 600 600 600 600 254.8 1406 1406 n.a. 0.5 0.5 14.35 320 570 9 0.5 70 n.a. n.a. 3.5
Method AnPTSemY AnTVcirValVis SynVisVar SynVisVar AnPTSemYVal AnTValY AnPTSemY AnTValY AnTValY AnTValY SynNonPcTc AnTVcir AnTVcirVis SynVisVar AnSpecY AnSpecY AnTVcir AnPTSemYVis AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTCon AnTValY AntCapVal AnPTSemY AnTLcirVis SynVis AnPTSemY AnTValY AnTValVis SynVisVar AnT SynVisVar AnTValY AnTValY AnTValY AnTValY AnTValY AnPTSemY AnTValVIs SynVisVar SynVisVar AnTVLcirValVis SynVisVar AnTVLcirValVis AnPTSemY AnPTSemY SynVisVar AnPTSemY AnPTSemY AnPTSemXY AnPTSemXY AnTVcir AnPTSemY AnPTSemY AnPTSemY AnPTSemY SynT SynVisPcTc SynVisPcTc AnTValVis AnTValY AnTValY SynVis AnTVLcirValVis AnTValVis SynVisVar AnTValY AnTLcirVis SynNon SynVis SynVis
Diethyl carbonate Diethyl ethylmalonate Diethyl methylmalonate Diethyl methylphosphonate Diethyl n-butylmalonate Diethyl oxalate Diethyl phthalate Diethyl succinate Diethylene glycol (DEG) Diethylene glycol butyl ether Diethylene glycol dibutyl ether Diethylene glycol diethyl ether Diethylene glycol hexyl ether Diuoromethane (HFC-32)
Dimethyl 2H-1-benzopyran-2,3-dicarboxylate Dimethyl 6-bromo-2H-1-benzopyran-2,3-dicarboxylate Dimethyl carbonate Dimethyl ether Dimethyl sulfoxide Dimethyl-3Hnaphtho[2,1-b]pyran-2,3-dicarboxylate Dimethylsulfoxide Dimethylterephthalate Diphenylcarbonate
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 4 (Continued ) X di-tert-Butyl-3H-naphtho[2,1-b]pyran-2,3dicarboxylate Divinyl adipate d-Lactone Docosahexaenoic acid ethylester Dodecanoic acid Double Tail Fluoroalkyl -Tocopherol -Caprolactone Echium oil Eucimibe Eicosapentaenoic acid ethylester Erythromycin Ethane Ethanol Reference Bahramifar et al. [39] Mesiano et al. [512] Xu et al. [721] Jaubert et al. [382] Scheidgen and Schneider [603] Powell and Beckman [571] Pereira et al. [561] Xu et al. [721] Gaspar et al. [325] Sauceau et al. [600] Jaubert et al. [382] Burgos-Solrzano et al. [194] Horstmann et al. [356] Horstmann et al. [358] Bae et al. [158] Chen et al. [223] Elbaccouch and Elliot [279] Galicia-Luna et al. [47] Joung et al. [394] Stuart et al. [654] Tsivintzelis et al. [676] Vega-Gonzalez et al. [692] Yeo et al. [732] Kho et al. [413] da Silva et al. [244] Tian et al. [670] Byun [197] Feng et al. [291] Ismadji and Bhatia [375] Hwu et al. [369] Hwu et al. [369] Hwu et al. [369] Ismadji and Bhatia [375] Cheng et al. [230] Byun and McHugh [104] Shen et al. [627] Tian et al. [670] Ismadji and Bhatia [375] Lopes et al. [483] Fukn-Kokot et al. [107] Fukn-Kokot et al. [107] Fukn-Kokot et al. [304] Cruz Francisco and Sivik [239] Cruz Francisco and Sivik [239] Cruz Francisco and Sivik [239] Cheng et al. [68] Murga et al. [528] Sovova [651] Li et al. [460] Yamini and Bahramifar [722] Shi et al. [629] Duarte et al. [275] Byun et al. [195] Kilic et al. [418] Kilic et al. [418] Kilic et al. [418] Kilic et al. [418] Kilic et al. [418] Kilic et al. [418] Kilic et al. [418] Xu et al. [721] Xu et al. [721] Potluri et al. [569] Xu et al. [721] Fink and Beckman [295] Sovova et al. [650] Bae et al. [157] Bae et al. [157] Gamse and Marr [315] Ghaziaskar and Nikravesh [328] Lee et al. [450] T (K) 308348 323323 313343 303353 273393 295295 306333 313363 283328 308318 303353 313333 291305 298300 314314 323323 323333 312373 313344 313313 313328 314324 298413 298298 295313 333393 313393 308328 308333 308328 308328 308328 308333 308328 313373 295375 313373 308333 313313 314338 314338 314338 313333 313333 313333 308328 313333 301333 313333 308348 297297 303323 313393 295295 295295 295295 295295 295295 295295 295295 313363 323363 298298 323363 295338 313313 323353 323353 298373 313353 333413 P (MPa) 12.235.5 1035 9.826.7 4.724.2 0100 6.515.1 926.4 8.327.2 630 9.830.1 623.3 1030 4.96.8 5.16.8 5.57.9 58.2 0.79.4 0.414.3 5.411.9 4.87.5 1.69.4 78.2 6.115.1 0.86.4 1.98.5 3.911.9 1.710.7 1.312.2 8.519.5 1.79.2 1.79.2 1.79.2 8.519.5 1.410.1 114 1.323.8 2.910.9 8.519.5 2020 0.129.5 0.119.8 0.119.8 825 825 825 1.412.5 1050 1228 11.749 12.135.4 1547 8.924.5 3.326.4 1923 1322 913 1236 644 1123 517 8.525.2 10.219.2 2047 10.221.9 3442 1529 2.313.8 0.814 2050 7.514 16 V (cm3 ) 0.5 n.a. 26 12.4 80 n.a. 30 26 334 n.a. 12.4 32 10 10 25 100 40 40 50 28 202.1 9 26.71 130 23 100 28 300 8 300 300 300 8 300 28 30 100 8 35 14 20 20 30 30 30 300 4.4 n.a. n.a. 1 100 30 28 n.a. n.a. n.a. n.a. n.a. n.a. n.a. 26 26 100 26 n.a. 8 25 25 50 63 600 Method AnTValY
17
Ethoxynonauorobutane Ethyl acetate Ethyl acrylate Ethyl benzoate Ethyl butyrate Ethyl caprate Ethyl caproate Ethyl caprylate Ethyl isovalerate Ethyl laurate Ethyl methacrylate Ethyl phenyl sulde Ethyl propanoate Ethyl proprionate Ethylene glycol Ethyl-o-vanillin
Eucalyptus leaf oil (E, Dives) Eucalyptus leaf oil (E, Polybractea) Eucalyptus leaf oil (E, Radiata) Eugenol Ferulic acid Florfenicol Fluoranthene Fluorinated telechelic disulfates Flurbiprofen Formic acid Functionalized siloxane copolymer: butyl methyl ketone Functionalized siloxane copolymer: methylbutyrate Functionalized siloxane copolymer: propy ltrimethyl carbon Functionalized siloxane copolymer: propyl acetate Functionalized siloxane copolymer: propyl ethyl ether Functionalized siloxane copolymer: propyl methyl carbonate Functionalized siloxane copolymer: propyl trimethyl silane -Butyrolactone -Caprolactone -Cyclodextrin tetracosaacetate -Decalactone Grafted poly(oxyethylene)siloxane Grape seed oil Heptadecauorodecyl acrylate Heptadecauorodecyl methacrylate Hexabromcyclododecane Hexanoic acid Hexyl acetate
SynVisVar SynVis SynVis AnT SynVisVar AnTVcirValVis SynVis AnPTSemY AnPTSemY SynVis AnTVcirValVis SynVisPcTc SynVisTc SynVisVar AnTVcirVis AnTVLcirVal AnTCapValVis AnTVLcirValVisPc SynVisVar AnTVLcirValVis SynVisVar SynVisVar AnTVisVar AnTVis AnTCapVisVar SynVisVar AnPTSemXY AnTBlo AnPTSemXY AnPTSemXY AnPTSemXY AnTBlo AnPTSemY SynVisVar SynVis AnTCapVisVar AnTBlo AnT SynVis SynTVis SynTVis AnPTSemY AnPTSemY AnPTSemY AnPTSemXY AnPTSemY AnPTSemY AnTVcir AnTValY SynVisVar AnTCapValVis SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVis SynVis SynVisVar SynVis SynVisVar AnPTSemY SynVisVar SynVisVar AnT AnPTSemY AnPTSemY
18 Table 4 (Continued ) X Hexyl acrylate Hexyl methacrylate High MW poly(2,6-dimethyl-1,4-phenylene ether) (PPO)(H) Hydrogen Hydroquinone (1,4-dihydroxybenzene) Imipramine hcl Iron tris(pentane-2,4-dionate) Iron(2,2,6,6-tetramethyl-3,5-octanedionate) chelate Iron(2,2,7-trimethyl-3,5-octanedionate) chelate Iron(2,4-pentanedionate) chelate Isoamyl acetate Isobutyraldehyde Ketoprofen Komplex Double Tail Fluoroalkyl: AuCl4Komplex Double Tail Fluoroalkyl: PtCl6Komplex Single Tail Fluoroalkyl: PtCl6Krytox 157 FSL Lemon oil Lemon peel oilCitrus latifolia Lidocaine Limonene
Reference Byun et al. [201] Byun et al. [201] Sato et al. [599] Bezanehtak et al. [173] Ke et al. [411] Garca-Gonzlez et al. [323] Deiters [259] Jara-Morante et al. [378] Roggeman et al. [589] Andersen et al. [42] Andersen et al. [42] Andersen et al. [42] da Silva et al. [244] Feng et al. [291] Ke et al. [411] Stassi et al. [652] Weinstein et al. [704] Powell and Beckman [571] Powell and Beckman [571] Powell and Beckman [571] Casimiro et al. [204] de la Fuente and Bottini [255] Franceschi et al. [99] Weinstein et al. [704] Benvenuti and Gironi [170] Berna et al. [171] Corazza et al. [236] Cruz Francisco and Sivik [239] Fonseca et al. [59] Gamse et al. [316] Leeke et al. [452] Berna et al. [171] Fonseca et al. [59] Raeissi and Peters [575] Chen et al. [222] Sato et al. [599] Liu et al. [475] Tsuji et al. [677] Tsuji et al. [677] Gaspar et al. [325] Cheng et al. [231] Asghari-Khiavi et al. [154] Webster and Kidney [703] Bezanehtak et al. [173] Elbaccouch and Elliot [279] Joung et al. [394] Laursen et al. [38] Liu et al. [473] Yeo et al. [732] Asghari-Khiavi and Yamini [153] Yamini et al. [726] Kho et al. [413] Byun [197] Murga et al. [527] Fang et al. [289] Nasrifar et al. [533] Asghari-Khiavi and Yamini [153] Cheng et al. [68] Garmroodi et al. [40] Shamsipur et al. [617] Skripov et al. [645] Wu et al. [709] Byun et al. [199] Byun and Jeon [196] Byun et al. [199] Byun and Jeon [196] Byun et al. [199] Duran-Valencia et al. [36] Abbott et al. [94] Diefenbacher and Trk [267] Diefenbacher and Trk [267] Fukn-Kokot et al. [107] Fukn-Kokot et al. [107] Garca-Gonzlez et al. [322] Goodarznia and Esmaeilzadeh [334]
T (K) 313393 313393 373473 278290 296303 333363 313323 313333 313333 313333 313333 295313 308328 311330 313328 313313 295295 295295 295295 313343 303313 313343 298318 315315 318318 313323 313333 323323 303324 318323 318328 323323 283371 313333 373473 308318 344344 344345 283328 308328 308348 230270 278308 313313 313342 298313 304512 298423 308348 308348 298308 318398 313333 313353 263353 308348 308328 308348 308348 825825 326377 318398 313373 318398 313373 318398 293338 318318 308308 332334 333353 332353 308308 308308
P (MPa) 2.514.6 3.517.2 1.920.2 4.819.2 9.113.8 1035 3050 927.5 9.430.6 917.7 9.835.3 1.78.1 19 89.7 925 925 6.518.2 615.6 8.316.2 217 0.98.7 1.719 725.2 3.18.5 6.910.5 7.98.1 825 8.79.5 3.18.4 0.39.6 7.111.1 8.710.3 1.414.7 5.424.1 219.9 13.622.8 4.120.1 2.15.4 630 10.123 12.235.5 0.88.4 1.57.4 1.17.5 612.4 1.26.3 7.416.3 5.816.4 12.235.5 12.235.5 1.37.1 1.911.4 1050 5.122.3 0.411.3 12.235.5 1.513.2 12.235.5 12.448.6 1.81.8 11.619.4 2.422.6 1.517.9 2.920.7 1.817.1 3.820.6 0.411.5 920 8.820.8 10.626.3 0.120 0.120 13.820.4 9.820
V (cm3 ) 28 28 n.a. 60 n.a. 50 0 n.a. 50 2.8 2.8 2.8 23 300 n.a. 125 5.530 n.a. n.a. n.a. 35 4080 27 5.530 200 n.a 25 30 3.4 140 500 n.a. 3.4 3.5 n.a. n.a. 40 500 52.5 334 300 1 n.a. 60 40 50 570 18 26.7 1 1 130 28 4.4 170 3.5 1 300 1 1 n.a. 14 28 n.a. 28 n.a. 28 50 25 600 1310 14 20 50 n.a.
Method SynVisVar SynVisVar AnGrav AnTLcirVal SynNonPcTc AnTVcirVal Comments AnPTSemY AnTVal AnSpecY AnSpecY AnSpecY AnTVis AnPTSemXY SynNonPcTc AnPTSemY SynVisVar SynVisVar SynVisVar SynVisVar AnTValVis SynVisVar SynVisVar SynVisVar AnPTSemY AnPTSemY SynVisVar AnPTSemY AnPTCon AnTVcirVis AnTVcir AnPTSemY AnPTCon SynVis SynOthVLcirVis AnGrav SynVis AnTVLcirBloVis SynOthVisVar AnPTSemY AnPTSemY AnTValY AnTVcir AnTLcirVal AnTVLcirVal AnTVLcirValVisPc AnTValVis SynVis SynVisVar AnTValY AnTValY AnTVisVar SynVisVar AnPTSemY AnTVLcirBlo SynVisPcTc AnTValY AnPTSemXY AnTValY AnTValY SynNonPcTc SynVis SynVisVarPc SynVisVarPc SynVisVarPc SynVisVarPc SynVisVarPc AnTVal AnOth AnT SynVis SynVis SynTVis AnTVcirVal AnPTSemY
Linalool
Linoleic acid Low MW poly(2,6-dimethyl-1,4-phenylene ether) (PPO)(L) Ls-54 surfactant Lubricating oil PAG-1 Lunaria oil Mandelic acid Medroxyprogesterone Methane Methanol
Methimazole Methoxynonauorobutane Methyl acrylate Methyl gallate Methyl oleate Methylcyclohexane Methylparaben Methylsaliylate Metronidazole benzoate m-Nitrophenol Mobil EAL Arctic 22 oil Monochlorobenzene N,N-Dibutylformamide N,N-Diethylacetamide N,N-Diethylformamide N,N-Dimethylacetamide N,N-Dimethylformamide Naphthalene
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 4 (Continued ) X Reference Lee et al. [447] Pauchon et al. [75] Ren et al. [584] Sauceau et al. [71] Sherman et al. [55] Stassi et al. [652] Takeshita and Sato [73] Wagner et al. [37] Wang et al. [699] Garmroodi et al. [40] Jara-Morante et al. [378] da Silva and Barbosa [243] da Silva and Barbosa [246] Zhang et al. [734] Blanchard et al. [133] Ke et al. [411] Eustaquio-Rincn and Trejo [286] Shaver et al. [625] Tsuji et al. [677] Tsuji et al. [677] Gardeler et al. [324] Nieuwoudt and du Rand [536] Nieuwoudt du Rand [536] Furuya and Teja [314] Fenghour et al. [292] Furuya and Teja [314] Eustaquio-Rincn and Trejo [286] Nieuwoudt du Rand [536] Rose et al. [591] Scheidgen and Schneider [601] Skripov et al. [645] Liu et al. [473] Nieuwoudt du Rand [536] Medina and Bueno [510] Horstmann et al. [357] Rajasingam et al. [581] Kamps et al. [400] Kamps et al. [401] Furuya and Teja [314] Elbaccouch et al. [282] Eustaquio-Rincn and Trejo [286] Nieuwoudt du Rand [536] Fischer et al. [296] Scheidgen and Schneider [603] Furuya and Teja [314] Chen et al. [226] Furuya and Teja [314] Nieuwoudt du Rand [536] Scheidgen and Schneider [601] Bae et al. [158] Heo et al. [352] Shen et al. [628] Bristow et al. [189] Bristow et al. [189] Galia et al. [56] Fink and Beckman [295] Stuart et al. [654] Gordillo [336] Iwai et al. [376] Murga et al. [527] Murga et al. [528] Maeda et al. [489] Mishima et al. [516] Curren and Burk [241] Shen et al. [628] Mishima et al. [515] Shen et al. [628] Shen et al. [628] Kho et al. [413] Lee et al. [448] Goodarznia and Esmaeilzadeh [334] Guney and Akgerman [344] Sane et al. [31] Sherman et al. [55] Yamini et al. [726] Garca-Gonzlez et al. [322] T (K) 328328 308308 328328 308318 308308 308308 308308 308328 308308 308348 323323 303303 303303 313333 313337 308308 344344 344344 344345 318318 313343 315348 313313 301362 313313 308308 313323 305311 393393 720720 304507 344366 313333 304309 298318 313353 313313 313313 313313 310353 338366 303323 273393 313313 312326 310310 329357 393393 324355 313353 295374 308328 318318 318327 295338 308343 308328 313313 313323 313333 308318 333333 293332 294366 308318 294367 295367 298298 318328 308308 318318 308328 318318 308348 333363 P (MPa) 12.525.3 7.132.1 716.2 829.9 13.113.1 9.725.2 9.824.5 830.1 8.525.2 12.235.5 1619.3 2.95.2 2.95.2 09.5 8.210.3 8.912.7 0.812.7 3.611.5 2.510.9 0.98.9 7.914.3 7.730.3 1052.3 3.44.3 13.841.3 8.312.4 8.516.8 7.617.2 01000 4.84.8 311.7 20.1297.5 1025 7.27.3 0.98.4 0.17.5 0.84.8 12.417.8 0.28.6 1020 1428.9 0.11.3 0100 15.236 7.78.5 12.945.9 16.630.1 01000 218.1 5.820.5 6.236.7 816.5 11.220.2 10.222 2637 7.313.5 1035 1515 8.525 8.550 9.125.3 10.125.3 9.724.6 5.920.3 9.125.3 5.618.7 5.919.7 1.56.3 1227 10.118.1 13.126.5 1228 16.516.5 12.235.5 1035 V (cm3 ) 50 12 0.8 5 47 125 n.a. 10 88 1 n.a. 23 23 10 n.a. n.a. n.a. 500 52.5 n.a. 132 132 31.6 207 31.6 n.a. 132 n.a. 80 n.a. 18 n.a. 15 10 70 30 30 31.6 9.5 n.a. n.a. n.a. 80 31.6 2050 31.6 n.a. 80 25 33 30 n.a. n.a 85.3 n.a. 28 25.5 26.5 4.4 4.4 210 210 105 30 210 30 30 130 50 n.a. n.a. 45 47 1 50 Method
19
Naproxen n-Butanal
N-Butylpyridinium tetrauoroborate [N-bupy][BF4] n-Butyraldehyde n-Decane
n-Dodecane n-Eicosane n-Heptacosane n-Heptane n-Hexacosane n-Hexadecane
n-Hexane n-Hexatriacontane Nimodipine Nitrous oxide N-Methyl-2-pyrrolidone N-Methyldiethanolamine (MDEA) n-Nonacosane n-Nonadecane n-Octadecane n-Octaosane N-Octyl-2-pyrrolidone Nonanoic acid n-Pentacosane n-Pentane n-Tetracosane n-Tetradecane n-Vinyl-2-pyrrolidone octanoic acid Octyl 2,5-dichlorobenzoate o-Hydroxybenzoic acid
Oligo(oxyethylene)siloxane Orange peel oil Palmitic acid p-Coumaric acid p-Dimethylaminoazobenzene Pentachlorophenol Pentadecauorodecyl 2,5-dichlorobenzoate Pentadecanolactone Pentauorobutyl 2,5-dichlorobenzoate Pentauoropropyl 2,5-dichlorobenzoate Peruorohexane (PFC-72) Phenanthene Phenanthrene
Phenazopyridine Phenol
AnPTSemY AnPTSemYVal AnPTSemY AnPTSemY AnTIns AnPTSemY AnPTSemY AnTVcirVal AnPTSemY AnTValY AnPTSemY AnTValVis AnTValVis Comments SynT SynNonPcTc AnPTSemY AnTVcirVal AnTVLcirBloVis SynOthVisVar AnTVal SynVisVar SynVisVar SynVisVar SynNon SynVisVar AnPTSemY SynVisVar AnPTSemY AnT SynNonPcTc SynVis SynVisVar AnPTSemY SynVisTc AnTLcirVis SynVis SynVis SynVisVar SynTVis AnPTSemY SynVisVar SynT AnT SynVisVar SynVisVarPcTc SynVisVar SynVisVar AnT SynVisVar SynVisVar SynVisVar AnPTSemYSpec AnTVcirVal AnTIns SynVisVar SynVisVar AnPTSemY AnTVcirSpec AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnTVal SynVisVar AnPTSemY SynVisVar SynVisVar AnTVisVar AnPTSemY AnPTSemY AnPTSemY AnTVisVarVal AnTIns AnTValY AnTVcirVal
20 Table 4 (Continued ) X Phenyl acetate p-Hydroxyazobenzene Picric acid p-Nitrophenol Poly(-olen) Poly(-hydroxybutyrate) Poly(butylene succcinate-co-adipate) Poly(butylene succinate) Poly(di-1H,1H,2H,2H-peruoroalkyl diitaconate) Poly(di-1H,1H,2H,2H-peruoroalkyl monoitaconate) Poly(-caprolactone) Poly(ethyl vinyl ether) 1500 Poly(ethylene glycol) 1500 Poly(ethylene glycol) 200 Poly(ethylene glycol) 400 Poly(ethylene glycol) 4000 Poly(ethylene glycol) 600 Poly(ethylene glycol) 8000 Poly(ethylene glycol) dimethyl ether 500 Poly(ethylene glycol) diol 200 Poly(ethylene glycol) diol 300 Poly(ethylene glycol) diol 400 Poly(ethylene glycol) diol 600 Poly(ethylene glycol) monomethylether 1000 Poly(ethylene glycol) monomethylether 350 Poly(ethylene glycol) monomethylether 550 Poly(ethylene glycol) monomethylether 750 Poly(ethylene glycol-block-propylene glycol) EO6-PO21-EO6 Poly(ethylene glycol-block-propylene glycol) EO-PO16-EO Poly(ethylene glycol-block-propylene glycol) PO15-EO10-PO15 Poly(ethylene glycol-block-propylene glycol) PO9-EO23-PO9 Poly(ethylene) (LDPE) Poly(methyl methacrylate) Poly(methyl methacrylate) (PMMA) Poly(propylene glycol) diol 1000 Poly(propylene glycol) diol 2000 Poly(propylene glycol) diol 425 Poly(propylene glycol) diol 725 Poly(propylene glycol) monobutoxy 1200 Poly(propylene glycol) monobutylether 1000 Poly(propylene glycol) monomethylether 1000 Poly(propylene glycol) monomethylether 1200 Poly(propylene) Poly(vinyl chloride) Poly(vinylacetate) Polyalkylene glycol Polycarbonate Polydimethylsiloxane 100cst Polydimethylsiloxane 20cst Polydisperse uorinated polyester (Mw = 1800) Polyuoroacrylate (poly(heptadecauorodecyl acrylate)) Polyolester Polystyrene
Reference Margon et al. [498] Lee et al. [450] Maeda et al. [489] Mishima et al. [516] Shamsipur et al. [617] Shamsipur et al. [617] Hauk and Weidner [350] Khosravi-Darani et al. [414] Sato et al. [43] Sato et al. [43] Li et al. [456] Li et al. [456] Cotugno et al. [85] Drohmann and Beckman [272] Wiesmet et al. [33] Lopes et al. [483] Lopes et al. [483] Wiesmet et al. [33] Lopes et al. [483] Wiesmet et al. [33] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Davis et al. [252] Fukn-Kokot et al. [107] Shieh and Liu [630] Boudouris et al. [44] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Drohmann and Beckman [272] Palamara et al. [84] Muth et al. [530] Palamara et al. [84] Sato et al. [88] Hauk and Weidner [350] Tang et al. [664] Alessi et al. [67] Alessi et al. [67] Mesiano et al. [512] Shi et al. [629] Hauk and Weidner [350] Boudouris et al. [44] Nikitin et al. [57] Nikitin et al. [58] Sato et al. [88] Shieh and Liu [630] Garca-Gonzlez et al. [323] Deiters [259] Weinstein et al. [704] May et al. [117] Smejkal et al. [646] Webster and Kidney [703] Ke et al. [411] Yamini et al. [726] Shen et al. [628] Cheng et al. [231] Byun [198]
T (K) 343453 333413 308318 333333 308348 308348 278373 308348 323453 323453 294424 293402 343358 295295 338373 313313 313313 328373 313313 353353 295295 295295 295295 295295 295295 295295 295295 295295 295295 295295 295295 295295 295295 423423 358385 305305 308308 295295 295295 295295 295295 295295 298343 295295 295295 323323 313343 313313 313373 278373 313333 313333 313333 323323 297297 278373 308318 311311 311311 373473 305305 333363 298318 310310 295354 230270 305343 308348 294373 308328 313393
P (MPa) 113 29 9.125.3 10.125.3 12.448.6 12.448.6 0.115 12.235.5 120.1 120.1 8.140.2 14.253.9 0.26 2835 4.127.4 2020 2020 0.528 2020 425.6 1011 1324 1525 1831 2032 1523 912 1326 2340 4446 1418 2430 3541 0.66.5 0.130.1 234 0.15.2 1421 1825 711 814 1018 1131 1119 1626 0.51.3 540 3.36.3 0.217.4 0.115 2040 1019 1019 1825 810 0.115 0.15.8 99 99 2.120.1 234 1035 6.925.2 2.72.8 6.28.4 03.1 67.1 12.235.5 6.226.7 9.422 3.516
V (cm3 ) 3.5 600 210 210 1 1 1000 1 n.a. n.a. 30 30 n.a. n.a. 1000 35 35 1000 35 1000 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. 72 14 10 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. 30 n.a. n.a. 1000 10 n.a. n.a. n.a. 100 1000 n.a. n.a. n.a. n.a. 10 50 5.530 185 35 n.a. n.a. 1 30 300 n.a.
Method SynVis AnPTSemY AnPTSemY AnPTSemY AnTValY AnTValY AnT AnTValY AnGrav AnGrav SynVisVar SynVisVar AnGrav SynVis AnTCap AnT AnT AnTCap AnT AnTCap SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynT SynVis AnT AnOth SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis AnGrav SynT AnGrav AnGrav AnT SynT AnPTSemY AnPTSemY SynVisVar SynVisVar AnT AnOth AnTMla AnTMla AnGrav AnT AnTVcirVal Comments SynVisVar SynNonVcirVar SynVisPcTc AnTVcir SynVisVarPcTc AnTValY SynVisVar AnPTSemY SynVisVar
p-Quinone (1,4-benzoquinone) Procaine Propane
Propene Propranolol Propyl 2,5-dichlorobenzoate Propyl 4-hydroxybenzoate Propyl acrylate
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 4 (Continued ) X Propyl methacrylate Propylene carbonate Protocatechualdehyde Protocatechuic acid P-tolylboronic acid Pyrocatechol Quinizarin Racemic (S)- and (R)-Boc-piperazine Salicylic acid Seawater Single Tail Fluoroalkyl Sodium 2-methyl-2-sulfosuccinate-semi[poly(dimethylsiloxane)ester] Sodium 2-sulfosuccinate-semi[poly(dimethylsiloxane)ester] Sodium bis[poly(dimethylsiloxane)ester]2-sulfosuccinate Soysolv Styrene Sulfathiazole Sulfur hexauoride SF6 Syringic acid TCMTB (2-(thiocyanomethylthio) benzothiazole) Tebuconazole (R-[2-(4-chlorophenyl)ethyl]-R-(1,1dimethylethyl)-1H-1,2,4-triazole-1-ethanol) Terbium(2,2,6,6-tetramethyl-3,5-octanedionate) chelate Terbium(2,2,7-trimethyl-3,5-octanedionate) chelate tert-Butanol Tetrabrombisphenyl-A Tetradecanoic acid Tetraethylene glycol n-laurel ether (C12E4) Tetrahydrofuran Tetrahydropyran Thiamphenicol Thioxanthone Titanocene dichloride Toluene Reference Byun [198] Williams et al. [707] Murga et al. [527] Murga et al. [527] Leeke et al. [453] Garca-Gonzlez et al. [322] Ferri et al. [74] Uchida et al. [679] Abbott et al. [94] Stassi et al. [652] Holder et al. [355] Powell and Beckman [571] Fink and Beckman [295] Fink and Beckman [295] Fink and Beckman [295] Elbaccouch et al. [282] Akgn et al. [149] Kordikowski et al. [66] Horstmann et al. [358] Murga et al. [529] Sahle-Demessie et al. [595] Sahle-Demessie et al. [595] Andersen et al. [42] Andersen et al. [42] Chen et al. [225] Gamse and Marr [315] Scheidgen and Schneider [603] Liu et al. [474] Im et al. [371] Nasrifar et al. [533] Li et al. [460] Shamsipur et al. [619] Wang et al. [699] Cheng et al. [230] Lee et al. [449] Wu et al. [709] Zhang et al. [735] Florusse et al. [301] Florusse et al. [301] Florusse et al. [301] Scurto et al. [606] Scurto et al. [606] Shen et al. [628] Ribeiro and Aguiar-Ricardo [586] Di Nicola et al. [142] Fernandez et al. [294] Powell and Beckman [571] Chen et al. [222] Rovetto et al. [592] Yamini and Bahramifar [722] Pauchon et al. [75] Wagner et al. [37] Powell and Beckman [571] Shi et al. [629] Wagner et al. [37] Wagner et al. [37] Ren et al. [584] Petrova et al. [562] Petrova et al. [562] Petrova et al. [562] Scheidgen and Schneider [603] Mishima et al. [515] Burgos-Solrzano et al. [194] Wai and Waller [696] Wai and Waller [696] Wai and Waller [696] Wai and Waller [696] T (K) 313393 298333 313333 313333 353383 333363 353393 308328 318318 313328 275277 295295 295338 295338 295338 298343 333348 298353 299309 313333 323338 323338 313333 313333 331351 298373 273393 313323 311331 263353 313333 308348 337337 311311 352352 323386 304335 278368 278368 278368 303333 303333 295375 307336 252285 272373 295295 313333 351450 308348 308328 300330 295295 297297 300320 300320 308328 313333 313333 313333 273393 308318 313333 313313 313313 313313 313313 P (MPa) 1.616.5 4.111 1050 1050 9.531.7 1035 1630 10.220.4 9.819.5 9.625 1527 5.510.1 2427 2427 2628 0.19 613 1035 4.56.6 1050 1030 1030 12.435.2 12.431.8 512 2050 0100 10.219.6 0.88.1 0.411.1 18.547.4 12.135.4 17.930 1.47.3 0.13 11.115.5 7.410.5 1.914.3 1.814.3 1.314.5 19.8 19.8 5.820.1 7.610.3 1.53.8 0.630 5.68.6 10.124.2 3.611.2 12.135.4 6.528.3 7.330.4 714.6 14.517.5 6.912 718.9 819 1.613.5 1.313.1 2.411.6 0100 9.125.3 1029.9 1032 1032 1032 1032 V (cm3 ) n.a. 725 4.4 4.4 25 50 32 240 25 125 40 n.a. n.a. n.a. n.a. 9.5 115 10 10 4.4 43.9 43.9 2.8 2.8 n.a. 50 80 40 320 3.5 n.a. 1 88 300 n.a. 14 2050 3.5 3.5 3.5 n.a. 5.4 30 5 251 n.a. n.a. n.a. 3.5 1 12 10 n.a. 100 10 10 0.8 4.014.0 4.014.0 4.014.0 80 210 32 3.5 or 15 3.5 or 15 3.5 or 15 3.5 or 15 Method SynVisVar AnT AnPTSemY AnPTSemY SynVis AnTVcirVal AnPTSemY AnPTSemY AnOth AnPTSemY SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar
21
SynTVis AnTBlo AnPTSemYSpec SynVisTc AnPTSemY AnPTSemYVis AnPTSemYVis AnSpecY AnSpecY AnTVcirVisVar AnT AnT SynVis AnTVLcirValVis SynVisPcTc AnTVcir AnTValY AnPTSemY AnPTSemY AnT SynVis SynVisVarTc SynVisVar SynVisVar SynVisVar AnTVisVar SynVisPc SynVisVar SynNonPcTc SynOth AnSpecY SynVisVar SynOthVLcirVis SynVis AnTValY AnPTSemYVal AnTVcirVal SynVisVar SynVisVar AnTVcirVal AnTVcirVal AnPTSemY SynVisVar SynVisVar SynVisVar AnT AnPTSemY AnTVcirValVis AnTVal AnTVal AnTVal AnTVal
Tributyrin Tricaproin Tricaprylin Trichloromethane (HCC-20) Tridecauorooctyl 2,5-dichlorobenzoate Triethylamine Triuoromethane (HFC-23) Triiodomethane Trioctylamin Triolein Tripalmitin Triphenylene Triphenylmethane Triphenylphosphine Triple tail Fluoroalkyl tris(2-Peruorobutyl ethyl)tin uoride tris(Pentauorophenyl)phosphine tris(p-Fluorophenyl)phosphine) Troegers base Undec-10-en-1-ol Undecan-2-ol Undecan-6-ol Undecanoic acid Undecanolide Uracil Uranyl-thenoyltriuoroaceton-tributhyl phosphate (UO2(TTA)2 * TBP) Uranyl-thenoyltriuoroaceton-tributylphosphine oxide (UO2(TTA)2 * TBPO) Uranyl-thenoyltriuoroaceton-triethyl phosphate (UO2(TTA)2 * TEP) Uranyl-thenoyltriuoroaceton-trioctylphosphine oxide (UO2(TTA)2 * TOPO)
22 Table 4 (Continued ) X Uranyl-thenoyltriuoroaceton-water (UO2(TTA) * 2H2O) Valeric acid Vanillic acid Vanillin
Reference Wai and Waller [696] Byun et al. [195] Murga et al. [529] Stassi et al. [652] Fukn-Kokot et al. [107] Fukn-Kokot et al. [107] Fukn-Kokot et al. [304] Byun and Shin [200] Byun and Shin [200] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Addicks et al. [147] Anderson [151] Bamberger et al. [61] Chapoy et al. [217] Jarne et al. [381] Jarne et al. [381] Kiepe et al. [134] Li et al. [461] Mooijer-van den Heuvel et al. [521] Servio and Englezos [614] Valtz et al. [688] Yang et al. [729] Zatsepina and Buffett [126] Li et al. [461] Ribeiro et al. [585] Skripov et al. [645] Medina and Bueno [510]
T (K) 313313 313393 313333 313328 343353 343353 343353 313393 318398 303353 336382 313353 411352 313353 347379 293293 274288 323351 274351 251288 251288 313393 332332 276286 273283 278318 277280 271281 332332 282299 890890 313333
P (MPa) 1032 2.520.7 8.550 8.625 0.119.7 0.117.4 0.117.4 2.412.6 4.613.8 7.930.2 0.227.2 9.729.8 0.330.1 8.130.7 0.231.7 12.5 02.1 414.1 0.19.3 0.14.1 0.14.1 09.2 3.319.8 1.87.3 26 0.47.9 4.914.2 2.83 1.720.8 5.97.2 77 1025
V (cm3 ) 3.5 or 15 28 4.4 125 14 20 20 28 28 120 14 120 14 120 14 450 1119 38 n.a. n.a. n.a. n.a. 500 n.a. n.a. 28 n.a. n.a. 500 5 n.a. 15
Method AnTVal SynVisVar AnPTSemY AnPTSemY SynVis SynTVis SynTVis SynVisVarPc SynVisVarPc AnT SynVis AnT SynVis AnT SynVis AnTVarVis SynT AnPTCon SynNonVar AnPTSemY SynVis SynT AnTVar SynVis AnTVis AnTValVis AnTVcirVisVar SynNon AnTVar SynNonPcTc SynNonPcTc AnPTSemY
Vinyl acetate Vinyl acrylate Vitamin D2 Vitamin D3 Vitamin K3 Water
Weyburn formation brine Xenon XMPA refrigeration oil Zopiclone
Table 5 Binary systems: water + X. 1,8-Cineol (1,8-epoxy-p-menthane or eucalyptol) 1-Octanol 2,2,4-Trimethylpentane 2-Methylpropane (isobutane) Acetophenone Air Ammonia Anisole Benzene Miller and Hawthorne [513] Brown et al. [190] Miller and Hawthorne [514] Tian et al. [669] Brown et al. [190] Mohammadi et al. [91] Munakata et al. [526] Brown et al. [190] Jou and Mather [392] Marche et al. [497] Mathis et al. [502] Miller and Hawthorne [514] Ivanic et al. [128] Ivanic et al. [128] Ivanic et al. [128] Addicks et al. [147] Anderson [151] Bamberger et al. [61] Chapoy et al. [217] Jarne et al. [381] Jarne et al. [381] Kiepe et al. [134] Li et al. [461] Mooijer-van den Heuvel et al. [521] Servio and Englezos [614] Valtz et al. [688] Yang et al. [729] Zatsepina and Buffett [126] Miller and Hawthorne [513] Matsuo et al. [504] Azevedo et al. [156] Marche et al. [497] Bazaev et al. [165] Miller and Hawthorne [513] Chapoy et al. [215] Kim et al. [422] Mohammadi et al. [518] 298473 354542 298473 625695 339502 274283 310400 344551 279453 343424 298473 298473 287293 279284 282286 293293 274288 323351 274351 251288 251288 313393 332332 276286 273283 278318 277280 271281 298473 273313 310319 343424 517680 298473 278303 277298 274343 6.46.8 6.86.8 6.56.5 25.7306 6.86.8 1745.1 0.54.5 6.88.1 02 1.71.7 55 0.140 6.616.8 37.8 4.616.3 12.5 02.1 414.1 0.19.3 0.14.1 0.14.1 09.2 3.319.8 1.87.3 26 0.47.9 4.914.2 2.83 6.16.5 0.1400 0.140 1.71.7 3.537.4 6.97.2 0.34.6 1.420.1 0.34.9 10.4 20 10.4 60.1 20 150 n.a. 20 n.a. 530 10 10.4 300 300 300 450 1119 38 n.a. n.a. n.a. n.a. 500 n.a. n.a. 28 n.a. n.a. 10.4 n.a. n.a. 530 n.a. 10.4 34 n.a. 34 AnPTSemY SynVisVar AnPTSemY SynVis SynVisVar SynNon SynNonVar SynVisVar AnTLcirVis AnT AnT AnPTSemY SynNon SynNon SynNon AnTVarVis SynT AnPTCon SynNonVar AnPTSemY SynVis SynT AnTVar SynVis AnTVis AnTValVis AnTVcirVisVar SynNon AnPTSemY AnTVar SynVis AnT SynOthPcTc AnPTSemY AnTVal SynVisVar AnTValVis
Black oil AWestport Technology Center Black oil BWestport Technology Center Black oil CWestport Technology Center Carbon dioxide
Carvone (p-mentha-6,8-dien-2-one) Cesium chloride Copoly(PNIPAAM/VS) Cyclohexane Deuterium oxide d-Limonene ((R)-p-mentha-1,8,diene) Ethane
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 5 (Continued ) Mohammadi et al. [519] Morita et al. [523] Song et al. [647] Wang et al. [700] Hu et al. [364] Haruki et al. [349] Mathis et al. [502] Miller and Hawthorne [513] Matsuo et al. [505] Morris et al. [93] Matsuo et al. [505] Matsuo et al. [505] Abdulagatov and Azizov [146] Matsuo et al. [505] Matsuo et al. [505] Addicks et al. [147] Chapoy et al. [214] Chapoy et al. [214] Chapoy et al. [218] Chapoy et al. [220] Chapoy et al. [220] Huo et al. [367] Kharrat and Dalmazzone [412] Kiepe et al. [415] Kim et al. [422] Link et al. [102] Mohammadi et al. [519] Mohammadi et al. [91] Ohmura et al. [547] Servio and Englezos [615] Song et al. [647] Wang et al. [700] Yang et al. [730] Yang et al. [730] Bazaev et al. [166] Yokoyama and Uematsu [733] Mathis et al. [502] Miller and Hawthorne [514] Hodes et al. [354] Ostergaard et al. [551] Tian et al. [669] Haruki et al. [63] Shimoyama et al. [634] Miller and Hawthorne [513] Rudolph et al. [594] Abdulagatov et al. [145] Kamilov et al. [399] Rudolph et al. [594] Chapoy et al. [216] Mohammadi et al. [91] Miller and Hawthorne [514] Jou and Mather [48] Mohammadi et al. [91] Tan et al. [69] Miller and Hawthorne [514] Fang et al. [98] Azevedo et al. [156] Hodes et al. [354] Chapoy et al. [219] Makogon [495] Mooijer-van et al. [522] Song et al. [647] Haruki et al. [349] Jou and Mather [392] Sue et al. [30] Valyashko et al. [122] Jarne et al. [380] Ivanic et al. [128] Avila et al. [155] Avila et al. [155] Sugahara et al. [655] Brown et al. [190] Haruki et al. [349] Haruki et al. [63] Jou and Mather [392] Kiselev et al. [424] Miller and Hawthorne [514] Rabezkii et al. [574] Ohgaki et al. [545] 282293 298323 201281 283303 523647 553583 298473 298473 298298 460583 298298 298298 423573 298298 298298 298298 283318 283293 275313 283318 283293 275275 281284 313373 276298 278293 282313 278278 273281 274284 196270 283303 298298 273286 373673 320420 298473 298473 342362 277288 622695 573593 573593 298473 315331 643651 395494 339352 274363 274283 298473 273453 273284 300300 298473 298943 305321 373382 277368 278278 276278 211276 553583 288448 573673 590647 244288 288296 224270 224270 276317 340524 573583 553573 273458 623673 298473 630641 283320 0.52.9 89479 3.43.4 0.54 3.922.1 10.426.4 55 6.46.9 0.1400 4.215.5 0.1400 0.1400 0.48.5 0.1400 0.1400 7.317.8 0.934.6 1035 0.917.9 0.934.6 1035 3030 5.77.7 09.2 2.316.6 8.69.6 20.5 4.74.7 2.65.7 3.56.5 3.46.9 240 2.312.6 3.619.3 090.9 01.3 55 66 2525 113.9 23.2306 12.130.3 1520 6.87 3.598.9 835 0.65.2 3.799.3 0.97.1 1945.3 6.56.5 03.6 13.543.7 110 66 1102600 0.140 2525 0.33.9 0.535 0.39.8 0.81.1 10.226.5 01.1 34.539.9 00 0.14.1 414 0.27.3 0.27.3 7.4317 6.86.8 10.515.3 15.130.5 01.7 11.439.1 55 19.428.8 0.969 34 0.2 n.a. 600 18 31 10 10.4 n.a. n.a. n.a. n.a. 95.5 n.a. n.a. 450 34 34 34 34 34 1 n.a. n.a. n.a. 40 34 150 201 n.a. n.a. 540 n.a. n.a. n.a. 1624 10 10.4 n.a. 540 60.1 31 31 10.4 n.a. n.a. n.a. n.a. 28 150 10.4 n.a. 150 500 10.4 0.00005 n.a. n.a. 28 160210 n.a. n.a. 31 n.a. 17.4 101 n.a. 300 n.a. n.a. 0.2 20 31 31 n.a. n.a. 10.4 n.a. n.a.
23
Ethyl acetate Ethylbenzene Eugenol (4-allyl-2-methoxyphenol) Glycine Hydrogen l-Alanine l-Isoleucine Lithium sulfate l-Leucine l-Valine Methane
Methanol m-Xylene Na2 SO4 Natural near critical reservoir uid (C1C20+) n-Butane n-Decane Nerol (cis-3,7-dimethyl-2,6-octadien-1-ol) n-Heptyltetraoxyethylene (C7E4) n-Hexane n-Hexyltetraoxyethylene (C6E4) Nitrogen n-Octane n-Pentane Oxygen p-Cymene poly(ethylene) 68 000 Poly(N-isopropylacrylamide) (PNIPAAM) Potassium sulfate Propane
p-Xylene Silicone dioxide Sodium sulfate Synthethic natural gas Synthetic Green Canyon gas Synthetic natural gas Tetrauoromethane (CFC-14) Toluene
Xenon
AnTValVis SynVisSpec AnPTSemY AnTVal SynVis AnPTConVis AnT AnPTSemY AnTVar AnOth AnTVar AnTVar SynT AnTVar AnTVar AnTVarVis AnTVal AnTVal AnTVal AnTVal AnTVal AnTSpec SynNon SynT SynVisVar SynVis AnTValVis SynNon SynNon AnTVis AnPTSemY AnTVLcirVar AnTVcirVisVar AnTVcirVisVar SynOthPcTc SynNonVar AnT AnPTSemY SynVisCon SynVis SynVis AnPTConVis AnPTConVis AnPTSemY SynVis SynOthPcTc SynNon SynVis AnTValVis SynNon AnPTSemY AnTVcir SynNon AnPTSemX AnPTSemY SynVisSpec SynVis SynVisCon AnTValVis SynVisVar SynVis AnPTSemY AnPTConVis AnTLcirVis AnTBlo SynNon SynVis SynNon AnPTCon SynVis SynVisSpec SynVisVar AnPTConVis AnPTConVis AnTLcirVis SynOthPcTc AnPTSemY SynOthPcTc SynVis
24 Table 6 Binary systems: ammonia + X. X Potassium iodide Sodium bromide Sodium iodide Sodium thiocyanate Water Reference
T (K) 134668 404408 406408 409409 310400
P (MPa) 1.976.2 1111.9 11.511.8 11.912 0.54.5
V (cm3 ) n.a. n.a. n.a. n.a. n.a.
Method SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynNonVar
Brandt et al. [187] Brandt et al. [187] Brandt et al. [187] Brandt et al. [187] Munakata et al. [526]
Table 7 Binary systems: hydrogen sulde + X. X Benzene Carbonyl sulde Diethylene glycol (DEG) N-Methyldiethanolamine (MDEA) N-Octyl-2-pyrrolidone Reference Fischer et al. [296] Guilbot et al. [343] Guilbot et al. [343] Jou et al. [388] Kamps et al. [400] Fischer et al. [296] T (K) 304323 232293 366378 298398 313353 306323 P (MPa) 0.11.2 0.11.7 6.38.9 07.4 0.12.7 0.11.1 V (cm3 ) n.a. 30 10 n.a. 30 n.a. Method SynT SynVis SynVisConPcTc AnTVcir SynVis SynT
Table 8 Binary systems: hydrogen + X. X 1-Butanol 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] 1-Propanol -Methylbenzyl alcohol -Methylstyrene Carbon dioxide Cumene Cyclohexane Ethanol Gasoil Methanol Methyl palmitate n-Decane n-Hexadecane n-Hexane n-Octacosane Water Reference dAngelo and Francesconi [242] Anthony et al. [83] dAngelo and Francesconi [242] Giles and Wilson [330] Phiong and Lucien [54] Bezanehtak et al. [173] Ke et al. [411] Phiong and Lucien [54] Ronze et al. [590] dAngelo and Francesconi [242] Ronze et al. [590] Bezanehtak et al. [173] dAngelo and Francesconi [242] Rovetto et al. [593] Florusse et al. [300] Florusse et al. [300] Gao et al. [318] Gao et al. [319] Florusse et al. [300] Morris et al. [93] T (K) 295524 298298 299513 323423 308323 278290 296303 323323 304373 299476 298645 278308 314476 361450 283450 298448 504505 344410 342447 460583 P (MPa) 3.98.8 01.3 3.610.1 3.410.3 313 4.819.2 9.113.8 111.7 0.14.6 3.79 0.25.6 211 4.410.9 3.514.2 1.214.2 1.115.1 33.1 1.26.2 1.414 4.215.5 V (cm3 ) 1128 n.a. 1128 2000 60 60 n.a. 60 300 1128 300 60 1128 3.5 n.a. n.a. 50 25 n.a. n.a. Method SynT AnGrav SynT AnT AnTLcirX AnTLcirVal SynNonPcTc AnTLcirX AnTVal SynT AnTVal AnTLcirVal SynT SynVisVar SynVis SynVis SynVisVarPcTc SynT SynVis AnOth
Table 9 Binary systems: nitrogen + X. X 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] 2-Methyltetrahydrofuran -Pinene Dimethyl ether Dimethylether Ethane Ethanol Methanol 1-Propanol Oleic acid Poly(ethylene glycol) 1500 Poly(ethylene glycol) 4000 Poly(ethylene glycol) 8000 Poly(ethylene) (LDPE) Polyvinylidene uoride Vitamin K3 Water Reference Anthony et al. [83] Fischer and Wilken [129] Laursen et al. [50] Laursen et al. [38] Teodorescu Rasmussen [666] Wallbruch et al. [697] Raabe et al. [53] Raabe and Khler [573] Fischer and Wilken [129] Laursen and Andersen [434] Fischer and Wilken [129] Laursen et al. [50] Wiesmet et al. [33] Wiesmet et al. [33] Wiesmet et al. [33] Davis et al. [252] Grolier et al. [341] Knez and Skerget [425] Chapoy et al. [216] Mohammadi et al. [91] T (K) 298298 311311 298318 298318 278318 160276 209270 114138 298398 298318 298398 298318 323373 338373 353393 423423 411436 377383 274363 274283 P (MPa) 01.3 09 3.114.5 0.610.3 0.48.4 20.4200 1.19 0.73.2 09.2 0.63 09.9 3.214.6 4.919.2 6.220 5.817.8 0.66.5 0.1190 0.627.6 0.97.1 1945.3 V (cm3 ) n.a. n.a. 90 570 700 n.a. n.a. n.a. n.a. 570 n.a. 90 1000 1000 1000 72 36.3 14 28 150 Method AnGrav SynT AnTVcirX AnTValVis AnTVal SynVisVar AnTLcirBlo AnTLcirBlo SynT AnTValVis SynT AnTVcirX AnTCap AnTCap AnTCap SynT SynNon SynVis AnTValVis SynNon
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 10 Binary systems: oxygen + X. X 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] Acetonitrile (ethanenitrile) Dibutyl ether Methanol n-Octane 1-Propanol Toluene Water Reference Anthony et al. [83] Horstmann et al. [362] Fischer and Wilken [129] Fischer and Wilken [129] Fischer and Wilken [129] Fischer and Wilken [129] Fischer and Wilken [129] Mohammadi et al. [91] Tan et al. [69] T (K) 298298 305353 298298 298348 298348 298348 298348 273284 300300 P (MPa) 01.3 02.6 02.1 09.1 08.9 09.2 09 13.543.7 110 V (cm3 ) n.a. n.a. n.a. n.a. n.a. n.a. n.a. 150 500 Method
25
AnGrav SynT SynT SynT SynT SynT SynT SynNon AnPTSemX
Table 11 Binary systems: carbon monoxide + X. X 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] Carbon dioxide Cyclohexane Dichloromethane (HCC-30) n-Hexane Reference Anthony et al. [83] Ke et al. [411] Gao et al. [319] Jnasson et al. [386] Gao et al. [318] T (K) 298298 280298 344410 303363 501505 P (MPa) 01.3 8.19.9 1.55.1 0.47 33.3 V (cm3 ) n.a. n.a. 25 700 50 Method AnGrav SynNonPcTc SynT AnTVal SynVisVarPcTc
Table 12 Binary systems: nitrous oxide + X. X Biphenyl C.I. Disperse modied Yellow 119 C.I. Disperse Red 60 Dimethylterephthalate Fluoromethane (HFC-41) Reference Fischer et al. [297] Fischer et al. [297] Lin et al. [472] Tuma et al. [678] Fischer et al. [297] Fischer et al. [297] Di Nicola et al. [266] T (K) 388413 352352 353393 310310 314342 419419 283345 P (MPa) 0.113.2 013.6 1530 7130 0.17.5 014.3 0.14.9 V (cm3 ) n.a. n.a. 16.6 n.a. n.a. n.a. 105 Method SynNon SynVis AnPTSemY SynVisSpec SynNon SynVis SynOth
Table 13 Binary systems: methane + X. X 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] 2-Ethyl-hexyl-C8C10 2-Ethyl-hexyl-oleate Acenaphthene Carbon dioxide cis-Decahydronaphthaline (decalin) Decalin Ethane Ethanol Isobutyl-C12C14 Methanol n-Butane n-Hexane Reference Anthony et al. [83] Bureau et al. [193] Bureau et al. [193] Bureau et al. [193] Tobaly et al. [672] Webster and Kidney [703] Tohidi et al. [674] Tobaly et al. [672] Raabe et al. [53] Ukai et al. [681] Bureau et al. [193] Ukai et al. [681] Xia et al. [719] Dandekar and Stenby [250] Cebola et al. [206] Chylinski et al. [51] Uribe-Vargas and Trejo [682] Xia et al. [719] May et al. [507] Webster and Kidney [703] Randzio et al. [125] Machado and de Loos [488] Addicks et al. [147] Chapoy et al. [214] Chapoy et al. [214] T (K) 298298 363423 363423 363423 398453 230270 323423 294423 239270 280280 363423 280280 298298 311344 348383 348348 338338 310310 290293 230270 317322 337472 298298 283318 283293 P (MPa) 01.3 3060 3570 70100 4.6144.1 0.88.4 34.666.1 0.176.7 1.56.6 1.55.6 3060 2.16 5.412 11.512.6 2.319.6 2.211.6 0.310.3 2.16 5.38.6 09.2 30103.8 1.6193.1 7.317.8 0.934.6 1035 V (cm3 ) n.a. n.a. n.a. 220 2.49.3 n.a. 1 2.49.3 n.a. 134 n.a. 134 200360 80 n.a. 650 n.a. 200360 n.a. n.a. n.a. n.a. 450 34 34 Method AnGrav AnTVar AnTVar AnTVisVar AnSpecVar AnTVcir SynVis AnSpecVar AnTLcirBlo SynOthX AnTVar SynOthX AnTLcirVar SynVisVar AnTVLcirPc AnTVLcirValVis AnTVal AnTLcirVar SynNonVcirVar AnTVcir SynNon SynVisPcTc AnTVarVis AnTVal AnTVal
Propane Tetracosane Triacontane Water
26 Table 13 (Continued ) X Reference Chapoy et al. [218] Chapoy et al. [220] Chapoy et al. [220] Huo et al. [367] Kharrat and Dalmazzone [412] Kiepe et al. [415] Kim et al. [422] Link et al. [102] Mohammadi et al. [519] Mohammadi et al. [91] Ohmura et al. [547] Servio and Englezos [615] Song et al. [647] Wang et al. [700] Yang et al. [730] Yang et al. [730]
T (K) 275313 283318 283293 275275 281284 313373 276298 278293 282313 278278 273281 274284 196270 283303 298298 273286
P (MPa) 0.917.9 0.934.6 1035 3030 5.77.7 09.2 2.316.6 8.69.6 20.5 4.74.7 2.65.7 3.56.5 3.46.9 240 2.312.6 3.619.3
V (cm3 ) 34 34 34 1 n.a. n.a. n.a. 40 34 150 201 n.a. n.a. 540 n.a. n.a.
Method AnTVal AnTVal AnTVal AnTSpec SynNon SynT SynVisVar SynVis AnTValVis SynNon SynNon AnTVis AnPTSemY AnTVLcirVar AnTVcirVisVar AnTVcirVisVar
Table 14 Binary systems: ethane + X. X 1-Butanol 1-Decanol 1-Methylnaphthalene 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] 1-Propanol 2-Propanol (isopropanol) Acetone Adamantane Carbon dioxide Eicosane Ethanol Hydrogen chloride Lemon oil Limonene Linalool Methane N.N-Dimethylformamide n-Butane n-Decane N-Formyl morpholine n-Heptane n-Hexadecane n-Hexane Nitrogen Nitrous oxide n-Nonane n-Octacosane n-Octane n-Pentane n-Tetracosane Orange peel oil Reference Kodama et al. [428] Gardeler et al. [324] Shaver et al. [626] Anthony et al. [83] Kodama et al. [426] Kodama et al. [427] Mu et al. [524] Poot and de Loos [568] Horstmann et al. [356] Horstmann et al. [358] Gregorowicz [340] Mu et al. [524] Florusse and Peters [299] de la Fuente and Bottini [255] Raeissi and Peters [576] Raeissi and Peters [579] Raeissi et al. [577] Raeissi and Peters [578] Raabe et al. [53] Duran-Valencia et al. [277] Horstmann et al. [357] Gardeler et al. [324] Singh et al. [643] Jou et al. [391] Jou et al. [391] Singh et al. [643] du Rand and Nieuwoudt [273] Singh et al. [643] Raabe et al. [53] Raabe and Khler [573] Horstmann et al. [357] Singh et al. [643] du Rand and Nieuwoudt [273] Singh et al. [643] Mu et al. [525] Singh et al. [643] du Rand and Nieuwoudt [273] de Sousa et al. [256] de Sousa et al. [256] Raeissi and Peters [580] Martin et al. [500] Horstmann et al. [357] Nanu et al. [532] Horstmann et al. [358] Gregorowicz [339] Chapoy et al. [215] Kim et al. [422] Mohammadi et al. [518] Mohammadi et al. [519] Morita et al. [523] Song et al. [647] Wang et al. [700] T (K) 313313 448448 344344 283283 314314 308313 309309 293505 291305 298300 310370 309309 278324 298308 283357 273372 278368 280350 239270 264313 305424 410444 309324 298403 298403 310325 312352 308324 209270 114138 299309 312327 337352 308326 309309 306324 332352 282363 282363 284363 295373 305369 248472 300312 310350 278303 277298 274343 282293 298323 201281 283303 P (MPa) 2.35.4 0.514.3 0.114.2 01.3 1.65.5 2.15.3 4.84.9 0.3192.1 4.96.8 5.16.8 3.412.4 55.1 2.78.2 0.44.9 3.16.1 0.510.5 2.611.4 36 1.56.6 0.518.2 3.75.8 0.711.4 5.36.5 020.3 020.3 5.26.4 4.910.5 5.16 1.19 0.73.2 4.87.2 5.46.5 4.910.5 5.16.4 3.15 4.95.8 9.314.4 17.3 1.39.9 3.17.3 630 4.25 0.316.2 3.94.6 5.412.2 0.34.6 1.420.1 0.34.9 0.52.9 89479 3.43.4 0.54 V (cm3 ) 320 n.a. n.a. n.a. 320 320 2050 n.a. 10 10 43 2050 3.5 4080 n.a. 3.5 3.5 3.5 n.a. n.a. 10 n.a. 55 n.a. n.a. 55 132 55 n.a. n.a. 10 55 132 55 73 55 132 3.5 3.5 3.5 50 10 n.a. 10 43 34 n.a. 34 34 0.2 n.a. 600 Method AnTVLcirVal AnTVal AnTVcirVal AnGrav AnTVLcirVal AnTVLcirVal SynVisVarTc SynVisPcTc SynVisPcTc SynVisTc AnPTSemY SynVisVarTc SynVis SynVisVar SynVisPcTc SynVis SynVis SynVis AnTLcirBlo AnTVal SynVisTc AnTVal SynVisPcTc AnTVcir AnTVcir SynVisPcTc SynVis SynVisPcTc AnTLcirBlo AnTLcirBlo SynVisTc SynVisPcTc SynVis SynVisPcTc SynNonPcTc SynVisPcTc SynVis SynVis SynVis SynVis SynVisVar SynVisTc SynVis SynVisTc AnPTSemY AnTVal SynVisVar AnTValVis AnTValVis SynVisSpec AnPTSemY AnTVal
Poly(propylene glycol) Propane Squalane Sulfur hexauoride SF6 Tetracosane Water
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 15 Binary systems: propane + X. X 1,1,1,2,2-Pentauoroethane (HFC-125) Reference Bobbo et al. [184] Kim et al. [420] Lim et al. [468] Park and Jung [558] Takagi et al. [118] Bobbo et al. [182] Valtz et al. [685] Bobbo et al. [179] Bobbo et al. [180] Marteau et al. [499] Gardeler et al. [324] Marteau et al. [499] Lim et al. [467] Poot and de Loos [568] Skerget et al. [644] May et al. [117] Smejkal et al. [646] Webster and Kidney [703] Cruz Duarte et al. [238] Tobaly et al. [673] Bobbo et al. [183] Coquelet et al. [26] Coquelet et al. [26] Kim et al. [421] Lee et al. [440] Giles and Wilson [330] Horstmann et al. [360] Horstmann et al. [360] Schwarz and Nieuwoudt [605] Horstmann et al. [357] Joung et al. [396] Schwarz and Nieuwoudt [604] Schwarz and Nieuwoudt [604] Schwarz and Nieuwoudt [604] May et al. [507] Webster and Kidney [703] Joung et al. [396] Rovetto et al. [593] Tobaly et al. [673] Gardeler et al. [324] Horstmann et al. [357] Schwarz and Nieuwoudt [604] Tan et al. [663] Wiesmet et al. [33] Wiesmet et al. [33] Wiesmet et al. [33] Wiesmet et al. [33] Chan et al. [211] Chan et al. [212] Oliveira et al. [549] Tan et al. [663] Nanu et al. [532] Horstmann et al. [358] Giles and Wilson [330] Chan et al. [213] uszczyk and Radosz [485] Schwarz and Nieuwoudt [604] Schwarz and Nieuwoudt [604] Schwarz and Nieuwoudt [604] Wang et al. [699] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Chapoy et al. [219] Makogon [495] Mooijer-van et al. [522] Song et al. [647] T (K) 258303 253323 268313 273313 243333 278308 293353 283313 283323 394419 408448 394444 273303 301503 303353 310310 295354 230270 277368 392439 248294 278343 342344 253323 268318 273323 313313 298313 378408 305369 313349 378408 378408 378408 290293 230270 313343 312450 373443 419457 309369 378408 303453 323393 303393 333393 353393 453453 302453 368403 303453 263473 318369 283333 300433 312435 378408 378408 378408 383408 303353 323378 303353 308318 313353 367375 277368 278278 276278 211276 P (MPa) 0.21.8 0.22.8 0.42.2 0.42 0.23.8 0.21.2 0.43.3 0.11.3 0.11.7 2.97 0.36.2 0.77.3 0.11 0.310 9.631.1 2.72.8 6.28.4 03.1 0.43.8 1.77.7 0.21.9 0.55.4 5.25.5 0.23.6 0.43.2 0.21.7 0.91.3 0.51.3 4.69.3 4.25 0.32.8 8.214.2 6.211.6 4.39.9 5.38.6 09.2 0.22.5 1.29.7 0.68.7 0.47.6 4.27.2 4.610 36.3132.9 0.118 0.824.6 0.925 1.125 44.644.8 18140 1926.3 35.7154.6 0.111.9 3.74.2 02.1 4.3120.8 2118.9 5.111 7.413.6 5.211.4 1035.2 0.410.9 0.826.5 0.914.4 0.50.8 1.110.6 0.726.5 0.33.9 0.535 0.39.8 0.81.1 V (cm3 ) n.a. 150 85 128 n.a. 50 n.a. 50 50 2.49.3 n.a. 2.49.3 85 n.a. 120 185 35 n.a. 3.5 2.49.3 n.a. n.a. n.a. 150 85 300 n.a. n.a. 40 10 50 40 40 40 n.a. n.a. 50 3.5 2.49.3 n.a. 10 40 10 1000 1000 1000 1000 10 10 28 10 n.a. 10 300 10 10 40 40 40 88 120 14 120 14 120 14 28 160210 n.a. n.a. Method
27
1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,2,3,3-Hexauoropropane (HFC-236ea) 1,1,1,3,3,3-Hexauoropropane (HFC-236fa) 1,2,3,4-Tetrahydronaphthalene 1-Decanol 1-Methylnaphthalene 2-Methylpropane (isobutane) Adamantane -Tocopherol Carbon dioxide
Cyclobutanone Decahydronaphthalene (decalin) Diuoromethane (HFC-32)
Dimethyl ether
Dotriacontane Ethane Ethanol Hexacontane Hexatetracontane Hexatriacontane Methane Methanol Methyl palmitate Naphthalene n-Dodecane Nitrous oxide Octatriacontane Poly (4-methyl styrene) Poly(ethylene glycol) 1500 Poly(ethylene glycol) 200 Poly(ethylene glycol) 4000 Poly(ethylene glycol) 8000 Poly(ethylene-co-hexene-1) Poly(ethylene-co-octene-1) Poly(propylene) Polystyrene Squalane Sulfur hexauoride SF6 tert-Butyl mercaptan Tetracontane
Tetrapentacontane Tetratetracontane Titanocene dichloride Vitamin D2 Vitamin D3 Vitamin K3 Water
AnTVcirVis AnTVcirVis AnTVLcirVis AnTVcir SynNon AnTVcirVis AnTValVis AnTVcirVis AnTVcirVis AnSpecVar AnTVal AnSpecVar AnTVLcirVis SynVisPcTc AnT SynNonVcirVar SynVisPcTc AnTVcir SynVis AnSpecVisVar AnTVcirVis AnTValVis AnTValVisVar AnTVcirVis AnTVLcirVis SynT AnTValVis SynT SynVisVar SynVisTc AnTVLcirValVis SynVisVar SynVisVar SynVisVar SynNonVcirVar AnTVcir AnTVLcirValVis SynVisVar AnSpecVisVar AnTVal SynVisTc SynVisVar SynVisVarPc AnTCap AnTCap AnTCap AnTCap SynVisVarPc SynVisVar SynVisVar SynVisVarPc SynVis SynVisTc SynT SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar AnPTSemY AnT SynVis AnT SynVis AnT SynVis AnTValVis SynVisVar SynVis AnPTSemY
28 Table 16 Binary systems: n-butane + X. X 1,1-Diuoroethane (HFC-152a) Adamantane Diamantane Ethane Ethyl mercaptan Methane Poly(propylene) Poly(propylene) (metallocene) Poly(propylene) (Ziegler Natta) Water Reference
T (K) 283313 285493 343523 305424 323373 311344 358423 358423 358423 622695
P (MPa) 0.12.4 0.25.7 0.86.9 3.75.8 0.11.5 11.512.6 1.211.4 1.711 1.711 23.2306
V (cm3 ) 163 n.a. n.a. 10 300 80 28 27 27 60.13
Method AnTVLcirValVis SynVisVar SynVisVar SynVisTc SynT SynVisVar SynVisVar SynVisVar SynVisVar SynVis
Shimawaki and Fujii [632] Poot et al. [565] Poot et al. [565] Horstmann et al. [357] Giles and Wilson [330] Dandekar and Stenby [250] Oliveira et al. [549] Ndiaye et al. [534] Ndiaye et al. [534] Tian et al. [669]
Table 17 Binary systems: n-hexane + X. X 1-Propanol 2-Propanol (isopropanol) Carbon dioxide Carbon monoxide Ethane Ethanol FCC-DO (PAHs mixture) Hexatriacontane Hydrogen Methane Reference Oh et al. [543] Seo et al. [611] Liu et al. [473] Gao et al. [318] Singh et al. [643] Seo et al. [609] Kim et al. [420] Joyce et al. [397] Gao et al. [318] Gao et al. [319] Cebola et al. [206] Chylinski et al. [51] Uribe-Vargas and Trejo [682] Xia et al. [719] Liu et al. [473] Belonenko et al. [169] Drozd-Rzoska et al. [114] Chen et al. [229] Chen et al. [229] Chen et al. [229] Joyce et al. [397] Abdulagatov et al. [145] Kamilov et al. [399] T (K) 483513 483503 304507 501505 308324 473503 493553 521621 504505 344410 348383 348348 338338 310310 480512 298298 285297 393473 373473 373473 473622 643651 395494 P (MPa) 243.4 2.14.5 311.7 33.3 5.16 18.155.6 1.14.3 0.76.4 33.1 1.26.2 2.319.6 2.211.6 0.310.3 2.16 38.1 31148 0112 0.67.2 0.48.2 0.44.7 0.65.1 835 0.65.2 V (cm3 ) 100 100 18 50 55 100 100 12 50 25 n.a. 650 n.a. 200360 18 0.8 n.a. 620 620 620 12 n.a. n.a. Method AnTVLcirValVisPc AnTVLcirVisPc SynVis SynVisVarPcTc SynVisPcTc AnTVLcirVis AnPTConVis AnPTConVis SynVisVarPcTc SynT AnTVLcirPc AnTVLcirValVis AnTVal AnTLcirVar SynVis SynNonVar SynNon SynVisVar SynVisVar SynVisVar AnPTConVis SynOthPcTc SynNon
Methanol n-Hexadecane Nitrobenzene Poly(ethylene) (LDPE) Poly(ethylene) 108k Poly(ethylene) 15k Tetracosane Water
Table 18 Binary systems: ethene + X. X 1-Decanol 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] 1-Propanol Benzene Eicosane Impact poly(propylene) copolymer (ICPPP) N,N-Dimethylformamide Poly(ethylene) Poly(ethylene) (LDPE) Poly(ethylene) (LLDPE) Poly(ethylene-co-octene-1) Poly(ethylene-co-propylene) Tetracosane Reference Gardeler et al. [324] Anthony et al. [83] Kodama et al. [116] Kodama et al. [116] Liu et al. [478] Gregorowicz [340] Sato et al. [78] Duran-Valencia et al. [277] Moore and Wanke [86] Davis et al. [252] Trumpi et al. [675] Chan et al. [210] de Vries et al. [257] Gregorowicz [339] T (K) 308318 298323 283283 283283 282563 287348 323363 293323 301361 423423 395440 385453 312342 330350 P (MPa) 112.4 01.3 2.25.4 5.15.7 511.5 4.615.8 0.33 0.718.7 0.13.5 0.66.5 139.8172.5 18166.8 141.3218.1 4.914 V (cm3 ) n.a. n.a. 320 78134 n.a. 43 90 n.a. n.a. 72 n.a. 10 n.a. 43 Method AnTVal AnGrav AnTVLcirValVis SynNonVLcirVisVar SynVisPcTc AnPTSemY SynT AnTVal AnGrav SynT SynVis SynVisVar SynVis AnPTSemY
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 19 Binary systems: propene + X. X 1,1,1,2-Tetrauoroethane (HFC-134a) 2,2,4,6,6-Pentamethylheptane Acetophenone Benzene Carbon dioxide Cumene Dichloromethane (HCC-30) Dimethyl ether Impact poly(propylene) copolymer (ICPPP) Poly(propylene) Toluene Table 20 Binary systems: 1-butene + X. X Dichloromethane (HCC-30) Poly(ethylene) Poly(propylene) Poly(propylene) (metallocene) Poly(propylene) (Ziegler Natta) Table 21 Binary systems: methanol + X. X Carbon dioxide Reference Bezanehtak et al. [173] Elbaccouch and Elliot [279] Joung et al. [394] Laursen et al. [38] Liu et al. [473] Yeo et al. [732] Teodorescu Rasmussen [666] Bezanehtak et al. [173] dAngelo [242] Ukai et al. [681] Xia et al. [719] Liu et al. [473] Laursen and Andersen [434] Fischer and Wilken [129] Joung et al. [396] Bazaev et al. [166] Yokoyama and Uematsu [733] T (K) 278308 313313 313342 298313 304512 298423 353353 278308 314476 280280 298298 480512 298318 298348 313343 373673 320420 P (MPa) 1.57.4 1.17.5 612.4 1.26.3 7.416.3 5.816.4 0.12.2 211 4.410.9 2.16 5.412 38.1 0.63 09.1 0.22.5 090.9 01.3 V (cm3 ) 60 40 50 570 18 26.7 700 60 1128 134 200360 18 570 n.a. 50 n.a. 1624 Method Reference Jnasson et al. [386] Moore and Wanke [86] Oliveira et al. [549] Ndiaye et al. [534] Ndiaye et al. [534] T (K) 303363 301361 358423 348422 348422 P (MPa) 0.11.1 0.11.2 1.413.3 1.713.5 1.713.5 V (cm3 ) 700 n.a. 28 27 27 Method Reference Ho et al. [353] Dariva et al. [251] Horstmann et al. [361] Guo et al. [345] Wang et al. [698] Ke et al. [411] Wang et al. [698] Jnasson et al. [386] Horstmann et al. [360] Horstmann et al. [360] Sato et al. [78] Oliveira et al. [549] Sato et al. [78] Dariva et al. [251] T (K) 273313 299328 323323 453543 364562 305343 562631 303363 313313 313313 323363 368388 323363 299328 P (MPa) 0.21.9 0.10.5 02 1.56 4.66.7 67.1 3.34.8 0.22 0.81.6 0.81.6 0.23 2226.7 0.23.6 0.10.5 V (cm3 ) 85 23 n.a. 500 18 n.a. 18 700 n.a. n.a. 90 28 90 23 Method
29
AnTVLcirVis SynT SynT AnTCap SynVisPcTc SynVisVarPcTc SynVisPcTc AnTVal AnTValVis SynT SynT SynVisVar SynT SynT
AnTVal AnGrav SynVisVar SynVisVar SynVisVar
Dimethyl ether Hydrogen Methane n-Hexane Nitrogen Oxygen Propane Water
AnTLcirVal AnTVLcirVal AnTVLcirValVisPc AnTValVis SynVis SynVisVar AnTVal AnTLcirVal SynT SynOthX AnTLcirVar SynVis AnTValVis SynT AnTVLcirValVis SynOthPcTc SynNonVar
Table 22 Binary systems: ethanol + X. X 1-Butyl-3-methylimidazoium hexyuorophosphate [bmim][PF6] Acetic acid (ethanoic acid) Carbon dioxide Reference Najdanovic-Visak et al. [103] Hu et al. [364] Bae et al. [158] Chen et al. [223] Elbaccouch and Elliot [279] Galicia-Luna et al. [47] Joung et al. [394] Stuart et al. [654] Tsivintzelis et al. [676] Vega-Gonzalez et al. [692] Yeo et al. [732] Elbaccouch and Elliot [279] Dahlhoff et al. [248] Elbaccouch et al. [280] Mu et al. [524] Hu et al. [364] dAngelo and Francesconi [242] Ukai et al. [681] Seo et al. [610] Seo et al. [609] Fischer and Wilken [129] Seo et al. [608] Joung et al. [396] T (K) 284325 516590 314314 323323 323333 312373 313344 313313 313328 314324 298413 343382 300463 332373 309309 515523 299476 280280 483523 473503 298398 422500 313349 P (MPa) 0.140.1 5.77.5 5.57.9 58.2 0.79.4 0.414.3 5.411.9 4.87.5 1.69.4 78.2 6.115.1 0.54.8 02.2 0.13.1 55.1 3.96.2 3.79 1.55.6 1.15.6 18.155.6 09.2 0.95.7 0.32.8 V (cm3 ) 1 18 25 100 40 40 50 28 202.1 9 26.71 40 70 40 2050 18 1128 134 100 100 n.a. 100 50 Method SynVisVar SynVis SynVisVar AnTVcirVis AnTVLcirVal AnTCapValVis AnTVLcirValVisPc SynVisVar AnTVLcirValVis SynVisVar SynVisVar AnTVLcirVal SynT AnTVLcirVal SynVisVarTc SynVis SynT SynOthX AnTVLcirVis AnTVLcirVis SynT AnTVLcirVisPcTc AnTVLcirValVis
Chlorodiuoromethane (HCFC-22) Cyclohexanone oxime Dimethyl ether Ethane Ethyl acetate Hydrogen Methane n-Heptane n-Hexane Nitrogen n-Pentane Propane
30 Table 23 Binary systems: dimethyl ether + X. X 1,1,1,2,2-Pentauoroethane (HFC-125) 1,1,1,2,3,3-Hexauoropropane (HFC-236ea) 1,1,1,3,3,3-Hexauoropropane (HFC-236fa) 2-Methylpropane (isobutane) 2-Propanol (isopropanol) Argon Carbon dioxide Ethanol Ethyl cellulose Krypton Methanol Nitrogen Nitrogen n-Propyl acetate Poly(d,l-lactide) Poly(d,l-lactide-co-glycolide) Propane
Reference Bobbo et al. [184] Bobbo et al. [179] Bobbo et al. [179] Bobbo et al. [176] Elbaccouch and Elliot [281] Wallbruch et al. [697] Laursen et al. [38] Elbaccouch et al. [280] Li and McHugh [458] Wallbruch et al. [697] Teodorescu Rasmussen [666] Laursen et al. [38] Teodorescu Rasmussen [666] Wallbruch et al. [697] Daiguji and Hihara [249] Kuk et al. [431] Kuk et al. [431] Giles and Wilson [330] Horstmann et al. [360] Horstmann et al. [360] Horstmann et al. [360] Horstmann et al. [360] Florusse et al. [298] Knez and Skerget [425] Knez and Skerget [425] Knez and Skerget [425] Wallbruch et al. [697]
T (K) 258303 283313 283283 280320 323373 157267 298320 332373 314432 130149 353353 298318 278318 160276 253443 327375 303373 273323 313313 298313 313313 313313 288450 378380 289289 341366 130206
P (MPa) 0.11.5 0.10.8 0.10.3 0.21 0.11.5 23.5202 0.67.3 0.13.1 120 20.6138 0.12.2 0.610.3 0.48.4 20.4200 0.13.9 1.613.8 8.561.3 0.21.7 0.91.3 0.51.3 0.81.6 0.81.6 0.910 0.30.6 0.30.3 0.81.6 19.2167
V (cm3 ) n.a. 50 50 50 40 n.a. 570 40 28 n.a. 700 570 700 n.a. 156 31 31 300 n.a. n.a. n.a. n.a. 3.5 14 14 14 n.a.
Method AnTVcirVis AnTVcirVis AnTVcirVis AnTVcirVis AnTVLcirVal SynVisVar AnTValVis AnTVLcirVal SynVisVar SynVisVar AnTVal AnTValVis AnTVal SynVisVar SynT SynVisVar SynVisVar SynT AnTValVis SynT AnTValVis SynT SynVis SynVis SynVis SynVis SynVisVar
Propene Tripalmitin Vitamin D2 Vitamin D3 Vitamin K3 Xenon
Table 24 Binary systems: chlorodiuoromethane (HCFC-22) + X. X Ethanol Ethyl cellulose Poly(d,l-lactide) Poly(d,l-lactide-co-glycolide) Poly(dimethylsiloxane) (PDMS) Poly(l-lactide) Poly(methyl methacrylate) (PMMA) Polystyrene Reference Elbaccouch and Elliot [279] Li and McHugh [458] Kuk et al. [432] Lee et al. [443] Lee et al. [443] Pfohl et al. [132] Lee et al. [443] Boudouris et al. [44] Boudouris et al. [44] T (K) 343382 305403 338383 346392 313383 298343 334393 308348 308358 P (MPa) 0.54.8 226 315.6 4.215.7 3.431.4 00.2 3.220.2 0.12 0.13.9 V (cm3 ) 40 28 31 31 31 345 31 n.a. n.a. Method AnTVLcirVal SynVisVar SynVisVar SynVisVar SynVisVar SynTVis SynVisVar AnOth AnOth
Table 25 Binary systems: triuoromethane (HFC-23) + X. X 1,1,1,2,2-Pentauoroethane (HFC-125) 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,2-Tetrauoroethane (HFC-134a) 1,1,1-Triuoroethane (HFC-143a) 1,1-Diuoroethane (HFC-152a) 1-Ethyl-3-methylimidazolium hexauorophosphate Carbon dioxide Diuoromethane (HFC-32) Naphthalene Poly(d,l-lactide) Sulphur hexauoride Reference Lim et al. [463] Lim et al. [464] Lim et al. [464] Lim et al. [465] Lim et al. [465] Shariati and Peters [622] Di Nicola et al. [142] Lim et al. [463] Diefenbacher and Trk [267] Kuk et al. [432] Diefenbacher and Trk [268] T (K) 283293 283293 283293 283293 283293 308367 252285 283293 345346 303373 265295 P (MPa) 0.94.1 0.24.2 0.44.2 0.84.2 0.34.2 1.651.6 1.53.8 1.14.1 9.220.6 4984.7 1.64.3 V (cm3 ) 85 85 85 85 85 3.5 251 85 1310 31 1406 Method AnTVLcirVis AnTVLcirValVis AnTVLcirValVis AnTVLcirValVis AnTVLcirValVis SynVisVar SynOth AnTVLcirVis SynVis SynVisVar AnTVis
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 26 Binary systems: diuoromethane (HFC-32) + X. X 1,1,1,2,2-Pentauoroethane (HFC-125) Reference Horstmann et al. [359] Jung et al. [398] Kato et al. [407] Kato et al. [408] Weber [702] Koo et al. [429] Park et al. [555] Bobbo et al. [177] Deiters [258] Di Nicola et al. [261] Lim et al. [462] Kim and Park [419] Abbott et al. [94] Hansen et al. [348] Hansen et al. [348] Di Nicola et al. [263] Diefenbacher and Trk [101] Diefenbacher and Trk [268] Rivollet et al. [587] Li and McHugh [458] Abbott et al. [94] Abbott et al. [94] Abbott et al. [94] Abbott et al. [94] Abbott et al. [94] Abbott et al. [94] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Tesser et al. [668] Tesser et al. [668] Abbott et al. [94] Kuk et al. [432] Bobbo et al. [183] Coquelet et al. [26] Coquelet et al. [26] Kim et al. [421] Lee et al. [440] Abbott et al. [94] Abbott et al. [94] Valtz et al. [35] Diefenbacher and Trk [268] Lim et al. [463] T (K) 308308 268308 318349 318349 294333 298312 283303 288318 254364 303323 263313 363363 313343 328358 287294 304351 280318 283343 392450 363363 363363 363363 363363 363363 363363 323363 303363 303363 238323 239277 363363 305375 248294 278343 342344 253323 268318 363363 363363 288403 265310 283293 P (MPa) 1.72.1 0.52.1 2.35.5 2.35.5 1.43.9 0.42.4 0.21.9 0.12.7 0.11.9 0.73.1 0.42.4 7.922 5.826.2 5.514.8 1.33.5 5.77.4 1.67.5 1.17.4 75115 8.925.2 1024.8 6.922 8.918.8 13.522.1 12.225.8 0.11.7 0.11.7 0.21.9 0.13.1 0.10.1 8.924 3355.5 0.21.9 0.55.4 5.25.5 0.23.6 0.43.2 918 1424.1 0.47.3 1.23.9 1.14.1 V (cm3 ) n.a. 128 n.a. n.a. 550 320 85 50 254.8 85 128 25 n.a. n.a. 254.8 1406 1406 n.a. 28 25 25 25 25 25 25 n.a. n.a. n.a. n.a. n.a. 25 31 n.a. n.a. n.a. 150 85 25 25 n.a. 1406 85 Method
31
1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,2,3,3-Hexauoropropane (HFC-236ea)
1,1,1,2-Tetrauoroethane (HFC-134a) 1,1,1-Triuoroethane (HFC-143a) Anthracene -Carotene Capsaicin Carbon dioxide
Ethyl cellulose m-Hydroxybenzoic acid o-Chlorobenzoic acid p-Aminobenzoic acid p-Aminophenol p-Chlorobenzoic acid p-Chlorophenol Pentaerythritol tetra-2-ethylbutanoate Pentaerythritol tetra-2-ethylhexanoate Pentaerythritol tetranonanoate Peruoropolyether lubricant oil Fomblin YLOX100 Peruoropolyether lubricant oil Fluorolink D10H p-Hydroxybenzoic acid Poly(d,l-lactide) Propane
p-Toluic acid Salicylic acid Sulphur dioxide Sulphur hexauoride Triuoromethane (HFC-23)
SynT AnTVcir AnTVisPcTc AnTVisPcTc AnTVLcir AnTVLcirValVis AnTVLcirVis AnTVcirVis Comments SynT AnTVLcirValVis AnTVcirVis AnOth AnSpecY AnPTSemYVal SynT SynVisPcTc SynVisPcTc AnTValVis SynVisVar AnOth AnOth AnOth AnOth AnOth AnOth AnT AnT AnT SynOthVis SynOthVis AnOth SynVisVar AnTVcirVis AnTValVis AnTValVisVar AnTVcirVis AnTVLcirVis AnOth AnOth AnTCapValVis AnTVis AnTVLcirVis
Table 27 Binary systems: 1,1,1,2,2-pentauoroethane (HFC-125) + X. X 1,1,1,2,3,3-Hexauoropropane (HFC-236ea) Reference Bobbo et al. [177] Deiters [258] Di Nicola et al. [261] Di Nicola et al. [262] Lim et al. [463] Lee et al. [439] Di Nicola et al. [263] Horstmann et al. [359] Jung et al. [398] Kato et al. [407] Kato et al. [408] Weber [702] Bobbo et al. [184] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Otake et al. [554] Tesser et al. [668] Bobbo et al. [184] Kim et al. [420] Lim et al. [468] Park and Jung [558] Takagi et al. [118] Lim et al. [463] Uchida et al. [680] Widiatmo et al. [706] T (K) 288318 254364 253372 293293 293313 284304 308308 268308 318349 318349 294333 258303 32336 303363 302363 339406 273313 258303 253323 268313 273313 243333 283293 339377 279349 P (MPa) 0.12.2 0.11.9 0.12.3 0.51.2 0.32 1.63.3 1.72.1 0.52.1 2.35.5 2.35.5 1.43.9 0.11.5 0.11.7 0.11.8 02.1 2.83.7 0.11.8 0.21.8 0.22.8 0.42.2 0.42 0.23.8 0.94.1 3.63.7 0.42.5 V (cm3 ) 50 254.8 254.8 85 80 254.8 n.a. 128 n.a. n.a. 550 n.a. n.a. n.a. n.a. 16 n.a. n.a. 150 85 128 n.a. 85 16 n.a. Method AnTVcirVis Comments SynT SynT AnTVLcirVis AnTVLcirVal SynT SynT AnTVcir AnTVisPcTc AnTVisPcTc AnTVLcir AnTVcirVis AnT AnT AnT SynVisVarPcTc SynOthVis AnTVcirVis AnTVcirVis AnTVLcirVis AnTVcir SynNon AnTVLcirVis SynVisVarPcTc SynVisVar
1,1,1,3,3,3-Hexauoropropane (HFC-236fa) 1,1-diuoroethane (HFC-152a) 2-Methylpropane (isobutane) Carbon dioxide Diuoromethane (HFC-32)
Dimethyl ether Pentaerythritol tetra-2-ethylbutanoate Pentaerythritol tetra-2-ethylhexanoate Pentaerythritol tetranonanoate Pentauoromethoxyethane Peruoropolyether lubricant oil fomblin ylox100 Propane
Triuoromethane (HFC-23) Triuoromethoxymethane Triuoromethyl methyl ether (HFC-143m)
32 Table 28 Binary systems: 1,1,1,2-tetrauoroethane (HFC-134a) + X. X 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,3,3,3-Hexauoropropane (HFC-236fa) 1,1,1,3,3-Pentauoropropane (HFC-245fa) 1,1,1-Triuoroethane (HFC-143a) 1,1-Diuoroethane (HFC-152a) 1-Chloro-2,2,2-triuoroethane (HCFC-133a) -Carotene Capsaicin Carbon dioxide Diuoromethane (HFC-32) Heptylbenzene Oleic acid Pentaerythritol tetra-2-ethylbutanoate Pentaerythritol tetra-2-ethylhexanoate Pentaerythritol tetranonanoate Pentauoromethoxyethane Peruoropolyether lubricant oil Fomblin YLOX100 Peruoropolyether lubricant oil Fluorolink D10H Phenyloctane Poly(d,l-lactide) Polyalkylene glycol Propene Squalene Triethylene glycol dimethyl ether Triuoromethane (HFC-23) Triuoromethoxymethane Triuoromethyl methyl ether (HFC-143m)
Reference Koo et al. [429] Park et al. [555] Di Nicola et al. [262] Bobbo et al. [181] Kim et al. [49] Lim et al. [466] Shimawaki et al. [631] He et al. [351] Hansen et al. [348] Hansen et al. [348] Duran-Valencia et al. [276] Silva-Oliver et al. [641] Lim et al. [462] Poot and de Loos [566] Catchpole and Proells [205] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Otake et al. [554] Tesser et al. [668] Tesser et al. [668] Poot and de Loos [567] Kuk et al. [432] Park et al. [559] Ho et al. [353] Catchpole and Proells [205] Coronas et al. [237] Lim et al. [464] Uchida et al. [680] Widiatmo et al. [706]
T (K) 298312 303323 253372 293313 263313 273313 263293 300357 313343 308328 252292 329354 303323 258414 303363 323363 303363 302363 374406 239323 239248 259398 302373 253333 273313 303353 283353 283293 374377 279349
P (MPa) 0.40.9 0.51.3 0.12.3 0.11 0.21.8 0.21.8 0.21.3 0.22.6 6.434.3 10.318.8 0.12 1.97.3 0.73.1 0.112.1 420 0.11 01 0.11.2 2.84 0.11.2 0.10.1 0.112.4 21.740.1 01.6 0.21.9 66 02.2 0.44.2 3.64 0.32.3
V (cm3 ) 320 85 254.8 50 128 85 163 25 n.a. n.a. 50 40 85 n.a. n.a. n.a. n.a. n.a. 16 n.a. n.a. n.a. 31 72 85 n.a. 149 85 16 n.a.
Method AnTVLcirValVis AnTVLcirVis SynT AnTVcir AnTVcirBloVis AnTVLcirVis AnTVLcirValVis SynVis AnSpecY AnPTSemYVal AnTVal AnTValVis AnTVLcirValVis SynVis AnPTCon AnT AnT AnT SynVisVarPcTc SynOthVis SynOthVis SynVisPcTc SynVisVar SynVis AnTVLcirVis AnPTCon SynT AnTVLcirValVis SynVisVarPcTc SynVisVar
Table 29 Binary systems: 1,1,1-triuoroethane (HFC-143a) + X. X 1,1,1,2-Tetrauoroethane (HFC-134a) 1,1,1,3,3,3-Hexauoropropane (HFC-236fa) 1,1-Diuoroethane (HFC-152a) 2-Methylpropane (isobutane) -Carotene Diuoromethane (HFC-32) Pentaerythritol tetra-2-ethylbutanoate Pentaerythritol tetra-2-ethylhexanoate Pentaerythritol tetranonanoate Peruoropolyether lubricant oil Fomblin YLOX100 Peruoropolyether lubricant oil Fluorolink D10H Triuoromethane (HFC-23) Reference Lim et al. [466] Kim et al. [49] Bobbo et al. [178] Lim et al. [466] Lim et al. [462] Hansen et al. [348] Kim and Park [419] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Wahlstrm and Vamling [695] Tesser et al. [668] Tesser et al. [668] Lim et al. [465] T (K) 273313 263313 283313 273313 323333 313343 263313 323363 303363 303363 237323 239239 283293 P (MPa) 0.21.8 0.21.8 0.11.8 0.21.8 0.62.8 6.133.2 0.42.4 0.11.9 0.11.8 0.11.9 0.12.2 0.10.1 0.84.2 V (cm3 ) 85 128 50 85 85 n.a. 128 n.a. n.a. n.a. n.a. n.a. 85 Method AnTVLcirVis AnTVcirBloVis AnTVcirVis AnTVLcirVis AnTVLcirValVis AnSpecY AnTVcirVis AnT AnT AnT SynOthVis SynOthVis AnTVLcirValVis
Table 30 Binary systems: 1,1-diuoroethane (HFC-152a) + X. X 1,1,1,2,2-Pentauoroethane (HFC-125) 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,2-Tetrauoroethane (HFC-134a) 1,1,1-Triuoroethane (HFC-143a) Ethyl cellulose n-Butane Pentaerythritol tetranonanoate Poly(methyl methacrylate) (PMMA) Polystyrene Triuoromethane (HFC-23) References. Lim et al. [463] Park et al. [555] Shimawaki et al. [631] Lim and McHugh et al. [466] Li and McHugh [458] Shimawaki and Fujii [632] Wahlstrm and Vamling [695] Boudouris et al. [44] Boudouris et al. [44] Lim et al. [465] T (K) 293293 283303 263293 273313 392450 283313 303363 308348 308348 283293 P (MPa) 0.51.2 0.20.6 0.21.3 0.21.8 5578 0.12.4 0.11 0.11.7 0.11.7 0.34.2 V (cm3 ) 85 85 163 85 28 163 n.a. n.a. n.a. 85 Method AnTVLcirVis AnTVLcirVis AnTVLcirValVis AnTVLcirVis SynVisVar AnTVLcirValVis AnT AnOth AnOth AnTVLcirValVis
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 31 Binary systems: X + Y. X 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,2,3,3-Hexauoropropane (HFC-236ea) 1-Chloro-1,1-diuoroethane 1-Hexene 2-Methyl-1-propanol (isobutanol) Y 2-Methylpropane (isobutane) Pentauoromethoxyethane Pentauoromethoxyethane Ethyl cellulose Poly(ethylene) 1-Butyl-3-methylimidazoium bis(triuoromethylsulfonyl)amide [bmim][NTf2] 1,1,1,3,3-Pentauoropropane (HFC-245fa) Acetonitrile (ethanenitrile) Diamantane Acetonitrile (ethanenitrile) Titanyl phthalocyanine 1-n-Butyl-3-methylimidazolium hexauorophosphate [bmim][PF6] Vitamin K3 Cumene Ethylbenzene 1-Amino-4-hydroxy-2-phenoxy9,10-anthraquinone (C, I, Disperse Red 60) Eicosane n-Hexadecane n-Octadecane n-Tridecane Deuterium oxide Quinoline Biphenyl Dimethylterephthalate n-Eicosane n-Octacosane Polystyrene 1-Octanol Polystyrene 2-Propanol (isopropanol) 1-Octanol 1-Propanol 1-Octanol Polystyrene Poly(dimethylsiloxane) (PDMS) 1-Octanol Polystyrene n-Alkane mixture n-Tetradecane Polystyrene perdeuterated 90 000 Polystyrene perprotonated 90 000 Polystyrene perdeuterated 90 000 Polystyrene perprotonated 13 000 Polystyrene perprotonated 130 000 Polystyrene perprotonated 26 600 Polystyrene perprotonated 30 000 Polystyrene perprotonated 90 000 Poly(hexylmethylsiloxane) 2-Methylpentane 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1-Amino-4-hydroxy-2-phenoxy9,10-anthraquinone (C,I, Disperse Red 60) quinoline Hydrogen chloride 2-Methylpropane (isobutane) 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,2,3,3-Hexauoropropane (HFC-236ea) Polyvinylidene uoride Reference Lee et al. [439] Otake et al. [554] Otake et al. [554] Li and McHugh [458] Moore and Wanke [86] Najdanovic-Visak et al. [103] T (K) 303323 375406 406412 340430 301361 284303 P (MPa) 0.41 2.82.9 2.83.4 2082 0.10.2 0.14.4 V (cm3 ) Method 80 16 16 28 n.a. 1 AnTVLcirVal SynVisVarPcTc SynVisVarPcTc SynVisVar AnGrav SynVisVar
33
2-Methylpropane (isobutane)
Bobbo et al. [181] Uusi-Kyyny and Liukkonen [683] van Miltenburg et al. [690] Uusi-Kyyny and Liukkonen [683] Sue et al. [30] Anthony et al. [83] Knez and Skerget [425] Wang et al. [698] Al-Ghamdi and Kabadi [150] Tuma et al. [678]
293313 358358 328503 358358 508553 298298 375378 364631 453553 310310
0.10.6 0.11.4 0.77.8 0.11.3 4.726.1 01.3 0.719.8 3.38 0.34.2 7130
50 66 n.a. 66 17.4 n.a. 14 18 590 n.a.
AnTVcir AnTLcirVal SynVis AnTLcirVal AnTBlo AnGrav SynVis SynVisPcTc AnPTCon SynVisSpec
2-Methylpropene Acetone Argon
Benzene Chlorotriuoromethane (CFC-13)
Cyclohexane
Deuterium Ethylbenzene Helium Methyl 1,1-dimethylethyl ether n-Decane n-Dodecane n-Heptane n-Hexadecane n-Hexane n-Octane n-Pentane n-Tetradecane n-Tridecane Perdeuterated nitroethane Perprotonated nitroethane
Poly(dimethylsiloxane) Propylene oxide Sulfur dioxide Sulfur hexauoride
Domanska and Morawski [269] Domanska and Morawski [269] Domanska and Morawski [269] Domanska and Morawski [269] Morris et al. [93] Zhao and Kabadi [743] Fischer et al. [297] Fischer et al. [297] Domanska and Morawski [115] Domanska and Morawski [115] Imre et al. [373] Yang et al. [728] Imre et al. [373] Oh et al. [544] Yang et al. et al. [100] Oh et al. [543] Yang et al. [728] Imre et al. [373] Pfohl et al. [132] Yang et al. [100] Imre et al. [373] Daridon et al. [106] Daridon et al. [106] de Sousa and Rebelo [109] de Sousa and Rebelo [109] de Sousa and Rebelo [109] de Sousa and Rebelo [109] de Sousa and Rebelo [109] de Sousa and Rebelo [109] de Sousa and Rebelo [109] de Sousa and Rebelo [109] Imre et al. [374] Horstmann et al. [359] Valtz et al. [689] Tuma et al. [678]
313363 293353 303353 293353 446583 498653 342352 413425 313353 313353 284288 263293 293300 483523 275332 483513 262292 275279 308423 263313 302306 301321 270290 308312 336341 286288 265345 318323 268270 289298 309317 320379 323323 288403 310310
16.2523.1 9.2678.2 11.2455.1 23.3932.7 10.310.3 0.13.4 030 039.9 12.2980 50.11090 0.1100 20.1174.7 0.1100 1.14.7 5.3230.9 243.4 47.1201 0.1100 01.5 16.1178.5 0.1100 0.199.3 0.199.8 0.26.3 0.34.9 0.25.2 0.16.5 0.16.1 0.35.3 05.6 0.15.3 0.1120 00.1 0.25.5 7130
n.a. n.a. n.a. n.a. n.a. 590 n.a. n.a. n.a. n.a. n.a. n.a. n.a. 100 n.a. 100 n.a. n.a. 345 n.a. n.a. 0.03 0.03 1 1 1 1 1 1 1 1 n.a. n.a. n.a. n.a.
SynNonVar SynNonVar SynNonVar SynNonVar AnOth AnPTCon SynNon SynNon SynNonVar SynNonVar SynVis SynVis SynVis AnTVLcirVis SynVis AnTVLcirValVisPc SynVis SynVis SynTVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynT AnTValVis SynVisSpec
Tetralin Triuoroacetic acid Triuoromethane (HFC-23) Triuoromethoxymethane
Mahmood et al. [62] Giles and Wilson [330] Lim et al. [462] Uchida et al. [680] Uchida et al. [680] Grolier et al. [341]
598643 258278 283293 375377 377412 408445
0.51.5 02.9 0.24.2 2.93.6 3.43.6 0.1190
590 300 85 16 16 36.3
AnPTCon SynT AnTVLcirValVis SynVisVarPcTc SynVisVarPcTc SynNon
Vinylidene uoride
34 Table 32 Ternary systems: carbon dioxide + water + X. X 1,4-Dioxane 1-Butanol 1-Butyl-3-methylimidazolium tetrauoroborate 2,3,4,5-Tetrachlorophenol 2,4-Dichlorophenoxyacetic acid 2-Amino-2-ethyl-1,3-propanediol 2-Amino-2-hydroxymethyl-1,3-Propanediol 2-Methoxyacetophenone 3-Buten-2-one 3-Methoxyacetophenone 3-Methyl-1-butanol (isopentanol) 3-Methyl-2-butanol Acetic acid (ethanoic acid) Acetonitrile (ethanenitrile) Acetophenone Acetylacetone Ammonium acetate Benzaldehyde Benzene Bis(2,2,3,3,4,4,5,5-octauoro-1-pentyl)-2-sulfosuccinate Bromobenzene Chlorobenzene Cobalt(II) diacetylacetonate Cobalt(II) dihexauoroacetylacetonate Cobalt(III) diethyldithiocarbamate Cobalt(III) uorodiethyldithiocarbamate Copper(II) sulfate Cyclobutanone Cyclohexane Cyclohexene Cyclopentene Diethanolamine (DEA) Dimethyl ether Ethanol Ethyl acetate Ethylbenzoate Ethylene glycol Fluorobenzene Hexauoroacetylacetone Magnesium sulfate (1:1) Methane Methanol
Reference Lazzaroni et al. [436] Chen et al. [224] Zhang et al. [742] Curren and Burk [241] Curren and Burk [241] Park et al. [557] Park et al. [556] Timko et al. [671] Timko et al. [671] Timko et al. [671] Lee et al. [442] Lee et al. [442] Bamberger et al. [161] Lazzaroni et al. [436] Timko et al. [671] Gervais et al. [326] Xia et al. [712] Xia et al. [716] Timko et al. [671] Brandt et al. [186] Dong et al. [111] Timko et al. [671] Timko et al. [671] Gervais et al. [326] Gervais et al. [326] Gervais et al. [326] Gervais et al. [326] Clarke et al. [233] Mooijer-van den Heuvel et al. [521] Mooijer-van den Heuvel et al. [521] Timko et al. [671] Timko et al. [671] Timko et al. [671] Sidi-Boumedine et al. [637] Laursen et al. [38] Budich and Brunner [192] Chen et al. [223] Hu et al. [364] Timko et al. [671] Majumdar et al. [493] Timko et al. [671] Gervais et al. [326] Clarke et al. [233] Seo et al. [612] Jarne et al. [381] Jarne et al. [381] Levitin et al. [454] Levitin et al. [455] Xia et al. [718] Timko et al. [671] Mooijer-van den Heuvel et al. [521] Park et al. [557] Timko et al. [671] Kang et al. [404] Addicks et al. [147] Sidi-Boumedine et al. [637] Sidi-Boumedine et al. [637] Sidi-Boumedine et al. [637] Iwai et al. [376] Curren and Burk [241] Kamps et al. [402] Kiepe et al. [134] Clarke et al. [233] Kiepe et al. [416] Timko et al. [671] Xia et al. [712] Xia et al. [716] Bando et al. [162] Kiepe et al. [134] Ziegler et al. [745] Kiepe et al. [416] Lazzaroni et al. [436] Timko et al. [671] Mooijer-van den Heuvel et al. [521] Timko et al. [671] Chauhan et al. [221]
T (K) 313313 333353 278297 314314 313313 313333 313333 300300 300300 300300 313313 313313 313353 313313 300300 323323 313433 313433 300300 303605 288329 300300 300300 323323 323323 323323 323323 273286 279315 274288 300300 300300 300300 298348 298318 333333 323323 304546 300300 264276 300300 323323 275280 273285 246289 246289 342343 342343 313395 300300 277280 313313 300300 272284 313313 313313 298348 313313 313313 292332 313393 313353 275278 313373 300300 313433 313433 303333 313353 295295 313373 298333 300300 280291 300300 313333
P (MPa) 2.85.7 68 3.516 1027 1027 02.8 01.8 88 88 88 28.3 28.2 615 1.95.2 88 2727 0.19.6 0.19.6 88 1.9304 636 88 88 2727 2727 2727 2727 0.74.3 0.311.9 0.910.4 88 88 88 04.6 0.56.1 1010 99 7.114.9 88 1.23.1 88 2727 1.83.8 1.56.7 0.14.3 0.14.3 11.920 11.920 09.7 88 1.811.3 02.1 88 1.332.3 1.14 0.54.3 04.5 01.7 1515 10.728 09.5 010.5 1.83.5 010.2 88 09.7 09.7 1020 010.1 8.148.5 010.6 0.95.2 88 0.44.2 88 02.8
V (cm3 ) n.a. 100 50 105 105 450 450 50 50 50 n.a. n.a. 38 n.a. 50 280 30 30 50 40 54 50 50 280 280 280 280 n.a. n.a. n.a. 50 50 50 n.a. 570 800 100 18 50 n.a. 50 280 n.a. 50 n.a. n.a. 520 520 30 50 n.a. 450 50 70 450 n.a. n.a. n.a. 26.5 105 30 n.a. n.a. n.a. 50 30 30 414 n.a. 28 n.a. n.a. 50 n.a. 50 450
Method SynVisVar AnTVcirVis AnTBloVis AnTVal AnTVal AnTVal AnTVal AnTVLcirValVis AnTVLcirValVis AnTVLcirValVis AnTVLcirVal AnTVLcirVal AnPTCon SynVisVar AnTVLcirValVis AnTVal SynVis SynVis AnTVLcirValVis SynVisVar SynVis AnTVLcirValVis AnTVLcirValVis AnTVal AnTVal AnTVal AnTVal SynVisVar SynVis SynVis AnTVLcirValVis AnTVLcirValVis AnTVLcirValVis SynT AnTValVis AnTBlo AnTVcirVis SynVis AnTVLcirValVis SynVisVar AnTVLcirValVis AnTVal SynVisVar AnTValVis AnPTSemY SynVis SynVisVar SynVisVar SynVis AnTVLcirValVis SynVis AnTVal AnTVLcirValVis AnTValVis AnTVarVis AnTVal SynT SynT AnTVcirSpec AnTVal SynVis SynT SynVisVar SynT AnTVLcirValVis SynVis SynVis AnT SynT AnSpec SynT SynVisVar AnTVLcirValVis SynVis AnTVLcirValVis AnTVal
Methylbenzoate Methylcyclohexane Monoethanolamine (MEA) n-Hexane Nitrogen N-methyldiethanolamine (MDEA)
Palmitic acid Pentachlorophenol Piperazine Potassium chloride Potassium nitrate Propylbenzoate Sodium acetate Sodium chloride Sodium hydroxide Sodium nitrate Tetrahydrofuran Tetrahydropyran Toluene Triisopropanolamine
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 33 Ternary systems: carbon dioxide + methanol + X. X 1,4-Naphthoquinone 1-Butyl-3-methylimidazolium hexauorophosphate ([bmim][PF6]) 1-Methylnaphthalene 2-Methyl-2-butanol 2-Naphthol Carbon monoxide Cholesterol Cholesteryl benzoate Dimethyl ether Ethyl cellulose Hydrogen m-Hydoxybenzoic acid n-Hexane n-Tetradecane Sulfathiazole TCMTB (2-(thiocyanomethylthio) benzothiazole) Tebuconazole (R-[2-(4-chlorophenyl)ethyl]-R-(1,1-dimethylethyl)1H-1,2,4-triazole-1-ethanol) Water Reference Ngo et al. [124] Wu et al. [711] Gutirrez and Luks [140] Lee et al. [442] Ngo et al. [124] Zang et al. [737] Huang et al. [366] Huang et al. [366] Teodorescu Rasmussen [666] Li and McHugh [458] Bezanehtak et al. [174] Bristow et al. [189] Liu et al. [473] Foreman and Luks [302] Kordikowski et al. [66] Sahle-Demessie et al. [595] Sahle-Demessie et al. [595] Jarne et al. [381] Jarne et al. [381] Levitin et al. [454] Levitin et al. [455] Xia et al. [718] T (K) 313313 313313 288313 313313 313313 294327 318328 318328 313333 305403 278298 318318 304500 293313 298353 323338 323338 246289 246289 342343 342343 313395 P (MPa) 8.912.2 1515 4.78.3 28.1 8.512.4 8.113 1024 1327 0.16.4 1375 220 8.520 3.712.3 5.58.5 1020 1030 1030 0.14.3 0.14.3 11.920 11.920 09.7 V (cm3 ) n.a. 55 79 n.a. n.a. 2050 20 20 700 28 60 n.a. 18 79 10 43.92 43.92 n.a. n.a. 520 520 30 Method
35
SynNonSpec AnPTSemYVis SynOthVis AnTVLcirVal SynNonSpec SynVisVar AnPTSemY AnPTSemY AnTVal SynVisVar AnTVLcirValVis AnPTSemYSpec SynVis SynVis AnPTSemYSpec AnPTSemYVis AnPTSemYVis AnPTSemY SynVis SynVisVar SynVisVar SynVis
Table 34 Ternary systems: carbon dioxide + ethanol + X. X 1-Butyl-3-methylimidazolium tetrauoroborate ([bmim][BF4]) 2-Naphthol Acetaminophen Reference Wu et al. [711] Li et al. [459] Bristow et al. [189] Bristow et al. [189] Wubbolts et al. [95] Hu et al. [364] Li et al. [459] Borg et al. [185] Sovova et al. [649] Jin et al. [385] Berna et al. [65] Matias et al. [503] Laursen and Andersen [435] Sauceau et al. [600] Chafer et al. [208] Li and McHugh [457] Sovova [651] Duarte et al. [275] De Gioannis et al. [254] Liu et al. [480] Drescher et al. [271] Liu et al. [480] Tassaing et al. [665] Chafer et al. [209] Berna et al. [172] Budich and Brunner [192] Chen et al. [223] T (K) 313313 308328 313353 313353 295317 304547 308328 303333 313333 308328 313313 313313 298318 308318 313313 319413 313333 313313 312326 308318 333333 308318 398423 313313 313313 333333 323323 P (MPa) 1515 1030 825 10.524.6 715 7.417.3 1030 9.421.6 1528 823 813 1515 0.43.8 9.830.3 812 2082 1228 1818 1010 1.44.1 510 1.96.5 1530 812 814 1010 99 V (cm3 ) 55 377 n.a. n.a. 30 18 377 1.712.4 12 377 10 42.5 570 n.a. 10 28 n.a. 30 n.a. 200 3000 200 n.a. 10 10 800 100 Method AnPTSemYVis AnPTSemY AnPTSemYSpec AnTVcirVal SynVisVar SynVis AnPTSemY SynVisVar AnPTSemY AnPTSemY AnPTSemY AntCapVal AnTVis AnPTSemY AnPTSemY SynVisVar AnPTSemY AnTCapValVis SynVisVar AnTVcirVis AnTCap AnTVcirVis AnTVcirSpec AnPTSemY AnPTSemY AnTBlo AnTVcirVis
Acetic acid (ethanoic acid) Anthracene -Tetralol (1,2,3,4-tetrahydro-1-naphtol) -Carotene Benzoic acid Catechin Coenzyme Q10 (ubiquinone) Dimethyl ether Eucimibe Epicatechin Ethyl cellulose Ferulic acid Flurbiprofen Griseofulvin o-aminobenzoic acid Orange peel oil p-aminobenzoic acid Polystyrene Quercetin Resveratrol Water
Table 35 Ternary systems: carbon dioxide + ethyl acetate + X. X Behenic acid Benzoic acid o-Hydroxybenzoic acid p-Hydroxybenzoic acid Stearic acid Tetradecanoic acid Water Reference Liu et al. [481] Jin et al. [385] Liu et al. [479] Liu et al. [479] Liu et al. [481] Liu et al. [481] Hu et al. [364] T (K) 318318 308328 308318 308318 308318 308318 304546 P (MPa) 2.78 823 28.5 28.5 2.87.8 3.18.2 7.114.9 V (cm3 ) 200 377 200 200 200 200 18 Method AnTVcirVis AnPTSemY AnTVcirBlo AnTVcirBlo AnTVcirVis AnTVcirVis SynVis
36 Table 36 Ternary systems: carbon dioxide + dimethyl ether + X. X 1-Propanol Ethanol Methanol Poly(d,l-lactide) Poly(l-lactide) 110 000 Poly(l-lactide) 230 000 Poly(l-lactide) 80 000 Water Reference
T (K) 298318 298318 313333 303373 331412 332411 333410 298318
P (MPa) 0.43.5 0.43.8 0.16.4 2.472.4 3.122.8 6.324.9 3.622.6 0.56.1
V (cm3 ) 570 570 700 31 n.a. n.a. n.a. 570
Method AnTVis AnTVis AnTVal SynVisVar SynVisVar SynVisVar SynVisVar AnTValVis
Laursen and Andersen [435] Laursen and Andersen [435] Teodorescu Rasmussen [666] Kuk et al. [431] Lim et al. [469] Lim et al. [469] Lim et al. [469] Laursen et al. [38]
Table 37 Ternary systems: carbon dioxide + acetone + X. X 1-Methylnaphthalene 2-(Thiocyanomethylthio) benzothiazole (TCMTB) 2-Naphthol Anthracene Aspirin Cholesterol Cholesteryl benzoate Griseofulvin Limonene n-Pentane n-Tetradecane TCMTB (2-(thiocyanomethylthio) benzothiazole) Tebuconazole (R-[2-(4-chlorophenyl)ethyl]-R-(1,1-dimethylethyl)1H-1,2,4-triazole-1-ethanol) Reference Gutirrez and Luks [347] Hassan et al. [141] Li et al. [459] Li et al. [459] Huang et al. [365] Huang et al. [366] Liu et al. [482] Huang et al. [366] De Gioannis et al. [254] Corazza et al. [235] Chen et al. [227] Foreman and Luks [303] Sahle-Demessie et al. [595] Sahle-Demessie et al. [595] T (K) 288315 298308 308328 308328 318328 318328 308318 318328 312326 313343 311334 294313 323338 323338 P (MPa) 4.78.5 45.2 1030 1030 1020 1024 0.17.3 1327 610 5.310.5 7.89.4 5.58.5 1030 1030 V (cm3 ) 79 40 377 377 10 20 n.a. 20 n.a. 25 2050 79 43.9 43.9 Method SynOthVis SynOthVis AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnTVcirBlo AnPTSemY SynVisVar SynVisVar SynVisVarPcTc SynVis AnPTSemYVis AnPTSemYVis
Table 38 Ternary systems: carbon dioxide + limonene + X. X 1,8-Cineole Acetone Acetonitrile (ethanenitrile) Black currant seed oil Carvone (p-mentha-6,8-dien-2-one) Citral Dichloromethane (HCC-30) Linalool Reference Cruz Francisco and Sivik [239] Corazza et al. [235] Corazza et al. [235] Sovova et al. [72] Corazza et al. [235] Benvenuti and Gironi [170] Fonseca et al. [59] Corazza et al. [235] Chfer et al. [207] Fonseca et al. [59] T (K) 313333 313343 313343 313313 313343 315315 323323 313343 318328 323323 P (MPa) 825 5.310.5 5.610.4 812 7.912.4 8.48.4 9.510.3 6.212.3 711 8.79.4 V (cm3 ) 30 25 25 8 25 200 3.4 25 10 3.4 Method AnPTSemY SynVisVar SynVisVar AnPTSemY SynVisVar AnPTSemY AnPTCon SynVisVar AnPTSemY AnPTCon
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 39 Ternary systems: carbon dioxide + X + Y. X 1,1,1,2-Tetrauoroethane (HFC-134a) 1,8-Cineole 1-Butyl-3-methylimidazolium hexauorophosphate ([bmim][PF6]) 1-Decanol Y Salicylic acid -Pinene Acetonitrile (ethanenitrile) n-Tetradecane Reference Abbott et al. [144] Cruz Francisco and Sivik [239] Wu et al. [711] Scheidgen and Schneider [601] Scheidgen and Schneider [602] Scheidgen and Schneider [601] Scheidgen and Schneider [602] Scheidgen and Schneider [601] Scheidgen and Schneider [602] Scheidgen and Schneider [601] Ke et al. [410] Ke et al. [410] Scheidgen and Schneider [601] Shariati and Peters [105] Ghaziaskar et al. [329] Li et al. [459] Mesiano et al. [512] Yamini et al. [725] Funazukuri et al. [308] Li et al. [459] Chouchi et al. [232] Funazukuri et al. [307] Funazukuri et al. [77] Funazukuri et al. [306] Sovova et al. [649] Funazukuri et al. [77] Funazukuri et al. [306] Funazukuri et al. [309] Byun and McHugh [104] Tamura and Shinoda [662] Ngo et al. [535] Ke et al. [411] Lee et al. [444] Lee et al. [438] Lee et al. [438] Lee et al. [438] Rodrigues et al. [588] Funazukuri et al. [305] Joung et al. [395] Scheidgen and Schneider [603] Scheidgen and Schneider [603] Lee ad Kuk [437] Wubbolts et al. [95] Sauceau et al. [600] Funazukuri et al. [310] Funazukuri et al. [308] Funazukuri et al. [308] Drr et al. [270] de Vries et al. [257] Kinzl et al. [423] Byun and McHugh [104] Rodrigues et al. [588] Rodrigues et al. [588] Byun et al. [201] Byun et al. [201] Zhang et al. [736] Zhang et al. [735] Deiters [259] Garca-Gonzlez et al. [323] T (K) 323343 313333 313313 393393 280316 393393 281384 393393 272297 393393 308316 312320 393393 273367 313343 308328 323323 308348 308343 308328 323323 308343 313323 308333 313333 313323 308333 313313 298503 323383 313313 281302 302393 303373 302372 303373 283308 308328 353473 273393 273393 304375 292314 308318 313313 308343 308343 393493 312342 393493 298488 283288 293313 303435 313472 304326 307313 P (MPa) 12.129 825 1515 01000 561 01000 595 01000 590 01000 810.2 8.810.9 01000 113.9 13.813.8 1030 915 12.235.5 8.530.1 1030 9.39.3 9.530.2 12.122 8.530.3 1928.3 12.123 9.130.2 16.116.1 6210 1025 8.89.5 8.313.7 3.671.4 3.668.5 3.671.4 464 6.610 8.530.1 0.521.5 0100 0100 4.884.7 710 12.229.1 1025 9.230.1 8.630.1 118.6168.3 171.8213.2 108.3130.3 25100 6.67.8 1530 6.7255.3 6.7220.8 7.314 8.311.3 V (cm3 ) n.a. 30 55 80 80 80 80 80 80 80 4 4 80 3.5 10 377 n.a. 0.5 3.3 377 50 3.3 3.3 3.3 12 3.3 3.3 3.2 28 n.a. n.a. n.a. 31 31 31 31 500 3.3 33 80 80 31 30 n.a. 3.2 3.3 3.3 14.519.0 n.a. 14.519.0 28 500 500 28 29 2050 2050 Method AnOth AnPTSemY
37
AnPTSemYVis AnT AnT AnT AnT AnT AnT AnT SynNonPcTc SynNonPcTc AnT SynVisVar AnPTSemY AnPTSemY SynVisVar AnTValY AnPTChro AnPTSemY SynVis AnPTChro AnPTChro AnPTChro AnPTSemY AnPTChro AnPTChro AnPTChro SynVisVar AnPTSemY SynNonSpec SynNonPcTc SynVisVar SynVisVar SynVisVar SynVisVar AnPTSemY AnPTChro SynVisVar AnT AnT SynVisVar SynVisVar AnPTSemY AnPTChro AnPTChro AnPTChro SynVisVar SynVis SynVisVar SynVisVar AnPTSemY AnPTSemY SynVisVar SynVisVar SynVisVarPc SynVisVarTc Comments AnTVcirVal
1-Heptanol
n-Pentadecane
1-Hexanol
1-Heptanol n-Pentadecane n-Tetradecane
1-Hexene 1-n-Hexene 1-Octanol 1-Propanol 2-Ethyl-1-hexanol 2-Naphthol 3,3,4,4,5,5,6,6-Octauorooctan-1,8-diol 9-Nitroanthracene -Linolenic acid Anthracene -Pinene Arachidonic acid -Tocopherol -Carotene
Carbon monoxide Hydrogen n-Hexadecane Salicylic acid 2-Ethyl hexanoic acid Cyclohexane Divinyl adipate 2-Methylanthracene Poly(ethylene glycol) Cyclohexane Pinane Poly(ethylene glycol) Poly(ethylene glycol) Grape seed oil Poly(ethylene glycol)
Butyl methacrylate C,I, Disperse Blue 134 C,I, Disperse Orange 25 Carbon monoxide Chlorodiuoromethane (HCFC-22)
Clove oil Coenzyme Q10 (ubiquinone) Cyclohexane Decanoic acid
Poly(butylmethacrylate) C.I. Disperse Yellow 16 Poly(methyl methacrylate) Hydrogen Poly(l-lactide) Poly(l-lactide) 100 000 Poly(l-lactide) 2000 Poly(l-lactide) 50 000 Cellulosic structure Poly(ethylene glycol) Polybutadiene 1-Dodecanol n-Tetradecane
Dichloromethane (HCC-30) Diethyl ether Dimethylsulfoxide Diolein Docoahexaenoic acid Eicosapentaenoic acid Ethene
Ethyl methacrylate Eucalyptus oil Ginger oil Hexyl acrylate Hexyl methacrylate Hydrogen Hydroquinone (1,4-dihydroxybenzene)
Poly(l-lactide) Cholesterol Eucimibe Poly(ethylene glycol) Poly(ethylene glycol) Poly(ethylene glycol) Poly(ethylene-co-1-hexene) copolymer Poly(ethylene-co-propylene) Poly(ethylene-co-vinyl acetate) copolymer Poly(ethylmethacrylate) Cellulosic structure Cellulosic structure Poly(hexyl acrylate) Poly(hexyl methacrylate) Methylcyclohexane Toluene p-Quinone (1.4-benzoquinone)
333363
1035
50
38 Table 39 (Continued ) X Ligand bis-(2,4,4-trimethyl pentyl)-dithiophosphinic acid (cyanex 301) Y
Reference Pourmortazavi [570]
T (K) 308328
P (MPa) 1030
V (cm3 ) 1
Method AnPTSemY
ion Ag(I) in solid matrix
Linoleic acid Low MW poly(2,6-dimethyl-1,4-phenylene ether) (PPO)(L) Ls-54 surfactant
Ion Au(III) in solid matrix Ion Bi(III) in solid matrix Ion In(III) in solid matrix Ion Mn(II) in solid matrix Ion Pd(II) in solid matrix Poly(ethylene glycol) Polystyrene 1-Pentanol 1-Propanol Benzyl alcohol n-Heptanol Cyproterone acetate Propane Astaxantine Phycocyanine Poly(ethylene glycol) Poly(ethylene) Polyisobutylene Oleic acid Sodium sulfate Sulfuric acid Poly(vinyl pyrrolidone) Poly(ethylene glycol) Poly(ethylene glycol) Poly(ethylene glycol) Poly(ethylene glycol) Poly(methyl methacrylate) 1,1-Diuoroethane (HFC-152a) Chlorodiuoromethane (HCFC-22) Diuoromethane (HFC-32) Triuoromethane (HFC-23) Chlorodiuoromethane (HCFC-22) 1,1-Diuoroethane (HFC-152a) Chlorodiuoromethane (HCFC-22) Diuoromethane (HFC-32) Triuoromethane (HFC-23) 1,1-Diuoroethane (HFC-152a) Chlorodiuoromethane (HCFC-22) Diuoromethane (HFC-32) Triuoromethane (HFC-23) St. Lawrence River sediments Tripalmitin Carbon monoxide Hydrogen Methyl oleate Ethane n-Pentane Polysulfone Polybutadiene Iron tris(pentane-2.4-dionate) Naphthalene Poly(ethylene glycol) n-Hexadecane
Pourmortazavi [570] Pourmortazavi [570] Pourmortazavi [570] Pourmortazavi [570] Pourmortazavi [570] Funazukuri et al. [307] Sato et al. [599] Liu et al. [475] Liu et al. [475] Liu et al. [475] Liu et al. [475] Asghari-Khiavi et al. [154] Webster and Kidney [703] Valderrama et al. [684] Valderrama et al. [684] Funazukuri et al. [310] Joung et al. [395] Joung et al. [395] Laursen et al. [50] Kamps et al. [401] Kamps et al. [401] Bae et al. [158] Funazukuri et al. [310] Funazukuri et al. [310] Funazukuri et al. [310] Funazukuri et al. [77] Funazukuri et al. [309] Shieh et al. [82] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Lim et al. [469] Zhou et al. [744] Rovetto et al. [592] Ke et al. [410] Ke et al. [410] Ruivo et al. [60] Horstmann et al. [358] Liu et al. [474] Zhang and Kiran [740] Zhang and Kiran [741] Joung et al. [395] Roggeman et al. [589] Diefenbacher and Trk [267] Funazukuri et al. [310] Scheidgen and Schneider [603]
308328 308328 308328 308328 308328 308343 373473 308308 308308 308308 308323 308348 230270 333333 333333 313313 383503 323493 298318 313413 313413 321458 313313 313313 313313 308328 313313 305305 352415 333410 342416 333414 314395 354414 332409 334413 333413 354413 334408 344412 333415 313333 317451 299303 305305 313343 292304 313323 296426 296426 323473 333333 335338 313313 273393
1030 1030 1030 1030 1030 8.530.3 2.120.1 14.816.1 14.315.7 21.821.8 15.522.1 12.235.5 0.88 3030 3030 1025 0.633.5 0.423.7 2.514.6 3.84.5 7.810.6 18.4212 9.430.1 8.611 811 8.730.2 17.817.8 3535 54.361.3 3.726.1 77.393.6 94.1115.1 3.644.1 56.864.2 3.626.1 81.4111.3 96.1116 53.259.5 3.625.2 7791.6 93.1112.1 6.527 1.414.5 7.57.9 8.39 1121 4.46.2 8.819.6 13.854.9 13.854.9 1.923.7 13.727.5 7.829.6 9.114 0100
1 1 1 1 1 3.3 n.a. 40 40 40 40 1 n.a. 450 450 3.2 33 33 90 30 30 25 3.2 3.2 3.2 3.3 3.2 10 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. 50 3.5 4 4 n.a. 10 40 24.8 24.8 33 50 1310 3.2 80
AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTSemY AnPTChro AnGrav SynVis SynVis SynVis SynVis AnTValY AnTVcir AnPTSemY AnPTSemY AnPTChro SynVisVar SynVisVar AnTVcirX SynVis SynVis SynVisVar AnPTChro AnPTChro AnPTChro AnPTChro AnPTChro AnSpec SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar AnTVcirVal SynVis SynNonPcTc SynNonPcTc AnPTCon SynVisTc SynVis SynVisVar SynVisVar SynVisVar AnTVal SynVis AnPTChro AnT
Medroxyprogesterone Methane Microalga Haematococcus pluvialis Microalga Spirulina maxima Monoolein n-Heptane Nitrogen N-methyldiethanolamine (MDEA) n-Vinyl-2-pyrrolidone Oleic acid Oleic acid ethyl ester Oleic acid methyl ester Phenol Poly(ethylene oxide) Poly(l-lactide) 110 000
Poly(l-lactide) 2000 Poly(l-lactide) 230 000
Poly(l-lactide) 80 000
Polychlorinated biphenyl Propane Propene Squalene Sulfur hexauoride SF6 Tetraethylene glycol n-laurel ether (C12E4) Tetrahydrofuran Toluene Trichloromethane (HCC-20) Triuoromethane (HFC-23) Triolein Undecanoic acid
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 40 Ternary systems: water + methane + X. X 1,3-Dioxolane 1,4-Dioxane 2,2-Dimethylpentane 2-Methylbutane (isopentane) 2-Methylcyclohexanone 3,3-Dimethyl-2-Butanol (pinacolyl alcohol) 3,3-Dimethyl-2-butanone (pinacolone) 3-Methyl-1-butanol (isopentanol) 3-Methylcyclohexanone 4-Methylcyclohexanone Acetone Calcium chloride Carbon dioxide Cis-1,4-dimethylcyclohexane Cyclobutanone Cyclohexane Cyclooctane Cyclopentane Ethane Ethene Reference De Deugd et al. [253] Seo et al. [613] Ostergaard et al. [550] Ostergaard et al. [550] Ohmura et al. [547] Ohmura et al. [546] Ohmura et al. [546] Ohmura et al. [548] Ohmura et al. [547] Ohmura et al. [547] Seo et al. [613] Kharrat and Dalmazzone [412] Seo et al. [612] Nakamura et al. [531] Mooijer-van et al. [520] Sun et al. [659] Makino et al. [494] Sun et al. [659] Wang et al. [700] Zhang et al. [738] Ma et al. [486] Sugahara et al. [656] Sugahara et al. [656] Mahmoodaghdam and Bishnoi [492] Wang et al. [700] Maekawa [490] Zhang et al. [739] Kiepe et al. [415] Kiepe et al. [417] Kiepe et al. [415] Wang et al. [700] Mooijer-van et al. [520] Ohmura et al. [547] Sun et al. [660] Makino et al. [494] Ohmura et al. [546] Bruinsma et al. [191] Kiepe et al. [415] Kiepe et al. [415] Ma et al. [486] Seo et al. [613] Jager and Sloan [110] Kharrat and Dalmazzone [412] Link et al. [102] Mooijer-van et al. [520] De Deugd et al. [253] Seo et al. [613] De Deugd et al. [253] Mooijer-van et al. [520] Mooijer-van et al. [520] T (K) 282299 280292 274285 277287 273280 273280 273280 273281 273279 237280 279288 260284 273285 274287 293301 273291 274288 282301 275283 274274 273287 284293 293293 267277 283303 273284 274278 313313 313313 313353 283303 279288 275281 273290 274287 274280 263323 313353 313373 273283 283294 270303 269278 276293 273290 289306 292302 288302 293303 282297 P (MPa) 214 1.78.9 2.69.8 3.712 1.43.2 1.53.4 1.12.8 2.26.1 1.63.4 1.53.3 1.97.6 4.910.3 1.56.7 1.69.1 3.812.7 0.69.4 1.69.3 0.17.3 14 2.54 0.66 1.919 8.520.8 24.4 540 3.410.2 3.76.6 08.7 08.7 09.4 540 2.69.1 1.53.3 1.311.9 1.79.3 1.32.7 6.96.9 08.4 09.7 0.56.5 1.98.7 6.672.2 4.28.6 3.99.6 3.412.9 214 28.9 214 3.413.5 0.912.9 V (cm3 ) n.a. 50 540 540 201 200 200 200.0 201 201 50 n.a. 50 150 n.a. n.a. 150 n.a. 540 60 60 100 0.1 n.a. 540 500 60 n.a. n.a. n.a. 540 n.a. 201 n.a. 150 200 40280 n.a. n.a. 60 50 1 n.a. 40 n.a. n.a. 50 n.a. n.a. n.a. Method
39
Ethylene glycol Helium Hydrogen Lithium bromide Lithium cloride Methanol Methylcyclohexane
Methylcyclopentane Neohexane n-Heptane Potassium bromide Potassium chloride Propene Propylene oxide Sodium chloride Sodium dodecyl sulfate Tetrauoromethane (CFC-14) Tetrahydrofuran Tetrahydrofuran (THF) Tetrahydropyran Triuoromethane (HFC-23)
SynVis SynVis SynVis SynVis SynNon SynNon SynNon SynNon SynNon SynNon SynVis SynNon AnTValVis SynVis SynVis SynVisVar SynVis SynVisVar AnTVLcirVar AnTVarVis SynVis AnTVis SynVisSpec SynVisVar AnTVLcirVar SynVis SynVisVar SynT SynT SynT AnTVLcirVar SynVis SynNon SynVisVar SynVis SynNon AnTVcirValVar SynT SynT SynVis SynVis SynVisSpec SynNon SynVis SynVis SynVis SynVis SynVis SynVis SynVis
Table 41 Ternary systems: water + ethane + X. X Diethylene glycol (DEG) Ethylene glycol Helium Methane Methanol Propane Reference Mahmoodaghdam and Bishnoi [492] Majumdar et al. [493] Wang et al. [700] Maekawa [490] Wang et al. [700] Zhang et al. [738] Wang et al. [700] Ballard et al. [159] Ballard et al. [159] T (K) 274282 271282 283303 273287 275283 274274 283303 276279 277282 P (MPa) 0.62.2 0.52.6 0.54 0.74 14 2.54 0.54 0.52 0.52.5 V (cm3 ) n.a. n.a. 600 500 540 60 600 3 n.a. Method SynVisVar SynVisVar AnTVal SynVis AnTVLcirVar AnTVarVis AnTVal SynVis SynVis
40 Table 42 Ternary systems: water + propane + X. X Cyclobutanone Cyclohexane Diethanolamine (DEA) Diglycolamine (DGA) Di-isopropanolamine Ethane Hydrogen Methylcyclohexane Monoethanolamine (MEA) N-methyldiethanolamine (MDEA) Tetrahydropyran
Reference Mooijer-van et al. [522] Mooijer-van et al. [522] Jou et al. [390] Jou et al. [390] Jou et al. [390] Ballard et al. [159] Ballard et al. [159] Zhang et al. [739] Mooijer-van et al. [522] Jou et al. [390] Jou et al. [390] Mooijer-van et al. [522]
T (K) 276277 274276 313348 313348 313348 276279 277282 274278 274277 313313 313348 274276
P (MPa) 0.212.8 0.19.9 1.73.4 1.73.4 1.75.5 0.52 0.52.5 0.84 0.17.8 1.71.7 1.73.4 0.14.8
V (cm3 ) n.a. n.a. 250 250 250 3 n.a. 60 n.a. 250 250 n.a.
Method SynVis SynVis AnTVcirVal AnTVcirVal AnTVcirVal SynVis SynVis SynVisVar SynVis AnTVcirVal AnTVcirVal SynVis
Table 43 Ternary systems: water + nitrogen + X. X 1,4-Dioxane 2,2-Dimethylpentane 2-Methylbutane (isopentane) Acetone Carbon dioxide Dimethyl ether Propylene oxide Tetrahydrofuran (THF) Reference Seo et al. [613] Ostergaard et al. [550] Ostergaard et al. [550] Seo et al. [613] Kang et al. [404] Laursen et al. [38] Seo et al. [613] Seo et al. [613] T (K) 275283 275280 276282 274280 272284 298318 279285 287293 P (MPa) 3.711.8 1526.4 14.930.2 4.411.3 1.332.3 0.59.9 411.7 4.310.8 V (cm3 ) 50 540 540 50 70 570 50 50 Method SynVis SynVis SynVis SynVis AnTValVis AnTValVis SynVis SynVis
Table 44 Ternary systems: water + hydrogen sulde + X. X Ammonium acetate Ammonium chloride Ammonium nitrate Ammonium sulfate Diethanolamine (DEA) Ethylene glycol N-methyldiethanolamine (MDEA) Piperazine Sodium acetate Sodium chloride Sodium hydroxide Sodium nitrate Sodium sulfate Reference Xia et al. [715] Xia et al. [714] Xia et al. [713] Xia et al. [714] Sidi-Boumedine et al. [638] Majumdar et al. [493] Sidi-Boumedine et al. [638] Xia et al. [717] Xia et al. [715] Xia et al. [714] Xia et al. [713] Xia et al. [713] Xia et al. [714] T (K) 313393 313393 313393 313393 313373 272295 313373 313393 313393 313393 313393 313393 313393 P (MPa) 0.18.8 0.19.6 0.18.3 0.19.5 01.3 0.21.5 01 0.18.7 0.19.7 0.19.7 09.3 0.19.3 0.19.7 V (cm3 ) 30 30 30 30 n.a. n.a. n.a. 30 30 30 30 30 30 Method SynVis SynVis SynVis SynVis SynT SynVisVar SynT SynVis SynVis SynVis SynVis SynVis SynVis
Table 45 Ternary systems: water + X + Y. X Ammonia Chlorodiuoromethane (HCFC-22) Dimethyl ether Ethanethiol Ethene Methanol n-Decane n-Hexane Oxygen Propene Y Potassium hydroxide Sodium hydroxide Ethanol 2-Propanol (isopropanol) Ethanol Tetraethylene glycol 1-Propanol 2-Propanol (isopropanol) Natural near critical reservoir uid (C1-C20+) 2-Butanol 2-Propanol (isopropanol) 2-Propanol (isopropanol) n-Hexadecane Sodium carbonate Diethanolamine (dea) Di-isopropanolamine Monoethanolamine (mea) N-methyldiethanolamine (MDEA) Methanol Ethylbenzene n-Decane Reference Brass et al. [188] Brass et al. [188] Elbaccouch and Elliot [279] Elbaccouch and Elliot [281] Elbaccouch et al. [280] Jou et al. [389] Freitag et al. [52] Freitag et al. [52] Ostergaard et al. [551] Shimoyama et al. [634] Shimoyama et al. [634] Shimoyama et al. [634] Shimoyama et al. [633] Tan et al. [69] Jou and Mather [393] Jou and Mather [393] Jou and Mather [393] Jou and Mather [393] Jarne et al. [380] Shimoyama et al. [633] Shimoyama et al. [633] T (K) 303318 303318 351371 323373 333373 298403 287352 288353 276283 573573 573593 573573 573573 300300 313373 313333 280373 313333 247288 553553 553573 P (MPa) 0.11.1 0.11.3 0.63.7 0.12.4 0.22.5 01 3.521.6 6.117.9 5.324.2 2020 1520 2020 2020 0.710 1.720.6 1.72.7 0.15.5 1.72.7 0.12 2020 2020 V (cm3 ) n.a. n.a. 40 40 40 n.a. 30 30 540 31 31 31 31 500 250 250 250 250 n.a. 31 31 Method AnTLcirVis AnTLcirVis AnTVLcirVal AnTVLcirVal AnTVLcirVal AnTVcir AnTVLcirVisVal AnTVLcirVisVal SynVis AnPTConVis AnPTConVis AnPTConVis AnPTConVis AnPTSemX AnTVcirVar AnTVcirVar AnTVcirVar AnTVcirVar SynVis AnPTConVis AnPTConVis
Synthethic natural gas Toluene
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 46 Ternary systems: methane + X + Y. X Ethane Ethene n-Butane n-Heptane n-Hexane Tetracosane Y n-Butane Poly(ethylene-co-1-hexene) copolymer Poly(ethylene-co-vinyl acetate) copolymer n-Decane Cyclohexane ethanol n-Tetradecane Triacontane Reference Blanco et al. [175] Drr et al. [270] Kinzl et al. [423] Dandekar and Stenby [250] Xia et al. [719] Xia et al. [719] Chylinski et al. [51] Machado and de Loos [487] T (K) 253273 393493 393493 311364 303303 291303 383383 320473 P (MPa) 1.29.2 118.6202 108.3173.8 16.919 2.612 2.612 6.512 65.4193.1 V (cm3 ) n.a. 14.519.0 14.519.0 80 200360 200360 650 n.a. Method
41
SynVisCon SynVisVar SynVisVar SynVisVar AnTLcirVar AnTLcirVar AnTVLcirValVis SynVisPcTc
Table 47 Ternary systems: ethene + X + Y. X 1-Hexene 2,6-Di-tertbutyl-4-methylphenol Y Poly(ethylene-co-1-hexene) copolymer Ethylenebutyl acrylate copolymers Ethyleneethyl acrylate copolymers Ethylenemethyl acrylate copolymers Ethylenemethyl methacrylate copolymers Ethylenepropyl acrylate copolymers Ethylene-butyl methacrylate copolymers Poly(ethyl acrylate) Poly(ethylene) (ldpe) Poly(propyl acrylate) Ethylbenzene Poly(ethylene-co-1-hexene) copolymer Poly(ethylene-co-vinyl acetate) copolymer Poly(ethylene-co-1-hexene) copolymer Poly(ethylene-co-vinyl acetate) copolymer Poly(ethylene-co-1-hexene) copolymer Poly(ethylene-co-vinyl acetate) copolymer Impact poly(propylene) copolymer (icppp) Poly(ethylene) (ldpe) Poly(ethylene) 108k Poly(ethylene) 15k Poly(ethylene-co-1-hexene) copolymer Poly(ethylene-co-vinyl acetate) copolymer Reference Drr et al. [270] Becker et al. [167] Becker et al. [167] Becker et al. [167] Becker et al. [167] Becker et al. [167] Becker et al. [167] Becker et al. [167] Becker et al. [167] Becker et al. [167] Liu et al. [477] Drr et al. [270] Kinzl et al. [423] Drr et al. [270] Kinzl et al. [423] Drr et al. [270] Kinzl et al. [423] Sato et al. [78] Chen et al. [229] Chen et al. [229] Chen et al. [229] Drr et al. [270] Kinzl et al. [423] T (K) 393493 354530 353533 373493 353528 353532 353533 354533 403521 352531 282572 393493 393493 393493 393493 393493 393493 323363 393473 373473 373473 393493 393493 P (MPa) 25.6156 95.3114.4 98.2163.1 124.4211.5 103.9185.5 97.8152.7 81.3138 101161.3 120.4163.7 87.4109.3 511.9 112156 107.5126 118.6214.6 108.3209.4 101156 94.3125.9 0.62.4 0.615.7 0.417 0.420.9 106.6156 98125.9 V (cm3 ) 14.519.0 n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. n.a. 14.519.0 14.519.0 14.519.0 14.519.0 14.519.0 14.519.0 n.a. 620 620 620 14.519.0 14.519.0 Method SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisPcTc SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar AnPTChro SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar
Benzene Ethane Helium n-Butane n-Hexane
Propane
Table 48 Ternary systems: X + Y + Z. X 1-Butene Benzene Cyclohexane Diuoromethane (HFC-32) Dimethyl ether Y Toluene Propene Polystyrene Propane N,N-dimethyl formamide Tetrahydrofuran Ethane Carbon tetrachloride Cyclohexane Propane Trichloromethane (HCC-20) Carbon monoxide n-Hexadecane Propane N-methyldiethanolamine (MDEA) N-methyldiethanolamine (MDEA) n-Heptane Toluene Impact poly(propylene) copolymer (ICPPP) Impact poly(propylene) copolymer (ICPPP) Poly(ethylene) 15k Z Poly(propylene) Cumene Polystyrene 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) Polysulfone Polysulfone Poly(propylene glycol) Polystyrene Trans--carotene Poly(propylene glycol) n-Hexane Anthracene Methyl palmitate Sodium sulfate Sulfuric acid n-Hexadecane Poly(propylene) Ethene Propene Poly(ethylene) 108k Reference Oliveira et al. [549] Wang et al. [698] ter Horst et al. [667] Coquelet et al. [234] Li and McHugh [457] Li and McHugh [457] Martin et al. [500] ter Horst et al. [667] Nobre et al. [542] Martin et al. [500] Gao et al. [318] Minicucci et al. [113] Rovetto et al. [593] Anoufrikov et al. [152] Anoufrikov et al. [152] Fenghour et al. [292] Oliveira et al. [549] Sato et al. [78] Sato et al. [78] Chen et al. [229] T (K) 352423 364596 496516 269329 294452 293450 295373 388513 313348 295373 505506 n.a.650 361450 313393 313393 404447 358423 323363 323363 443473 P (MPa) 1.112.7 4.67 2.416 0.42.2 35210 35210 4.521.5 3.414.4 5.130.1 630 33 n.a.14 5.311.6 03.8 03.6 0.50.7 110.8 0.62.4 1.22.4 2.17.6 V (cm3 ) 28 18 3.5 n.a. 28 28 50 3.5 32 50 50 n.a. 3.5 30 30 207 28 n.a. n.a. 620 Method SynVisVar SynVisPcTc SynVis SynVisVar SynVisVar SynVisVar SynVisVar SynVis AnPTSemY SynVisVar SynVisVarPcTc SynNon SynVisVar SynVis SynVis SynNon SynVisVar AnPTChro AnPTChro SynVisVar
Hydrogen
Hydrogen sulde
n-Butane
n-Hexane
42 Table 48 (Continued ) X Nitrogen Y Cyclohexane Dimethyl ether n-Hexane n-Tridecane Propane Propene n-Tetradecane cyclohexane 2,6-Di-tertbutyl-4methylphenol 2,6-Di-tertbutyl-4methylphenol Ethene
Z Polystyrene Methanol n-Decane n-Pentadecane Polystyrene Poly(methyl acrylate) Poly(methyl methacrylate) Poly(ethylene-co-vinyl acetate) copolymer
Reference ter Horst et al. [667] Teodorescu Rasmussen [666] Uribe-Vargas and Trejo [682] Daridon et al. [106] ter Horst et al. [667] Becker et al. [167] Becker et al. [167] Kinzl et al. [423]
T (K) 437513 288313 258298 273293 438513 473531 427532 393493
P (MPa) 7.516 0.19.2 1.420.1 0.1100 2.512.4
V (cm3 ) 3.5 700 n.a. 0.03 3.5
Method SynVis AnTVal AnTVal SynVis SynVis SynVisVar SynVisVar SynVisVar
139.9275 n.a. 107.8270 n.a. 4.8125.9 14.519.0
Vinyl acetate
Table 49 Multicomponent systems: carbon dioxide + water + X (+Y + . . .). X (+Y + . . .) 1,8-Cineole + lecithin 1,8-Cineole + monoolein 1-Octene + tetrahydrofuran 1-Pentanol + uorosurfactant F-53B 1-Propanol + adenine 1-Propanol + anthranilate 1-Propanol + caffeine 1-Propanol + uorosurfactant F-53B 1-Propanol + l-phenylalanine 1-Propanol + salicyclic alcohol 1-Propanol + vanillin Acetic acid (ethanoic acid) + sodium acetate Acetic acid (ethanoic acid) + sodium chloride Diethanolamine (DEA) + N-methyldiethanolamine (MDEA) Ethanol + capsaicin Ethanol + dimethyl ether Ethanol + uorosurfactant F-53B Ethylene glycol + sodium cloride Fluorosurfactant F-53B + butanol Fluorosurfactant F-53B + heptanol Fluorosurfactant F-53B + hexanol Fluorosurfactant F-53B + octyl alcohol Methane + hydrogen sulde Methane + methanol Methane + N-methyldiethanolamine (MDEA) Methanol + dimethyl ether Methanol + tetramethylammonium bicarbonate Methanol + tetramethylammonium bicarbonate Nitric acid + tri-n-butyl phosphate Nitrogen + tetrahydrofuran N-methyldiethanolamine (MDEA) + diethanolamine (DEA) Phenol + potassium chloride Phenol + sodium bromide Phenol + sodium chloride Phenol + tetramethylammonium bromide Piperazine + N-methyldiethanolamine (MDEA) 2,2,3,3,4,4,5,5-Octauoro-1-pentanol + sodium bis(2-ethylhexyl)sulfosuccinate + dimidium bromice 2,2,3,3,4,4,5,5-Octauoro-1-pentanol + sodium bis(2-ethylhexyl)sulfosuccinate + methyl orange 2,2,3,3,4,4,5,5-Octauoro-1-pentanol + sodium bis(2-ethylhexyl)sulfosuccinate + thymol blue Ethanol + didecyldimethylammonium chloride + soysolv Methane + diethanolamine (DEA) + ethanethiol Methane + diethanolamine (DEA) + methanethiol Methane + toluene + N-methyldiethanolamine (MDEA) Nitrogen + dimethyl ether + methanol N-methyldiethanolamine (MDEA) + diethanolamine (DEA) + 2-amino-2-methyl-1-propanol Methane + diethanolamine (DEA) + hydrogen sulde + ethanethiol Methane + diethanolamine (DEA) + hydrogen sulde + methanethiol Reference Cruz Francisco et al. [80] Cruz Francisco et al. [240] Lazzaroni et al. [436] Gao et al. [320] Adrian et al. [148] Adrian et al. [148] Adrian et al. [148] Gao et al. [320] Adrian et al. [148] Adrian et al. [148] Adrian et al. [148] Sieder and Maurer [639] Sieder and Maurer [639] Sidi-Boumedine et al. [637] Duarte et al. [34] Laursen and Andersen [435] Gao et al. [320] Majumdar et al. [493] Gao et al. [320] Gao et al. [320] Gao et al. [320] Gao et al. [320] Sun et al. [658] Jarne et al. [379] Addicks et al. [147] Laursen et al. [38] Levitin et al. [454] Levitin et al. [455] Enokida et al. [285] Kang et al. [404] Rebolledo-Libreros and Trejo [582] Wagner et al. [694] Wagner et al. [694] Wagner et al. [694] Wagner et al. [694] Kamps et al. [402] Liu et al. [476] Liu et al. [476] Liu et al. [476] Elbaccouch et al. [282] Jou and Mather [387] Jou and Mather [387] Valtz et al. [686] Laursen et al. [38] Rebolledo-Libreros and Trejo [582] Jou and Mather [387] Jou and Mather [387] T (K) 308353 308353 298298 290334 313333 313333 313333 308334 313333 313333 313333 313353 313353 298348 313323 298318 308334 264272 308334 308334 308334 308334 274299 241288 313353 298318 298343 298343 313333 274295 313393 313313 313313 313313 313313 353353 311311 311311 311311 298333 313343 313343 333333 298318 313393 313343 313343 P (MPa) 1515 1515 0.225.6 7.513.5 7.116.1 7.116.1 7.116.1 1214.5 7.116.1 716.1 7.116.1 616.1 6.116.3 04.5 1214 0.54.2 824.5 1.33.1 1214.5 1214.5 8.515.5 1517 0.58.6 0.15.9 1020 0.45.5 1.527.1 1.527.1 716.5 0.212.9 01.9 2222 2222 830 830 0.16.4 34.534.5 34.534.5 34.534.5 0.28.7 6.86.8 6.86.8 0.50.5 0.49.9 01.9 6.86.8 6.86.8 V (cm3 ) n.a. n.a. 350 n.a. 30 30 30 n.a. 30 30 30 38 38 n.a. 36 570 n.a. n.a. n.a. n.a. n.a. n.a. 60 n.a. 450 570 520 520 n.a. 70 320 200 200 200 200 30 2.2 2.2 2.2 9.5 n.a. n.a. n.a. 570 320 n.a. n.a. Method AnSpecVis AnSpecVis AnTValVis SynVisVar AnTVcirLcir AnTVcirLcir AnTVcirLcir SynVisVar AnTVcirLcir AnTVcirLcir AnTVcirLcir AnPTCon AnPTCon SynT AnTCapVal AnTVis SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVisVar SynVis AnTVarVis AnTValVis SynVisVar SynVisVar SynVis AnTValVis AnTVcir AnTVLcirVis AnTVLcirVis AnTVLcirVis AnTVLcirVis SynVis AnSpec AnSpec AnSpec SynTVis AnTVcir AnTVcir AnTValVis AnTValVis AnTVcir AnTVcir AnTVcir
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 50 Multicomponent systems: carbon dioxide + X + Y (+ . . .). X (+ Y + . . .) 1,8-Cineole + limonene + -pinene 2-Ethyl-1-hexanol + 2-ethyl hexanoic acid + 2-ethyl-hexyl-2-ethyl hexanoate Reference Cruz Francisco and Sivik [239] Ghasziaskar and Daneshfar [327] Wu et al. [711] Laursen et al. [50] Valderrama et al. [684] Ke et al. [410] Ke et al. [410] Wu et al. [711] Wu et al. [711] Jin et al. [385] Yamini and Bahramifar [723] Sun and Chen [657] Smejkal et al. [646] Goodarznia and Esmaeilzadeh [334] Valderrama et al. [684] Zhou et al. [744] Laursen et al. [50] Souza et al. [648] Jiang et al. [384] Stradi et al. [653] Smejkal et al. [646] Ke et al. [411] Smejkal et al. [646] Stradi et al. [653] T (K) 313333 313353 P (MPa) 825 9.425.3 V (cm3 ) 30 10 Method AnPTSemY AnPTSemY
43
1-Butyl-3-methylimidazolium hexauorophosphate ([bmim][PF6]) + acetone + n-hexane Oleic acid + -pinene + abietic acid Ethanol + astaxantine + microalga Haematococcus pluvialis 1-n-Hexene + carbon monoxide + hydrogen Propene + carbon monoxide + hydrogen 1-Butyl-3-methylimidazolium hexauorophosphate ([bmim][PF6]) + ethanol + acetone 1-Butyl-3-methylimidazolium hexauorophosphate ([bmim][PF6]) + ethanol + n-hexane Ethanol + ethyl acetate + benzoic acid Acenaphthene + uoranthene + triphenylene
313313 298318 333333 305315 295304 313313 313313 308328 308338
1515 2.114.4 3030 8.312 7.910.8 1515 1515 823 12.135.4
55 90 450 4 4 55 55 377 1
AnPTSemYVis AnTVcirX AnPTSemY SynNonPcTc SynNonPcTc AnPTSemYVis AnPTSemYVis AnPTSemY AnTValY
Methane + hydrogen sulde + sulfur Propane + nitrogen + oxygen Anthracene + phenanthrene + carbazole
303363 327369 308308
2045 4.26.3 11.120.1
300 35 n.a.
AnTVar SynVisPcTc AnPTSemY
Ethanol + phycocyanine + microalga Spirulina maxima Methanol + polychlorinated biphenyl + St. Lawrence River sediments Nitrogen + oleic acid + -pinene + abietic acid Eugenol + -caryophyllene + eugenol acetate + -humulene Carbon monoxide + hydrogen + 1-hexene + heptanal Trans-2-hexen-1-ol + diisopropyl-l-tartrate + n-decane + tert-butylhydroperoxide Propane + nitrogen + oxygen + acetic acid (ethanoic acid) + acrylic acid Propene + carbon monoxide + hydrogen + n-butyraldehyde + isobutyraldehyde Propane + nitrogen + oxygen + acetic acid (ethanoic acid) + methanol Trans-2-hexen-1-ol + diisopropyl-l-tartrate + n-decane + tert-butylhydroperoxide + tertbutanol + titanium(IV) isopropoxide + (2R,3R)-(+)-3-propyloxiranemethanol Table 51 Multicomponent systems: methane + X + Y (+. . .). X (+Y + . . .) Diglycolamine (DGA) + ethylbenzene + water Ethane + water + ethylene glycol Ethane + water + methanol Ethane + water + n-butane Ethane + water + tetrahydrofuran Ethylene glycol + water + sodium chloride n-Butane + n-heptane + n-hexadecane n-Hexane + n-decane + n-tetradecane Nitrogen + water + 2,2-dimethylpentane Nitrogen + water + 2-methylbutane (isopentane) Water + benzene + diglycolamine (DGA) Water + ethane + propane Water + hydrogen + propane Water + methanethiol + diethanolamine (DEA) Water + methanol + sodium chloride Water + sodium chloride + magnesium chloride Water + toluene + diglycolamine (DGA) Water + toluene + N-methyldiethanolamine (MDEA) n-Pentane + 2-methylbutane (isopentane) + n-hexane + naphthalene n-Pentane + 2-methylbutane (isopentane) + n-hexane + n-tetracosane Reference Valtz et al. [686] Wang et al. [700] Wang et al. [700] Blanco et al. [175] Chapoy et al. [218] Zhang et al. [738] Eichholz et al. [278] Fenghour et al. [293] Chylinski et al. [51] Ostergaard et al. [550] Ostergaard et al. [550] Valtz et al. [686] Ostergaard et al. [552] Zhang et al. [739] Jou and Mather [387] Jager et al. [377] Jager et al. [377] Link et al. [102] Valtz et al. [686] Valtz et al. [686] Jensen et al. [383] Jensen et al. [383]
333333 313333 298318 303328 303348 313323 294300 297338 301306 313323
3030 6.527 2.514.5 5.816.7 6.518.2 2.86.2 8.79.4 8.111.8 77.8 3.47.4
450 50 90 25 2550 100 35 n.a. 35 100
AnPTSemY AnTVcirVal AnTVcirX SynVisVar SynVisVar AnTCap SynVisPcTc SynNonPcTc SynVisPcTc AnTCap
T (K) 298393 275283 275283 250288 278313 274284 262281 340372 296296 276286 276284 298393 276290 274280 313343 249281 260292 269293 298393 298393 277410 279413
P (MPa) 0.55 0.540 1.340 0.49.9 0.914.4 23 2.19.5 4.83.6 5.85.8 6.222.6 5.115.4 0.55 1.47.9 0.64.9 6.86.8 216 7.473.2 7.99.6 0.55 0.48.1 11.740 9.839.5
V (cm3 ) n.a. 540 540 n.a. 34 60 6474 207 650 540 540 n.a. 540 60 n.a. n.a. 1 40 n.a. n.a. 150 150
Method AnTValVis AnTVLcirVar AnTVLcirVar SynVisCon AnTVal AnTVarVis SynVisVar SynNon AnTVLcirValVis SynVis SynVis AnTValVis SynVis SynVisVar AnTVcir SynVis SynVisSpec SynVis AnTValVis AnTValVis SynVisVar SynVisVar
44 Table 51 (Continued ) X (+Y + . . .) Propane + n-pentane + n-decane + nhexadecane Water + ethane + cyclohexane + propane Water + ethane + propane + 2-methylbutane (isopentane) Water + ethane + propane + methylcyclohexane Water + ethane + propane + methylcyclopentane Water + ethylene glycol + potassium chloride + sodium chloride Water + hydrogen + ethane + propane Water + methanethiol + diethanolamine (DEA) + hydrogen sulde n-Pentane + 2-methylbutane (isopentane) + nhexane + n-tetracosane + naphthalene Water + benzene + N-methyldiethanolamine (MDEA) + ethylbenzene + toluene Water + ethane + propane + n-pentane + n-decane Ethane + propane + 2-methylpropane (isobutane) + n-butane + 2-methylbutane (isopentane) + n-pentane Water + ethane + propane + n-pentane + n-decane + 2,2dimethylpropane (neopentane) Water + ethane + propane + n-pentane + ndecane + cyclohexane Water + ethane + propane + n-pentane + ndecane + cyclopentane Water + ethane + propane + n-pentane + ndecane + cyclopentane + 2,2-dimethylpropane (neopentane) Table 52 Multicomponent systems: X + Y (+ . . .). X (+Y + . . .)
Reference Gozalpour et al. [32] Gozalpour et al. [337] Gozalpour et al. [338] Sun et al. [659] Ostergaard et al. [552] Sun et al. [660] Ostergaard et al. [552] Ostergaard et al. [552] Masoudi et al. [501] Zhang et al. [739] Jou and Mather [387] Jensen et al. [383] Valtz et al. [686] Ostergaard et al. [552] Dandekar and Stenby [250]
T (K) 303353 278383 278383 273289 275282 273288 280288 278288 259283 274279 313343 278419 333333 279286 298298
P (MPa) 19.430.4 10.441.4 10.441.4 0.66.2 25.1 0.96.1 2.68.1 27.7 3.946.6 1.17 6.86.8 8.940 0.50.5 1.23.8 7.47.4
V (cm3 ) 9000 9000 9000 n.a. 540 n.a. 540 540 n.a. 60 n.a. 150 n.a. 540 80
Method AnTValVisVar SynVisVar SynVisVar SynVisVar SynVis SynVisVar SynVis SynVis SynNon SynVisVar AnTVcir SynVisVar AnTValVis SynVis SynVisVar
Ostergaard et al. [552]
278286
0.93.4
540
SynVis
Ostergaard et al. [552] Ostergaard et al. [552] Ostergaard et al. [552]
276284 278287 278288
0.83.1 0.24.2 0.42.6
540 540 540
SynVis SynVis SynVis
Reference Furutaka and Ikawa [312] Chen et al. [229] Lee et al. [449] Furutaka and Ikawa [313] Gao et al. [318] Rebolledo-Libreros and Trejo [583] Sidi-Boumedine et al. [638] Majumdar et al. [493] Xia et al. [717]
T (K) 473648 443473 323423 473623 504506 313393 313373 273289 353353
P (MPa) 1035 2.814.8 0.52.5 1035 33.3 01 01.1 0.21.4 0.16.2
V (cm3 ) n.a. 620 n.a. n.a. 50 320 n.a. n.a. 30
Method AnSpecVis SynVisVar AnT AnSpecVis SynVisVarPcTc AnTVcir SynT SynVisVar SynVis
Benzene + water + deuterium oxide + deuterium protium oxide Ethene + n-hexane + poly(ethylene) 15k + poly(ethylene) 108k Ethene + toluene + norbornene + cyclic olen copolymer Ethylbenzene + water + deuterium oxide + deuterium protium oxide Hydrogen + carbon monoxide + methanol + n-hexane Hydrogen sulde + N-methyldiethanolamine (MDEA) + diethanolamine (DEA) + water Hydrogen sulde + N-methyldiethanolamine (MDEA) + water + diethanolamine (DEA) Hydrogen sulde + water + ethylene glycol + sodium cloride Hydrogen sulde + water + piperazine + N-methyldiethanolamine (MDEA) Nitrogen + dimethyl ether + water + methanol Nitrogen + ethanol + water + dimethyl ether Nitrogen + ethene + 1-hexene + poly(ethylene-co-1-hexene) copolymer Nitrogen + oleic acid + -pinene + abietic acid Nitrogen + vinyl acetate + ethene + poly(ethylene-co-vinyl acetate) copolymer n-Tridecane + n-tetradecane + n-pentadecane + n-hexadecane Hydrogen sulde + N-methyldiethanolamine (MDEA) + diethanolamine (DEA) + 2-amino-2-methyl-1-propanol + water n-Tridecane + n-tetradecane + n-pentadecane + nhexadecane + n-heptadecane Toluene + water + deuterium oxide + deuterium protium oxide + n-Tridecane + n-tetradecane + n-pentadecane + nhexadecane + n-heptadecane + n-octadecane n-Tridecane + n-tetradecane + n-pentadecane + nhexadecane + n-heptadecane + n-octadecane + n-nonadecane n-Tridecane + n-tetradecane + n-pentadecane + nhexadecane + n-heptadecane + n-octadecane + nnonadecane + n-eicosane n-Tridecane + n-tetradecane + n-pentadecane + nhexadecane + n-heptadecane + n-octadecane + nnonadecane + n-eicosane + n-heneicosane + n-docosane
Laursen et al. [38] Laursen and Andersen [435] Drr et al. [270] Laursen et al. [50] Kinzl et al. [423] Daridon et al. [106] Rebolledo-Libreros and Trejo [583]
298318 298318 393493 298318 393493 277296 313393
0.410.2 0.410.2 12.7206.5 3.714.7 26.7193 0.1100.3 01
570 570 14.519.0 90 14.519.0 0.03 320
AnTValVis AnTVis SynVisVar AnTVcirX SynVisVar SynVis AnTVcir
Daridon et al. [106] Furutaka and Ikawa [313] Daridon et al. [106] Daridon et al. [106] Daridon et al. [106]
279298 473623 283302 286305 289309
0.1100.3 1035 0.1100 0.198 0.1100
0.03 n.a. 0.03 0.03 0.03
SynVis AnSpecVis SynVis SynVis SynVis
Daridon et al. [106]
295315
0.1100
0.03
SynVis
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 53 Complex systems: X + Y (+ . . .). X Gas condensate reservoirs Parafnic system (n-c6 to n-c36) Synthetic legendre gas condensate Synthetic reservoir uid #1 Synthetic reservoir uid #2 Synthetic reservoir uid #3 Synthetic reservoir uid #4 Synthetic reservoir uid #5 Reservoir uid (North Sea) Synthethic natural gas Natural GasAlinta Gas Ltd., Perth, Australia Synthethic natural gas Y Z Reference Elsharkawy [284] Pauly et al. [45] May et al. [508] Yan et al. [727] Yan et al. [727] Yan et al. [727] Yan et al. [727] Yan et al. [727] Pedersen et al. [560] Ostergaard et al. [552] Gnanendran and Amin [333] T (K) 278444 256290 300310 312404 312425 303421 303421 303422 308473 276290 285293 277292 283288 278289 P (MPa) 10.881.6 0.150 6.29.5 6.558.1 6.151 5.949.5 648.4 5.946.4 70100 1.27.6 1.48 1.19.6 1.23.1 1.77 V (cm3 ) Method n.a. n.a. 40 n.a. n.a. n.a. n.a. n.a. 120 540 700 540 540 540
45
Water Water Para-toluene sulfonic acid Water Water
SynVis AnTVar SynNonVcirVar SynVis SynVis SynVisPcTc SynVisPcTc SynVisPcTc AnTVar SynVis SynNonVisVar SynVis SynVis SynVis
Cyclohexane Ostergaard et al. [552] Cyclopentane Ostergaard et al. [552] Methylcyclopentane Ostergaard et al. [552]
Table 54 Binary systems with hydrates: water + X. X Air Black oil AWestport Technology Center Black oil BWestport Technology Center Black oil CWestport Technology Center Carbon dioxide Reference Mohammadi et al. [91] Ivanic et al. [128] Ivanic et al. [128] Ivanic et al. [128] Mooijer-van den Heuvel et al. [521] Servio and Englezos [614] Yang et al. [729] Zatsepina and Buffett [126] Kim et al. [422] Morita et al. [523] Song et al. [647] Chapoy et al. [214] Chapoy et al. [220] Huo et al. [367] Kharrat and Dalmazzone [412] Kim et al. [422] Link et al. [102] Mohammadi et al. [91] Ohmura et al. [547] Servio and Englezos [615] Song et al. [647] Yang et al. [730] Ostergaard et al. [551] Mohammadi et al. [91] Mohammadi et al. [91] Makogon [495] Mooijer-van et al. [522] Song et al. [647] Ivanic et al. [128] Sugahara et al. [655] Ohgaki et al. [545] T (K) 274283 287293 279284 282286 276286 273283 277280 271281 277298 298323 201281 283293 283293 275275 281284 276298 278293 278278 273281 274284 196270 273286 277288 274283 273284 278278 276278 211276 288296 276317 283320 P (MPa) 1745.1 6.616.8 37.8 4.616.3 1.87.3 26 4.914.2 2.83 1.420.1 89479 3.43.4 1035 1035 3030 5.77.7 2.316.6 8.69.6 4.74.7 2.65.7 3.56.5 3.46.9 3.619.3 113.9 1945.3 13.543.7 0.535 0.39.8 0.81.1 414 7.4317 0.969 V (cm3 ) 150 300 300 300 n.a. n.a. n.a. n.a. n.a. 0.2 n.a. 34 34 1 n.a. n.a. 40 150 201 n.a. n.a. n.a. 540 150 150 160210 n.a. n.a. 300 0.2 n.a. Method SynNon SynNon SynNon SynNon SynVis AnTVis AnTVcirVisVar SynNon SynVisVar SynVisSpec AnPTSemY AnTVal AnTVal AnTSpec SynNon SynVisVar SynVis SynNon SynNon AnTVis AnPTSemY AnTVcirVisVar SynVis SynNon SynNon SynVisVar SynVis AnPTSemY SynNon SynVisSpec SynVis
Ethane
Methane
Natural near critical reservoir uid (C1C20+) Nitrogen Oxygen Propane
Synthetic Green Canyon gas Tetrauoromethane (CFC-14) Xenon
46 Table 55 Ternary systems with hydrates: water + X + Y. X Carbon dioxide Y Copper(II) sulfate Cyclobutanone Cyclohexane Ethylene glycol Magnesium sulfate (1:1) Methane Methylcyclohexane Nitrogen Potassium nitrate Tetrahydropyran Diethylene glycol (DEG) Ethylene glycol Helium Propane
Reference Clarke et al. [233] Mooijer-van den Heuvel et al. [521] Mooijer-van den Heuvel et al. [521] Majumdar et al. [493] Clarke et al. [233] Seo et al. [612] Mooijer-van den Heuvel et al. [521] Kang et al. [404] Clarke et al. [233] Mooijer-van den Heuvel et al. [521] Mahmoodaghdam and Bishnoi [492] Majumdar et al. [493] Maekawa [490] Ballard et al. [159] Ballard et al. [159] Zhang et al. [739] Majumdar et al. [493] De Deugd et al. [253] Seo et al. [613] Ostergaard et al. [550] Ostergaard et al. [550] Ohmura et al. [547] Ohmura et al. [546] Ohmura et al. [546] Ohmura et al. [548] Ohmura et al. [547] Ohmura et al. [547] Seo et al. [613] Kharrat and Dalmazzone [412] Nakamura et al. [531] Mooijer-van et al. [520] Sun et al. [659] Makino et al. [494] Sun et al. [659] Zhang et al. [738] Ma et al. [486] Sugahara et al. [656] Sugahara et al. [656] Mahmoodaghdam and Bishnoi [492] Maekawa [490] Zhang et al. [739] Mooijer-van et al. [520] Ohmura et al. [547] Sun et al. [660] Makino et al. [494] Ohmura et al. [546] Ma et al. [486] Seo et al. [613] Jager and Sloan [110] Kharrat and Dalmazzone [412] Link et al. [102] Mooijer-van et al. [520] De Deugd et al. [253] Seo et al. [613] De Deugd et al. [253] Mooijer-van et al. [520] Mooijer-van et al. [520] Ostergaard et al. [551] Seo et al. [613] Ostergaard et al. [550] Ostergaard et al. [550] Seo et al. [613] Seo et al. [613] Seo et al. [613] Mooijer-van et al. [522] Mooijer-van et al. [522] Mooijer-van et al. [522] Mooijer-van et al. [522]
T (K) 273286 279315 274288 264276 275280 273285 277280 272284 275278 280291 274282 271282 273287 276279 277282 274278 272295 282299 280292 274285 277287 273280 273280 273280 273281 273279 237280 279288 260284 274287 293301 273291 274288 282301 274274 273287 284293 293293 267277 273284 274278 279288 275281 273290 274287 274280 273283 283294 270303 269278 276293 273290 289306 292302 288302 293303 282297 276283 275283 275280 276282 274280 279285 287293 276277 274276 274277 274276
P (MPa) 0.74.3 0.311.9 0.910.4 1.23.1 1.83.8 1.56.7 1.811.3 1.332.3 1.83.5 0.44.2 0.62.2 0.52.6 0.74 0.52 0.52.5 0.84 0.21.5 214 1.78.9 2.69.8 3.712 1.43.2 1.53.4 1.12.8 2.26.1 1.63.4 1.53.3 1.97.6 4.910.3 1.69.1 3.812.7 0.69.4 1.69.3 0.17.3 2.54 0.66 1.919 8.520.8 24.4 3.410.2 3.76.6 2.69.1 1.53.3 1.311.9 1.79.3 1.32.7 0.56.5 1.98.7 6.672.2 4.28.6 3.99.6 3.412.9 214 28.9 214 3.413.5 0.912.9 5.324.2 3.711.8 1526.4 14.930.2 4.411.3 411.7 4.310.8 0.212.8 0.19.9 0.17.8 0.14.8
V (cm3 ) n.a. n.a. n.a. n.a. n.a. 50 n.a. 70 n.a. n.a. n.a. n.a. 500 3 n.a. 60 n.a. n.a. 50 540 540 201 200 200 200 201 201 50 n.a. 150 n.a. n.a. 150 n.a. 60 60 100 0.1 n.a. 500 60 n.a. 201 n.a. 150 200 60 50 1 n.a. 40 n.a. n.a. 50 n.a. n.a. n.a. 540 50 540 540 50 50 50 n.a. n.a. n.a. n.a.
Method SynVisVar SynVis SynVis SynVisVar SynVisVar AnTValVis SynVis AnTValVis SynVisVar SynVis SynVisVar SynVisVar SynVis SynVis SynVis SynVisVar SynVisVar SynVis SynVis SynVis SynVis SynNon SynNon SynNon SynNon SynNon SynNon SynVis SynNon SynVis SynVis SynVisVar SynVis SynVisVar AnTVarVis SynVis AnTVis SynVisSpec SynVisVar SynVis SynVisVar SynVis SynNon SynVisVar SynVis SynNon SynVis SynVis SynVisSpec SynNon SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis SynVis
Ethane
Hydrogen Hydrogen sulde Methane
Propane Ethylene glycol 1,3-Dioxolane 1,4-Dioxane 2,2-Dimethylpentane 2-Methylbutane (isopentane) 2-Methylcyclohexanone 3,3-Dimethyl-2-butanol (pinacolyl alcohol) 3,3-Dimethyl-2-butanone (pinacolone) 3-Methyl-1-butanol (isopentanol) 3-Methylcyclohexanone 4-Methylcyclohexanone Acetone Calcium chloride cis-1,4-Dimethylcyclohexane Cyclobutanone Cyclohexane Cyclooctane Cyclopentane Ethane Ethene
Ethylene glycol Helium Hydrogen Methylcyclohexane
Methylcyclopentane Neohexane Propene Propylene oxide Sodium chloride Sodium dodecyl sulfate Tetrauoromethane (CFC-14) Tetrahydrofuran Tetrahydrofuran (THF) Tetrahydropyran Triuoromethane (HFC-23) Natural near critical reservoir uid (C1C20+) 1,4-Dioxane 2,2-Dimethylpentane 2-Methylbutane (isopentane) Acetone Propylene oxide Tetrahydrofuran (THF) Cyclobutanone Cyclohexane Methylcyclohexane Tetrahydropyran
Methanol Nitrogen
Propane
R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154 Table 56 Multicomponent and complex systems with hydrates: water + X + Y (+. . .). X (+Y + . . .) Carbon dioxide + ethylene glycol + sodium cloride Carbon dioxide + methane + hydrogen sulde Carbon dioxide + nitrogen + tetrahydrofuran Hydrogen + methane + propane Hydrogen sulde + ethylene glycol + sodium cloride Methane + ethane + propane Methane + ethane + tetrahydrofuran Methane + ethylene glycol + sodium chloride Methane + magnesium chloride + sodium chloride Methane + methanol + sodium chloride Methane + nitrogen + 2,2-dimethylpentane Methane + nitrogen + 2-methylbutane (isopentane) Hydrogen + methane + ethane + propane Methane + ethane + cyclohexane + propane Methane + ethane + propane + methylcyclohexane Methane + ethane + propane + methylcyclopentane Methane + ethane + propane + 2-methylbutane (isopentane) Methane + ethane + propane + methylcyclohexane Methane + ethylene glycol + potassium chloride + sodium chloride Methane + ethane + propane + n-pentane + n-decane Methane + ethane + propane + n-pentane + n-decane + cyclohexane Methane + ethane + propane + n-pentane + n-decane + cyclopentane Methane + ethane + propane + n-pentane + n-decane + 2,2dimethylpropane (neopentane) Methane + ethane + propane + n-pentane + ndecane + cyclopentane + 2,2-dimethylpropane (neopentane) Synthethic natural gas Natural gasAlinta Gas Ltd., Perth, Australia + para-toluene sulfonic acid Synthethic natural gas + cyclohexane Synthethic natural gas + cyclopentane Synthethic natural gas + methylcyclopentane Reference Majumdar et al. [493] Sun et al. [658] Kang et al. [404] Zhang et al. [739] Majumdar et al. [493] Ostergaard et al. [552] Zhang et al. [738] Eichholz et al. [278] Link et al. [102] Jager et al. [377] Jager et al. [377] Ostergaard et al. [550] Ostergaard et al. [550] Zhang et al. [739] Sun et al. [659] Ostergaard et al. [552] Ostergaard et al. [552] Ostergaard et al. [552] Sun et al. [660] Masoudi et al. [501] Ostergaard et al. [552] Ostergaard et al. [552] Ostergaard et al. [552] Ostergaard et al. [552] T (K) 264272 274299 274295 274280 273289 276290 274284 262281 269293 249281 260292 276286 276284 274279 273289 280288 278288 275282 273288 259283 279286 276284 278287 278286 P (MPa) 1.33.1 0.58.6 0.212.9 0.64.9 0.21.4 1.47.9 23 2.19.5 7.99.6 216 7.473.2 6.222.6 5.115.4 1.17 0.66.2 2.68.1 27.7 25.1 0.96.1 3.946.6 1.23.8 0.83.1 0.24.2 0.93.4 V (cm3 ) n.a. 60 70 60 n.a. 540 60 6474 40 n.a. 1 540 540 60 n.a. 540 540 540 n.a. n.a. 540 540 540 540 Method SynVisVar SynVisVar AnTValVis SynVisVar SynVisVar SynVis AnTVarVis SynVisVar SynVis SynVis SynVisSpec SynVis SynVis SynVisVar SynVisVar SynVis SynVis SynVis SynVisVar SynNon SynVis SynVis SynVis SynVis
47
Ostergaard et al. [552]
278288
0.42.6
540
SynVis
Ostergaard et al. [552] Gnanendran and Amin [333] Ostergaard et al. [552] Ostergaard et al. [552] Ostergaard et al. [552]
276290 285293 277292 283288 278289
1.27.6 1.48 1.19.6 1.23.1 1.77
540 700 540 540 540
SynVis SynNonVisVar SynVis SynVis SynVis
Table 57 Articles containing corrigenda, comments or rebuttals to comments. Original article Nikitin et al. [537] Xia et al. [712] Bobbo et al. [177] da Silva and Barbosa [243] Lee et al. [445] Sako et al. [596] Garca-Gonzlez et al. [323] Kato et al. [407] Zhang and Kiran [740] Gozalpour et al. [337] Chapoy et al. [214] Kamps et al. [403] Kiepe et al. [415] Nikitin et al. [57] Glos et al. [331] Levitin et al. [454] Year 1998 1999 2000 2000 2000 2001 2002 2002 2003 2003 2003 2003 2003 2003 2004 2004 Components 1-Alkanols (C13C22) CO2 , water, sodium acetate, ammonium acetate HFC-125, HFC-236ea, HFC-32 CO2 , n-butanal CO2 , C.I. Disperse Blue 3, C.I. Disperse Blue 79 5 uorinated ethers and 2 uorinated ketones CO2 , hydroquinone, p-quinone HFC-32, HFC-125 CO2 , tetrahydrofuran, polysulfone Methane, propane, n-pentane, n-decane, n-hexadecane Methane, water, methane hydrate CO2 , [bmim][PF6] Methane, water, lithium bromide CO2 , polystyrene Propane, 2-methylpopane, n-butane, propylene CO2 , methanol, water, tetramethylammonium bicarbonate Article with corrigendum, comment, or rebuttal Nikitin et al. [538] Xia et al. [713] Deiters [258] Coquelet et al. [234] da Silva and Barbosa [246] Lee et al. [446] Sako et al. [597] Deiters [259] Kato et al. [408] Zhang and Kiran [741] Gozalpour et al. [338] Chapoy et al. [220] Kumelan et al. [433] Kiepe et al. [417] Nikitin et al. [58] Glos et al. [332] Levitin et al. [455] 2000 2000 2001 2002 2002 2001 2002 2003 2004 2006 2003 2005 2006 2004 2003 2006 2005 Corrigendum Corrigendum Comments Comments Rebuttal to Comments Corrigendum Corrigendum Comments Corrigendum Corrigendum Corrigendum Corrigendum Corrigendum Corrigendum Corrigendum Corrigendum Corrigendum
48
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High-Pressure Uid-Phase Equilibria: Experimental Methods and Systems Investigated (2000-2004)

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Fluid Phase Equilibria 288 (2010) 154

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Fluid Phase Equilibria

High-pressure uid-phase equilibria: Experimental methods and systems investigated (20002004)

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R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154

Fig. 2. Classication of experimental methods for high-pressure phase equilibria.

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R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154

R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154

R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154

R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 154

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10 Table 3 Pure-component systems: X. X

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1,1,1,2,2,3,3,4,4-Nonauorohexan-5-one 1,1,1,2,2,3,3-Heptauoropentan-4-one 1,1,1,2,2-Pentauoro-3-(1,1,2,2-tetrauoroethoxy)-propane 1,1,1,2,2-Pentauoro-3-butanone 1,1,1,2,2-Pentauoroethane (HFC-125)

1,1,1,2,2-Pentauoropentan-3-one 1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea)

1,1,1,3,3,3-Hexauoropropane (HFC-236fa) 1,1,1,3,3-Pentauoropropane (HFC-245fa) 1,1,1-Triuoro-2-(2,2,2-triuoroethoxy)ethane 1,1,1-Triuoroethane (HFC-143a)

1,1,2,2-Tetrauoro-1-(2,2,2-triuoroethoxy)ethane 1,1,2,2-Tetrauoro-2-(2,2-diuoroethoxy)ethane 1,1,2,2-Tetrauoro-3-(1,1,2,2-tetrauoroethoxy)propane 1,1,2,2-Tetrauorobutan-3-one 1,1-Diuoroethane (HFC-152a)

Chlorodiuoromethane (HCFC-22) Chlorotriuoromethane (CFC-13) Cumene Cyclohexane

Decanedioic acid Deuterium oxide Diamantane Diethyl sulde Diuoromethane (HFC-32)

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SynOthPcTc SynVis SynNonTc SynNonPcTc

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3,3,4,4,5,5,6,6-Octauorooctan-1,8-diol 3,3 ,4 ,5,7-Pentahydroxyavone (quercetin) 3-Methoxybenzamide 3-Methyl-1-butanol (isopentanol)

Atropine Azobenzene -Carotene -Cyclodextrin heneiicosaacetate Benzocaine Benzoic acid

Benzoin Bergamot peel oilCitrus bergamia -Estradiol Biphenyl

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N-Butylpyridinium tetrauoroborate [N-bupy][BF4] n-Butyraldehyde n-Decane

n-Dodecane n-Eicosane n-Heptacosane n-Heptane n-Hexacosane n-Hexadecane

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p-Quinone (1,4-benzoquinone) Procaine Propane

Propene Propranolol Propyl 2,5-dichlorobenzoate Propyl 4-hydroxybenzoate Propyl acrylate

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Vinyl acetate Vinyl acrylate Vitamin D2 Vitamin D3 Vitamin K3 Water

Weyburn formation brine Xenon XMPA refrigeration oil Zopiclone

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T (K) 134668 404408 406408 409409 310400

P (MPa) 1.976.2 1111.9 11.511.8 11.912 0.54.5

V (cm3 ) n.a. n.a. n.a. n.a. n.a.

Method SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynVisVarPcTc SynNonVar

AnGrav SynT SynT SynT SynT SynT SynT SynNon AnPTSemX

Propane Tetracosane Triacontane Water

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Poly(propylene glycol) Propane Squalane Sulfur hexauoride SF6 Tetracosane Water

Cyclobutanone Decahydronaphthalene (decalin) Diuoromethane (HFC-32)

Tetrapentacontane Tetratetracontane Titanocene dichloride Vitamin D2 Vitamin D3 Vitamin K3 Water

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V (cm3 ) 163 n.a. n.a. 10 300 80 28 27 27 60.13

AnTVal AnGrav SynVisVar SynVisVar SynVisVar

Dimethyl ether Hydrogen Methane n-Hexane Nitrogen Oxygen Propane Water

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Propene Tripalmitin Vitamin D2 Vitamin D3 Vitamin K3 Xenon

1,1,1,2,3,3,3-Heptauoropropane (HFC-227ea) 1,1,1,2,3,3-Hexauoropropane (HFC-236ea)

1,1,1,2-Tetrauoroethane (HFC-134a) 1,1,1-Triuoroethane (HFC-143a) Anthracene -Carotene Capsaicin Carbon dioxide

Triuoromethane (HFC-23) Triuoromethoxymethane Triuoromethyl methyl ether (HFC-143m)

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50 66 n.a. 66 17.4 n.a. 14 18 590 n.a.

2-Methylpropene Acetone Argon

Benzene Chlorotriuoromethane (CFC-13)

Poly(dimethylsiloxane) Propylene oxide Sulfur dioxide Sulfur hexauoride