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Sorry for me English, but I think that you could understood me. Necessary concomitant chem.

substances: - DMSO (dimethyl sulfoxide) - a chemical substance with the formula - (CH3) 2SO. Colorless liquid, an important dipolar aprotic solvent) - Sodium hydride in mineral oil. - Amyl bromide (Synonyms: 1-Brompentan, n-amyl bromide, 1-Bromopentane for synth esis; n-Amyl bromide Formula: C5H11Br; CAS: 110-53-2). - Ether. - Isopropyl alcohol. You will also need: - Flat-bottomed flask (4-6 liters). - Reflux (used to condense the steam and condensate return to the reaction mass. Place such refrigerators usually vertical). - Measuring cup heat resistant. Synthesis recipe of JWH 018 is not complicated, follow the instructions and prop ortions (for 1g nafindola, 0.2 sodium hydride, 0.76 amyl) end up with a quality product. In this manual, we describe how to get JWH-018 in the form of oil, its difference from the powder only in the fact that the powder is easier to transpo rt and store, and the rest "performance characteristics" are identical. (From '10 nafindola get 10-15 grams of oil, and 10 g of oil is obtained 50 g smo king mixture) So, in a dry flask 6l, equipped with a reflux condenser was placed 20 g of sodiu m hydride, pour 100 ml of dry DMSO, mixed, added in small portions (5-10g, and t he mixture is heated, you need good cooling) 100g 1 nafindola periodically stirr ed at room temperature 30 minutes. Then add 77g of n-pentilbromida (amyl bromide ). The reaction mixture was kept at 65 g. 3h Celsius on a hot plate with occasio nal stirring. PRODUCT fall as OILS The reaction mixture was washed three times w ith water in a 5-fold volume. Attention! Sodium hydride ignites on contact with water! Be careful when working with it! Solvents: The product is highly soluble at 35 g. Celsius in diethyl ether and isopropyl al cohol, worse in ethanol. Better to work with ether, maybe he flies at room temperature and the base dries faster! The water insoluble product! Applied at a concentration of 0.5 to 2g per 10 g basis, depending on the desired effect. ** How to wash? To wash pour into a beaker (1 liter) of oil and pour 200ml of water, mix well an d allow the oil to settle, then drain the water. Repeat 5 times until the water runs clear. ** For those who do not want to bother with washing questions The reaction mixture was poured into water five times its volume and mixed, then poured 200 ml of ether, stirred and allowed to stand. The reaction mixture was

separated into ies). Gathered of the oil was to stand, then oduct is ready

two layers (- oil in the air, the bottom - the water with impurit top layer. If necessary (if the previous operation to select all not possible), a further 200 ml of ether was stirred and allowed collected and combined with the previously collected. All, the pr for further action!

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