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Resource & Environmental Consultants Ltd

TRIAL PIT INVESTIGATION - ONGOING SITE INVESTIGATION Thornton Power Station, Thornton-Cleveleys

REC Report 43391 August 2010


Prepared for Ballard Properties c/o Plan A-Design 86 Church Lane Culcheth Warrington WA3 5DJ
By

REC Ltd Osprey House Pacific Quay Broadway Manchester M50 2UE

Telephone

0161 868 1300 Fax 0161 868 1301 Website www.recltd.co.uk

QUALITY ASSURANCE

Issue/revision Remarks Date Prepared by Signature

Issue 1 Draft August 2010 M Wright

Revision 2

Revision 3

Checked by Signature

A Edgar

Authorised by Signature

M Wright

Project number

43391

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

EXECUTIVE SUMMARY
Context The current site owners, Ballard Properties wish to sell the land of the former Thornton power station for residential redevelopment. In order to determine the nature of any environmental risk at the site and provide clear guidance to any future buyer as to the status of the site, Ballard Properties have commissioned REC to undertake a series of site investigations using a scope previously agreed with Wyre Borough Council, of which this is the first phase. The next phase is a groundwater investigation with ongoing gas monitoring. The results of the investigation will then be provided to the council to accelerate any future decisions regarding planning and outstanding issues. This report should be read in conjunction with RECs March 2007 geo-environmental Investigation, a copy of which is included on the CD attached to the rear of this report. Conceptual Site Model Following earlier investigations and a review of development requirements (raising land level by 1.0m from current), the only realistic exposure pathways will be from volatile compounds generating a vapour risk or soluble hydrocarbons or metals leaching to groundwater and migrating towards and off-site surface water bodies. Unless significant solvents or PCB concentrations are present the risk of downward migration to the minor aquifer is negligible. Exploratory Investigation Ground Conditions Made Ground was encountered in all exploratory hole locations from ground level to a maximum proven depth of 2.3m though deeper made ground is likely to exist. The Made Ground comprises 6F2 type crushed demolition rubble of between 0.4m and 1.0m placed after the recent works, overlying gravelly clay with cobbles of brick, concrete, sandstone and gravels. In addition, pockets of a medium sand type coal was also encountered, typically used as a backfill. The Made Ground is thicker in the northern third of the site and to the immediate north of the Ballard Building. Underlying natural drift deposits generally comprised silty sands and sandy clays of marine and estuarine origin. Bedrock was not encountered and has not previously been encountered within the first 10.45m. The site overlies the Kirkham Mudstones which are classified as a minor aquifer. Tier 1 Risk Assessment The Tier I Human Health Risk Assessment has determined that there are while there are 6 exceedances of the Tier 1 screening values, five of those are for dermal contact and ingestion in soils that will be at least 1.0m bgl. The only realistic exceedance where a viable pathway exists is for naphthalene in two areas, the Former Electrical Transfer Station and to the immediate north of the Ballard Building. Naphthalene was only detected at a maximum concentration of 2.8mg/kg compared to a Tier 1 value of 1.5mg/kg for residential development.

II

Trial Pit Investigation Former Power Station, Thornton Cleveleys

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Some more soluble compounds have been identified on site and risk to controlled waters, and risk from vapours from groundwater must therefore be reviewed. Recommendations A groundwater investigation will be completed in line with the scope previously agreed with the council. This will review risk to controlled waters as well as vapour risk to future site users. Given that there is organic matter in the Made and natural ground, a preliminary ground gas investigation should be completed. Rather than necessarily completing a specific number of visits, an initial 6 visits will be carried out followed by a review and recommendations for continuous sampling if necessary.

III

Trial Pit Investigation Former Power Station, Thornton Cleveleys

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TABLE OF CONTENTS QUALITY ASSURANCE EXECUTIVE SUMMARY TABLE OF CONTENTS 1.0


1.1 1.2 1.3 1.4 1.5

I II IV 1
1 1 1 2 2

INTRODUCTION
Background Proposed Development Objectives Sources of Information Limitations

2.0
2.1 2.2 2.3 2.4 2.5

INITIAL CONCEPTUAL SITE MODEL (ICSM)


Source Areas of Potential Concern and Associated Chemicals Pathways Receptors Complete Source Pathway Receptor Linkages Conclusions

3
3 3 4 4 6

3.0

SITE SETTING

7
7 7 8

3.1 Site Description 3.2 Current Site Use 3.3 Surrounding Area

4.0

SITE INVESTIGATION

9
9 10 10 10 11

4.1 Exploratory Fieldwork 4.2 Summary of Site Investigation Observations 4.2.1 Ground Conditions 4.2.2 Groundwater Conditions 4.3 Laboratory Testing Programme

5.0

TIER 1 HUMAN HEALTH RISK ASSESSMENT

12
12 15 15 15

5.1 Soil Guideline Values 5.1.1 Human Health Risk Assessment Soil 5.2 Controlled Water Risk Assessment 5.3 Ground Gas Assessment

6.0 7.0

REVISED CONCEPTUAL SITE MODEL CONCLUSIONS & RECOMMENDATIONS APPENDICES

16 17

Appendix I Appendix II Appendix III

Glossary Limitations Figure 1 Site Location Plan Figure 2 Former Site Layout Figure 3 Trial Pit Location Plan IV

Trial Pit Investigation Former Power Station, Thornton Cleveleys Appendix IV Appendix V Appendix VI Appendix VII Appendix VIII Approved Scope of Work 2007 REC Trial Pit Logs Chemical Testing Results 2010 Origin of Tier I Values March 2007 Shallow Soils Laboratory Analytical Results.

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A CD containing a complete PDF version of this report is attached to hard copy of the report. Copies of the 2007 REC Reports 42614p1r0 (Desk Study) and 42614p2r0 (geoEnvironmental Investigation) are also saved on the CD.

Trial Pit Investigation Former Power Station, Thornton Cleveleys

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1.0
1.1

INTRODUCTION
Background

Resource and Environmental Consultants Ltd (REC) have been commissioned by Plan A Design, acting on behalf of Ballard Properties, Gibraltar, to undertake a staged intrusive investigation in line with the proposed investigation originally approved by Wyre Borough Council (WBC) and the Environment Agency (EA) in January 2008 (REC ref: 23p42444, dated December 2007). A copy of the proposed work is included in Appendix IV; this includes a site plan showing former activities and proposed investigation locations for trial pits and probeholes. A variation has arisen at the site since the 2007 proposal as the site had been demolished at the time of this investigation; demolition crews assisted in the location of all former facilities. This report covers the initial trial pitting investigation carried out to determine the shallow impact across the site and to tie in with existing investigation information from earlier site works carried out by REC. The scope of work consisted of the excavation of 23 trial pits across the site at previously identified areas of concern where activities could have lead to contamination of the soils with various compounds. The results of the trial pit investigation will be used to direct a separate borehole investigation designed to determine the impact to groundwater across the site. All acronyms used within this report are defined in the Glossary presented in Appendix I. 1.2 Proposed Development

Ballard Properties wish to sell the site for residential development. The purpose of this report is to provide the purchaser with a degree of confidence in the site and an idea of any outstanding costs that may be incurred redeveloping the site and satisfying any conditions applied by either the WBC or EA. 1.3 Objectives

The objectives of the trial pit investigation are to: Establish ground conditions across the site post-demolition; Undertake a preliminary stage of sampling and analysis to provide an overview of environmental issues identified in the December 2007 scope of work; Assess the implications of any potential environmental risks, liabilities and development constraints associated with the site in relation to the future use of the site and in relation to off-site receptors; Provide a factual and interpretative report relating to the site investigation and provide preliminary recommendations on any outstanding issues that may affect the future sale; and, Assess the likely costs of future works required to meet any further planning conditions.

Trial Pit Investigation Former Power Station, Thornton Cleveleys 1.4 Sources of Information

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Background information was sought from the Geo-Environmental Investigation Reports, Proposed Residential Development, Bourne Road REC Report 42444p3r0 dated April and May 2007 1.5 Limitations

The limitations of this report are presented in Appendix II.

Trial Pit Investigation Former Power Station, Thornton Cleveleys

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2.0

INITIAL CONCEPTUAL SITE MODEL (ICSM)

The 2007 scope of work was developed following an assessment of the site in line with CLR11. This ICSM was developed following a review of the site history, various site walkovers and the results of two phases of intrusive investigation. This ICSM has also been developed bearing in mind that the site level will need to be raised 1.0m from existing, post demolition, levelled topography. 2.1 Source Areas of Potential Concern and Associated Chemicals

The scope of work was developed following provision of a former works drawing which identified nine specific areas of concern and associated chemicals. These are: 1. Black Oil Tanks black oil for power generation; 2. Coal Conveyor Housing and Associated Oil Filled Manholes coal dust/granular material (and associated metals) and associated machine oils; 3. Zinc and Phosphate Tanks metallic powders; 4. Ballard Building small diesel tank and connections to the black oil tanks (above ground feed); 5. Electrical Transfer Station transformer oils and possibly PCBs; 6. Former Transformer Station transformer oils and PCBs; 7. Caustic, Acid and Diesel Tanks Caustic soda, acids, and diesel which could inter-react to generate semi volatile chlorinated solvents (SVOCs); 8. Effluent Pit for site drainage all surface water run-off and site waters were processed through this pit prior to discharge. Chlorinated solvents for cleaning were believed to be used on site and could have discharged via this structure; and 9. Day Oil Storage solvents (VOCs) used for cleaning were stored here as was a black oil day tank used to supply the generators. In addition to these specific areas, the site has been historically raised and as such there is a risk that Made Ground could contain elevated metals concentrations or organic matter which may generate ground gas. In addition, the degradation of certain hydrocarbon oils and chlorinated compounds can also generate ground gases such as methane and carbon dioxide. 2.2 Pathways

The chemicals of potential concern range from the more volatile degreasing chlorinated solvents to the viscous black oil and dense PCBs. The likely pathways for exposure and risk to human health are therefore: Inhalation of vapours from solvents and the lighter fractions of diesel (C6-10) in outdoor and indoor air environments; Dermal contact and ingestion of aromatic and aliphatic hydrocarbons, semi-volatile and volatile chlorinated solvents, heavy metals and PCBs in soils and home grown vegetables; 3

Trial Pit Investigation Former Power Station, Thornton Cleveleys 2.3

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Soluble and separate phase compounds leaching to controlled surface and groundwaters; Dermal contact and ingestion of impacted controlled waters; Phytotoxic impact to vegetation from particular metals; and Ground gas infiltration into buildings and voids generating potentially toxic or explosive conditions. Receptors

The proposed development is residential. The receptors are therefore: Infants exposed to soil ingestion, dermal contact, vegetable uptake (with associated soils) and inhalation of hydrocarbon vapours both indoors and outdoors, along with dust impacted by heavier oils or heavy metals; Construction workers exposed to dermal contact and ingestion of organic and inorganic impacted soils, contaminant and ground gas vapours within trenches and manholes, and inhalation of dust impacted by heavy metals; Groundwaters impacted by leaching from unsaturated soil and downward migration of dissolved phase hydrocarbon and dissolved metals plumes from perched waters to underlying aquifers. Earlier investigations have reported site geology to consist of marine and estuarine alluvium over Kirkham Mudstones which are classified as a Minor Aquifer. Completed investigations have identified low permeability sediments to 10.45m bgl including stiff slightly sandy or gravelly clay from approximately 7.5m to 10.45m. Hydrocarbon and heavy metals dissolved phase impact to surface waters; and Impact to utilities which come into contact with the various hydrocarbons and could either be damaged or act as migration pathways for either vapours or liquid/dissolved phase migration. Complete Source Pathway Receptor Linkages

2.4

In assessing the complete linkages for the site, the development program must be taken into account. In order for the site to be developed, it must be raised from the existing levels by 1.0m. This will mean the placement of at least 0.4m of cap before any materials are imported for use in gardens. The cap will be validated to show it is suitable for use and devoid of asbestos, and there are no volatile or semi-volatile hydrocarbons or heavy metals present that could generate a risk to human health or the environment. As a direct result of the cap, there will be no accessible soils on the development within the upper 1.0m that could generate any risk through dermal contact or ingestion. Consequently, any hydrocarbon range (either aliphatic or aromatic) >C10 and any SVOCs (>C10) along with PCBs and heavy metals (with the exception of elemental mercury), will not pose a risk to the future residents. In addition, the use of basic PPE will remove the risk to any construction worker from these heavier hydrocarbons. The complete linkages during and post-development are outlined in Table 2.1.

Trial Pit Investigation Former Power Station, Thornton Cleveleys Table 2.1
Source Human Health Residents and Construction workers

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Identified Linkages for Human Exposure


Exposure Pathway Potential Receptor Probability of Exposure Discussion of Pollutant Linkage Residents will be protected from any impacted soils by the placement of a cap and the existing break layer. Construction workers using basic PPE and hygiene will not be exposed to any significant risk UNLIKELY While these hydrocarbons may be present, it would be typical on a brownfield site with made ground to need to install a vapour membrane. Providing concentrations are not elevated, this would not necessarily need to be chemical resistant. LIKELY Given the dilution of the vapours, exposure could be limited to sheds and protected areas but generally this is UNLIKELY. Other than during construction of confined space structures, the limited exposure time and lack of shelter means exposure probability is UNLIKELY. While these hydrocarbons may be present, it would be typical on a brownfield site with made ground to need to install a vapour membrane in houses. Providing concentrations are not elevated, this would not necessarily need to be chemical resistant. UNLIKELY A build-up in any confined space is unlikely to generate a toxic exposure, given odours etc but could generate an oxygen deficient atmosphere - LIKELY There is impacted surface water in a ditch to the northwest which unless made inaccessible could allow contact. LIKELY Recharge of separate phase into open excavations leading to smearing of walls after draining and then dermal contact. LIKELY The trench to the north west is already impacted with low solubility heavy chain hydrocarbons smeared to the side walls. Perched water containing dissolved phase metals and hydrocarbons may leach to this ditch but most separate phase hydrocarbon on site is relatively viscous and unlikely to migrate. LIKELY

All hydrocarbons and heavy metals

Dermal contact and ingestion

Low

Residents indoors Hydrocarbons in soils diesel (<C11), VOCs and SVOCs Vapour inhalation Residents outdoors

Moderate to low

Low

Construction workers

Low

Residents indoors Vapour inhalation Hydrocarbons in waters diesel (<C11), VOCs and SVOCs Both groundwater and surface water Construction workers

Moderate to low

Low

Dermal contact and ingestion

Residents

Moderate

Construction Workers

Moderate

Controlled Water

Soluble hydrocarbons, dense hydrocarbons and metals

Lateral migration to surface water

Ditch to northwest and wetland slightly further west

Moderate

Trial Pit Investigation Former Power Station, Thornton Cleveleys


Source Exposure Pathway Downward migration to the Minor Aquifer from the shallow groundwater Potential Receptor Probability of Exposure

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Discussion of Pollutant Linkage Chlorinated solvents need to be present in separate phase to overcome any interstitial resistance while PCBs also have to be present in sufficient quantity to migrate downwards. Historical investigations have not identified such impact. UNLIKELY

Minor Aquifer

Low

2.5

Conclusions

With the site capped, only vapour intrusion from contaminants and ground gas, and dissolved phase impact to controlled waters are likely to generate any significant risk to human health or the environment. This phase of investigation has been designed to determine the likely risk of vapours from the soils and upper saturated zone, and the risk to controlled waters.

Trial Pit Investigation Former Power Station, Thornton Cleveleys

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3.0
3.1

SITE SETTING
Site Description Former Power Station, Bourne Road, Thornton E333830 N444190 121.5ha

Site Address National Grid Reference Site Area

Current site location map and former site layout plan are presented in Appendix III as Figure 1 and 2. 3.2 Current Site Use

The site was demolished in the first half of 2010 with the asbestos remediation completed at an earlier date. All concrete and brick was processed on site and used to raise the level of the site and remove any depressions or low spots. This involved significantly increasing the height of the northern sector previously occupied by the fuel storage and delivery area to the north of the site. Site Description The site is roughly rectangular in shape, narrowing to the south. Formerly the centre of the site was occupied by the main power station with support buildings and infrastructure mainly to the north and east. The site is currently flat, capped with 6F2 type material, with the exception of the Ballard Building which contains an oil powered generator. The only other feature of note is an impacted ditch to the northwest of the Ballard Building which was impacted by a line leak. There is still evidence of impact to the sides of the ditch. The ditch shallows to the south, running just west of the Ballard Building and a former diesel tank. There is no evidence of impact in the southern part of the ditch. The former power station was originally coal fired but then black oil, stored in the two former large vertical tanks at the northern boundary was used to run the Ballard Building generator. Animal tallow was also reportedly used at one stage. Hazardous Materials Storage Previous reports identified various contaminants on site ranging from diesel, transformer oils, black oil, some cleaning solvents and combinations of the two which may have generated semi-volatile chlorinated solvents. Polychlorinated Biphenyls (PCBs) The transformers located to the south of the main building had been operation before the PCB ban. These oils were known to have been spilled during vandalism of the site when unoccupied. The demolition works included pumping out shallow chambers and disposing of oils within said chambers. However, impact to ground was known to have occurred.

Trial Pit Investigation Former Power Station, Thornton Cleveleys Waste Storage

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Only limited waste was ever stored on site, as most products imported were combusted as part of the electrical generation process. There is no evidence of ash having been stored on site but coal dust/fines were present. There was some waste storage in a drum area but this was limited to 200 litre drums and there was no evidence of an historical loss in this area. However this Day Oil Storage area was identified as requiring further investigation. Drainage Issues A drainage survey was not undertaken as part of the site walkover. Former drains discharged to various locations, one of which is a partially above ground separator located off-site to the north of the Ballard Building. All other drains across the site have been destroyed or damaged during the demolition process. Asbestos Containing Materials (ACMs) Pre-demolition, during ecological surveys for bats, significant asbestos containing materials were identified. These were removed in 2008, prior to any demolition. The site was clear of all asbestos when demolished. During site works, no evidence of buried asbestos was observed in the Made Ground beneath the recently laid 6F2 type material. 3.3 Surrounding Area

The REC 42444p3r0 report which includes the desk study for this site is included on the CD at the rear of this report. The report identifies former ICI works to the east and north with residential properties to the west and south.

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4.0

SITE INVESTIGATION

The original proposed investigation consisted of 22 trial pits but the final number of locations excavated was 25. The trial pits were excavated over a series of site visits utilising contractor machinery. 4.1 Exploratory Fieldwork
nd

The full trial pit exploratory fieldwork was completed on 22 summarised in Table 3.1. Table 4.1 Summary of Fieldwork
No. of Positions 23 Location References TP301-TP323 TP324 and TP325

June 2010. The works are

Investigation Method Trial Pit Locations

Maximum Depth (m bgl) 2.5 1.9

Monitoring Wells NA

Notes m bgl metres below ground level.

The trial pits were located to provide environmental information to investigate the potential sources and pathways for contamination identified within 2007 proposed scope of work. The trial pit locations were chosen according to the 2007 scope which was based on nine identified potential areas of concern. The trial pit locations are illustrated in Figure 3 (Appendix III) along with the historical borehole, window sample and trial pit locations. The ground conditions encountered and details of monitoring well response zones are indicated on the logs which are provided in Appendix V. Soil samples destined for chemical analysis were collected at regular intervals in appropriate sampling containers. All samples were subsequently stored in cooled boxes prior to submission to Scientific Analysis Laboratories (SAL) for analysis in accordance with their UKAS accreditation where applicable. All samples were collected using appropriate PPE and sampling equipment that was cleaned at each sampling location. A detailed copy of REC Ltd sampling methodology, QA procedures and laboratory chain of custody forms can be provided upon request.

Trial Pit Investigation Former Power Station, Thornton Cleveleys

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4.2 4.2.1

Summary of Site Investigation Observations Ground Conditions

Made Ground Having crushed all site materials, the majority of the site is now covered by 6F2 type rubble of brick, concrete and occasional stone. Only the land to the very south of the site and along the western periphery is not covered by this material. There is a mound of this material still left on-site. Beneath the recently laid crushed demolition material is a Made Ground of predominantly clay with various percentages of silt, sand and gravels. In addition, historical excavations such as for sub-surface utility installation or around repairs have been backfilled with a black medium to fine sand of coal. Samples of this material were identified and collected for analysis. The Made Ground across the northern end of the site typically extends to between 1.5m to 2.3m bgl with historical structures usually governing the locations of the deeper Made Ground. Along the western boundary, just north of the Ballard Building, a number of excavations encountered consistently deep Made Ground. The Made Ground consisted of railway sleeper timbers and concrete slabs, as well as historical wiring, pipes and drains and an occasional ruptured, partially crushed drum. The sleepers had a strong kerosene odour and were below groundwater. To the south of the site, with the exception of around the former effluent pit (2.1m bgl), the depth of Made Ground was typically proven to between approximately 1.0m and 1.6m bgl. Drains were encountered sporadically across the site, installed within the Made Ground. Typically they contained a relatively small amount of water but oil sheens were observed at a number of locations, TP315, TP316 and TP319 (250mm clay pipe with visible transparent oil drops on the water). Natural Strata Underlying natural drift deposits generally comprised a mixture of lithologies with the Made Ground variously overlying typically compact or firm silty fine Sand, sandy Clays, clayey Sands but occasionally also soft to firm Clays and silty Clays. There was little consistency across the site. Bedrock was not encountered. 4.2.2 Groundwater Conditions

Other than from occasional drainage pipes or pockets within permeable backfill (now the site has no hard-surfacing), the only groundwater entries observed were typically associated with the interface between Made Ground and the more clayey natural strata. The depths varied according to the thickness of the Made Ground but there was evidence within the overlying strata that standing water levels would typically be around 1.0m bgl.

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4.3 Laboratory Testing Programme Selected soil samples were submitted for a range of analysis comprising, metals, pH, total sulphate, water soluble sulphate (2:1 extract), sulphide, cyanide, phenols, speciated polyaromatic hydrocarbons (PAHs), organic carbon and total plus speciated petroleum hydrocarbon (with and without BTEX) (TPH, SpTPH Ali/Aro and SpTPH CWG). In addition samples were analysed for volatile and semi-volatile organic compounds and PCBs (EC7). Scientific Analysis Laboratories (SAL) Ltd of Manchester undertook the analytical work and the testing results are included in Appendix VI.

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5.0
5.1

TIER 1 HUMAN HEALTH RISK ASSESSMENT


Soil Guideline Values

REC has undertaken a Tier 1 human health risk assessment to determine if any potential contaminants within the underlying soils and groundwater pose an unacceptable level of risk to the identified receptors. At a Tier 1 stage the long term (chronic) human health toxicity of the soil has been assessed with reference to EA Contaminated Land Exposure Assessment (CLEA) Soil Guideline Values (SGV) and where absent, General Acceptance Criteria (GACs) published by LQM/CIEH (2nd edition). The results of this comparison have been summarised within Table 5.1 (overleaf). An earlier investigation completed in March 2007 and reported in REC report 42614p2r0 also included a Tier 1 human health risk assessment. A copy of that report is included on the CD attached to the rear of the hard copy. The investigation locations are included on Figure 3 in Appendix III and the laboratory soils analytical results are included in Appendix VIII. Given that GAC values have changed, REC has re-reviewed the data for the volatile fractions given that this is the most likely realistic exposure pathway.

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Trial Pit Environmental Investigation Former Power Station, Thornton Cleveleys Table 5.1 Summary of Inorganic and Hydrocarbon Toxicity Assessment for a Residential End Use with Plant Uptake
Determinand Arsenic Cadmium Chromium (Hexavalent) Chromium VII Lead Mercury Nickel Selenium Copper Zinc Cyanide - Total Phenols - Total. VIII PCBs Total EC7 Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene (i) Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(ghi)Perylene Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg GAC 32 10 4.3 3000 450 11 130 350 2330 3750 791 210 0.01 1.5 170 210 160 92 2300 260 560 3.1 6 14.1 0.83 3.2 0.76 44 n 13 13 6 13 13 13 13 6 13 14 13 13 5 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 MC and other exceedances 94 (33) 2 <1 83 300 <1 760 <3 260 490 <1 <1 0.00106 2.8 (0.68) 0.69 0.24 0.68 3.8 1.7 7.5 6.0 4.4 3.9 6.8 3.6 1.9 0.83 Location of MC (as numbered Section 2.1) Former Transformers TP317 1.4mbgl Ballard Building - TP310 0.5mbgl Former Transformers TP317 1.4mbgl Ballard Building - TP310 0.6mbgl Transformer Building TP317 1.4mbgl Ballard Building - TP310 0.5mbgl Transformer Building - TP317 1.4mbgl Transformer Building - TP317 1.4mbgl Pathway 1 1 1 1 1 2 1 1 1 1 1 1 1 2 3 1 1 3 3 3 3 3 3 3 3 3 3 3

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Assessment for Human Health No exposure pathway No further assessment No further assessment No further assessment No further assessment No further assessment No exposure pathway No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment Further assessment required No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment No exposure pathway No further assessment No exposure pathway No further assessment

Former Transformers - TP317 0.8m Ballard Building - WS205 0.5mbgl Electrical Transfer Station - TP315 -1.6mbgl Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station - TP315 -1.6mbgl Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station Electrical Transfer Station

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Determinand Benzene (ii) Toluene (ii) Ethylbenzene (ii)(iii) Xylenes TPH C5-C6 (aliphatic)* TPH C6-C8 (aliphatic)* TPH C8-C10 (aliphatic)* TPH C10-C12 (aliphatic)* TPH C12-C16 (aromatic)* TPH C16-C21 (aromatic)* TPH C21-C35 (aromatic)*
(ii)

Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

GAC 0.33 610 350 230 30 73 19 69 140 250 890

n 5 5 5 5 15 15 15 15 15 15 15

MC and other exceedances <0.001 0.003 <0.001 0.004 <0.01 0.056 0.23 400 54 29 24

Location of MC (as numbered Section 2.1) Ballard Building - TP310 -1.8mbgl Ballard Building - TP310 - 1.8mbgl Caustic,Acid,Diesel TP319 1.5mbgl Caustic,Acid,Diesel TP319 -1.5mbgl Coal Conveyor Housing - TP303 1.9mbgl Coal Conveyor Housing - TP303 1.9mbgl Coal Conveyor Housing - TP303 1.9mbgl Caustic,Acid,Diesel TP319 -1.5mbgl

Pathway 2 2 2 2 2 2 2 2 1 1 1

Assessment for Human Health No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment No further assessment Further Assessment Required No further assessment No further assessment No further assessment

Notes Main Exposure Pathways: 1 = Soil Ingestion, 2 = Vapour Inhalation (indoor), 3 = Dermal Contact & Ingestion, 4 = Dust Inhalation. Abbreviations: HCV = Human Criteria Value, n = number of samples, MC = Maximum concentration; US95 = The upper 95th percentile bound of the samples. i) The Tier 1 GAC for the hydrocarbon fraction is derived from the CIEH assessment for petroleum hydrocarbons Criteria Working Group (CWG) for both aliphatic and aromatic compounds. 5 12 12 REC has utilised the Tier 1 values for aliphatic compounds for the volatile and semi volatile fractions (C -C ) and the Tier 1 values for aromatic compound for the non volatile fractions (C 35 C ). The comparison of a total (aliphatic/aromatic) compounds to an individual fraction is considered to be a conservative approach and satisfactory for the protection of human health. ii) Methyl Mercury SGV. iii) Benzo (b) Fluoranthene (5.6mg/kg) Benzo (k) Fluoranthene (8.5mg/kg) iv) Xylenes based on p-xylene (o-xylene 250mg/kg, m-xylene 240mg/kg) v) BTEX based on 6% SOM. vi) Lead exposure based on former SGV as CLEA 1.06 not appropriate model for lead exposure and the calculated concentration is 924mg/kg. Issues raised by HPC and EU on lead exposure suggest a lower number is more appropriate. vii) Screening value based on child soil ingestion, generated using Tox 12 - Dioxin Like PCBs modelled with RBCA for 100mg/day soil consumption and SR3 child stats.

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In addition to the listed compounds, REC also analysed for the SVOC and VOC in select soil samples at locations identified within the 2007 scope of works. The analysis for VOCs did not detect any VOCs while the analysis for SVOCs only detected low concentrations of PAHs. 5.1.1 Human Health Risk Assessment Soil

For the purposes of the Tier 1 assessment REC have compared the laboratory test data directly to the relevant Tier 1 GAC value for the protection of human health. In total there were six exceedances of the Tier 1 values. However, of those six, four are based on ingestion and since the site will have a significant protective cap, no pathway actually exists. The only compounds for which there was an exceedance, based on indoor air inhalation were naphthalene in WS205 in shallow soil (0.5mbgl) and aliphatic C10-12 in TP303 at 1.9mbgl. The impact in WS205 was not reflected in the deeper samples of the 2010 investigation or other samples from 2007. The impact in TP303 was not identified laterally to the north or east, which mark the north side and adjacent locations to the former conveyor housing. Further delineation is required in this area to determine whether this is an actual risk. This will include monitoring of in-situ vapour concentrations and an assessment of the depth to groundwater. Impact beneath the saturated zone can only volatilise from dissolved phase and as such, an assessment of the dissolved phase in this area will provide further information regarding the possible risk. 5.2 Controlled Water Risk Assessment

Lighter, soluble fractions of fuel range hydrocarbons have been detected on-site and a groundwater investigation will be required to determine the risk presented by the identified impact. This investigation will include dissolved metals and PCBs. 5.3 Ground Gas Assessment

The initial conceptual site model identified the following possible sources of ground gas that may affect the subject site: Made Ground associated with historical site raising and construction/demolition activities.

As part of a groundwater investigation, the monitoring wells will also be gauged for ground gases and gas flow rates.

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6.0

REVISED CONCEPTUAL SITE MODEL

Following the completion of the trial pit investigation, chemical analysis and assessment, REC Ltd has identified only one potentially significant pollutant linkage based on a residential redevelopment of the site. Further work is proposed to investigate this linkage as well as determine the risk to controlled waters across and beyond the site. Based on the soils investigation carried out to date, there is no significant impediment to the residential redevelopment of the site.

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7.0

CONCLUSIONS & RECOMMENDATIONS

Environmental The Tier I Human Health Risk Assessment has determined that there is only one location where volatile organic hydrocarbons are present that could generate a risk to human health through indoor air inhalation. However, further work is required to confirm the extent of the impacted area as well as complete general site coverage. As a result of the cap that will be placed to raise the site, providing any imported material is suitably screened, there is are no unacceptable concentrations of potential contaminants within the underlying soils that would pose a potential risk to human health of future site occupants or controlled waters. Given the organic materials (debris) identified during the investigation, a ground gas investigation will also be required. Recommendations An intrusive investigation comprising the installation of environmental monitoring wells is required to determine impact to groundwater across the site from the more soluble compounds and to determine what potential risk they pose as a source of vapours. The installation of wells will also allow a full assessment of the ground gas regime. Since the site has been demolished, certain wells that were proposed as augmenting the 2007 proposal have been destroyed and consequently some additional wells on top of the proposed 15 should be installed. Once the data is available, further investigation to finalise delineation may be required.

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Trial Pit Investigation Former Power Station, Thornton Cleveleys

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APPENDIX I GLOSSARY

Trial Pit Investigation Former Power Station, Thornton Cleveleys TERMS AST UST EA CSM GL ND NR BSI BGS CLEA SGV GAC CIEH PID CIRIA GSV EQS DWS PAH TPH (CWG) VOC SVOC SPT VCCs QA

August 2010 43391p1r0

Above ground Storage Tank Underground Storage Tank Environment Agency Conceptual Site Model Ground Level Not Detected Not Recorded British Standards Institute British Geological Survey Contaminated Land Exposure Assessment Soil Guideline Value General Assessment Criteria Chartered Institute of Environmental Health Photo Ionisation Detector Construction Industry Research Association Gas Screening Value Environmental Quality Standard Drinking Water Standard Poly Aromatic Hydrocarbon Total Petroleum Hydrocarbon (Criteria Working Group) Volatile Organic Compound Semi Volatile Organic Compound Standard Penetration Test Vibro Concrete Columns Quality Assurance

UNITS m km % %v/v mb 1/hr g/l ppb mg/kg ppm mg/m3 m bgl m bcl mAOD kN/m2 m

Metres Kilometres Percent Percent volume in air Milli Bars (atmospheric pressure) Litres per hour Micrograms per Litre (parts per billion) Parts Per Billion Milligrams per kilogram (parts per million) Parts Per Million Milligram per metre cubed Metres Below Ground Level Metre Below Cover Level Metres Above Ordnance Datum (sea level) Kilo Newtons per metre squared Micro metre

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

APPENDIX II LIMITATIONS

Trial Pit Investigation Former Power Station, Thornton Cleveleys


1. 2.

August 2010 43391p1r0

This report and its findings should be considered in relation to the terms of reference and objectives agreed between REC Ltd and the Client as indicated in Section 1.2. For the work, reliance has been placed on publicly available data obtained from the sources identified. The information is not necessarily exhaustive and further information relevant to the site may be available from other sources. When using the information it has been assumed it is correct. No attempt has been made to verify the information. This report has been produced in accordance with current UK policy and legislative requirements for land and groundwater contamination which are enforced by the local authority and the Environment Agency. Liabilities associated with land contamination are complex and requires advice from legal professionals. During the site walkover reasonable effort has been made to obtain an overview of the site conditions. However, during the site walkover no attempt has been made to enter areas of the site that are unsafe or present a risk to health and safety, are locked, barricaded, overgrown, or the location of the area has not be made known or accessible. Access considerations, the presence of services and the activities being carried out on the site limited the locations where sampling locations could be installed and the techniques that could be used. In addition to the above REC Ltd note that when investigating, or developing, potentially contaminated land it is important to recognise that sub-surface conditions may vary spatially and also with time. The absence of certain ground, ground gas, and contamination or groundwater conditions at the positions tested is not a guarantee that such conditions do not exist anywhere across the site. Due to the presence of existing buildings and structures access could not be obtained to all areas. Additional contamination may be identified following the removal of the buildings or hard standing. Site sensitivity assessments have been made based on available information at the time of writing and are ultimately for the decision of the regulatory authorities. Where mention has been made to the identification of Japanese Knotweed and other invasive plant species and asbestos or asbestos-containing materials this is for indicative purposes only and do not constitute or replace full and proper surveys. The executive summary, conclusions and recommendations sections of the report provide an overview and guidance only and should not be specifically relied upon without considering the context of the report in full.

3.

4.

5. 6.

7. 8.

9.

10. This report presents an interpretation of the geotechnical information established by excavation, observation and testing. Whilst every effort is made in interpretative reporting to assess the soil conditions over the Site it should be noted that natural strata vary from point to point and that man made deposits are subject to an even greater diversity. Groundwater conditions are dependent on seasonal and other factors. Consequently there may be conditions present not revealed by this investigation. 11. REC can not be held responsible for any use of the report or its contents for any purpose other than that for which it was prepared. The copyright in this report and other plans and documents prepared by REC is owned by them and no such plans or documents may be reproduced, published or adapted without written consent. Complete copies of this may, however, be made and distributed by the client as is expected in dealing with matters related to its commission. Should the client pass copies of the report to other parties for information, the whole report should be copied, but no professional liability or warranties shall be extended to other parties by REC in this connection without their explicit written agreement there to by REC. 12. Rather, this investigation has been undertaken to provide a preliminary characterisation of the existing subsurface geotechnical characteristics and make up and the findings of this study are our best interpretation of the data collected, within the scope of work and agreed budget. New information, revised practices or changes in legislation may necessitate the re-interpretation of the report, in whole or in part. 13. This investigation has been undertaken to reasonably characterise existing sub-surface conditions and the findings of this study are our best interpretation of the data collected, within the scope of work and agreed budget. New information, revised practices or changes in legislation may necessitate the re-interpretation of the report, in whole or in part.

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

APPENDIX III FIGURES

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

APPENDIX IV 2007 SCOPE OF WORK REC 23P42444

Resource & En iron!ent"# $onsu#t"nts Ltd

<s#rey Ho se Pacific = ay ,roadway *anchester *>0 2?E "ele#hone3 0191-595-1;00 :a73 0191-595-1;01 E-mail3 sales@recltd(co( & htt#388www(recltd(co( &

ADDITIONAL PHASES OF INVESTIGATION PROPOSED RESIDENTIAL DEVELOPMENT, BOURNE ROAD, THORNTON Introduction A way-forward meeting was held on 11 December 2007 at the NPL Estates office at Hill Ho se! "hornton to disc ss what information was needed to #ro$ide the reg latory a thorities with s fficient confidence to a##ro$e conditional #lanning for the #ro#osed residential de$elo#ment %and associated wor&s' referenced abo$e( "he meeting was attended by re#resentati$es of the En$ironment Agency %EA' %)t art *cDonald'! the en$ironmental health de#artment %EHD' %+orinne *ason' and their cons ltants! Encia %Phil Hill'! NPL Estates %)imon "owers'! *iller Homes %*i&e ,owman' and -E+ Limited %*arc s .right and /ayne +arric&'( 0t is -E+1s nderstanding from that meeting that the o$er-riding concern of the EA and EHD is that as de$elo#ment contin es! costs materialise that ca se *iller Homes %and conse2 ently NPL Estates' to abandon the de$elo#ment #lans with #ro#osed remediation left nfinished( "he concerns were in two #arts! the first directly relate to a #ercei$ed lac& of in$estigati$e co$er for3 "he former #ower station area4 and "he former 0+0 #lant land on the northern bo ndary of the #ro#osed de$elo#ment(

"he second iss e was raised by the EA! who #ointed o t that a remedial target for aniline had not been de$elo#ed in the b ried dr m area and that this co ld not arri$ed at ntil the dissol$ed #hase #l me had been f lly delineated or at least st died in s fficient detail( Additional minor concerns were raised o$er #resentation s ch as identifying areas by an agreed! recognisable name and #ro$iding a scaled ma# of the entire area of the de$elo#ment with gro ndwater tied in across the rele$ant areas( As a conse2 ence! -E+ was #ro$ided with "hornton Power )tation Plan No( 56611 %Location of Plant E2 i#ment' which indicated the location and contents of all #ossible contaminants of concern %+o+s'( A co#y of this #lan is attached for the EA! EHD and Encia and has been referenced thro gho t this doc ment( ,ased on the meeting! -E+ wo ld obser$e on behalf of its client! *iller Homes! that historical e7#erience of im#act from single de$elo#ment8single se #ower stations indicates that significant dissol$ed #hase im#act is nli&ely and that most contaminants ha$e a low sol bility! mobility and $olatility! ma&ing them relati$ely low ris& where residential de$elo#ment is concerned( )imilarly! significant wor&s ha$e been com#leted at the aniline area and that! allied to e7tensi$e historical &nowledge! ma&es -E+ confident that no significant! as yet ndetected contaminant iss es are #resent in the aniline area( -E+ ac&nowledges that a lea&ing drainage system co ld ha$e generated gro ndwater iss es along the northern bo ndary at the former 0+0 #lant and that information for this area was limited(

-egistered Address3 Hadfield Ho se! Hadfield )treet! *anchester! *19 6:E( +om#any -egistration No( ;1;;5;2

*iller Homes ,o rne -oad! "hornton

20 December 2007 2;#8A2AAA

O%&ecti e -E+ has re$iewed all a$ailable soil and gro ndwater data a$ailable for the site and identified #ossible e7isting wells beyond the railway that may #ro$ide downgradient delineation in the aniline area( "he res lt of that re$iew has been sed to de$elo# the following #ro#osed sco#e of wor&( "he obBecti$e of this #ro#osed wor& is to3 1( Pro$ide s fficient confidence to *iller Homes and NPL Estates that remediation costs %and conse2 ently land $al e' are not significantly different to those already antici#ated4 and 2( Pro$ide the EA and EHD s fficient information to show that no ne7#ected costs e7ist in the three areas of concern %#ower station! aniline area! northern bo ndary 0+0 area'( :or the EA and EHD! this information will incl de soil and s rface8gro ndwater iss es across the sites! remedial targets for the aniline %if needed' and gro nd gas information #ertinent to fo ndation design8#rotection( Sco'e o( )or* 0t is intended that the sco#e of wor& will be com#leted in discrete #hases! which wo ld allow for a cost effecti$e and fle7ible strategy to be im#lemented( "his essentially means that while in some areas! both drilling and trial #itting will be carried o t side by side! there may be some locations where some acti$ities change as a res lt of soils analysis or well locations change from those re#resented on the attached #lans( :or the # r#ose of this o tline sco#e of wor&! a##licable names ha$e been assigned to each area of concern %A<+' with an o tline of acti$ities e7#ected in each area and #ro#osed intr si$e wor&s! analysis and e7#lanation for the analysis( .here access is c rrently not #ossible! these areas ha$e been left o t( 0t is not the # r#ose of this doc ment to com#letely re#rod ce #re$io s assessments of the sites( PROPOSED SITE )OR+ , FORMER PO)ER STATION "he wor& in this area has been bro&en down into s b-sections based on #otential contaminants of concern and the #otential im#act from those contaminants( :or instance! blac& oil has a $ery low sol bility and is relati$ely immobile in se#arate #hase( "herefore! e7tensi$e in$estigation away from any blac& oil so rce wo ld! at this stage! be #ointless! b t has not been r led o t( ,ased on the re$iew of this site with the EA and e7isting -E+-identified areas of concern! combined with a wal&-o$er com#leted on 11 December 2007! -E+ ha$e identified the following A<+s in the Power )tation re2 iring f rther intr si$e in$estigation3 1( 2( ;( A( >( 9( 7( 5( "he ,lac& <il "an&s %1;! 2A' +oal +on$eyor Ho sing %and associated manhole' %10! 11' Cinc and Phos#hate "an&s %15! 16! 20' ,allard Pro#erties %with associated diesel tan& o$er-fill' "he Day <il "an& and .aste <il Dr m Area %6! 19! 17' "he Effl ent Pit %9!7!2>!27' +a stics! Acids and Diesel "an&s %1! 2! ;' "he "ransformer Area

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-eso rce D En$ironmental +ons ltants Ltd

*iller Homes ,o rne -oad! "hornton

20 December 2007 2;#8A2AAA

"he referenced n mbers refer to n mbered locations and contents for tan&s etc( on Plan No(56611( A site #lan o tlining these areas is incl ded as :ig re 1( D e to the #otential im#act of contaminants of concern %+o+' on controlled waters and the #ossible #resence of haEardo s gro nd gas in the $icinity of the site! additional intr si$e wor&s followed by gro nd gas and gro ndwater monitoring is #ro#osed( "he sco#e for each A<+ is as follows3 -. B#"c* Oi# t"n*s Pre$io s in$estigations consisted of a n mber of window sam#les and trial #its( "esting detected $ery little hydrocarbon im#act that wo ld generate a ris& to either h man health or the en$ironment( Howe$er! the #re$io s in$estigation was not close eno gh to detect any iss es associated with the former diesel tan& %2A' located between the two main blac& oil tan&s %1;' and adBacent to the #i#ing r ns( -E+ will attem#t to com#lete a trial #it in this area to #ro$ide confidence of bo ndary co$er( ,ased on to#ogra#hy! im#act in this area is li&ely to be migrating north and as s ch! one trial #it will be e7ca$ated between .)201 and .)202( )oil sam#les will be collected to be analysed for s#eciated total #etrole m hydrocarbons %)#("PH' and s#eciated #oly-cyclic aromatic hydrocarbons %PAH' across the water table interface while made gro nd will be characterised for inorganics( D e to str ct res in #lace! this area cannot be f lly characterised ntil after demolition( -E+ does not en$isage testing either soils or waters in this A<+ for $olatile and semi$olatile organic com#o nds %F<+s and )F<+s' at this stage( /. $o"# $on e0or Housin1 "he main so rce area re2 iring in$estigation is a #artly bac&filled waste water transfer manhole located in the northwestern area of this A<+( <ne trial #it com#letely near the manhole did not identify any significant im#act b t additionally testing will #ro$ide all-ro nd co$er( "wo trial #its and one window sam#le location will be com#leted here( "he secondary area is the coal container areas %11' and an associated oil stained area on the so th side of the main ho sing( "P209 was com#leted adBacent to this b t no significant im#act was #ro$en( A total of three trial #its and two window sam#le locations will be com#leted aro nd the +on$eyor area! all to be #ositioned to the so theast of a c l$ert attached to nearby s rface water( 0n total! fi$e trial #its and three window sam#le #robeholes will be com#leted in this area with wells installed in all window sam#le locations( )oil sam#les will be tested for )#("PH! PAH and inorganics( -E+ does not en$isage the need to analyse soils for F<+s and )F<+s in this A<+( "esting for gro ndwater will target identified +o+( Any oils within the manhole will be tested for Prod ct 0D( 2. 3inc "nd P4os'4"te T"n*s Gi$en that Einc is #hytoto7ic as well as #otentially haEardo s to h mans and #hos#hates can also destabilise s rface water en$ironments! a single trial #it will be e7ca$ated adBacent to these tan&s %15! 16! 20' to test for Einc and #hos#hates( A sam#le from across the nsat rated8sat rated soil interface will also be tested for )#("PH(

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-eso rce D En$ironmental +ons ltants Ltd

*iller Homes ,o rne -oad! "hornton

20 December 2007 2;#8A2AAA

5. B"##"rd Pro'erties Diesel im#acted nsat rated and sat rated soil were identified in the $icinity of the former diesel tan& in this area and with its #ro7imity to s rface waters! -E+ ha$e identified the need for fi$e additional trial #its to delineate the e7tent of the significant hydrocarbon im#act and three window sam#le boreholes %com#leted as wells' to confirm $ertical im#act as well as im#act to gro ndwater( "he three wells are needed to triang late gro ndwater flow and to determine $elocities if necessary( A s rface water sam#le will be collected from the ndrained area adBacent to this site( "he soils and waters will be analysed for )#("PH! PAH and inorganics( A limited n mber of soils will be tested for F<+s and )F<+s4 if any F<+s or )F<+s are detected! then waters will be analysed for the a##ro#riate s ites( "he s rface water sam#le will be tested for all s ites listed( 6. T4e D"0 Oi# T"n* "nd )"ste Oi# Dru! Are" "he Day "an& %6' contained ,lac& <il and as s ch! only significant ongoing s#ills %of which there is no e$idence' wo ld ha$e generated a significant im#act in this area( "he waste dr m area has been re$iewed and little e$idence of any s#ills was identified( .ithin the adBacent b ilding howe$er was the tri&lone8waste oil storage %17'( Altho gh c rrently inaccessible! -E+ will test for F<+s in this area( Gi$en the machinery and other inaccessible A<+s in the $icinity of this area! -E+ #ro#ose com#leting two trial #its and two window sam#le wells in areas where access is #ossible aro nd the former dr mmed waste oil storage and Day "an& areas( "he soils and water sam#les will be tested for )#("PH! PAH and inorganics and sam#les will be held #ending initial res lts from the Effl ent Pit! to be tested for other +o+( 7. T4e E((#uent Pit .ater and oil draining from inside the main b ilding are di$erted to this area( "hese oils are #robably either l bricant or coolant based and ha$e low sol bility( Howe$er! there co ld be some resid al P+, contamination from earlier se that may ha$e mobilised beyond the #it and sol$ents sed within the site co ld be #resent within the oils( )tr ct res still in #lace both abo$e and below gro nd will limit the e7tent of any in$estigation in this area b t intr si$e wor&s can be com#leted that will highlight the le$el of any significant ris& in this area( -E+ #ro#oses to com#lete three trial #its and install two monitoring wells aro nd the #it( "he soil and water sam#les will be tested for )#("PH! PAH! inorganics and F<+s % sed in machine maintenance and cleaning'( 8. $"ustic, Acid "nd Diese# T"n*s .hilst the ca stic tan& and acid tan& #rod cts will ha$e ne tralised #on im#act with soils and gro ndwater! any diesel s#ills in this area co ld still be #resent either in the soils and8or gro ndwater( "he reaction of any acids on the hydrocarbons is also n&nown( ,ased on access iss es and #re$io s site in$estigation! -E+ #ro#oses two trial #its in this area to identify any im#act to soils and any #erched waters( "he soil sam#les will be tested for )#("PH! PAH and )F<+s in the e$ent of any acid-diesel reactions generating any hea$ier chlorinated hydrocarbons( "he #ro7imity of this site to the transformer area means that sam#les will be held for P+, testing #ending the res lts of the soils analysis in the "ransformer Area(

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-eso rce D En$ironmental +ons ltants Ltd

*iller Homes ,o rne -oad! "hornton

20 December 2007 2;#8A2AAA

9. Tr"ns(or!er Are" "he b ilding in this area was $andalised and finally set alight( <il losses d ring this time are n&nown( .hile P+,s were no longer in ser$ice and most transformers sho ld ha$e had oils drained and re#laced with non-P+, oils! some resid al im#act is #ossible( 0n addition to the transformer b ilding! there is a $ery large ndergro nd concrete str ct re c rrently holding water and hea$y oils and an electrical distrib tion b ilding in the northwest of this A<+( 0t is -E+1s o#inion that gi$en the low sol bility of the oils sed in these areas! that this in$estigation will s ##ort earlier intr si$e wor&s that did not identify any significant dee# contaminant iss es in this area( 0n total! -E+ #ro#oses to e7ca$ate three additional trial #its in this area and install two monitoring wells %bearing in mind that wells .)205 and +P207 are #resent in this area'( "he soils will be tested for s#eciated "PH! PAH and inorganics along with P+,s( .aters will be tested for )#("PH! PAH %and P+,s if detected in soils' while any #rod ct within the holding tan& will also be tested for identification %carbon range! density'( Po:er St"tion Ground G"s In esti1"tion -E+ #ro#oses to com#lete site co$erage with three additional gro nd gas monitoring wells( "hese wells along with the monitoring wells from the aforementioned wor&s will be monitored for gro nd gas concentrations %carbon dio7ide and methane' and flow rates( Tot"# Intrusi e )or*s "t Po:er St"tion -E+ #ro#oses com#leting 2;No( trial #its to a##ro7imately 2(0m de#th %a##ro7imately 1(0m below water table' and 1>No( #robeholes com#leted as monitoring wells %incl ding the gas monitoring wells'( "he #ro$isional locations of all the o tlined trial #its and window sam#ling locations are incl ded on the attached :ig re 1( "he drilling will be com#leted sing a window sam#ling rig ca#able of allowing the installation of >0mm diameter monitoring wells( All the wells will be screened from abo$e the water table to a##ro7imately ;(0m below it( 0t is #ro#osed that trial #itting will be nderta&en within this sector of the site by the se of a /+, ;+H e7ca$ator fitted with a hydra lic brea&er( :ollowing installation of wells! all locations will be s r$eyed s ch that a single scale #lan can be #rod ced showing all locations acc rately and allowing gro ndwater flow direction to be determined across the site( PROPOSED SITE )OR+ , FORMER NPL LAND "he wor& in this area has been bro&en down into two sections based on #otential contaminants of concern and the #otential im#act from those contaminants( ,ased on the re$iew of this site with the EA and e7isting -E+-identified areas of concern! combined with a wal&-o$er com#leted on 11 December 2007! -E+ ha$e identified the following areas of concern %A<+' in the northern de$elo#ment area3 1( "he :ormer 0+0 :acility %Phosgene and - bber #rod ction' 2( "he :ormer Air Prod cts Plant 0n addition! -E+ has identified $ario s s rface water bodies and areas where gro nd gas monitoring has not been com#leted(
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-eso rce D En$ironmental +ons ltants Ltd

*iller Homes ,o rne -oad! "hornton

20 December 2007 2;#8A2AAA

A site #lan o tlining these areas is incl ded as :ig re 2( D e to the #otential im#act of contaminants of concern %+o+' on controlled waters and the #ossible #resence of haEardo s gro nd gas in the $icinity of the site! -E+ #ro#ose to com#lete additional intr si$e wor&s followed by gro nd gas and gro ndwater monitoring is #ro#osed( "he sco#e for each A<+ is as follows3 -. T4e For!er I$I F"ci#it0 E7isting drain s m#s and #otentially im#acted drain lines are li&ely to be #resent in this area that formally ho sed a Phosgene #lant and -0 - bber #lant( "hese drains co ld #otentially be acting as so rces for ongoing im#act to gro ndwater( "hese im#acts are relati$ely small and co ld be localised( An in$estigation s#acing of a##ro7imately 1>m #er trial #it is s ggested for a sco#e of wor& designed to identify and characterise localised im#act( 0n total -E+ estimate e7ca$ating 20No( trial #its across this area with m ch of the wor& re2 iring brea&ing of concrete( )oil sam#les will be selecti$ely tested for )#("PH! F<+! )F<+ and inorganics %the )F<+ s ite incl des the EPA 19 PAH s ite'( :ollowing the recei#t of the res lts of the soil sam#le analysis! a total of fo r additional monitoring wells will be installed in this area sing the window sam#ling techni2 e( 0t sho ld be noted that there are # to fo r s r$i$ing monitoring wells in this area that will also be tested( "he e7act locations of the new wells will be based on any hydrocarbon im#act detected( Gro ndwater sam#les will be tested for a s ite com#osed of those determinants identified in soils and considering the formerly identified aniline im#act to the northeast( /. T4e For!er Air Products Are" "he #re$io s in$estigation identified significant limestone gra$el bac&fill in this area( "his is a #otential so rce of ele$ated carbon dio7ide( A gro nd gas monitoring well will be installed in this area( Are" )ide Ground G"s Monitorin1 -E+ ha$e allowed for three additional gro nd gas monitoring wells o tside of the former 0+0 and Air Prod cts areas where gro nd gas monitoring #oints will be installed to allow chec& for carbon dio7ide and methane( "hese wells will be in areas re#resentati$e of the former NPL land sector of the site! where $ery little acti$ity has e$er ta&en #lace( Sur("ce )"ter S"!'#in1 "here are significant lengths of interconnecting wetland8drains on the site( -E+ #ro#oses collecting s rface water sam#les from fi$e locations in this area %a total of si7 incl ding the s rface water adBacent to and referenced in the Power )tation sco#e of wor&'( "he sam#les will be tested for )#( "PH! inorganics! )F<+s and F<+s to #ro$ide a reference concentration #rior to any significant site wor&s( Tot"# Intrusi e )or*s in For!er NPL L"nd -E+ #ro#oses com#leting 20No( trial #its to a##ro7imately 2(0m de#th %a##ro7imately 1(0m below water table' and 6No( #robeholes com#leted as monitoring wells %incl ding the gas monitoring wells'( "he #ro$isional locations of all the o tlined trial #its and window sam#ling locations are incl ded on the attached :ig re 2( "he drilling will be com#leted sing a window sam#ling
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-eso rce D En$ironmental +ons ltants Ltd

*iller Homes ,o rne -oad! "hornton

20 December 2007 2;#8A2AAA

rig ca#able of allowing the installation of >0mm diameter monitoring wells( All the wells will be screened from abo$e the water table to a##ro7imately ;(0m below it( 0t is #ro#osed that trial #itting will be nderta&en within this sector of the site by the se of a /+, ;+H e7ca$ator fitted with a hydra lic brea&er( :ollowing installation of wells! all locations will be s r$eyed s ch that a single scale #lan can be #rod ced showing all locations acc rately and allowing gro ndwater flow direction to be determined across the site( PROPOSED SITE )OR+ , BURIED ANILINE DRUM AREA A n mber of in$estigations ha$e been com#leted in this area and to the east of it which ha$e identified $ario s hydrocarbon #l mes migrating east towards the .yre est ary and associated saltwater #onds( :ollowing disc ssions with the EA! it is considered that a down gro ndwater gradient ga# e7ists in the dissol$ed #hase delineation and that a remedial target is re2 ired that they can agree to that does not generate a de$elo#ment-#rohibiting cost( "he following wor& is therefore re2 ired in the aniline dr m area and associated downgradient areas3 1( "o#ogra#hic s r$ey to tie in all wells on c rrent and former NPL #ro#erty from $ariI o s in$estigations and determine gro ndwater flow regime( 0ncl de any trenches! inI cl ding de#th and dimensions( Prod ce a single scale drawing of the b ried aniline dr m area! the railway line and the land f rther to the east containing all rele$ant wells and tie this into the :ormer NPL land( 2( Prod ce scaled cross-sections as an initial +once#t al )ite *odel %0+)*' showing so rces! #athways and rece#tors %incl ding ecological'( "he fig re will incl de the se#arate #hase #re$io sly ma##ed! dissol$ed #hase %estimated'! down-gradient s rI face-water body rece#tors! on-site ditches and f t re rece#tors when sed as # blic o#en s#ace( "he 0+)* sho ld also show #ro#osed monitoring wells %or e7isting a##ro#riately #laced wells' designed to com#lete the nderstanding of the hydrogeological regime and contaminant migration( "he #lan drawing and cross section wo ld then be sent to the EA for confirmation of #lans( ;( 0nstall any wells identified as necessary to ca#t re contaminant migration( +ollect all soil sam#les and analyse for all necessary #arameters( A( <nce soil sam#les are a$ailable! determine the analytical regime and com#lete gro ndwater sam#ling at select wells to delineate contaminant #l me migration( "ie in new wells to new s r$ey( "he to#ogra#hic s r$ey m st be com#leted ahead of any new well installation in this area( >( +om#lete -"* model %EA gro ndwater fate and trans#ort model' calibrated sing the act al gro ndwater sam#ling data to determine ris& to -i$er .yre! any s rface waters! ecology and determine remedial action target for contaminants( 9( <nce a remedial target has been agreed for the Aniline! determine areas to be reI mediated! and the $ol mes in$ol$ed(

7
-eso rce D En$ironmental +ons ltants Ltd

*iller Homes ,o rne -oad! "hornton

20 December 2007 2;#8A2AAA

7( 0dentify additional well locations where #ost remediation installations can be sed to monitor nat ral atten ation of the $ario s #l mes( 5( Prod ce a re#ort in line with +L-11 setting o t the findings of the in$estigation! the res lts of any modelling %gro ndwater! h man health! ecological rece#tors' and o tI line remedial action #lan to be followed once asbestos remediation is com#lete( "he soil and gro ndwater testing sched le will address &nown contaminants rather than be all-encom#assing( -E+ #ro#oses testing any soils and all gro ndwaters for )#("PH! )F<+s! and F<+s( 0norganics %s ch as hea$y metals' ha$e not been identified as significant contaminants of concern in this area( )ite #lans showing e7isting im#act are a$ailable in re#orts already iss ed b t no single #lan ties in all locations in and east of the aniline area( 0n the interests of time and acc racy! -E+ will iss e a #ro#osed borehole location #lan once the recommended to#ogra#hical s r$ey has been com#leted( REMEDIAL A$TION PLANS Prior to any on-site de$elo#ment! *iller Homes and NPL Estates will coordinate8ens re that the asbestos in the #ower station and the asbestos8aniline in the b ried dr m area ha$e been remo$ed( -emedial method statements sho ld be s bmitted and agreed to ens re there is no im#act to the s rro nding land from these acti$ities( "he #lans for dealing with the asbestos and b ried aniline dr ms to the north and the asbestos in the e7isting #ower station b ildings in the so th will therefore ha$e to be a##ro$ed before any wor&s can ta&e #lace( -E+ will therefore coordinate obtaining o#erating #roced res and monitoring #roced res for the acti$ities in the two areas and ens re the #ro#osed o#erating #roced res #ro$ide the confidence that remediation can ta&e #lace witho t ris& to the s rro nding land(

5
-eso rce D En$ironmental +ons ltants Ltd

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

APPENDIX V REC TRIAL PIT LOGS

Trial Pit Record


Trial Pit Number: TP301
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 5/5/10 Date Completed: 5/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

MADE GROUND: Coal dirt. DG 1.20

1.70 MADE GROUND: Firm to stiff slightly silty grey clay with occasional sand inclusions.

DG

1.70

2.0 2.20 Light brown slightly silty slightly clayey fine SAND. No odour. 2.50 DG 2.30

Trial pit completed at 2.50m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.50m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 1.70m bgl.

Water strike at 1.70m bgl.

1.0

1.00

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP302
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 5/5/10 Date Completed: 5/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

1.0

1.30 MADE GROUND: Soft black very silty clay. DG Damp. No odour. 1.70 MADE GROUND: Very gravelly fine to coarse sand. Gravel is fine and rounded. 1.40

2.0 2.10 Light grey silty CLAY.

2.50 Trial pit completed at 2.50m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.50m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 1.40m bgl.

Water strike at 1.40m bgl.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP303
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 5/5/10 Date Completed: 5/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.60 MADE GROUND: Brown soft to firm gravelly clay with occasional cobbles. Gravel is angular to sub-rounded of concrete, brick and mixed lithology. 1.0

1.70 Dark grey/black slightly clayey gravelly SAND. DG 2.0 2.00 Light grey slightly silty clayey SAND. 2.10 1.90

Trial pit completed at 2.50m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.00m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 1.90m bgl.

Water srtike at 1.90m bgl.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP304
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 5/5/10 Date Completed: 5/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.40 MADE GROUND: Brown soft to firm slightly gravelly clay. Gravel is angular to sub-rounded of mixed lithology.

1.0

1.80 Black fine gravelly SAND. 2.0 2.00 Grey/green sandy fine to coarse angular to subrounded GRAVEL of mixed lithology. 2.30 Light grey slightlky silty slightly clayey fine SAND. 2.40

Trial pit completed at 2.40m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.40m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 2.10m bgl.

Water strike at 2.10m bgl.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP305
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 5/5/10 Date Completed: 5/5/10 Elevation AOD (m): N?A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.40 MADE GROUND: Brown clayey gravelly sand. Gravel is fine to coarse and angular to subrounded.

DG

0.60

1.0 Water strike at 1.80m bgl. DG 2.00 Trial pit completed at 2.00m bgl. 1.80 T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

1.70 Brown gravelly softr to firm CLAY. Gravel is sub-angular to sub-rounded of mixed lithology.

2.0

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

Notes

Dimensions: 1.00m x 1.00m x 2.00m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 1.80m bgl.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP306
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 5/5/10 Date Completed: 5/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2 combined with black coal ash/fine gravel. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

DG 0.70 MADE GROUND: Brown clayey dirt with ash, coal, gravel, brick and concrete.

0.60

1.0

1.50 Firm grey slightly silt CLAY with a fine bluish mottle at the top.

DG

1.50

2.0 2.20 Trial pit completed at 2.20m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.20m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 2.20m bgl.

Water strike at 2.20m bgl.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP307
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 5/5/10 Date Completed: 5/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

1.0

1.00 MADE GROUND: Red/brown Type 1 from old road...Variable.

1.40 Grey firm gravelly CLAY. Gravel is coarse and sub-angular to angular. 1.60 DG 1.60

Trial pit completed at 1.60m bgl.

2.0

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 1.60m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 1.40m bgl.

Water strike at 1.60m bgl.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP308
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 7/5/10 Date Completed: 7/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.40 MADE GROUND: Black coal ash. DG DG

1.0

1.30 MADE GROUND: Brown clayey gravelly soil with cobbles. Gravel is fine to coarse of mixed lithology. Cobbles are of brick.

DG 2.0 At 2.20m bgl...Pipe with possible oil encountered. 2.30 Trial pit completed at 2.30m bgl.

DG

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.30m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Moist at 1.90m bgl.

Moisture encountered at 1.90m bgl.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP309
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 7/5/10 Date Completed: 7/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.30 MADE GROUND: Black ash and coal.

0.90 1.0 MADE GROUND: Sand and clay matrix in ground of brick, concrete and stone.

1.30 MADE GROUND: Concrete pad with brick...Dry on top. 1.50 Firm grey silty CLAY. 1.70 Brown firm slightly silty CLAY.

2.0 2.20 Trial pit completed at 2.20m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.30m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP310
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 7/5/10 Date Completed: 7/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.30 MADE GROUND: Red/brown sand matrix with brick, concrete and stone.

DG

0.60

At 0.80m bgl...Water pipe encountered.

1.0 1.20 MADE GROUND: Brown clayey gravel.

Between 1.70m bgl-1.90m bgl...Staining. 1.90 Grey silty CLAY. 2.0

DG

1.90

2.40 Trial pit completed at 2.40m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.40m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP311
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 7/5/10 Date Completed: 7/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: Brown sandy gravel with pockets of clayey matrix. Gravel is fine to coarse angular to sub-angular of brick, concrete and mixed lithology. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

DG 1.00 MADE GROUND: Grey stained at the top/light brown firm slightly silty slightly gravelly clay. 1.30 Red/brown firm to stiff CLAY.

0.80

1.0

1.80 Trial pit completed at 1.80m bgl. 2.0

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 1.80m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered.

Date: 3/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP312
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 7/5/10 Date Completed: 7/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

1.0

2.0

3.0

4.0

5.0

6.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 1.30m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater:

Date: Status:

Trial Pit Record


Trial Pit Number: TP313
Project Number: 43391 Contract Name: Thornton Power Stations Client: Engineer: Marcus Wright Date Started: 7/5/10 Date Completed: 7/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.90 1.0 MADE GROUND: Firm grey mottled brown slightly silty clay with traces of organics.

DG

0.90

1.60 Firm brown slightly silty CLAY.

2.0 Trial pit completed at 2.00m bgl.

2.00

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.00m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater:

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP314
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 7/5/10 Date Completed: 7/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F5. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.60 MADE GROUND. 0.80 MADE GROUND: Concrete pad. 1.0 1.00 Firm grey silty CLAY. 1.10

Trial pit completed at 1.10m bgl.

2.0

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 1.00m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered.

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP315
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.30 MADE GROUND: ??? Water strike at 1.20m bgl. DG 1.60 T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector 0.50 MADE GROUND: Red brick.

1.0

1.00 MADE GROUND: Grey slightly silty clay with some organic material in upper layer. Pipe at 1.20m bgl.

1.60 Soft brown peaty CLAY with gravel to top of strata. 1.80 Light grey soft to firm silty CLAY. 2.0 2.10 Trial pit completed at 2.10m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

Notes

Dimensions: 1.00m x 1.00m x 2.10m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Water strike at 1.20m bgl.

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP316
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.40 MADE GROUND: Dark brown sandy gravel.

1.0 Moist at 1.70m bgl. T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

1.50 Firm grey sandy CLAY. 1.70 Brown peaty gravelly CLAY. Gravel is fine angular to sub-angular of mixed lithology. 1.90 2.0

DG DG

1.50 1.60

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

Notes

Dimensions: 1.00m x 1.00m x 1.90m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Moist at 1.70m bgl.

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP317
Project Number: 43391 Contract Name: Thorton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2-Brick, concrete, stone. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.30 MADE GROUND: Sandy ??? and large cobbles of concrete.

1.0

1.00 MADE GROUND: Soft to firm dark grey gravelly clay and organic materials...Occasional staining...Dry. Firm grey CLAY. 1.50 Trial pit completed at 1.50m bgl.

DG

1.00

1.20

2.0

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 1.150m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP318
Project Number: 43391 Contract Name: Thorton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.70 MADE GROUND: Brick, concrete, stone sand clay matrix.

1.0

1.30 MADE GROUND: SOft to firm re-worked clay with occasional brick and concrete.

DG

1.30

DG

1.60

2.0 2.10 Trial pit completed at 2.10m bgl.

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.10m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: Pocket of water encountered at 1.40m bgl.

Pocket of water encountered at 1.40m bgl.

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP319
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.40 MADE GROUND: Brick, concrete, sand, pockets of clay matrix...Pocket of black ash. DG 0.60

1.0

DG 1.70 Trial pit completed at 1.70m bgl.

1.50

2.0

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 1.70m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered.

Date: 51/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP320
Project Number: 43391 Contract Name: Thorton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.60 MADE GROUND: Soft to firm grey mottled silty clay with traces of organic matter to top of strata. DG 0.70

1.0

Between 0.70m bgl-1.00m bgl...Staining.

DG 1.80 Trial pit completed at 1.80m bgl. 2.0

1.70

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.0m x 1.80m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered.

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP322A
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND: 6F2. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.60 MADE GROUND: Clayey brick, concrete, stone.

1.0

DG

1.60

2.0 Trial pit completed at 2.10m bgl.

2.00

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.00m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater: None encountered.

Date: 15/6/10 Status: Prelim 1

Trial Pit Record


Trial Pit Number: TP323
Project Number: 43391 Contract Name: Thornton Power Station Client: Engineer: Marcus Wright Date Started: 26/5/10 Date Completed: 26/5/10 Elevation AOD (m): N/A Co-ordinates: N/A Excavation Method:
Resource & Environmental Consultants Ltd Osprey House Pacific Quay Broadway Manchester, M50 2UE Tel: 0161 868 1300 / Fax: 0161 868 1301 www.recltd.co.uk

SUBSURFACE PROFILE
Legend Depth (mbgl) Description MADE GROUND. Depth of Strata (mbgl) Type

SAMPLES AND IN-SITU TESTING


Depth (mbgl) Water Level (mbgl) P.I.D (ppm) 0 25 50 75 100 Field / Laboratory Testing

0.70 MADE GROUND: Fine black coal dust/ash. 0.90 MADE GROUND: Soft brown sandy clay. 1.0 Grey soft to firm CLAY. 1.00 DG 0.90

1.40 Grey silty SAND with traces of clay and gravel. Gravel is angular to sub-angular of mixed lithology.

DG 2.00 Trial pit completed at 2.00m bgl.

1.80

2.0

3.0

Key

B. Bulk (Bag) W. Water U100. 100mm Undisturbed U38. 38mm Undisturbed Sample SPT. Standard Penetration Test

D. Disturbed G. Amber Glass Jar / Bottle CPT. Cone Penetration Test U100. Blows (Recovery mm) V. 40ml Glass Vial

T. Plastic Tub N. 'N' Value HV. Hand Shear Vane PID. Photo Ionisation Detector

Notes

Dimensions: 1.00m x 1.00m x 2.00m Services: Prior to excavation the trial pit location was scanned with a Cable Avoidance Tool (CAT). Stability: Stable Groundwater:

Date: 15/6/10 Status: Prelim 1

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

APPENDIX VI CHEMICAL TESTING RESULTS - 2010

Scientific Analysis Laboratories


Certificate of Analysis
Scientific Analysis Laboratories is a limited company registered in England and Wales (No 2514788) whose address is at Hadfield House, Hadfield Street, Manchester M16 9FE

Hadfield House Hadfield Street Cornbrook Manchester M16 9FE Tel : 0161 874 2400 Fax : 0161 874 2468

Report Number: 198707-1 Date of Report: 12-May-2010 Customer: Resource Environmental Consultants Ltd Osprey House Pacific Quay Broadway Salford M50 2UE Customer Contact: Mr Marcus Wright Customer Job Reference: Date Job Received at SAL: Date Analysis Started: Date Analysis Completed: 43391 05-May-2010 06-May-2010 12-May-2010

The results reported relate to samples received in the laboratory Opinions and interpretations expressed herein are outside the scope of UKAS accreditation This report should not be reproduced except in full without the written approval of the laboratory Tests covered by this certificate were conducted in accordance with SAL SOPs

1549

Report checked and authorised by : Miss Carrie Hughes Senior Project Manager

Issued by : Miss Carrie Hughes Senior Project Manager

Signature Not Verified


Digitally signed by Carrie Hughes Date: 2010.05.12 15:40:11 BST Reason: Issue Location: SAL

Page 1 of 5
This document has been printed from a digitally signed master copy

Index to symbols used in 198707-1


Value AR 2 U N As Received LOD Raised Due to Matrix Interference Analysis is UKAS accredited Analysis is not accredited Description

Method Index
Value T54 T6 T149 T2 T4 T8 T7 Description GC/MS (Headspace) ICP/OES GC/MS (SIR) Grav Colorimetry GC/FID Probe

Accreditation Summary
Determinand Arsenic Cadmium Chromium Lead Mercury Selenium Boron (water-soluble) Copper Nickel Zinc pH SO4(Total) SO4(2:1) Sulphide Sulphur(Free) Cyanide(Total) Phenols(Mono) Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene PAH(total) TPH (C6-C8 aliphatic) TPH (C8-C10 aliphatic) TPH (C10-C12 aliphatic) TPH (C12-C16 aliphatic) TPH (C16-C21 aliphatic) TPH (C21-C35 aliphatic) TPH (C6-C7 aromatic) TPH (C7-C8 aromatic) TPH (C8-C10 aromatic) TPH (C10-C12 aromatic) TPH (C12-C16 aromatic) TPH (C16-C21 aromatic) TPH (C21-C35 aromatic) Method T6 T6 T6 T6 T6 T6 T6 T6 T6 T6 T7 T6 T6 T4 T2 T4 T4 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T54 T54 T8 T8 T8 T8 T54 T54 T54 T8 T8 T8 T8 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR 0.01 0.1 10 500 1 1 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.010 0.010 1 1 1 1 0.010 0.010 0.010 1 1 1 1 % g/l mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg LOD 1 1 1 1 1 3 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Symbol U U U U U U N U U U U N N N N U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 001,006,008,010 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 002,004-005,007,009,011 SAL References

Produced by Scientific Analysis Laboratories, Hadfield House, Hadfield Street, Cornbrook, Manchester, M16 9FE This document has been printed from a digitally signed master copy

Page 2 of 5

SAL Reference: 198707 Customer Reference: 43391 Soil REC Ltd 001S SAL Reference 198707 001 198707 006 198707 008 198707 010 Customer Sample Reference Determinand Arsenic Cadmium Chromium Lead Mercury Selenium Boron (water-soluble) Copper Nickel Zinc pH SO4(Total) SO4(2:1) Sulphide Sulphur(Free) Cyanide(Total) Phenols(Mono) Method T6 T6 T6 T6 T6 T6 T6 T6 T6 T6 T7 T6 T6 T4 T2 T4 T4 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR 0.01 0.1 10 500 1 1 % g/l mg/kg mg/kg mg/kg mg/kg LOD 1 1 1 1 1 3 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 14 <1 22 52 <1 <3 <1 39 23 140 7.7 2.6 0.1 <10 <500 <1 <1 13 <1 41 27 <1 <3 <1 30 41 140 8.2 0.47 0.1 <10 <500 <1 <1 27 <1 38 90 <1 <3 <1 56 39 170 8.5 0.18 <0.1 <10 <500 <1 <1 26 1 39 56 <1 <3 <1 150 82 120 8.4 0.28 <0.1 <10 <500 <1 <1 TP301 1.2 TP304 0.6 TP305 0.6 TP306 0.5 Analysed as Soil

SAL Reference: 198707 Customer Reference: 43391 Soil Analysed as Soil

Total and Speciated USEPA16 PAH SAL Reference 198707 002 198707 004 198707 005 198707 007 198707 009 Customer Sample Reference Determinand Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene PAH(total) Method T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR LOD 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 0.01 <0.01 <0.01 <0.01 0.02 <0.01 0.03 0.03 0.02 0.01 0.03 0.02 0.01 <0.01 0.01 0.19 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.02 0.02 0.01 0.01 0.03 0.02 0.01 <0.01 0.01 0.13 0.11 0.01 0.04 0.21 0.32 0.01 0.07 0.06 0.03 0.08 0.06 0.03 0.01 0.01 0.02 1.1 0.01 <0.01 <0.01 0.01 0.02 <0.01 0.02 0.02 0.01 0.01 0.02 0.02 0.01 <0.01 0.01 0.16 0.05 0.01 0.01 0.01 0.10 0.03 0.19 0.16 0.09 0.08 0.15 0.09 0.05 0.01 0.06 1.1 TP301 1.7 TP302 1.4 TP303 1.9 TP304 1.9 TP305 1.8

Produced by Scientific Analysis Laboratories, Hadfield House, Hadfield Street, Cornbrook, Manchester, M16 9FE This document has been printed from a digitally signed master copy

Page 3 of 5

SAL Reference: 198707 Customer Reference: 43391 Soil Analysed as Soil

Total and Speciated USEPA16 PAH SAL Reference 198707 011 Customer Sample Reference Determinand Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene PAH(total) Method T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR LOD 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 0.02 <0.01 <0.01 0.01 0.05 0.01 0.06 0.05 0.03 0.02 0.05 0.03 0.02 <0.01 0.02 0.37 TP306 1.5

SAL Reference: 198707 Customer Reference: 43391 Soil Analysed as Soil

Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference 198707 002 198707 004 198707 005 198707 007 198707 009 Customer Sample Reference Determinand TPH (C6-C8 aliphatic) TPH (C8-C10 aliphatic) TPH (C10-C12 aliphatic) TPH (C12-C16 aliphatic) TPH (C16-C21 aliphatic) TPH (C21-C35 aliphatic) TPH (C6-C7 aromatic) TPH (C7-C8 aromatic) TPH (C8-C10 aromatic) TPH (C10-C12 aromatic) TPH (C12-C16 aromatic) TPH (C16-C21 aromatic) TPH (C21-C35 aromatic) Method T54 T54 T8 T8 T8 T8 T54 T54 T54 T8 T8 T8 T8 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR LOD 0.010 0.010 1 1 1 1 0.010 0.010 0.010 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.010 <0.010 <1 <1 <1 <1 <0.010 <0.010 <0.010 <1 <1 <1 <1
(2) <0.20 (2) <0.20 (2) <0.20 (2) <0.20 (2) <0.20 (2) <0.20

TP301 1.7

TP302 1.4

TP303 1.9

TP304 1.9

TP305 1.8

<0.010 <0.010 <1 <1 2 9 <0.010 <0.010 <0.010 <1 1 11 25

<1 <1 14 44
(2) <0.20 (2) <0.20 (2) <0.20

400 250 <1 <1


(2) <0.20 (2) <0.20 (2) <0.20

<1 2 4 22
(2) <0.20 (2) <0.20 (2) <0.20

<1 <1 5 24

49 54 <1 <1

<1 <1 <1 4

Produced by Scientific Analysis Laboratories, Hadfield House, Hadfield Street, Cornbrook, Manchester, M16 9FE This document has been printed from a digitally signed master copy

Page 4 of 5

SAL Reference: 198707 Customer Reference: 43391 Soil Analysed as Soil

Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference 198707 011 Customer Sample Reference Determinand TPH (C6-C8 aliphatic) TPH (C8-C10 aliphatic) TPH (C10-C12 aliphatic) TPH (C12-C16 aliphatic) TPH (C16-C21 aliphatic) TPH (C21-C35 aliphatic) TPH (C6-C7 aromatic) TPH (C7-C8 aromatic) TPH (C8-C10 aromatic) TPH (C10-C12 aromatic) TPH (C12-C16 aromatic) TPH (C16-C21 aromatic) TPH (C21-C35 aromatic) Method T54 T54 T8 T8 T8 T8 T54 T54 T54 T8 T8 T8 T8 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR LOD 0.010 0.010 1 1 1 1 0.010 0.010 0.010 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.010 <0.010 <1 <1 <1 <1 <0.010 <0.010 <0.010 <1 <1 <1 <1 TP306 1.5

Produced by Scientific Analysis Laboratories, Hadfield House, Hadfield Street, Cornbrook, Manchester, M16 9FE This document has been printed from a digitally signed master copy

Page 5 of 5

Scientific Analysis Laboratories


Certificate of Analysis
Scientific Analysis Laboratories is a limited company registered in England and Wales (No 2514788) whose address is at Hadfield House, Hadfield Street, Manchester M16 9FE

Hadfield House Hadfield Street Cornbrook Manchester M16 9FE Tel : 0161 874 2400 Fax : 0161 874 2468

Report Number: 199667-1 Date of Report: 19-May-2010 Customer: Resource Environmental Consultants Ltd Osprey House Pacific Quay Broadway Salford M50 2UE Customer Contact: Mr Marcus Wright Customer Job Reference: Date Job Received at SAL: Date Analysis Started: Date Analysis Completed: 43391 05-May-2010 14-May-2010 19-May-2010

The results reported relate to samples received in the laboratory Opinions and interpretations expressed herein are outside the scope of UKAS accreditation This report should not be reproduced except in full without the written approval of the laboratory Tests covered by this certificate were conducted in accordance with SAL SOPs

1549

Report checked and authorised by : Miss Carrie Hughes Senior Project Manager

Issued by : Miss Carrie Hughes Senior Project Manager

Signature Not Verified


Digitally signed by Carrie Hughes Date: 2010.05.19 11:02:21 BST Reason: Issue Location: SAL

Page 1 of 3
This document has been printed from a digitally signed master copy

Index to symbols used in 199667-1


Value AR U N As Received Analysis is UKAS accredited Analysis is not accredited Description

Method Index
Value T11 T6 IC ICP/OES Description

Accreditation Summary
Determinand Method Phosphate Zinc T11 T6 Test Sample AR AR LOD 1 1 Units mg/kg mg/kg Symbol N U 001 001 SAL References

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SAL Reference: 199667 Customer Reference: 43391 Soil Miscellaneous SAL Reference 199667 001 Analysed as Soil

Customer Sample Reference TP307 1.6 198707/012 Determinand Phosphate Zinc Method T11 T6 Test Sample AR AR LOD 1 1 Units mg/kg mg/kg <1 85

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Scientific Analysis Laboratories


Certificate of Analysis
Scientific Analysis Laboratories is a limited company registered in England and Wales (No 2514788) whose address is at Hadfield House, Hadfield Street, Manchester M16 9FE

Hadfield House Hadfield Street Cornbrook Manchester M16 9FE Tel : 0161 874 2400 Fax : 0161 874 2468

Report Number: 199061-1 Date of Report: 13-May-2010 Customer: Resource Environmental Consultants Ltd Osprey House Pacific Quay Broadway Salford M50 2UE Customer Contact: Mr Marcus Wright Customer Job Reference: Date Job Received at SAL: Date Analysis Started: Date Analysis Completed: 43391 07-May-2010 10-May-2010 13-May-2010

The results reported relate to samples received in the laboratory Opinions and interpretations expressed herein are outside the scope of UKAS accreditation This report should not be reproduced except in full without the written approval of the laboratory Tests covered by this certificate were conducted in accordance with SAL SOPs

1549

Report checked and authorised by : Miss Carrie Hughes Senior Project Manager

Issued by : Miss Carrie Hughes Senior Project Manager

Signature Not Verified


Digitally signed by Carrie Hughes Date: 2010.05.13 17:02:40 BST Reason: Issue Location: SAL

Page 1 of 8
This document has been printed from a digitally signed master copy

Index to symbols used in 199061-1


Value AR N.D. 13 9 U N As Received Not Detected Results have been blank corrected. LOD raised due to dilution of sample Analysis is UKAS accredited Analysis is not accredited Description

Method Index
Value T7 T6 T16 T85 T4 T8 T149 T2 T54 Probe ICP/OES GC/MS Calc Colorimetry GC/FID GC/MS (SIR) Grav GC/MS (Headspace) Description

Accreditation Summary
Determinand Arsenic Cadmium Chromium Lead Mercury Selenium Boron (water-soluble) Copper Nickel Zinc pH SO4(Total) SO4(2:1) Sulphide Sulphur(Free) Cyanide(Total) Phenols(Mono) Benzene M/P Xylene O Xylene Methyl tert-Butyl Ether TPH (C5-C6 aliphatic) TPH (C6-C8 aliphatic) TPH (C8-C10 aliphatic) TPH (C10-C12 aliphatic) TPH (C12-C16 aliphatic) TPH (C16-C21 aliphatic) TPH (C21-C35 aliphatic) TPH (Aliphatic) total TPH (C6-C7 aromatic) TPH (C7-C8 aromatic) TPH (C8-C10 aromatic) TPH (C10-C12 aromatic) TPH (C12-C16 aromatic) TPH (C16-C21 aromatic) TPH (C21-C35 aromatic) TPH (Aromatic) total TPH (Aliphatic+Aromatic) (sum) 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Method T6 T6 T6 T6 T6 T6 T6 T6 T6 T6 T7 T6 T6 T4 T2 T4 T4 T54 T54 T54 T54 T54 T54 T54 T8 T8 T8 T8 T85 T54 T54 T54 T8 T8 T8 T8 T85 T85 T16 T16 T16 T16 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR 0.1 0.1 0.1 0.1 0.010 0.010 0.010 1 1 1 1 0.01 0.1 10 500 1 1 0.001 0.001 0.001 0.001 0.010 0.010 0.010 1 1 1 1 % g/l mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg LOD 1 1 1 1 1 3 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Symbol U U U U U U N U U U U N N N N U U U U U U N N N N N N N N N N N N N N N N N U U U U 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 001,004,006 002-003,005,007 002-003,005,007 002-003,005,007 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002-003,005,007-008 002,008 002,008 002,008 002,008 SAL References

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Determinand 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-methyl phenol 2-Methylnaphthalene 2-Nitroaniline 2-Nitrophenol 3-Nitroaniline 3/4-Methylphenol 4-Bromophenyl phenylether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl phenylether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Azobenzene Benzo(a)Anthracene Benzo(a)Pyrene Benzo(b/k)Fluoranthene Benzo(ghi)Perylene Bis (2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl)phthalate Butyl benzylphthalate Carbazole Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenzo(ah)Anthracene Dibenzofuran Diethyl phthalate Dimethyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(123-cd)Pyrene Isophorone Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene

Method T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149

Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR

LOD 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01

Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Symbol U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 002,008 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007 001,003,005,007

SAL References

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Determinand Benzo(ghi)Perylene PAH(total) Total Petroleum Hydrocarbons 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethylene 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloropropene 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 4-Chlorotoluene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane Cis-1,2-Dichloroethylene Cis-1,3-Dichloropropene Dibromomethane Dichlorodifluoromethane Dichloromethane EthylBenzene Isopropyl benzene n-Propylbenzene p-Isopropyltoluene S-Butylbenzene Styrene T-Butylbenzene Tetrachloroethylene Toluene Trans-1,2-Dichloroethene Trans-1,3-Dichloropropene Trichlorofluoromethane Vinyl chloride

Method T149 T149 T8 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54

Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR

LOD 0.01 0.01 1 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.050 0.001 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.001 0.005 0.005 0.005 0.005

Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Symbol U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U N U U U U U U U U U U U U U 001,003,005,007 001,003,005,007 006 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002-003,005,007 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002,007-008 002-003,005,007 002,007-008 002,007-008 002,007-008 002,007-008

SAL References

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SAL Reference: 199061 Customer Reference: 43391 Soil REC Ltd 001S SAL Reference 199061 001 199061 004 199061 006 Customer Sample Reference Determinand Arsenic Cadmium Chromium Lead Mercury Selenium Boron (water-soluble) Copper Nickel Zinc pH SO4(Total) SO4(2:1) Sulphide Sulphur(Free) Cyanide(Total) Phenols(Mono) Method T6 T6 T6 T6 T6 T6 T6 T6 T6 T6 T7 T6 T6 T4 T2 T4 T4 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR 0.01 0.1 10 500 1 1 % g/l mg/kg mg/kg mg/kg mg/kg LOD 1 1 1 1 1 3 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 18 <1 83 72 <1 <3 <1 77 100 210 8.2 1.5 <0.1 <10 <500 <1 <1 33 <1 74 67 <1 <3 <1 65 760 140 8.3 0.65 0.1 <10 <500 <1 <1 7 <1 17 39 <1 <3 <1 8 16 37 8.5 0.22 <0.1 25 <500 <1 <1 TP308 0.6 TP310 0.5 TP311 0.8 Analysed as Soil

SAL Reference: 199061 Customer Reference: 43391 Soil Analysed as Soil

Total and Speciated USEPA16 PAH SAL Reference 199061 001 199061 003 199061 005 199061 007 Customer Sample Reference Determinand Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene PAH(total) Method T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR LOD 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 1.5 0.01 0.02 0.03 0.38 0.06 0.05 0.05 0.04 0.05 0.03 0.02 <0.01 <0.01 0.01 2.3 0.01 <0.01 <0.01 <0.01 0.01 <0.01 0.01 0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.04 0.05 0.01 0.01 0.01 0.08 0.01 0.08 0.07 0.04 0.04 0.06 0.03 0.02 0.01 0.03 0.55 <0.01 <0.01 <0.01 <0.01 0.01 <0.01 0.02 0.02 0.01 0.01 0.01 0.01 <0.01 <0.01 0.01 0.10 TP308 0.6 TP309 1.9 TP310 1.8 TP313 0.9

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SAL Reference: 199061 Customer Reference: 43391 Soil REC TPH (CWG) SAL Reference 199061 002 199061 003 199061 005 199061 007 199061 008 Customer Sample Reference Determinand Benzene Toluene EthylBenzene M/P Xylene O Xylene Methyl tert-Butyl Ether TPH (C5-C6 aliphatic) TPH (C6-C8 aliphatic) TPH (C8-C10 aliphatic) TPH (C10-C12 aliphatic) TPH (C12-C16 aliphatic) TPH (C16-C21 aliphatic) TPH (C21-C35 aliphatic) TPH (Aliphatic) total TPH (C6-C7 aromatic) TPH (C7-C8 aromatic) TPH (C8-C10 aromatic) TPH (C10-C12 aromatic) TPH (C12-C16 aromatic) TPH (C16-C21 aromatic) TPH (C21-C35 aromatic) TPH (Aromatic) total TPH (Aliphatic+Aromatic) (sum) Method T54 T54 T54 T54 T54 T54 T54 T54 T54 T8 T8 T8 T8 T85 T54 T54 T54 T8 T8 T8 T8 T85 T85 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR 0.010 0.010 0.010 1 1 1 1 LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.010 0.010 0.010 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
(13) <0.001 (13) <0.001 (13) <0.001 (13) <0.001 (13) <0.001

Analysed as Soil

TP308 1.9

TP309 1.9

TP310 1.8

TP313 0.9

TP314 0.9

<0.001 <0.001 <0.001 <0.001 <0.001 <0.010 <0.010 <0.010 <1 1 3 7 11 <0.010 <0.010 <0.010 <1 <1 <1 2 2.0 13

<0.001 <0.001 <0.001 <0.001 <0.001 <0.010 <0.010 <0.010 <1 1 2 6 9.0 <0.010 <0.010 <0.010 <1 <1 <1 <1 N.D. 9.0

0.003 <0.001 0.002 0.002 <0.001 <0.010 <0.010 0.25


(9) <10 (9) <10

<0.001 <0.001 <0.001 <0.001 <0.001 <0.010 <0.010 <0.010 <1 <1 2 7 9.0 <0.010 <0.010 <0.010 <1 <1 <1 1 1.0 10

<0.001 <0.001 <0.001 <0.001 <0.001 <0.010 <0.010 <0.010 <1 1 3 7 11 <0.010 <0.010 <0.010 <1 1 <1 2 3.0 14

14 69 83 <0.010 <0.010 0.060


(9) <10 (9) <10 (9) <10

22 22 110

SAL Reference: 199061 Customer Reference: 43391 Soil Miscellaneous SAL Reference 199061 006 Customer Sample Reference Determinand Total Petroleum Hydrocarbons Method T8 Test Sample AR LOD 1 Units mg/kg 37 TP311 0.8 Analysed as Soil

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SAL Reference: 199061 Customer Reference: 43391 Soil Analysed as Soil

Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 199061 002 199061 008 Customer Sample Reference Determinand 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-methyl phenol 2-Methylnaphthalene 2-Nitroaniline 2-Nitrophenol 3-Nitroaniline 3/4-Methylphenol 4-Bromophenyl phenylether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl phenylether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Azobenzene Benzo(a)Anthracene Benzo(a)Pyrene Benzo(b/k)Fluoranthene Benzo(ghi)Perylene Bis (2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl)phthalate Butyl benzylphthalate Carbazole Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenzo(ah)Anthracene Dibenzofuran Diethyl phthalate Dimethyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(123-cd)Pyrene Isophorone Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene Method T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR LOD 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.2 <0.1 <0.1 <0.1 <0.1 <0.1 TP308 1.9 TP314 0.9

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SAL Reference: 199061 Customer Reference: 43391 Soil Analysed as Soil

Volatile Organic Compounds (USEPA 624) SAL Reference 199061 002 199061 007 199061 008 Customer Sample Reference Determinand 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethylene 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloropropene 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 4-Chlorotoluene Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane Cis-1,2-Dichloroethylene Cis-1,3-Dichloropropene Dibromomethane Dichlorodifluoromethane Dichloromethane EthylBenzene Isopropyl benzene M/P Xylene n-Propylbenzene O Xylene p-Isopropyltoluene S-Butylbenzene Styrene T-Butylbenzene Tetrachloroethylene Toluene Trans-1,2-Dichloroethene Trans-1,3-Dichloropropene Trichlorofluoromethane Vinyl chloride Method T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 Test Sample AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR AR LOD 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.001 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.050 0.001 0.005 0.001 0.005 0.001 0.005 0.005 0.005 0.005 0.005 0.001 0.005 0.005 0.005 0.005 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

TP308 1.9

TP313 0.9

TP314 0.9

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.050 <0.001 <0.005 <0.001 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.050 <0.001 <0.005 <0.001 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.050 <0.001 <0.005 <0.001 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005

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Scientific Analysis Laboratories


Certificate of Analysis
Scientific Analysis Laboratories is a limited company registered in England and Wales (No 2514788) whose address is at Hadfield House, Hadfield Street, Manchester M16 9FE

Hadfield House Hadfield Street Cornbrook Manchester M16 9FE Tel : 0161 874 2400 Fax : 0161 874 2468

Report Number: 201368-1 Date of Report: 04-Jun-2010 Customer: Resource Environmental Consultants Ltd Osprey House Pacific Quay Broadway Salford M50 2UE Customer Contact: Mr Marcus Wright Customer Job Reference: Date Job Received at SAL: Date Analysis Started: Date Analysis Completed: 43391 28-May-2010 01-Jun-2010 04-Jun-2010

The results reported relate to samples received in the laboratory Opinions and interpretations expressed herein are outside the scope of UKAS accreditation This report should not be reproduced except in full without the written approval of the laboratory Tests covered by this certificate were conducted in accordance with SAL SOPs

1549

Report checked and authorised by : Miss Emma Tibbitts Assistant Customer Services Manager

Issued by : Miss Emma Tibbitts Assistant Customer Services Manager


Page 1 of 8

This document has been printed from a digitally signed master copy

Index to symbols used in 201368-1


Value AR 13 2 U N As Received Not Required Results have been blank corrected. LOD Raised Due to Matrix Interference Analysis is UKAS accredited Analysis is not accredited Description

Method Index
Value T54 T16 T8 T149 T7 T6 T1 T4 Description GC/MS (Headspace) GC/MS GC/FID GC/MS (SIR) Probe ICP/OES GC/MS (HR) Colorimetry

Accreditation Summary
Determinand PCB BZ#101 PCB BZ#118 PCB BZ#138 PCB BZ#153 PCB BZ#180 PCB BZ#28 PCB BZ#52 Arsenic Cadmium Chromium Chromium VI Copper Cyanide(Total) Lead Mercury Nickel pH Phenols(Mono) Selenium SO4(Total) SO4(2:1) Zinc Phenol Bis (2-chloroethyl) ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Bis (2-chloroisopropyl) ether 2-methyl phenol 3/4-Methylphenol Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol Bis (2-chloroethoxy) methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-methylphenol Method T1 T1 T1 T1 T1 T1 T1 T6 T6 T6 T6 T6 T4 T6 T6 T6 T7 T4 T6 T6 T6 T6 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 Test Sample 1 3 0.01 100 1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 mg/kg mg/kg % mg/l mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg LOD 0.00005 0.00005 0.00005 0.00005 0.00005 0.00005 0.00005 1 1 1 1 1 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Symbol U U U U U U U U U U N U U U U U U U U N N U U U U U U U U U U U U U U U U U U U U U U 001,003-006 001,003-006 001,003-006 001,003-006 001,003-006 001,003-006 001,003-006 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 001-002,006,012,014-015 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 SAL References

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Page 2 of 8

Determinand 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl phthalate 2,6-Dinitrotoluene Acenaphthylene Acenaphthene 3-Nitroaniline 2,4-Dinitrophenol Dibenzofuran 2,4-Dinitrotoluene 4-Nitrophenol Diethyl phthalate Fluorene 4-Chlorophenyl phenylether 4-Nitroaniline Azobenzene 4-Bromophenyl phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-butylphthalate Fluoranthene Pyrene Butyl benzylphthalate Benzo(a)Anthracene Chrysene Bis (2-ethylhexyl)phthalate Di-n-octylphthalate Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene PAH(total) Total Petroleum Hydrocarbons TPH (C6-C8 aliphatic) TPH (C8-C10 aliphatic) TPH (C10-C12 aliphatic) TPH (C12-C16 aliphatic) TPH (C16-C21 aliphatic) TPH (C21-C35 aliphatic) TPH (C6-C7 aromatic) TPH (C7-C8 aromatic) TPH (C8-C10 aromatic) TPH (C10-C12 aromatic) TPH (C12-C16 aromatic) TPH (C16-C21 aromatic) TPH (C21-C35 aromatic) 1,1,1,2-Tetrachloroethane

Method T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T8 T54 T54 T8 T8 T8 T8 T54 T54 T54 T8 T8 T8 T8 T54

Test Sample -

LOD 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.010 0.010 1 1 1 1 0.010 0.010 0.010 1 1 1 1 0.005

Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Symbol U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N U 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 009,011 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 001-002,007-008,010 002-003,005,017 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 001,004,007-008,011-012,014-016 012-015

SAL References

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Page 3 of 8

Determinand 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethylene 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloropropene 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 4-Chlorotoluene Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane Cis-1,2-Dichloroethylene Cis-1,3-Dichloropropene Dibromomethane Dichlorodifluoromethane Dichloromethane EthylBenzene Isopropyl benzene M/P Xylene n-Propylbenzene O Xylene p-Isopropyltoluene S-Butylbenzene Styrene T-Butylbenzene Tetrachloroethylene Toluene Trans-1,2-Dichloroethene Trans-1,3-Dichloropropene Trichlorofluoromethane Vinyl chloride

Method T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54

Test Sample -

LOD 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.001 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.050 0.001 0.005 0.001 0.005 0.001 0.005 0.005 0.005 0.005 0.005 0.001 0.005 0.005 0.005 0.005

Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Symbol U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U N U U U U U U U U U U U U U U U 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015 012-015

SAL References

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Page 4 of 8

SAL Reference: 201368 Customer Reference: 43391 Soil REC Ltd 002S SAL Reference 201368 001 201368 002 201368 006 201368 012 201368 014 201368 015 Customer Sample Reference Determinand Arsenic Cadmium Chromium Chromium VI Copper Cyanide(Total) Lead Mercury Nickel pH Phenols(Mono) Selenium SO4(Total) SO4(2:1) Zinc Method T6 T6 T6 T6 T6 T4 T6 T6 T6 T7 T4 T6 T6 T6 T6 Test Sample 1 3 0.01 100 1 mg/kg mg/kg % mg/l mg/kg LOD 1 1 1 1 1 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 21 1 21 <1 44 <1 97 <1 30 7.1 <1 <3 0.34 <100 330 9 <1 31 <1 12 <1 30 <1 22 6.9 <1 <3 0.07 <100 53 94 2 34 <1 260 <1 300 <1 91 7.4 <1 <3 0.88 <100 490 12 <1 28 <1 17 <1 35 <1 21 6.7 <1 <3 0.40 100 58 14 <1 29 <1 28 <1 46 <1 28 8.1 <1 <3 0.17 <100 88 4 <1 25 <1 7 <1 10 <1 22 8.3 <1 <3 <0.01 <100 43 TP315 1.6 TP316 1.6 TP317 1.4 TP320 0.7 TP321 0.9 TP322 1.6 Analysed as Soil

SAL Reference: 201368 Customer Reference: 43391 Soil Analysed as Soil

Total and Speciated USEPA16 PAH SAL Reference 201368 001 201368 002 201368 007 201368 008 201368 010 Customer Sample Reference Determinand Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene PAH(total) Method T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 T149 Test Sample LOD 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 0.68 0.69 0.24 0.68 3.8 1.7 7.5 6.0 4.4 3.9 6.8 3.6 1.9 0.83 1.7 44 0.01 0.01 <0.01 <0.01 0.05 0.01 0.09 0.07 0.04 0.04 0.07 0.03 0.02 0.01 0.02 0.47 0.05 0.03 0.03 0.03 0.24 0.08 0.44 0.40 0.15 0.16 0.26 0.14 0.08 0.03 0.08 2.2 <0.01 <0.01 0.01 0.02 0.02 <0.01 0.02 0.02 0.01 0.01 0.01 0.01 <0.01 <0.01 <0.01 0.13 0.23 <0.01 <0.01 0.01 0.13 0.02 0.11 0.13 0.06 0.08 0.11 0.05 0.03 0.01 0.03 1.0 TP315 1.6 TP316 1.6 TP317 1.0 TP318 1.3 TP319 0.6

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SAL Reference: 201368 Customer Reference: 43391 Soil Analysed as Soil

Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference 201368 001 201368 004 201368 007 201368 008 201368 011 201368 012 201368 014 201368 015 201368 016 Customer Sample Reference Determinand TPH (C6-C8 aliphatic) TPH (C8-C10 aliphatic) TPH (C10-C12 aliphatic) TPH (C12-C16 aliphatic) TPH (C16-C21 aliphatic) TPH (C21-C35 aliphatic) TPH (C6-C7 aromatic) TPH (C7-C8 aromatic) TPH (C8-C10 aromatic) TPH (C10-C12 aromatic) TPH (C12-C16 aromatic) TPH (C16-C21 aromatic) TPH (C21-C35 aromatic) Method T54 T54 T8 T8 T8 T8 T54 T54 T54 T8 T8 T8 T8 Test Sample LOD 0.010 0.010 1 1 1 1 0.010 0.010 0.010 1 1 1 1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.010 <0.010 <1 <1 <1 2 <0.010 <0.010 0.011 <1 <1 4 10 <0.010 <0.010 <1 <1 4 4 <0.010 <0.010 <0.010 <1 <1 1 2
(2) <0.020 (2) <0.020

TP315 1.6

TP316 1.5B

TP317 1.0

TP318 1.3

TP319 1.5

TP320 0.7

TP321 0.9

TP322 1.6

TP323 0.9

<0.010 0.076 <1 10 20 11 <0.010 <0.010 0.012 <1 <1 2 1

0.056 0.23 <1 42 310 210


(2) <0.020 (2) <0.020 (2) <0.020

<0.010 <0.010 <1 <1 2 3 <0.010 <0.010 <0.010 <1 <1 <1 <1

<0.010 <0.010 <1 <1 3 3 <0.010 <0.010 <0.010 <1 <1 <1 <1

<0.010 <0.010 <1 <1 <1 <1 <0.010 <0.010 <0.010 <1 <1 <1 <1

<0.010 <0.010 6 3 <1 3 <0.010 <0.010 <0.010 <1 <1 2 3

<1 3 22 21
(2) <0.020 (2) <0.020 (2) <0.020

<1 <1 3 3

<1 3 29 24

SAL Reference: 201368 Customer Reference: 43391 Soil Miscellaneous SAL Reference 201368 002 201368 003 201368 005 201368 017 Customer Sample Reference Determinand Total Petroleum Hydrocarbons Method T8 Test Sample LOD 1 Units mg/kg 4 360 160 <1 TP316 1.6 TP316 1.5A TP317 0.8 TP323 1.8 Analysed as Soil

SAL Reference: 201368 Customer Reference: 43391 Soil PCB EC7 SAL Reference 201368 001 201368 003 201368 004 201368 005 201368 006 Customer Sample Reference Determinand PCB BZ#101 PCB BZ#118 PCB BZ#138 PCB BZ#153 PCB BZ#180 PCB BZ#28 PCB BZ#52 Method T1 T1 T1 T1 T1 T1 T1 Test Sample LOD 0.00005 0.00005 0.00005 0.00005 0.00005 0.00005 0.00005 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 0.00011 0.00005 0.00021 0.00028 0.00041 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 TP315 1.6 TP316 1.5A TP316 1.5B TP317 0.8 TP317 1.4 Analysed as Soil

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Page 6 of 8

SAL Reference: 201368 Customer Reference: 43391 Soil Analysed as Soil

Volatile Organic Compounds (USEPA 624) SAL Reference 201368 012 201368 013 201368 014 201368 015 Customer Sample Reference Determinand 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethylene 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloropropene 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 4-Chlorotoluene Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane Cis-1,2-Dichloroethylene Cis-1,3-Dichloropropene Dibromomethane Dichlorodifluoromethane Dichloromethane EthylBenzene Isopropyl benzene M/P Xylene n-Propylbenzene O Xylene p-Isopropyltoluene S-Butylbenzene Styrene T-Butylbenzene Tetrachloroethylene Toluene Trans-1,2-Dichloroethene Trans-1,3-Dichloropropene Trichlorofluoromethane Vinyl chloride Method T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 T54 Test Sample LOD 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.001 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.050 0.001 0.005 0.001 0.005 0.001 0.005 0.005 0.005 0.005 0.005 0.001 0.005 0.005 0.005 0.005 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

TP320 0.7

TP320 1.7

TP321 0.9

TP322 1.6

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.050 <0.001 <0.005 <0.001 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.050 <0.001 <0.005 <0.001 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.050 <0.001 <0.005 <0.001 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.050 <0.001 <0.005 <0.001 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.005
(13) <0.001

<0.005 <0.005 <0.005 <0.005

<0.005 <0.005 <0.005 <0.005

<0.005 <0.005 <0.005 <0.005

<0.005 <0.005 <0.005 <0.005

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Page 7 of 8

SAL Reference: 201368 Customer Reference: 43391 Soil Analysed as Soil

Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 201368 009 201368 011 Customer Sample Reference Determinand Phenol Bis (2-chloroethyl) ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Bis (2-chloroisopropyl) ether 2-methyl phenol 3/4-Methylphenol Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol Bis (2-chloroethoxy) methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl phthalate 2,6-Dinitrotoluene Acenaphthylene Acenaphthene 3-Nitroaniline 2,4-Dinitrophenol Dibenzofuran 2,4-Dinitrotoluene 4-Nitrophenol Diethyl phthalate Fluorene 4-Chlorophenyl phenylether 4-Nitroaniline Azobenzene 4-Bromophenyl phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-butylphthalate Fluoranthene Pyrene Butyl benzylphthalate Benzo(a)Anthracene Chrysene Bis (2-ethylhexyl)phthalate Di-n-octylphthalate Benzo(b/k)Fluoranthene Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Benzo(ghi)Perylene Method T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 T16 Test Sample LOD 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.5 0.1 <0.1 <0.1 0.7 0.7 <0.1 0.2 0.2 <0.1 <0.1 0.2 0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.3 <0.1 <0.1 <0.1 0.5 0.5 <0.1 0.2 0.2 <0.1 <0.1 0.2 0.1 <0.1 <0.1 <0.1 TP318 1.6 TP319 1.5

Produced by Scientific Analysis Laboratories, Hadfield House, Hadfield Street, Cornbrook, Manchester, M16 9FE This document has been printed from a digitally signed master copy

Page 8 of 8

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

APPENDIX VII ORIGIN OF TIER I VALUES

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

Origin of REC Tier I Values - Residential (Medium Terrace) with plant uptake

End Use
Constituent Arsenic Cadmium Chromium (Hexavalent) Lead Mercury Nickel Selenium Copper Zinc Cyanide - Inorganic Phenol PCBs total EC7 Benzene Toluene Ethylbenzene Xylenes (p) Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)Anthracene Chrysene Benzo(b/k)Fluoranthene
(iii) (

Unit mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Tier 1 HCV 32 10 4.3 450 11 130 350 2330 3750 791 210 0.01 2009 SGV LQM CIEH 2 LQM CIEH 2

Origin of Risk Assessment Value

nd nd

Edition 2009 Edition 2009

2003 EA SGV CLEA 1.06 not appropriate 2009 SGV 2009 SGV Soil guideline value, DEFRA/Environment Agency LQM CIEH 2 LQM CIEH 2
nd nd

Edition 2009 Edition 2009

CLEA 1.06 Derived Value LQM CIEH 2


nd

Edition 2009

RBCA model using Tox 12 and SR3 2009 SGV (6% SOM) 2009 SGV (6% SOM) 2009 SGV (6% SOM) 2009 SGV (6% SOM)

1.5 170 210 160 92 2300 260 560 3.1 6 14.1 0.83 3.2 0.76 44

General Assessment Criteria (GAC) developed by CIEH / LQM the using CLEA 1-06 with supporting data from SR3, SR7 and existing Tox report where applicable.

Benzo(a)Pyrene Indeno(123-cd)Pyrene Dibenzo(a,h)Anthracen e Benzo(ghi)Perylene

TPH C5-C7 (aliphatic)

(i) (i) (i)

mg/kg mg/kg mg/kg

30 73 19

TPH C7-C8 (aliphatic)

TPH C8-C10 (aliphatic)

Trial Pit Investigation Former Power Station, Thornton Cleveleys


TPH C10-C12 (i) (aromatic) TPH C12-C16 (i) (aromatic) TPH C16-C21 (i) (aromatic) TPH C21-C35 (i) (aromatic) mg/kg mg/kg mg/kg mg/kg 93 140 250 890

August 2010 43391p1r0

Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

APPENDIX VIII 2007 SHALLOW SOILS LABORATORY ANALYTICAL RESULTS

Scientific Analysis Laboratories

Report Number: Date of Report: Client:

96545-1 12-Mar-2007 Resource Environmental Consultants Ltd, Osprey House, Pacific Quay, Broadway, Salford. M50 2UE

Client Contact: Client Job Reference: Client Site Reference:

Ms Jayne Carrick 42614 Former power station, Thornton

Date Job Received at SAL: 28-Feb-2007 Date Analysis Started: 07-Mar-2007 Date Analysis Completed: 12-Mar-2007

The results reported relate to samples received at the laboratory Opinions and interpretations expressed herein are outside the scope of UKAS or MCERTS accreditation This report should not be reproduced except in full without the written approval of the laboratory Tests covered by this certificate were conducted in accordance with SAL SOPs

Key to symbols used in this report: W: Analysis was performed at another SAL Laboratory S: Analysis was sub-contracted N: Analysis is not UKAS accredited U: Analysis is UKAS accredited M: Analysis is MCERTS accredited

Report checked and authorised by:

Miss Debra Hau Project Manager


1549 Group 1549

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 1 of 76

Index to caveats used in this report


Value ND AR A105 A40 2 3 9 33 43 62 63 Description Not Detected As Received Air Dried 105C Air Dried <40C LOD Raised Due to Matrix Interference LOD Raised Due to Elevated Blank LOD raised due to dilution of sample Sample is outside the scope of MCERTS accreditation. Results are UKAS only Sample is outside of the scope of our accreditation LOD was raised due to the method performance of the analytical procedure used LOD was raised because an alternative analytical procedure was used

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Page 2 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil REC Ltd 001S M Analysed as Soil

SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Arsenic Arsenic Arsenic Cadmium Cadmium Cadmium Chromium Chromium Chromium Lead Lead Lead Mercury Mercury Mercury Selenium Selenium Selenium Boron Copper Copper Copper Nickel Nickel Nickel Zinc Zinc Zinc Technique ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES LOD 2.0 2.0 2 1.0 1.0 1 1.0 1.0 1 1.0 1.0 1 1.0 1 1.0 2.0 2 2.0 1 1.0 1 1.0 1.0 1.0 1 1.0 1.0 1 Units Symbol mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M

96545 001 WS203 0.4 AR Clay 0.4

96545 001 WS203 0.4 A40 Clay 0.4

96545 96545 96545 96545 002 002 003 003 TP217 0.2 TP217 0.2 TP216 0.1 TP216 0.1 AR Fill 0.2 A40 Fill 0.2 AR Clay 0.1 A40 Clay 0.1

<1 -

5 <1 17 7 <1 <2 86 11 59

<1 -

(33) 140

(33) 2.4 (33) 37 (33) 120 (33) <1.0 (33) <2.0 (33) 150 (33) 92 (33) 150 -

<1 -

37 1 40 300 16 <2 2200 250 3100

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Page 3 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil REC Ltd 001S M Analysed as Soil

SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Arsenic Arsenic Arsenic Cadmium Cadmium Cadmium Chromium Chromium Chromium Lead Lead Lead Mercury Mercury Mercury Selenium Selenium Selenium Boron Copper Copper Copper Nickel Nickel Nickel Zinc Zinc Zinc Technique ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES LOD 2.0 2.0 2 1.0 1.0 1 1.0 1.0 1 1.0 1.0 1 1.0 1 1.0 2.0 2 2.0 1 1.0 1 1.0 1.0 1.0 1 1.0 1.0 1 Units Symbol mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M

96545 006 WS206 0.2 AR Fill 0.2

96545 006 WS206 0.2 A40 Fill 0.2

96545 007 WS205 0.5 AR Fill 0.5

96545 007 WS205 0.5 A40 Fill 0.5

96545 96545 008 008 TP213 1.9 TP213 1.9 AR Other 1.9 A40 Other 1.9

<1 -

(33) 18

(33) <1.0

(33) 38

(33) 42

(33) <1.0 (33) <2.0 (33) 46 (33) 33

(33) 170

<1 -

(33) 18

(33) 1.0

(33) 62

(33) 68

(33) 1.1 (33) <2.0 (33) 62 (33) 56

(33) 260

<1 -

(43) 13

(43) <1.0 (43) 84 (43) 53 (43) <1.0 (43) <2.0

(43) 39

(43) 15

(43) 97

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Page 4 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil REC Ltd 001S M Analysed as Soil

96545 96545 009 009 Customer Sample Reference TP213 2.4 TP213 2.4 Test Sample Type Date Sampled Depth Determinant Arsenic Arsenic Arsenic Cadmium Cadmium Cadmium Chromium Chromium Chromium Lead Lead Lead Mercury Mercury Mercury Selenium Selenium Selenium Boron Copper Copper Copper Nickel Nickel Nickel Zinc Zinc Zinc Technique ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES LOD 2.0 2.0 2 1.0 1.0 1 1.0 1.0 1 1.0 1.0 1 1.0 1 1.0 2.0 2 2.0 1 1.0 1 1.0 1.0 1.0 1 1.0 1.0 1 Units Symbol mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M AR Clay 2.4 A40 Clay 2.4

SAL Reference

96545 010 WS212 0.3 AR Fill 0.3

96545 010 WS212 0.3 A40 Fill 0.3

96545 011 WS211 0.4 AR Clay 0.4

96545 011 WS211 0.4 A40 Clay 0.4

<1 -

12 <1 37 13 <1 <2 11 32 60

<1 -

(33) 7.9

(33) <1.0 (33) 16 (33) 120 (33) <1.0 (33) <2.0 (33) 11 (33) 11 (33) 69 -

<1 -

7 <1 23 18 <1 <2 8 17 58

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Page 5 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil REC Ltd 001S M Analysed as Soil

SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Arsenic Arsenic Arsenic Cadmium Cadmium Cadmium Chromium Chromium Chromium Lead Lead Lead Mercury Mercury Mercury Selenium Selenium Selenium Boron Copper Copper Copper Nickel Nickel Nickel Zinc Zinc Zinc Technique ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES LOD 2.0 2.0 2 1.0 1.0 1 1.0 1.0 1 1.0 1.0 1 1.0 1 1.0 2.0 2 2.0 1 1.0 1 1.0 1.0 1.0 1 1.0 1.0 1 Units Symbol mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M

96545 012 WS210 0.4 AR Sand 0.4

96545 012 WS210 0.4 A40 Sand 0.4

96545 96545 014 014 TP214 1.6 TP214 1.6 AR Clay 1.6 A40 Clay 1.6

96545 015 CP201 0.3 AR Clay 0.3

96545 015 CP201 0.3 A40 Clay 0.3

<1 -

38 <1 56 67 1 <2 110 73 110

<1 -

6 <1 17 10 <1 <2 4 13 27

<1 -

92 3 170 88 4 <2 130 1800 300

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Page 6 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil REC Ltd 001S M Analysed as Soil

SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Arsenic Arsenic Arsenic Cadmium Cadmium Cadmium Chromium Chromium Chromium Lead Lead Lead Mercury Mercury Mercury Selenium Selenium Selenium Boron Copper Copper Copper Nickel Nickel Nickel Zinc Zinc Zinc Technique ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES LOD 2.0 2.0 2 1.0 1.0 1 1.0 1.0 1 1.0 1.0 1 1.0 1 1.0 2.0 2 2.0 1 1.0 1 1.0 1.0 1.0 1 1.0 1.0 1 Units Symbol mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M

96545 016 WS213 0.3 AR Clay 0.3

96545 016 WS213 0.3 A40 Clay 0.3

96545 96545 017 017 TP212 0.4 TP212 0.4 AR Fill 0.4 A40 Fill 0.4

96545 018 CP202 0.8 AR Clay 0.8

96545 018 CP202 0.8 A40 Clay 0.8

<1 -

9 <1 19 49 1 <2 120 29 190

<1 -

(33) 38

(33) <1.0 (33) 33 (33) 43 (33) <1.0 (33) <2.0 (33) 200 (33) 110 (33) 99 -

<1 -

8 <1 22 33 <1 <2 9 18 38

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Page 7 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil REC Ltd 001S M Analysed as Soil

SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Arsenic Arsenic Arsenic Cadmium Cadmium Cadmium Chromium Chromium Chromium Lead Lead Lead Mercury Mercury Mercury Selenium Selenium Selenium Boron Copper Copper Copper Nickel Nickel Nickel Zinc Zinc Zinc Technique ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES ICP/OES LOD 2.0 2.0 2 1.0 1.0 1 1.0 1.0 1 1.0 1.0 1 1.0 1 1.0 2.0 2 2.0 1 1.0 1 1.0 1.0 1.0 1 1.0 1.0 1 Units Symbol mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M

96545 019 WS202 0.9 AR Clay 0.9

96545 019 WS202 0.9 A40 Clay 0.9

96545 020 WS208 0.9 AR Clay 0.9

96545 020 WS208 0.9 A40 Clay 0.9

96545 021 WS209 0.4 AR Clay 0.4

96545 021 WS209 0.4 A40 Clay 0.4

<1 -

9 <1 30 13 <1 <2 10 23 55

<1 -

12 <1 25 31 <1 <2 15 19 96

<1 -

9 <1 19 19 <1 <2 22 15 50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 8 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

96545 001 Customer Sample Reference WS203 0.4 Test Sample AR Type Clay Date Sampled Depth 0.4 Determinant pH pH pH Sulphate (Total) Sulphate(2:1) Sulphide Sulphur (Free) Cyanide (Total) Cyanide (Total) Technique LOD Units Symbol Probe N Probe U Probe M ICP/OES 0.01 % N ICP/OES Colorimetry Grav Colorimetry Colorimetry 0.1 10 500 1.0 1 g/l mg/kg mg/kg mg/kg mg/kg N N N N U

SAL Reference

96545 001 WS203 0.4 A40 Clay 0.4

96545 002 TP217 0.2 AR Fill 0.2

96545 002 TP217 0.2 A40 Fill 0.2

96545 003 TP216 0.1 AR Clay 0.1

96545 003 TP216 0.1 A40 Clay 0.1

8.2 <0.1 <10 <1

0.17 <500 -

(33) 7.7

<0.1 <10 <1

0.57 <500 -

7.1 <0.1 <10 <1

0.28 <500 -

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

96545 006 Customer Sample Reference WS206 0.2 Test Sample AR Type Fill Date Sampled Depth 0.2 Determinant pH pH pH Sulphate (Total) Sulphate(2:1) Sulphide Sulphur (Free) Cyanide (Total) Cyanide (Total) Technique LOD Units Symbol Probe N Probe U Probe M ICP/OES 0.01 % N ICP/OES Colorimetry Grav Colorimetry Colorimetry 0.1 10 500 1.0 1 g/l mg/kg mg/kg mg/kg mg/kg N N N N U

SAL Reference

96545 006 WS206 0.2 A40 Fill 0.2

96545 007 WS205 0.5 AR Fill 0.5

96545 007 WS205 0.5 A40 Fill 0.5

96545 008 TP213 1.9 AR Other 1.9

96545 008 TP213 1.9 A40 Other 1.9

(33) 7.7

<0.1 <10 4

0.66 <500 -

(33) 7.6

<0.1 <10 <1

1.4 <500 -

(43) 8.1

<0.1 <10 <1.0 -

2.4 <500 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 9 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant pH pH pH Sulphate (Total) Sulphate(2:1) Sulphide Sulphur (Free) Cyanide (Total) Cyanide (Total) Technique LOD Units Symbol Probe N Probe U Probe M ICP/OES 0.01 % N ICP/OES Colorimetry Grav Colorimetry Colorimetry 0.1 g/l 10 mg/kg 500 mg/kg 1.0 mg/kg 1 mg/kg N N N N U

96545 009 TP213 2.4 AR Clay 2.4

96545 009 TP213 2.4 A40 Clay 2.4

96545 010 WS212 0.3 AR Fill 0.3

96545 010 WS212 0.3 A40 Fill 0.3

96545 011 WS211 0.4 AR Clay 0.4

96545 011 WS211 0.4 A40 Clay 0.4

9.0 <0.1 <10 <1

0.06 <500 -

(33) 11.7

<0.1 <10 <1

0.55 <500 -

9.3 <0.1 <10 <1

0.07 <500 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 10 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

96545 012 Customer Sample Reference WS210 0.4 Test Sample AR Type Sand Date Sampled Depth 0.4 Determinant pH pH pH Sulphate (Total) Sulphate(2:1) Sulphide Sulphur (Free) Cyanide (Total) Cyanide (Total) Technique LOD Units Symbol Probe N Probe U Probe M ICP/OES 0.01 % N ICP/OES Colorimetry Grav Colorimetry Colorimetry 0.1 10 500 1.0 1 g/l mg/kg mg/kg mg/kg mg/kg N N N N U

SAL Reference

96545 012 WS210 0.4 A40 Sand 0.4

96545 014 TP214 1.6 AR Clay 1.6

96545 014 TP214 1.6 A40 Clay 1.6

96545 015 CP201 0.3 AR Clay 0.3

96545 015 CP201 0.3 A40 Clay 0.3

8.9 <0.1 <10 <1

0.57 <500 -

8.5 <0.1 <10 <1

0.07 <500 -

9.5 0.2 <10 <1

0.63 <500 -

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

96545 016 Customer Sample Reference WS213 0.3 Test Sample AR Type Clay Date Sampled Depth 0.3 Determinant pH pH pH Sulphate (Total) Sulphate(2:1) Sulphide Sulphur (Free) Cyanide (Total) Cyanide (Total) Technique LOD Units Symbol Probe N Probe U Probe M ICP/OES 0.01 % N ICP/OES Colorimetry Grav Colorimetry Colorimetry 0.1 10 500 1.0 1 g/l mg/kg mg/kg mg/kg mg/kg N N N N U

SAL Reference

96545 016 WS213 0.3 A40 Clay 0.3

96545 017 TP212 0.4 AR Fill 0.4

96545 017 TP212 0.4 A40 Fill 0.4

96545 018 CP202 0.8 AR Clay 0.8

96545 018 CP202 0.8 A40 Clay 0.8

8.3 <0.1 <10 <1

0.24 <500 -

(33) 8.9

<0.1 <10 <1

0.45 <500 -

8.0 <0.1 <10 <1

0.14 <500 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 11 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

96545 019 Customer Sample Reference WS202 0.9 Test Sample AR Type Clay Date Sampled Depth 0.9 Determinant pH pH pH Sulphate (Total) Sulphate(2:1) Sulphide Sulphur (Free) Cyanide (Total) Cyanide (Total) Technique LOD Units Symbol Probe N Probe U Probe M ICP/OES 0.01 % N ICP/OES Colorimetry Grav Colorimetry Colorimetry 0.1 g/l 10 mg/kg 500 mg/kg 1.0 mg/kg 1 mg/kg N N N N U

SAL Reference

96545 019 WS202 0.9 A40 Clay 0.9

96545 020 WS208 0.9 AR Clay 0.9

96545 020 WS208 0.9 A40 Clay 0.9

96545 021 WS209 0.4 AR Clay 0.4

96545 021 WS209 0.4 A40 Clay 0.4

7.3 0.2 <10 <1

0.16 <500 -

7.5 <0.1 <10 <1

0.15 <500 -

7.3 <0.1 <10 <1

0.23 <500 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 12 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Phenols - Total Mono. SAL Reference 96545 001 Customer Sample Reference WS203 0.4 Test Sample AR Type Clay Date Sampled Depth 0.4 Determinant Phenols (Total-Mono) Phenols (Total-Mono) Technique LOD Units Symbol Colorimetry 1.0 mg/kg N Colorimetry 1 mg/kg U 96545 002 TP217 0.2 AR Fill 0.2 96545 003 TP216 0.1 AR Clay 0.1 96545 006 WS206 0.2 AR Fill 0.2 96545 007 WS205 0.5 AR Fill 0.5 96545 008 TP213 1.9 AR Other 1.9

<1

<1

<1

<1

<1

<1.0 -

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Phenols - Total Mono. SAL Reference 96545 009 Customer Sample Reference TP213 2.4 Test Sample AR Type Clay Date Sampled Depth 2.4 Determinant Phenols (Total-Mono) Phenols (Total-Mono) Technique LOD Units Symbol Colorimetry 1.0 mg/kg N Colorimetry 1 mg/kg U 96545 010 WS212 0.3 AR Fill 0.3 96545 011 WS211 0.4 AR Clay 0.4 96545 012 WS210 0.4 AR Sand 0.4 96545 014 TP214 1.6 AR Clay 1.6 96545 015 CP201 0.3 AR Clay 0.3

<1

<1

<1

<1

<1

<1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 13 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Phenols - Total Mono. SAL Reference 96545 016 Customer Sample Reference WS213 0.3 Test Sample AR Type Clay Date Sampled Depth 0.3 Determinant Phenols (Total-Mono) Phenols (Total-Mono) Technique LOD Units Symbol Colorimetry 1.0 mg/kg N Colorimetry 1 mg/kg U 96545 017 TP212 0.4 AR Fill 0.4 96545 018 CP202 0.8 AR Clay 0.8 96545 019 WS202 0.9 AR Clay 0.9 96545 020 WS208 0.9 AR Clay 0.9 96545 021 WS209 0.4 AR Clay 0.4

<1

<1

<1

<1

<1

<1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 14 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil PAH (USEPA 16) (SVOC 625) SAL Reference 96545 96545 96545 96545 96545 96545 001 002 003 006 007 008 Customer Sample Reference WS203 TP217 TP216 WS206 WS205 TP213 0.4 0.2 0.1 0.2 0.5 1.9 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Fill Fill Other Date Sampled Depth 0.4 0.2 0.1 0.2 0.5 1.9 Determinant Naphthalene Naphthalene Naphthalene Acenaphthylene Acenaphthylene Acenaphthene Acenaphthene Acenaphthene Fluorene Fluorene Fluorene Phenanthrene Phenanthrene Phenanthrene Anthracene Anthracene Fluoranthene Fluoranthene Fluoranthene Pyrene Pyrene Pyrene Benzo(a)Anthracene Benzo(a)Anthracene Benzo(a)Anthracene Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg U M N U N U M N U M N M U N U N M U N M U N M U

<0.1 <0.1 <0.1 -

(33) 0.6

(9) <10

(33) <0.1

(43) <0.10 (33) 2.8

<0.1 (33) <0.1

(9) <10

<0.1 (33) <0.1

<0.1 (33) <0.1

(43) <0.10

(43) <0.1

(9) <10

(43) <0.10

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

(33) 0.1

(9) <10

(9) <10

(33) <0.1

(33) 0.6

(43) <0.10

<0.1 (33) <0.1

(9) <10

(43) <0.10

<0.1 (33) <0.1

<0.1 (33) 0.1

(43) <0.10

(9) <10

(33) <0.1

(9) <10

(33) <0.1

(43) <0.10

(33) 0.1

(33) <0.1

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 15 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil PAH (USEPA 16) (SVOC 625) SAL Reference 96545 96545 96545 96545 96545 96545 001 002 003 006 007 008 Customer Sample Reference WS203 TP217 TP216 WS206 WS205 TP213 0.4 0.2 0.1 0.2 0.5 1.9 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Fill Fill Other Date Sampled Depth 0.4 0.2 0.1 0.2 0.5 1.9 Determinant Chrysene Chrysene Chrysene Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg M U N M U N M U N U M N M U N M U

<0.1 <0.1 <0.1 -

(33) <0.1

(9) <10

(43) <0.10

(33,2) <0.2 (33) <0.1

Benzo(b/k)Fluoranthene GC/MS(MCERTS) 0.10 mg/kg Benzo(b/k)Fluoranthene GC/MS(MCERTS) 0.1 mg/kg Benzo(b/k)Fluoranthene GC/MS(MCERTS) 0.1 mg/kg Benzo(a)Pyrene Benzo(a)Pyrene Benzo(a)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

(33) <0.1

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

(33) <0.1

(33) <0.1

(43) <0.10

(33) <0.1

Indeno(123-cd)Pyrene GC/MS(MCERTS) 0.1 mg/kg Dibenzo(ah)Anthracene GC/MS(MCERTS) 0.10 mg/kg Dibenzo(ah)Anthracene GC/MS(MCERTS) 0.1 mg/kg Dibenzo(ah)Anthracene GC/MS(MCERTS) 0.1 mg/kg Benzo(ghi)Perylene Benzo(ghi)Perylene Benzo(ghi)Perylene GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg

<0.1 <0.1 <0.1 -

(33) <0.1

(9) <10

(9) <10

(33) <0.1

(33) <0.1

(43) <0.10

(33) <0.1

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 16 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil PAH (USEPA 16) (SVOC 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant Naphthalene Naphthalene Naphthalene Acenaphthylene Acenaphthylene Acenaphthene Acenaphthene Acenaphthene Fluorene Fluorene Fluorene Phenanthrene Phenanthrene Phenanthrene Anthracene Anthracene Fluoranthene Fluoranthene Fluoranthene Pyrene Pyrene Pyrene Benzo(a)Anthracene Benzo(a)Anthracene Benzo(a)Anthracene Chrysene Chrysene Chrysene Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Benzo(a)Pyrene Benzo(a)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.10 0.1 0.1 0.10 0.1 0.1 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 Units Symbol mg/kg N mg/kg U mg/kg M <0.1 mg/kg N mg/kg U <0.1 mg/kg N mg/kg U mg/kg M <0.1 mg/kg N mg/kg U mg/kg M <0.1 mg/kg N mg/kg M <0.1 mg/kg U mg/kg N mg/kg U <0.1 mg/kg N mg/kg M <0.1 mg/kg U mg/kg N mg/kg M <0.1 mg/kg U mg/kg N mg/kg M <0.1 mg/kg U mg/kg N mg/kg M <0.1 mg/kg U mg/kg N mg/kg M <0.1 mg/kg U mg/kg N mg/kg M <0.1 mg/kg U mg/kg N mg/kg U mg/kg M <0.1 mg/kg N 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

<0.1 (33) <0.1 (33) <0.1 (33) 0.1 <0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 0.1 <0.1 0.1 0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 17 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil PAH (USEPA 16) (SVOC 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Benzo(ghi)Perylene Benzo(ghi)Perylene Benzo(ghi)Perylene Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.1 0.1 0.10 0.1 0.1 Units Symbol mg/kg M <0.1 mg/kg U mg/kg N mg/kg M <0.1 mg/kg U 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

(33) <0.1

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 -

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil PAH (USEPA 16) (SVOC 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant Naphthalene Naphthalene Naphthalene Acenaphthylene Acenaphthylene Acenaphthene Acenaphthene Acenaphthene Fluorene Fluorene Fluorene Phenanthrene Phenanthrene Phenanthrene Anthracene Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.10 0.1 0.1 0.10 0.1 0.1 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 Units Symbol mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N

<0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 (33) <0.1 <0.1 (33) <0.1 <0.1 <0.1 (33) 0.3 (33) 0.5

<0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 18 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil PAH (USEPA 16) (SVOC 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant Anthracene Fluoranthene Fluoranthene Fluoranthene Pyrene Pyrene Pyrene Benzo(a)Anthracene Benzo(a)Anthracene Benzo(a)Anthracene Chrysene Chrysene Chrysene Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Benzo(a)Pyrene Benzo(a)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Benzo(ghi)Perylene Benzo(ghi)Perylene Benzo(ghi)Perylene Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 Units Symbol mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 (33) <0.1 (33) 0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1 (33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 0.6 0.6 0.2 0.2 0.3 0.1 <0.1 <0.1 <0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 19 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference 96545 001 Customer Sample Reference WS203 0.4 Test Sample AR Type Clay Date Sampled Depth 0.4 Determinant Total Petroleum Hydrocarbons (C6 C7 aromatic) Total Petroleum Hydrocarbons (C6-C8 aliphatic) Total Petroleum Hydrocarbons (C7-C8 aromatic) Total Petroleum Hydrocarbons (C8-C10 aliphatic) Total Petroleum Hydrocarbons (C8-C10 aromatic) Total Petroleum Hydrocarbons (C10-C12 aliphatic) Total Petroleum Hydrocarbons (C10-C12 aromatic) Total Petroleum Hydrocarbons (C12-C16 aliphatic) Total Petroleum Hydrocarbons (C12-C16 aromatic) Total Petroleum Hydrocarbons (C16-C21 aliphatic) Total Petroleum Hydrocarbons (C16-C21 aromatic) Total Petroleum Hydrocarbons (C21-C35 aliphatic) Total Petroleum Hydrocarbons (C21-C35 aromatic) Technique LOD Units Symbol GC/MS 10 g/kg N (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) 10 g/kg N 96545 001 WS203 0.4 A105 Clay 0.4 96545 96545 96545 96545 002 003 003 006 TP217 TP216 TP216 0.1 WS206 0.2 0.1 0.2 A105 AR A105 AR Fill Clay Clay Fill 0.2 0.1 0.1 0.2

(63,62) <100

(63,62) <100

(63,62) <100

(63,62) <100

10 g/kg

(63,62) <100

(63,62) <100

10 g/kg

(63,62) <100

(63,62) <100

10 g/kg

(63,62) <100

(63,62) <100

GC/FID

mg/kg

<1

(9) <5

(9) <5

GC/FID

mg/kg

<1

(9) <5

(9) <5

GC/FID

mg/kg

<1

170

170

GC/FID

mg/kg

<1

25

14

GC/FID

mg/kg

1200

530

GC/FID

mg/kg

<1

100

66

GC/FID

mg/kg

4500

1200

GC/FID

mg/kg

<1

89

86

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 20 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference 96545 001 Customer Sample Reference WS203 0.4 Test Sample AR Type Clay Date Sampled Depth 0.4 Determinant Total Petroleum Hydrocarbons Total Petroleum Hydrocarbons Technique LOD Units Symbol GC/FID 1.0 mg/kg U GC/FID 1 mg/kg M 96545 001 WS203 0.4 A105 Clay 0.4 96545 96545 96545 96545 002 003 003 006 TP217 TP216 TP216 0.1 WS206 0.2 0.1 0.2 A105 AR A105 AR Fill Clay Clay Fill 0.2 0.1 0.1 0.2

(33) 18

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Total Petroleum Hydrocarbons (C6 C7 aromatic) Total Petroleum Hydrocarbons (C6-C8 aliphatic) Total Petroleum Hydrocarbons (C7-C8 aromatic) Total Petroleum Hydrocarbons (C8-C10 aliphatic) Total Petroleum Hydrocarbons (C8-C10 aromatic) Technique LOD Units Symbol GC/MS 10 g/kg N (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) 10 g/kg N
(63,62) <100

96545 006 WS206 0.2 A105 Fill 0.2

96545 96545 96545 96545 96545 007 008 008 009 010 WS205 TP213 TP213 1.9 TP213 WS212 0.5 1.9 2.4 0.3 A105 AR A105 A105 A105 Fill Other Other Clay Fill 0.5 1.9 1.9 2.4 0.3

(63,62) <100

(63,62) <100

(63,62) <100

10 g/kg

N
(63,62) <100

(63,62) <100

10 g/kg

N
(63,62) <100

(62,63) 2000

10 g/kg

N
(63,62) <100

(63,62) <100

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 21 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Total Petroleum Hydrocarbons (C10-C12 aliphatic) Total Petroleum Hydrocarbons (C10-C12 aromatic) Total Petroleum Hydrocarbons (C12-C16 aliphatic) Total Petroleum Hydrocarbons (C12-C16 aromatic) Total Petroleum Hydrocarbons (C16-C21 aliphatic) Total Petroleum Hydrocarbons (C16-C21 aromatic) Total Petroleum Hydrocarbons (C21-C35 aliphatic) Total Petroleum Hydrocarbons (C21-C35 aromatic) Total Petroleum Hydrocarbons Total Petroleum Hydrocarbons Technique LOD Units Symbol GC/FID 1 mg/kg N 96545 006 WS206 0.2 A105 Fill 0.2 96545 96545 96545 96545 96545 007 008 008 009 010 WS205 TP213 TP213 1.9 TP213 WS212 0.5 1.9 2.4 0.3 A105 AR A105 A105 A105 Fill Other Other Clay Fill 0.5 1.9 1.9 2.4 0.3

18

GC/FID

mg/kg

<1

GC/FID

mg/kg

190

GC/FID

mg/kg

GC/FID

mg/kg

12

GC/FID

mg/kg

<1

GC/FID

mg/kg

15

GC/FID

mg/kg

GC/FID GC/FID

1.0 mg/kg 1 mg/kg

U M

(33) <1.0

<1

(33) 19

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 22 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference 96545 96545 011 012 Customer Sample Reference WS211 WS210 0.4 0.4 Test Sample AR AR Type Clay Sand Date Sampled Depth 0.4 0.4 Determinant Total Petroleum Hydrocarbons (C6 C7 aromatic) Total Petroleum Hydrocarbons (C6-C8 aliphatic) Total Petroleum Hydrocarbons (C7-C8 aromatic) Total Petroleum Hydrocarbons (C8-C10 aliphatic) Total Petroleum Hydrocarbons (C8-C10 aromatic) Total Petroleum Hydrocarbons (C10-C12 aliphatic) Total Petroleum Hydrocarbons (C10-C12 aromatic) Total Petroleum Hydrocarbons (C12-C16 aliphatic) Total Petroleum Hydrocarbons (C12-C16 aromatic) Total Petroleum Hydrocarbons (C16-C21 aliphatic) Total Petroleum Hydrocarbons (C16-C21 aromatic) Total Petroleum Hydrocarbons (C21-C35 aliphatic) Total Petroleum Hydrocarbons (C21-C35 aromatic) Technique LOD Units Symbol GC/MS 10 g/kg N (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) 10 g/kg N 96545 012 WS210 0.4 A105 Sand 0.4 96545 96545 96545 014 015 016 TP214 CP201 WS213 1.6 0.3 0.3 A105 A105 AR Clay Clay Clay 1.6 0.3 0.3

(63,62) <100

(63,62) <100

10 g/kg

(63,62) <100

10 g/kg

(63,62) <100

10 g/kg

(63,62) <100

GC/FID

mg/kg

<1

<1

GC/FID

mg/kg

<1

<1

GC/FID

mg/kg

GC/FID

mg/kg

<1

<1

GC/FID

mg/kg

GC/FID

mg/kg

GC/FID

mg/kg

GC/FID

mg/kg

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 23 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference 96545 96545 011 012 Customer Sample Reference WS211 WS210 0.4 0.4 Test Sample AR AR Type Clay Sand Date Sampled Depth 0.4 0.4 Determinant Total Petroleum Hydrocarbons Total Petroleum Hydrocarbons Technique GC/FID GC/FID LOD Units Symbol 1.0 mg/kg U 1 mg/kg M 96545 012 WS210 0.4 A105 Sand 0.4 96545 96545 96545 014 015 016 TP214 CP201 WS213 1.6 0.3 0.3 A105 A105 AR Clay Clay Clay 1.6 0.3 0.3

<1

<1

<1

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Total Petroleum Hydrocarbons (C6 - C7 aromatic) Total Petroleum Hydrocarbons (C6-C8 aliphatic) Total Petroleum Hydrocarbons (C7-C8 aromatic) Total Petroleum Hydrocarbons (C8-C10 aliphatic) Total Petroleum Hydrocarbons (C8-C10 aromatic) Technique LOD Units Symbol GC/MS 10 g/kg N (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) 10 g/kg N
(63,62) <100

96545 016 WS213 0.3 A105 Clay 0.3

96545 96545 96545 96545 017 017 018 019 TP212 TP212 0.4 CP202 WS202 0.4 0.8 0.9 AR A105 A105 AR Fill Fill Clay Clay 0.4 0.4 0.8 0.9

96545 019 WS202 0.9 A105 Clay 0.9

(63,62) <100 (63,62) <100

(63,62) <100

(63,62) <100

(63,62) <100

10 g/kg

N
(63,62) <100

(63,62) <100

(63,62) <100

10 g/kg

N
(63,62) <100

(63,62) <100

(63,62) <100

10 g/kg

N
(63,62) <100

(63,62) <100

(63,62) <100

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 24 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Total Petroleum Hydrocarbons (C10-C12 aliphatic) Total Petroleum Hydrocarbons (C10-C12 aromatic) Total Petroleum Hydrocarbons (C12-C16 aliphatic) Total Petroleum Hydrocarbons (C12-C16 aromatic) Total Petroleum Hydrocarbons (C16-C21 aliphatic) Total Petroleum Hydrocarbons (C16-C21 aromatic) Total Petroleum Hydrocarbons (C21-C35 aliphatic) Total Petroleum Hydrocarbons (C21-C35 aromatic) Total Petroleum Hydrocarbons Total Petroleum Hydrocarbons Technique LOD Units Symbol GC/FID 1 mg/kg N 96545 016 WS213 0.3 A105 Clay 0.3 96545 96545 96545 96545 017 017 018 019 TP212 TP212 0.4 CP202 WS202 0.4 0.8 0.9 AR A105 A105 AR Fill Fill Clay Clay 0.4 0.4 0.8 0.9 96545 019 WS202 0.9 A105 Clay 0.9

<1

<1

GC/FID

mg/kg

<1

<1

GC/FID

mg/kg

10

<1

GC/FID

mg/kg

<1

GC/FID

mg/kg

50

GC/FID

mg/kg

<1

GC/FID

mg/kg

130

11

GC/FID

mg/kg

<1

GC/FID GC/FID

1.0 mg/kg 1 mg/kg

U M

<1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 25 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Total Petroleum Hydrocarbons (C6-C35 aliphatic/aromatic) 96545 020 Customer Sample Reference WS208 0.9 Test Sample A105 Type Clay Date Sampled Depth 0.9 Determinant Total Petroleum Hydrocarbons (C6 - C7 aromatic) Total Petroleum Hydrocarbons (C6-C8 aliphatic) Total Petroleum Hydrocarbons (C7-C8 aromatic) Total Petroleum Hydrocarbons (C8-C10 aliphatic) Total Petroleum Hydrocarbons (C8-C10 aromatic) Total Petroleum Hydrocarbons (C10-C12 aliphatic) Total Petroleum Hydrocarbons (C10-C12 aromatic) Total Petroleum Hydrocarbons (C12-C16 aliphatic) Total Petroleum Hydrocarbons (C12-C16 aromatic) Total Petroleum Hydrocarbons (C16-C21 aliphatic) Total Petroleum Hydrocarbons (C16-C21 aromatic) Total Petroleum Hydrocarbons (C21-C35 aliphatic) Total Petroleum Hydrocarbons (C21-C35 aromatic) Total Petroleum Hydrocarbons Total Petroleum Hydrocarbons Technique GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/MS (Headspace) GC/FID GC/FID GC/FID GC/FID GC/FID GC/FID GC/FID GC/FID GC/FID GC/FID LOD Units Symbol 10 g/kg N 10 g/kg 10 g/kg 10 g/kg 10 g/kg N N N N SAL Reference 96545 96545 021 021 WS209 WS209 0.4 0.4 AR A105 Clay Clay 0.4 0.4

(63,62) <100 (63,62) <100 (63,62) <100 (63,62) <100 (63,62) <100

1 1 1 1 1 1 1 1

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

N N N N N N N N U M

<1

<1 <1 <1 <1 3 <1 8 3 -

1.0 mg/kg 1 mg/kg

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 26 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil BTEX GRO MTBE Analysed as Soil

SAL Reference 96545 96545 96545 96545 96545 96545 001 002 003 007 009 010 Customer Sample Reference WS203 TP217 TP216 WS205 TP213 WS212 0.4 0.2 0.1 0.5 2.4 0.3 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 2.4 0.3 Determinant Benzene Benzene EthylBenzene EthylBenzene Gasoline Range Organics Meta/Para-Xylene Meta/Para-Xylene Methyl-tert-Butyl Ether Methyl-tert-Butyl Ether Ortho-Xylene Ortho-Xylene Toluene Toluene Technique LOD Units Symbol GC/MS(Head 10 g/kg U Space)(MCERTS) GC/MS(Head 10 g/kg M Space)(MCERTS) GC/MS(Head 10 g/kg U Space)(MCERTS) GC/MS(Head 10 g/kg M Space)(MCERTS) GC/MS 100 g/kg N (Headspace) GC/MS(Head 10 g/kg U Space)(MCERTS) GC/MS(Head 10 g/kg M Space)(MCERTS) GC/MS(Head 10 g/kg U Space)(MCERTS) GC/MS(Head 10 g/kg M Space)(MCERTS) GC/MS(Head 10 g/kg U Space)(MCERTS) GC/MS(Head 10 g/kg M Space)(MCERTS) GC/MS(Head 10 g/kg U Space)(MCERTS) GC/MS(Head 10 g/kg M Space)(MCERTS)

<10 <10 <10 <10 (3) <30

(33) <10

<10 <10 <10 <10 (3) <30

(33) <10

<10 <10 <100 <10 <10 <10 (3) <30

(33) <10

(33) <10

(33) <10

(33) <10

(33) <10

<100
(33) <10

(33) <10

(33) <10

(33) <10

(33) <10

(33) <10

(3,33) <30

(3,33) <30

(3,33) <30

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 27 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil BTEX GRO MTBE Analysed as Soil

SAL Reference 96545 96545 96545 96545 96545 96545 011 014 015 016 018 019 Customer Sample Reference WS211 TP214 CP201 WS213 CP202 WS202 0.4 1.6 0.3 0.3 0.8 0.9 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Clay Clay Clay Clay Clay Date Sampled Depth 0.4 1.6 0.3 0.3 0.8 0.9 Determinant Benzene Benzene EthylBenzene EthylBenzene Gasoline Range Organics Meta/Para-Xylene Meta/Para-Xylene Methyl-tert-Butyl Ether Methyl-tert-Butyl Ether Ortho-Xylene Ortho-Xylene Toluene Toluene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS (Headspace) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 10 g/kg U 10 g/kg 10 g/kg 10 g/kg 100 g/kg 10 g/kg 10 g/kg 10 g/kg 10 g/kg 10 g/kg 10 g/kg 10 g/kg 10 g/kg M U M N U M U M U M U M

<10 <10 <100 <10 <10 <10 (3) <30

<10 <10 <10 <10 (3) <30

<10 <10 <100 <10 <10 <10 (3) <30

<10 <10 <10 <10 (3) <30

<10 <10 <10 <10 (3) <30

<10 <10 <10 <10 (3) <30

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 28 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil BTEX GRO MTBE Analysed as Soil

SAL Reference 96545 020 96545 021 Customer Sample Reference WS208 0.9 WS209 0.4 Test Sample A105 A105 Type Clay Clay Date Sampled Depth 0.9 0.4 Determinant Benzene Benzene EthylBenzene EthylBenzene Gasoline Range Organics Meta/Para-Xylene Meta/Para-Xylene Methyl-tert-Butyl Ether Methyl-tert-Butyl Ether Ortho-Xylene Ortho-Xylene Toluene Toluene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS (Headspace) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD 10 10 10 10 100 10 10 10 10 10 10 10 10 Units Symbol g/kg U g/kg M g/kg U g/kg M g/kg N g/kg U g/kg M g/kg U g/kg M g/kg U g/kg M g/kg U g/kg M

<10 <10 <100 <10 <10 <10 (3) <30

<10 <10 <10 <10 (3) <30

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 29 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

SAL Reference 96545 96545 96545 001 001 002 Customer Sample Reference WS203 WS203 TP217 0.4 0.4 0.2 Test Sample AR A105 AR Type Clay Clay Fill Date Sampled Depth 0.4 0.4 0.2 Determinant Asbestos (Screen Only) Azobenzene Azobenzene Azobenzene Butylated Hydroxytoluene Phenazine 2-Nitrothiophene Technique Visual GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS GC/MS GC/MS LOD Units Symbol N 0.10 0.1 0.1 0.10 mg/kg mg/kg mg/kg mg/kg N U M N N N

96545 002 TP217 0.2 A105 Fill 0.2

96545 96545 003 003 TP216 TP216 0.1 0.1 AR A105 Clay Clay 0.1 0.1

ND -

<0.1 <0.10 <0.10 <0.10

ND -

(33) <0.1

ND -

(9) <10

0.10 mg/kg 0.10 mg/kg

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

SAL Reference 96545 96545 96545 006 007 008 Customer Sample Reference WS206 WS205 TP213 0.2 0.5 1.9 Test Sample AR AR AR Type Fill Fill Other Date Sampled Depth 0.2 0.5 1.9 Determinant Technique LOD Units Symbol Asbestos (Screen Visual N Only) Azobenzene GC/MS(MCERTS) 0.10 mg/kg N Azobenzene GC/MS(MCERTS) 0.1 mg/kg U Azobenzene GC/MS(MCERTS) 0.1 mg/kg M Butylated GC/MS 0.10 mg/kg N Hydroxytoluene Phenazine GC/MS 0.10 mg/kg N 2-Nitrothiophene GC/MS 0.10 mg/kg N

96545 008 TP213 1.9 A105 Other 1.9

96545 96545 010 010 WS212 WS212 0.3 0.3 AR A105 Fill Fill 0.3 0.3

ND -

ND -

ND -

(43) <0.10

ND -

(33) <0.1

<0.10 <0.10 <0.10

<0.10 <0.10 <0.10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 30 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

SAL Reference 96545 96545 96545 96545 96545 96545 011 012 014 015 016 016 Customer Sample Reference WS211 WS210 TP214 CP201 WS213 WS213 0.4 0.4 1.6 0.3 0.3 0.3 Test Sample AR AR A105 AR AR A105 Type Clay Sand Clay Clay Clay Clay Date Sampled Depth 0.4 0.4 1.6 0.3 0.3 0.3 Determinant Technique LOD Units Symbol Asbestos (Screen Visual N Only) Azobenzene GC/MS(MCERTS) 0.10 mg/kg N Azobenzene GC/MS(MCERTS) 0.1 mg/kg U Azobenzene GC/MS(MCERTS) 0.1 mg/kg M Butylated GC/MS 0.10 mg/kg N Hydroxytoluene Phenazine GC/MS 0.10 mg/kg N 2-Nitrothiophene GC/MS 0.10 mg/kg N SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Miscellaneous Analysed as Soil

ND -

ND -

<0.1 <0.10 <0.10 <0.10

ND -

ND -

<0.1 -

SAL Reference 96545 96545 96545 96545 96545 96545 017 018 019 020 021 021 Customer Sample Reference TP212 CP202 WS202 WS208 WS209 WS209 0.4 0.8 0.9 0.9 0.4 0.4 Test Sample AR A105 A105 A105 AR A105 Type Fill Clay Clay Clay Clay Clay Date Sampled Depth 0.4 0.8 0.9 0.9 0.4 0.4 Determinant Technique LOD Units Symbol Asbestos (Screen Visual N Only) Azobenzene GC/MS(MCERTS) 0.10 mg/kg N Azobenzene GC/MS(MCERTS) 0.1 mg/kg U Azobenzene GC/MS(MCERTS) 0.1 mg/kg M Butylated GC/MS 0.10 mg/kg N Hydroxytoluene Phenazine GC/MS 0.10 mg/kg N 2-Nitrothiophene GC/MS 0.10 mg/kg N

ND -

<0.1 <0.10 <0.10 <0.10

<0.1 <0.10 <0.10 <0.10

<0.1 <0.10 <0.10 <0.10

ND -

<0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 31 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant Phenol Phenol Phenol Bis (2-chloroethyl) ether Bis (2-chloroethyl) ether Bis (2-chloroethyl) ether 2-Chlorophenol 2-Chlorophenol 2-Chlorophenol 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene Bis (2-chloroisopropyl) ether Bis (2-chloroisopropyl) ether Bis (2-chloroisopropyl) ether 2-methyl phenol 2-methyl phenol 2-methyl phenol Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg M U N M U N M U N M U N M U N U M N M U N U M 96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

<0.1 <0.1 <0.1 <0.1 <0.1 -

(33) <0.1

(9) <10

(43) <0.10

(33) <0.1

(9) <10

(43) <0.10

(33) <0.1

(9) <10

(43) <0.10

(33) <0.1

(9) <10

(43) <0.10

(33) <0.1

(9) <10

(43) <0.10

(33) <0.1

(43) <0.10

(43) <0.10

<0.1 <0.1 -

(9) <10

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

<0.1

(9) <10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 32 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant 3/4-Methylphenol 3/4-Methylphenol 3/4-Methylphenol Hexachloroethane Hexachloroethane Nitrobenzene Nitrobenzene Nitrobenzene Isophorone Isophorone 2-Nitrophenol 2-Nitrophenol 2,4-Dimethylphenol 2,4-Dimethylphenol Bis (2-chloroethoxy) methane Bis (2-chloroethoxy) methane Bis (2-chloroethoxy) methane 2,4-Dichlorophenol 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg U M N U
(33) <0.1 (33) <0.1 (9,33) <10

96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

(43) <0.10

(43) <0.10

(33) <0.1

<0.1 -

(9) <10

N M U N U

<0.1 -

(33) <0.1

(9) <10

(43) <0.10

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N U

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N U

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N U M N U

(43) <0.10

(33) <0.1

<0.1 -

(9) <10

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

(43) <0.10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 33 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant 1,2,4-Trichlorobenzene 1,2,4-Trichlorobenzene Naphthalene Naphthalene Naphthalene 4-Chloroaniline 4-Chloroaniline Hexachlorobutadiene Hexachlorobutadiene Hexachlorobutadiene 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 2-Methylnaphthalene Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg U GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg M N U M N U
(33) <0.1 (33) <0.1 (9,33) <10

96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

(33) <0.1

(33) 0.6 (9) <10

(33) <0.1

(33) 2.8

(43) <0.10

<0.1 <0.1 -

(9) <10

(43) <0.10

N M U N M U N U M N U

<0.1 <0.1 <0.1 -

(33) <0.1

(9) <10

(43) <0.10

(33) <0.1

(9) <10

(43) <0.10

(33) 0.5

(9) <10

(43) <0.10

2-Methylnaphthalene GC/MS(MCERTS) 0.1 mg/kg 2-Methylnaphthalene GC/MS(MCERTS) 0.1 mg/kg Hexachlorocyclopentadiene GC/MS(MCERTS) 0.10 mg/kg Hexachlorocyclopentadiene GC/MS(MCERTS) 0.1 mg/kg 2,4,6-Trichlorophenol 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4,5-Trichlorophenol GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) 0.5

(43) <0.10

(33) <0.1

(9,33) <10

N U

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N U

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 34 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant 2-Chloronaphthalene 2-Chloronaphthalene 2-Chloronaphthalene 2-Nitroaniline 2-Nitroaniline 2-Nitroaniline Dimethyl phthalate Dimethyl phthalate 2,6-Dinitrotoluene 2,6-Dinitrotoluene Acenaphthylene Acenaphthylene Acenaphthene Acenaphthene Acenaphthene 3-Nitroaniline 3-Nitroaniline 2,4-Dinitrophenol 2,4-Dinitrophenol Dibenzofuran Dibenzofuran Dibenzofuran Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.1 0.1 0.1 0.1 mg/kg mg/kg mg/kg mg/kg M U N M U N U
(33) <0.1 (33) <0.1 (9,33) <10

96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

<0.1 <0.1 -

(33) <0.1

(9) <10

(43) <0.10

(33) <0.1

(9) <10

(43) <0.10

(43) <0.10

N U

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N U N M U N U

<0.1 <0.1 -

<0.1 (33) <0.1

(9) <10

<0.1 (33) <0.1

(43) <0.10

(9) <10

<0.1 (33) <0.1

(43) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N U

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N M U

<0.1 -

(33) <0.1

(9) <10

(43) <0.10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 35 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant 2,4-Dinitrotoluene 2,4-Dinitrotoluene 2,4-Dinitrotoluene 4-Nitrophenol 4-Nitrophenol Diethyl phthalate Diethyl phthalate Fluorene Fluorene Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg U M N U
(33) <0.1 (33) <0.1 (9,33) <10

96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

(43) <0.10

(43) <0.10

(33) <0.1

<0.1 -

(9) <10

N U

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N U M N U M N U

(33) <0.1

(43) <0.10

(33) <0.1

(33) <0.1

Fluorene GC/MS(MCERTS) 0.1 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.10 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg 4-Nitroaniline GC/MS(MCERTS) 0.10 mg/kg 4-Nitroaniline Azobenzene Azobenzene GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg

<0.1 -

(9) <10

(43) <0.10

(43) <0.10

(33) <0.1

<0.1 -

(9) <10

(33) <0.1 (33) <0.1 (9,33) <10

N U M N U M

(43) <0.10

(43) <0.10

(33) <0.1

Azobenzene GC/MS(MCERTS) 0.1 mg/kg 4-Bromophenyl phenylether GC/MS(MCERTS) 0.10 mg/kg 4-Bromophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg 4-Bromophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg

<0.1 -

(9) <10

(33) <0.1

<0.1

(9) <10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 36 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant Hexachlorobenzene Hexachlorobenzene Hexachlorobenzene Pentachlorophenol Pentachlorophenol Phenanthrene Phenanthrene Phenanthrene Anthracene Anthracene Carbazole Carbazole Di-n-butylphthalate Di-n-butylphthalate Di-n-butylphthalate Fluoranthene Fluoranthene Fluoranthene Pyrene Pyrene Pyrene Butyl benzylphthalate Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg M U N U
(33) <0.1 (33) <0.1 (9,33) <10

96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

<0.1 -

(33) <0.1

(9) <10

(43) <0.10

(43) <0.10

N U M N U N U

<0.1 <0.1 -

(33) 0.1

(9) <10

(33) <0.1

(43) <0.10 (33) 0.6

<0.1 -

(9) <10

<0.1 -

<0.1 -

(43) <0.10

(43) <0.10

(33) <0.1 (33) <0.1 (9,33) <10

N M U N M U N U M N

<0.1 <0.1 -

(33) <0.1

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

(9) <10

(43) <0.10

(33) 0.1

(33) <0.1

(33) <0.1

(43) <0.10 (33) 0.1

(43) <0.10

<0.1 -

(9) <10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 37 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant Butyl benzylphthalate Benzo(a)Anthracene Benzo(a)Anthracene Benzo(a)Anthracene Chrysene Chrysene Chrysene Bis (2-ethylhexyl)phthalate Bis (2-ethylhexyl)phthalate Bis (2-ethylhexyl)phthalate Di-n-octylphthalate Di-n-octylphthalate Di-n-octylphthalate Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Benzo(a)Pyrene Benzo(a)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg U
(33) <0.1

96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

(33) 0.1

(9,33) <10

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.1 0.10 0.1 0.1 0.10 mg/kg mg/kg mg/kg mg/kg mg/kg

N M U N U M N U M N M U N U M N U M N M U N

<0.1 -

(33) <0.1

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

(33) <0.1

(43) <0.10

(33,2) <0.2 (33) <0.1

<0.1 <0.1 <0.1 -

(33) 0.1

(9) <10

(9) <10

(33) <0.1

(9) <10

(33) <0.1

(43) 0.10

(43) <0.10

GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg

(33) <0.1

(43) <0.10

(33) <0.1

<0.1 -

(9) <10

(33) <0.1

(43) <0.10

(33) <0.1

(33) <0.1

<0.1 <0.1 -

(33) <0.1

(9) <10

(9) <10

(33) <0.1

(33) <0.1

(43) <0.10

(43) <0.10

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 38 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 001 002 003 Customer Sample Reference WS203 TP217 TP216 0.4 0.2 0.1 Test Sample A105 A105 A105 Type Clay Fill Clay Date Sampled Depth 0.4 0.2 0.1 Determinant Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Benzo(ghi)Perylene Benzo(ghi)Perylene Benzo(ghi)Perylene Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg U GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg M N U M 96545 96545 96545 006 007 008 WS206 WS205 TP213 0.2 0.5 1.9 A105 A105 A105 Fill Fill Other 0.2 0.5 1.9

(33) <0.1

(9) <10

(33) <0.1

(33) <0.1

<0.1 -

(33) <0.1

(43) <0.10

(33) <0.1

(33) <0.1

<0.1

(9) <10

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant Phenol Phenol Phenol Bis (2-chloroethyl) ether Bis (2-chloroethyl) ether Bis (2-chloroethyl) ether 2-Chlorophenol 2-Chlorophenol Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.10 0.1 0.1 Units Symbol mg/kg N mg/kg M mg/kg U N M U N M 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

<0.1 <0.1 <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 39 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant 2-Chlorophenol 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene Bis (2-chloroisopropyl) ether Bis (2-chloroisopropyl) ether Bis (2-chloroisopropyl) ether 2-methyl phenol 2-methyl phenol 2-methyl phenol 3/4-Methylphenol 3/4-Methylphenol 3/4-Methylphenol Hexachloroethane Hexachloroethane Nitrobenzene Nitrobenzene Nitrobenzene Isophorone Isophorone 2-Nitrophenol Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg U GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg N M U N M U N U M N M U N U M N U M N U N M U N U N 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

(33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 (33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 (33) <0.1

(33) <0.1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 40 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant 2-Nitrophenol 2,4-Dimethylphenol 2,4-Dimethylphenol Bis (2-chloroethoxy) methane Bis (2-chloroethoxy) methane Bis (2-chloroethoxy) methane 2,4-Dichlorophenol 2,4-Dichlorophenol 1,2,4-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2,4-Trichlorobenzene Naphthalene Naphthalene Naphthalene 4-Chloroaniline 4-Chloroaniline Hexachlorobutadiene Hexachlorobutadiene Hexachlorobutadiene 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 2-Methylnaphthalene 2-Methylnaphthalene Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg U GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg N U N U M N U N U M N U M N U N M U N M U N U M N 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 -

<0.1 -

(33) <0.1

<0.1 (33) <0.1

<0.1 -

(33) <0.1

<0.1 -

(33) <0.1

<0.1 <0.1 (33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 <0.1 <0.1 -

(33) <0.1

(33) <0.1

2-Methylnaphthalene GC/MS(MCERTS) 0.1 mg/kg Hexachlorocyclopentadiene GC/MS(MCERTS) 0.10 mg/kg

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 41 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant Technique LOD Units Symbol Hexachlorocyclopentadiene GC/MS(MCERTS) 0.1 mg/kg U 2,4,6-Trichlorophenol 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Chloronaphthalene 2-Chloronaphthalene 2-Nitroaniline 2-Nitroaniline 2-Nitroaniline Dimethyl phthalate Dimethyl phthalate 2,6-Dinitrotoluene 2,6-Dinitrotoluene Acenaphthylene Acenaphthylene Acenaphthene Acenaphthene Acenaphthene 3-Nitroaniline 3-Nitroaniline 2,4-Dinitrophenol 2,4-Dinitrophenol Dibenzofuran Dibenzofuran Dibenzofuran 2,4-Dinitrotoluene GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.10 0.1 0.1 0.1 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg N U N U N M U N M U N U N U N U N M U N U N U N M U N 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 -

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 <0.1 (33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 (33) <0.1

<0.1 <0.1 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg

(33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 42 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant 2,4-Dinitrotoluene 2,4-Dinitrotoluene 4-Nitrophenol 4-Nitrophenol Diethyl phthalate Diethyl phthalate Fluorene Fluorene Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg U GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg M N U N U N U M N U M N U N U M N U M N M U N U N U M N 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

(33) <0.1

<0.1 0.1 -

<0.1 (33) <0.1

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 -

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 <0.1 (33) <0.1

Fluorene GC/MS(MCERTS) 0.1 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.10 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg 4-Nitroaniline GC/MS(MCERTS) 0.10 mg/kg 4-Nitroaniline GC/MS(MCERTS) 0.1 mg/kg Azobenzene Azobenzene GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

(33) <0.1

(33) <0.1

<0.1 <0.1 <0.1 (33) <0.1

Azobenzene GC/MS(MCERTS) 0.1 mg/kg 4-Bromophenyl phenylether GC/MS(MCERTS) 0.10 mg/kg 4-Bromophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg 4-Bromophenyl phenylether Hexachlorobenzene Hexachlorobenzene Hexachlorobenzene Pentachlorophenol Pentachlorophenol Phenanthrene Phenanthrene Phenanthrene Anthracene GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.1 0.10 0.1 0.1 mg/kg mg/kg mg/kg mg/kg

(33) <0.1

(33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.10 0.1 0.1 0.10 mg/kg mg/kg mg/kg mg/kg

(33) <0.1

(33) 0.1

<0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 43 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant Anthracene Carbazole Carbazole Di-n-butylphthalate Di-n-butylphthalate Di-n-butylphthalate Fluoranthene Fluoranthene Fluoranthene Pyrene Pyrene Pyrene Butyl benzylphthalate Butyl benzylphthalate Benzo(a)Anthracene Benzo(a)Anthracene Benzo(a)Anthracene Chrysene Chrysene Chrysene Bis (2-ethylhexyl)phthalate Bis (2-ethylhexyl)phthalate Bis (2-ethylhexyl)phthalate Di-n-octylphthalate Di-n-octylphthalate Di-n-octylphthalate Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.1 0.10 0.1 Units Symbol mg/kg U <0.1 mg/kg N mg/kg U N M U N M U N U M N U N M U N U M N U M N M U N U M N <0.1 <0.1 <0.1 <0.1 <0.1 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

<0.1 (33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 0.1 0.1 <0.1 <0.1 <0.1 -

<0.1 (33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.1 0.10 0.1 0.1 0.10 0.1 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

(33) <0.1

<0.1 <0.1 <0.1 (33) <0.1

(33) <0.1

(33) <0.1

(33) 0.2 (33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 -

(33) <0.1

(33) 0.4 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg

(33) <0.1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 44 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 009 010 011 012 Customer Sample Reference TP213 WS212 WS211 WS210 2.4 0.3 0.4 0.4 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Sand Date Sampled Depth 2.4 0.3 0.4 0.4 Determinant Benzo(a)Pyrene Benzo(a)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Benzo(ghi)Perylene Benzo(ghi)Perylene Benzo(ghi)Perylene Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg U GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.1 0.10 0.1 0.1 mg/kg mg/kg mg/kg mg/kg M N M U N U M N U M 96545 96545 014 015 TP214 CP201 1.6 0.3 A105 A105 Clay Clay 1.6 0.3

(33) <0.1

(33) <0.1

<0.1 <0.1 <0.1 <0.1

<0.1 <0.1 <0.1 <0.1

<0.1 <0.1 <0.1 <0.1

<0.1 <0.1 <0.1 <0.1

<0.1 <0.1 <0.1 <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

(33) <0.1

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant Phenol Phenol Phenol Bis (2-chloroethyl) ether Bis (2-chloroethyl) ether Bis (2-chloroethyl) ether Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.10 0.1 0.1 0.10 0.1 0.1 Units Symbol mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U

0.1 <0.1 -

0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 45 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant 2-Chlorophenol 2-Chlorophenol 2-Chlorophenol 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene Bis (2-chloroisopropyl) ether Bis (2-chloroisopropyl) ether Bis (2-chloroisopropyl) ether 2-methyl phenol 2-methyl phenol 2-methyl phenol 3/4-Methylphenol 3/4-Methylphenol 3/4-Methylphenol Hexachloroethane Hexachloroethane Nitrobenzene Nitrobenzene Nitrobenzene Isophorone Isophorone 2-Nitrophenol 2-Nitrophenol 2,4-Dimethylphenol 2,4-Dimethylphenol Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 Units Symbol mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U mg/kg M mg/kg N M U N U M N U M N U N M U N U N U N U

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 (33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 (33) <0.1

GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.10 0.1 0.1 0.10 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

(33) <0.1 (33) <0.1

<0.1 (33) <0.1

<0.1 -

<0.1 -

<0.1 (33) <0.1

(33) <0.1 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

(33) <0.1

(33) <0.1 (33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1 (33) <0.1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 46 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant Bis (2-chloroethoxy) methane Bis (2-chloroethoxy) methane Bis (2-chloroethoxy) methane 2,4-Dichlorophenol 2,4-Dichlorophenol 1,2,4-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2,4-Trichlorobenzene Naphthalene Naphthalene Naphthalene 4-Chloroaniline 4-Chloroaniline Hexachlorobutadiene Hexachlorobutadiene Hexachlorobutadiene 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 2-Methylnaphthalene 2-Methylnaphthalene 2-Methylnaphthalene Hexachlorocyclopentadiene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Chloronaphthalene 2-Chloronaphthalene Technique LOD Units Symbol GC/MS(MCERTS) 0.10 mg/kg N GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg U M N U N U M N U M N U N M U N M U N U M N U N U N U N M U

<0.1 (33) <0.1

(33) 0.5 -

<0.1 -

<0.1 -

<0.1 -

<0.1 (33) <0.1

(33) <0.1 (33) <0.1

<0.1 <0.1 (33) <0.1

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 (33) <0.1

(33) <0.1 (33) <0.1

<0.1 <0.1 <0.1 (33) <0.1

<0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 (33) <0.1

(33) <0.1 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

(33) <0.1

(33) <0.1 (33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1 (33) <0.1

<0.1 -

<0.1 -

<0.1 -

<0.1 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 47 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant 2-Nitroaniline 2-Nitroaniline 2-Nitroaniline Dimethyl phthalate Dimethyl phthalate 2,6-Dinitrotoluene 2,6-Dinitrotoluene Acenaphthylene Acenaphthylene Acenaphthene Acenaphthene Acenaphthene 3-Nitroaniline 3-Nitroaniline 2,4-Dinitrophenol 2,4-Dinitrophenol Dibenzofuran Dibenzofuran Dibenzofuran 2,4-Dinitrotoluene 2,4-Dinitrotoluene 2,4-Dinitrotoluene 4-Nitrophenol 4-Nitrophenol Diethyl phthalate Diethyl phthalate Fluorene Fluorene Technique GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) LOD 0.10 0.1 0.1 0.10 0.1 Units Symbol mg/kg N mg/kg M mg/kg U mg/kg N mg/kg U N U N U N M U N U N U N M U N U M N U N U N U M N U

<0.1 (33) <0.1

<0.1 (33) <0.1

<0.1 -

<0.1 -

<0.1 <0.1 <0.1 -

<0.1 (33) <0.1

(33) <0.1 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.10 0.1 0.1 0.1 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg

(33) <0.1

(33) <0.1

(33) <0.1 (33) <0.1

<0.1 <0.1 (33) <0.1

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

(33) <0.1

(33) <0.1 (33) <0.1

(33) <0.1

(33) <0.1

(33) <0.1 (33) <0.1

<0.1 <0.1 (33) <0.1

<0.1 <0.1 -

<0.1 <0.1 -

<0.1 <0.1 (33) <0.1

(33) <0.1 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

(33) <0.1

(33) <0.1 (33) <0.1

<0.1 -

<0.1 -

<0.1 -

<0.1 -

Fluorene GC/MS(MCERTS) 0.1 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.10 mg/kg 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 48 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant Technique LOD Units Symbol 4-Chlorophenyl phenylether GC/MS(MCERTS) 0.1 mg/kg M 4-Nitroaniline GC/MS(MCERTS) 0.10 mg/kg N 4-Nitroaniline GC/MS(MCERTS) 0.1 mg/kg U Azobenzene Azobenzene Azobenzene 4-Bromophenyl phenylether 4-Bromophenyl phenylether 4-Bromophenyl phenylether Hexachlorobenzene Hexachlorobenzene Hexachlorobenzene Pentachlorophenol Pentachlorophenol Phenanthrene Phenanthrene Phenanthrene Anthracene Anthracene Carbazole Carbazole Di-n-butylphthalate Di-n-butylphthalate Di-n-butylphthalate Fluoranthene Fluoranthene Fluoranthene Pyrene Pyrene Pyrene Butyl benzylphthalate Butyl benzylphthalate Benzo(a)Anthracene GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.10 0.1 0.1 0.10 0.1 0.10 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg N U M N U M N M U N U N U M N U N U N M U N M U N U M N U N

<0.1 (33) <0.1

(33) 0.3

<0.1 -

<0.1 -

<0.1 <0.1 <0.1 <0.1 <0.1 -

<0.1 (33) <0.1

(33) <0.1 (33) <0.1

<0.1 <0.1 <0.1 (33) <0.1

<0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 (33) <0.1

(33) <0.1 (33) <0.1

<0.1 <0.1 (33) <0.1

<0.1 (33) <0.1

<0.1 <0.1 -

<0.1 <0.1 -

0.1 <0.1 (33) <0.1

(33) <0.1 (33) <0.1

<0.1 <0.1 <0.1 (33) <0.1

<0.1 <0.1 <0.1 -

<0.1 <0.1 <0.1 -

<0.1 0.6 0.6 (33) <0.1

(33) 0.1

(33) <0.1 (33) <0.1

GC/MS(MCERTS) 0.10 mg/kg

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 49 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Semi-Volatile Organic Compounds (USEPA 625) SAL Reference 96545 96545 96545 96545 96545 96545 016 017 018 019 020 021 Customer Sample Reference WS213 TP212 CP202 WS202 WS208 WS209 0.3 0.4 0.8 0.9 0.9 0.4 Test Sample A105 A105 A105 A105 A105 A105 Type Clay Fill Clay Clay Clay Clay Date Sampled Depth 0.3 0.4 0.8 0.9 0.9 0.4 Determinant Benzo(a)Anthracene Benzo(a)Anthracene Chrysene Chrysene Chrysene Bis (2-ethylhexyl)phthalate Bis (2-ethylhexyl)phthalate Bis (2-ethylhexyl)phthalate Di-n-octylphthalate Di-n-octylphthalate Di-n-octylphthalate Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(b/k)Fluoranthene Benzo(a)Pyrene Benzo(a)Pyrene Benzo(a)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Indeno(123-cd)Pyrene Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Dibenzo(ah)Anthracene Benzo(ghi)Perylene Benzo(ghi)Perylene Benzo(ghi)Perylene Technique LOD Units Symbol GC/MS(MCERTS) 0.1 mg/kg M GC/MS(MCERTS) 0.1 mg/kg U GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.1 0.10 0.1 0.1 0.10 0.1 0.1 0.10 0.1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg N U M N U M N M U N U M N U M N M U N U M N U M

<0.1 <0.1 0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

(33) <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

0.2 0.2 0.3 <0.1 0.3 0.1 <0.1 <0.1 <0.1

(33) <0.1

(33) <0.1

GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) GC/MS(MCERTS) 0.1 0.10 0.1 0.1 mg/kg mg/kg mg/kg mg/kg

(33) <0.1

(33) <0.1

GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.10 mg/kg GC/MS(MCERTS) 0.1 mg/kg GC/MS(MCERTS) 0.1 mg/kg

(33) <0.1

(33) <0.1

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 50 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant 1,1,1,2-Tetrachloroethane 1,1,1,2-Tetrachloroethane 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,1-Trichloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethane 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloroethylene 1,1-Dichloroethylene 1,1-Dichloropropene 1,1-Dichloropropene 1,1-Dichloropropene 1,2,3-Trichloropropane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U M N U N M U N M U N U M N U M N 96545 008 TP213 1.9 A105 Other 1.9 96545 009 TP213 2.4 A105 Clay 2.4

<50 <50 <50 <50 <50 <50 <50 -

(33) <50

<50 <50 <50 <50 <50 <50 <50 -

(43) <50

(43) <50

(33) <50

(43) <50

<50 (33) <50

(43) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 51 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2,4-Trimethylbenzene 1,2,4-Trimethylbenzene 1,2-dibromoethane 1,2-dibromoethane 1,2-dibromoethane 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloroethane 1,2-Dichloroethane 1,2-Dichloropropane 1,2-Dichloropropane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3,5-Trimethylbenzene 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg N M U N U M N U M N U M N M U N U M N 96545 008 TP213 1.9 A105 Other 1.9 96545 009 TP213 2.4 A105 Clay 2.4

<50 <50 <50 <50 <50 <50 <50 -

<50 (33) <50

<50 <50 <50 <50 <50 <50 <50 -

(43) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 52 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,3-Dichloropropane 1,3-Dichloropropane 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 2,2-Dichloropropane 2,2-Dichloropropane 2-Chlorotoluene 2-Chlorotoluene 4-Chlorotoluene 4-Chlorotoluene Benzene Benzene Benzene Bromobenzene Bromobenzene Bromobenzene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg M N U M N M U N U N U N U N M U N U M 96545 008 TP213 1.9 A105 Other 1.9 96545 009 TP213 2.4 A105 Clay 2.4

<50 <50 <50 <50 <50 <50 <10 <50

(33) <50

<50 <50 <50 <50 <50 <50 <10 <50

(33) <10

(43) <50

<10 -

(33) <50

(43) <50

(33) <50

(43) <50

<50 <50 <50 (33) <10

(43) <50

(43) <50

(43) <10

(43) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 53 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant Bromochloromethane Bromochloromethane Bromochloromethane Bromodichloromethane Bromodichloromethane Bromodichloromethane Bromoform Bromoform Bromoform Bromomethane Bromomethane Carbon tetrachloride Carbon tetrachloride Carbon tetrachloride Chlorobenzene Chlorobenzene Chlorobenzene Chlorodibromomethane Chlorodibromomethane Chlorodibromomethane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U M N M U N U N U M N M U N M U 96545 008 TP213 1.9 A105 Other 1.9 96545 009 TP213 2.4 A105 Clay 2.4

<50 <50 <50 <50 <50 <50 <50 -

(33) <50

<50 <50 <50 <50 <50 <50 <50 -

(43) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

<50 (33) <50

(43) <50

(43) <50

(33) <50

(43) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 54 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant Chloroethane Chloroethane Chloroethane Chloroform Chloroform Chloroform Chloromethane Chloromethane cis-1,2-Dichloroethylene cis-1,2-Dichloroethylene cis-1,2-Dichloroethylene cis-1,3-Dichloropropene cis-1,3-Dichloropropene cis-1,3-Dichloropropene Dibromomethane Dibromomethane Dibromomethane dichlorodifluoromethane dichlorodifluoromethane dichlorodifluoromethane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U M N U N M U N U M N U M N U M 96545 008 TP213 1.9 A105 Other 1.9 96545 009 TP213 2.4 A105 Clay 2.4

<50 <50 <50 <50 <50 <50 <50

(33) <50

<50 <50 <50 <50 <50 <50 <50

(43) <50

(43) <50

(33) <50

(43) <50

<50 (33) <50

(43) <50

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 55 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant Dichloromethane Dichloromethane EthylBenzene EthylBenzene EthylBenzene Isopropyl benzene Isopropyl benzene Isopropyl benzene Meta/Para-Xylene Meta/Para-Xylene Meta/Para-Xylene n-Propylbenzene n-Propylbenzene n-Propylbenzene Ortho-Xylene Ortho-Xylene Ortho-Xylene p-Isopropyltoluene p-Isopropyltoluene p-Isopropyltoluene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg U
(3) <500

96545 008 TP213 1.9 A105 Other 1.9

96545 009 TP213 2.4 A105 Clay 2.4

(3) <500

(3,43) <500

(43) <10

(3) <500

<10 <10 <10 -

N M U N U M N M U N M U N U M N U M

<10 <50 <10 <50 <10 <50

(33) <10

<10 <50 <10 <50 <10 <50

(33) <10

(43) <50

(33) <50

(33) <10

(43) <10

(33) <10

(43) <50

(33) <50

(33) <10

(43) <10

(33) <10

(43) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 56 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant sec-Butylbenzene sec-Butylbenzene sec-Butylbenzene Styrene Styrene tert-Butylbenzene tert-Butylbenzene tert-Butylbenzene Tetrachloroethylene Tetrachloroethylene Tetrachloroethylene Toluene Toluene Toluene trans-1,2-Dichloroethylene trans-1,2-Dichloroethylene trans-1,2-Dichloroethylene trans-1,3-Dichloropropene trans-1,3-Dichloropropene trans-1,3-Dichloropropene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U N M U N U M N M U N M U N U M 96545 008 TP213 1.9 A105 Other 1.9 96545 009 TP213 2.4 A105 Clay 2.4

<50 <50 <50 <50 (3) <30

(33) <50

<50 <50 <50 <50 (3) <30

(43) <50

(3) <30

(43) <50

(33) <50

(43) <50

(33) <50

(43) <50

(33) <50

(3,43) <30

(3,33) <30

(3,33) <30

<50 <50

(33) <50

<50 <50

(43) <50

(43) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 57 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 001 002 003 007 Customer Sample Reference WS203 TP217 TP216 WS205 0.4 0.2 0.1 0.5 Test Sample A105 A105 A105 A105 Type Clay Fill Clay Fill Date Sampled Depth 0.4 0.2 0.1 0.5 Determinant Trichloroethylene Trichloroethylene Trichloroethylene Trichlorofluoromethane Trichlorofluoromethane Trichlorofluoromethane Vinyl chloride monomer Vinyl chloride monomer Vinyl chloride monomer Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg M U N U M N U M 96545 008 TP213 1.9 A105 Other 1.9 96545 009 TP213 2.4 A105 Clay 2.4

<50 <50 <50

(33) <50

<50 <50 <50

(43) <50

(43) <50

(33) <50

(43) <50

(33) <50

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant 1,1,1,2-Tetrachloroethane Technique LOD Units Symbol GC/MS(Head 50 g/kg N Space)(MCERTS) 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 58 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Technique GC/MS(Head Space)(MCERTS) 1,1,1,2-Tetrachloroethane GC/MS(Head Space)(MCERTS) 1,1,1-Trichloroethane GC/MS(Head Space)(MCERTS) 1,1,1-Trichloroethane GC/MS(Head Space)(MCERTS) 1,1,1-Trichloroethane GC/MS(Head Space)(MCERTS) 1,1,2,2-Tetrachloroethane GC/MS(Head Space)(MCERTS) 1,1,2,2-Tetrachloroethane GC/MS(Head Space)(MCERTS) 1,1,2-Trichloroethane GC/MS(Head Space)(MCERTS) 1,1,2-Trichloroethane GC/MS(Head Space)(MCERTS) 1,1,2-Trichloroethane GC/MS(Head Space)(MCERTS) 1,1-Dichloroethane GC/MS(Head Space)(MCERTS) 1,1-Dichloroethane GC/MS(Head Space)(MCERTS) 1,1-Dichloroethane GC/MS(Head Space)(MCERTS) 1,1-Dichloroethylene GC/MS(Head Space)(MCERTS) 1,1-Dichloroethylene GC/MS(Head Space)(MCERTS) 1,1-Dichloroethylene GC/MS(Head Space)(MCERTS) 1,1-Dichloropropene GC/MS(Head Space)(MCERTS) 1,1-Dichloropropene GC/MS(Head Space)(MCERTS) 1,1-Dichloropropene GC/MS(Head Space)(MCERTS) 1,2,3-Trichloropropane GC/MS(Head Space)(MCERTS) Determinant 1,1,1,2-Tetrachloroethane LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg M N U M N U N M U N M U N U M N U M N 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

(33) <50

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

(33) <50

<50 (33) <50

(33) <50

(33) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 59 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2,4-Trimethylbenzene 1,2,4-Trimethylbenzene 1,2-dibromoethane 1,2-dibromoethane 1,2-dibromoethane 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloroethane 1,2-Dichloroethane 1,2-Dichloropropane 1,2-Dichloropropane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3,5-Trimethylbenzene 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg N M U N U M N U M N U M N M U N U M N 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

<50 (33) <50

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

(33) <50

(33) <50

(33) <50

(33) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 60 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,3-Dichloropropane 1,3-Dichloropropane 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 2,2-Dichloropropane 2,2-Dichloropropane 2-Chlorotoluene 2-Chlorotoluene 4-Chlorotoluene 4-Chlorotoluene Benzene Benzene Benzene Bromobenzene Bromobenzene Bromobenzene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg M N U M N M U N U N U N U N M U N U M 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

(33) <50

<10 -

<50 <50 <50 <50 <50 <50 <10 <50

<10 -

<50 <50 <50 <50 <50 <50 <10 <50

<50 <50 <50 <50 <50 <50 <10 <50

(33) <50

(33) <50

<50 <50 <50 (33) <10

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 61 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant Bromochloromethane Bromochloromethane Bromochloromethane Bromodichloromethane Bromodichloromethane Bromodichloromethane Bromoform Bromoform Bromoform Bromomethane Bromomethane Carbon tetrachloride Carbon tetrachloride Carbon tetrachloride Chlorobenzene Chlorobenzene Chlorobenzene Chlorodibromomethane Chlorodibromomethane Chlorodibromomethane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U M N M U N U N U M N M U N M U 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

(33) <50

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

(33) <50

(33) <50

<50 (33) <50

(33) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 62 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant Chloroethane Chloroethane Chloroethane Chloroform Chloroform Chloroform Chloromethane Chloromethane cis-1,2-Dichloroethylene cis-1,2-Dichloroethylene cis-1,2-Dichloroethylene cis-1,3-Dichloropropene cis-1,3-Dichloropropene cis-1,3-Dichloropropene Dibromomethane Dibromomethane Dibromomethane dichlorodifluoromethane dichlorodifluoromethane dichlorodifluoromethane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U M N U N M U N U M N U M N U M 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

(33) <50

<50 <50 <50 <50 <50 <50 <50

<50 <50 <50 <50 <50 <50 <50

<50 <50 <50 <50 <50 <50 <50

(33) <50

<50 (33) <50

(33) <50

(33) <50

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 63 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant Dichloromethane Dichloromethane EthylBenzene EthylBenzene EthylBenzene Isopropyl benzene Isopropyl benzene Isopropyl benzene Meta/Para-Xylene Meta/Para-Xylene Meta/Para-Xylene n-Propylbenzene n-Propylbenzene n-Propylbenzene Ortho-Xylene Ortho-Xylene Ortho-Xylene p-Isopropyltoluene p-Isopropyltoluene p-Isopropyltoluene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg U N M U N U M N M U N M U N U M N U M 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

(3) <500

(3) <500

(3) <500 (3) <500

(33) <10

<10 <10 <10 -

<10 <50 <10 <50 <10 <50

<10 <10 <10 -

<10 <50 <10 <50 <10 <50

<10 <50 <10 <50 <10 <50

(33) <50

(33) <10

(33) <50

(33) <10

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 64 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant sec-Butylbenzene sec-Butylbenzene sec-Butylbenzene Styrene Styrene tert-Butylbenzene tert-Butylbenzene tert-Butylbenzene Tetrachloroethylene Tetrachloroethylene Tetrachloroethylene Toluene Toluene Toluene trans-1,2-Dichloroethylene trans-1,2-Dichloroethylene trans-1,2-Dichloroethylene trans-1,3-Dichloropropene trans-1,3-Dichloropropene trans-1,3-Dichloropropene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U N M U N U M N M U
(3,33) <30

96545 016 WS213 0.3 A105 Clay 0.3

96545 018 CP202 0.8 A105 Clay 0.8

(33) <50

(3) <30

<50 <50 <50 <50 -

<50 <50 <50 <50 -

<50 <50 <50 <50 (3) <30

(33) <50

(33) <50

(33) <50

(3) <30 (3) <30 (3) <30

(33) <50

<50 <50

<50 <50

<50 <50

N M U N U M

(33) <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 65 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference 96545 96545 96545 96545 010 011 014 015 Customer Sample Reference WS212 WS211 TP214 CP201 0.3 0.4 1.6 0.3 Test Sample A105 A105 A105 A105 Type Fill Clay Clay Clay Date Sampled Depth 0.3 0.4 1.6 0.3 Determinant Trichloroethylene Trichloroethylene Trichloroethylene Trichlorofluoromethane Trichlorofluoromethane Trichlorofluoromethane Vinyl chloride monomer Vinyl chloride monomer Vinyl chloride monomer Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg M U N U M N U M 96545 016 WS213 0.3 A105 Clay 0.3 96545 018 CP202 0.8 A105 Clay 0.8

(33) <50

<50 <50 <50

<50 <50 <50

<50 <50 <50

(33) <50

(33) <50

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant 1,1,1,2-Tetrachloroethane Technique GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 66 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant 1,1,1,2-Tetrachloroethane 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,1-Trichloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethane 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloroethylene 1,1-Dichloroethylene 1,1-Dichloropropene 1,1-Dichloropropene 1,1-Dichloropropene 1,2,3-Trichloropropane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg M N U M N U N M U N M U N U M N U M N 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

Page 67 of 76

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2,4-Trimethylbenzene 1,2,4-Trimethylbenzene 1,2-dibromoethane 1,2-dibromoethane 1,2-dibromoethane 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloroethane 1,2-Dichloroethane 1,2-Dichloropropane 1,2-Dichloropropane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3,5-Trimethylbenzene 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg N M U N U M N U M N U M N M U N U M N 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,3-Dichloropropane 1,3-Dichloropropane 1,4-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 2,2-Dichloropropane 2,2-Dichloropropane 2-Chlorotoluene 2-Chlorotoluene 4-Chlorotoluene 4-Chlorotoluene Benzene Benzene Benzene Bromobenzene Bromobenzene Bromobenzene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg U 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg M N U M N M U N U N U N U N M U N U M 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

<50 <50 <50 <50 <50 <50 <10 <50

<10 -

<50 <50 <50 <50 <50 <50 <10 <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Bromochloromethane Bromochloromethane Bromochloromethane Bromodichloromethane Bromodichloromethane Bromodichloromethane Bromoform Bromoform Bromoform Bromomethane Bromomethane Carbon tetrachloride Carbon tetrachloride Carbon tetrachloride Chlorobenzene Chlorobenzene Chlorobenzene Chlorodibromomethane Chlorodibromomethane Chlorodibromomethane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U M N M U N U N U M N M U N M U 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

<50 <50 <50 <50 <50 <50 <50 -

<50 <50 <50 <50 <50 <50 <50 -

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Chloroethane Chloroethane Chloroethane Chloroform Chloroform Chloroform Chloromethane Chloromethane cis-1,2-Dichloroethylene cis-1,2-Dichloroethylene cis-1,2-Dichloroethylene cis-1,3-Dichloropropene cis-1,3-Dichloropropene cis-1,3-Dichloropropene Dibromomethane Dibromomethane Dibromomethane dichlorodifluoromethane dichlorodifluoromethane dichlorodifluoromethane Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U M N U N M U N U M N U M N U M 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

<50 <50 <50 <50 <50 <50 <50

<50 <50 <50 <50 <50 <50 <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Dichloromethane Dichloromethane EthylBenzene EthylBenzene EthylBenzene Isopropyl benzene Isopropyl benzene Isopropyl benzene Meta/Para-Xylene Meta/Para-Xylene Meta/Para-Xylene n-Propylbenzene n-Propylbenzene n-Propylbenzene Ortho-Xylene Ortho-Xylene Ortho-Xylene p-Isopropyltoluene p-Isopropyltoluene p-Isopropyltoluene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg U N M U N U M N M U N M U N U M N U M 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

(3) <500

<10 <10 <10 -

(3) <500

<10 <50 <10 <50 <10 <50

<10 <50 <10 <50 <10 <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant sec-Butylbenzene sec-Butylbenzene sec-Butylbenzene Styrene Styrene tert-Butylbenzene tert-Butylbenzene tert-Butylbenzene Tetrachloroethylene Tetrachloroethylene Tetrachloroethylene Toluene Toluene Toluene trans-1,2-Dichloroethylene trans-1,2-Dichloroethylene trans-1,2-Dichloroethylene trans-1,3-Dichloropropene trans-1,3-Dichloropropene trans-1,3-Dichloropropene Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 10 g/kg 10 g/kg 10 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg U M N U N M U N U M N M U N M U N U M 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

<50 <50 <50 <50 (3) <30

(3) <30

<50 <50 <50 <50 (3) <30

<50 <50

<50 <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil Volatile Organic Compounds (USEPA 624) (MCERTS) SAL Reference Customer Sample Reference Test Sample Type Date Sampled Depth Determinant Trichloroethylene Trichloroethylene Trichloroethylene Trichlorofluoromethane Trichlorofluoromethane Trichlorofluoromethane Vinyl chloride monomer Vinyl chloride monomer Vinyl chloride monomer Technique GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) GC/MS(Head Space)(MCERTS) LOD Units Symbol 50 g/kg N 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg 50 g/kg M U N U M N U M 96545 019 WS202 0.9 A105 Clay 0.9 96545 020 WS208 0.9 A105 Clay 0.9 96545 021 WS209 0.4 A105 Clay 0.4

<50 <50 <50

<50 <50 <50

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil MCERTS Preparation SAL Reference 96545 001 Customer Sample Reference WS203 0.4 Test Sample AR Type Clay Date Sampled Depth 0.4 Determinant Moisture @ 105 C Moisture Technique Grav (1 Dec) (105 C) Grav (1 Dec) (40 C) LOD Units Symbol 0.1 % N 0.1 % N 96545 002 TP217 0.2 AR Fill 0.2 96545 003 TP216 0.1 AR Clay 0.1 96545 006 WS206 0.2 AR Fill 0.2 96545 007 WS205 0.5 AR Fill 0.5 96545 008 TP213 1.9 AR Other 1.9

5.5 5.6

18 18

37 23

8.2 8.9

15 15

18 18

SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil MCERTS Preparation SAL Reference 96545 009 Customer Sample Reference TP213 2.4 Test Sample AR Type Clay Date Sampled Depth 2.4 Determinant Moisture @ 105 C Moisture Technique Grav (1 Dec) (105 C) Grav (1 Dec) (40 C) LOD Units Symbol 0.1 % N 0.1 % N 96545 010 WS212 0.3 AR Fill 0.3 96545 011 WS211 0.4 AR Clay 0.4 96545 012 WS210 0.4 AR Sand 0.4 96545 014 TP214 1.6 AR Clay 1.6 96545 015 CP201 0.3 AR Clay 0.3

18 18

18 14

18 19

12 13

17 18

22 18

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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SAL Reference: 96545 Project Site: Former power station, Thornton Customer Reference: 42614 Soil Analysed as Soil MCERTS Preparation SAL Reference 96545 016 Customer Sample Reference WS213 0.3 Test Sample AR Type Clay Date Sampled Depth 0.3 Determinant Moisture @ 105 C Moisture Technique Grav (1 Dec) (105 C) Grav (1 Dec) (40 C) LOD Units Symbol 0.1 % N 0.1 % N 96545 017 TP212 0.4 AR Fill 0.4 96545 018 CP202 0.8 AR Clay 0.8 96545 019 WS202 0.9 AR Clay 0.9 96545 020 WS208 0.9 AR Clay 0.9 96545 021 WS209 0.4 AR Clay 0.4

6.2 7.4

20 18

24 21

16 21

20 19

9.1 11

Produced by: Scientific Analysis Laboratories Ltd, Medlock House, New Elm Road, Manchester. M3 4JH

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Trial Pit Investigation Former Power Station, Thornton Cleveleys

August 2010 43391p1r0

CD CONTAINING; COMPLETE PDF COPY OF REC REPORTS 43391p1r0, REC 2007 REPORTS 42614P2R0 (DESK STUDY) AND 42614P2R0 (GEO-ENVIRONMENTAL INVESTIGATION)

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