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WSP CEL Limited CEL House, Westwood Way Westwood Business Park Coventry UK CV4 8HS Tel +44

(0)24 7686 2000 Fax +44 (0)24 7686 2200

HAZOP REPORT FOR CALABAR PORTSIDE INDUSTRIAL PARK FUEL RETICULATION PROJECT

For AIKENBECK RESOURCES LIMITED - NIGERIA

Issue No. Compiled By

1 Peter Dixon

Approved By Date
27/03/2012

Ref: E5178 HAZOP Report Issue: P1 Date: 27th March 2012

Registered office: WSP House, 70 Chancery Lane, London WC2A IAF | Registered in England No. 3877626 | VAT Reg. No. GB 747 8097 84

ver1 2010

CONTENTS

Page No

REVISION RECORD SECTION 1 SECTION 2 SECTION 3 SECTION 4 SECTION 5 SECTION 6 INTRODUCTION STUDY DATES STUDY TEAM DOCUMENTATION METHODOLOGY SUMMARY OF HAZOP & KEY ISSUES ARISING

1 2 2 2 3 3 4

ANNEX 1 ANNEX 2 ANNEX 3 ANNEX 4 ANNEX 5

HAZOP AGENDA HAZOP TEAM MEMBERS LIST HAZOP COPY OF P&ID HAZOP GUIDE WORD KEY SHEET HAZOP RECORD

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REVISION RECORD

Issue No. P1

Description of Revision

Page/Paragraph No.

Preliminary first issue for comment

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SECTION 1

INTRODUCTION The Cross River Sate Government (CRSG) is embarking on a Portside Development in the Calabar area of Nigeria for petroleum product receiving and storage. This report details the outcome of a HAZOP Study covering the proposed installation. Two dolphin berths are to be provided near the bank of the Calabar River to handle tankers of 25,000 DWT (Dead Weight Tonnage). Fuel is to be unloaded (or loaded) by hose connection to pipework which connects the dolphin platforms to a manifold system located in a common systems bunded area. The manifold system will initially allow for three different fuel types to be handled and distributed to seven separate tenant sites for storage. Mixed fuel from manifold flushing will be stored in an Intermix Tank within the common systems area. Intermix will then be either dosed back into bulk fuel during transfer or taken off site by road tanker. The three different fuel types are to be handled initially are gasoline, kerosene and fuel oil. The HAZOP study focussed on the unloading of unleaded gasoline due to its very low flash point (-46C) and high vapour pressure (boiling range 32 to 225C), compared to the other two products.

SECTION 2

STUDY DATES The HAZOP study took place over two days on 19th and 20th March 2012 at the La Cour Hotel, Ikoyi, Lagos. The agenda is included as Annex 1.

SECTION 3

STUDY TEAM The team members were: Niyi Oginni Unimawho Awafung Chief Op. Officer Aikenbeck Resources Ltd Proj. Devt Manager Aikenbeck Resources Ltd GWC GWC

Dr. Okey Onyemelukwe Principal Partner Chris Amgeehi Project Manager Ebola Lawal Dr. Ambekeh A Udida Margaret Eslen Manderson Okpo Utan Uye Utan Ukemeabasi Udo

Civil/Structural Eng. IAA Associates Director Director Director Terminal Manager Comml Manager Cross River State M of L&H Cross River State M of L&H Cross River State M of L&H ECM Terminal ECM Terminal
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John Wilmot Fransisco Doregos Richard Baard Jock Litterick Mark Pitout Clint Lakey Peter Dixon

Cost Consultant Design Manager Director Principal Associate Associate Mechanical Eng. Proc Eng / Leader

WSP Nigeria WSP Nigeria WSP Industrial WSP Consulting WSP Industrial WSP Industrial WSP CEL

A Team Members list completed at the meeting is included as Annex 2. Representatives from CAA Associates and the Ministry of Lands and Housing were present for the first day only, during which Section 1 was studied.

SECTION 4

DOCUMENTATION Copies of all design reports and drawings were available to the meeting. Principal documents referred to during the meeting were: W702 M-830 Rev. 6 W702 M-801 Rev. P2 W702 M-802 Rev. P1 W702 M-802 ?? W702 M-804 Rev. P2 W702 M-805 Rev. P2 W702 F-881 Rev. P1 510168 C1004 Rev. 1 GA Fuel Reticulation System Haz. Areas GA Fuel System, Dock Hazardous Areas Site Layout Foam System Site Plan P&ID Oil Pipeline Reticulation System 3D Model Fuel Reticulation System GA Fuel Reticulation System c/w Dock

SECTION 5

METHODOLOGY The conventional HAZOP technique was used for the study, that is: Define the intention for each line or sub-system. Identify relevant deviations (See Guide Word Sheet Checklist Annex 4). Look for causes of each deviation, assess the consequences and decide whether action(s) is required.
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The HAZOP record follows in Annex 5. The record sheets primarily capture those deviations where action(s) was identified; they are not an exhaustive record of all discussion.

SECTION 6

SUMMARY OF HAZOP & KEY ISSUES ARISING Due to the large number of attendees and extended discussion of many aspects of the project, the HAZOP could not be completed rigorously for all secondary operations. However, the primary operations of fuel transfer in either direction between ship and shore were considered in detail and significant discussion of the secondary operations occurred in parallel. These were then reviewed at the end of the meeting and the actions identified added to the HAZOP record. A follow-up review of the completed design should therefore be considered. In addition to recommended actions, the HAZOP record highlights the key safeguards intended to mitigate or prevent the consequences of potential process deviations. It should be ensured that these or equivalent safeguards are included within the completed design documentation, particularly a Trip and Interlock Schedule and control system User Requirement Specification. Key issues identified by the HAZOP were as follows: Gasoline has a boiling point range starting at 32C. Since ambient temperature in the Calabar region will often exceed this, it will be difficult to maintain a prime on the unloading pumps due to vapour formation. Alternatives such as running the ships pumps to provide backing pressure will need to be considered. The ability of the control system to reliably prevent overfilling of tanks should be carefully considered. All tanks should ideally have duplicate and dissimilar high level detection instruments and more than one trip action is likely to be required to achieve an appropriate safety integrity level (SIL). Consideration should also be given to supplementing the PLC by hard wiring or by an independent programmable safety system for these critical trip actions. A clear interface protocol should be defined between the common systems control PLC and the tenant control systems to ensure that fuel transfer can only commence when a permissive signal has been received by the upstream system, and that the downstream receiving system has the priority to immediately stop a transfer.

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The reliability of Emergency Stops should be considered in comparison to Process Stops acting through the process control PLC. Strict procedures will be required to control the back-loading of fuel to a ship if there is to be no direct link between ship and shore control systems. Consideration should be given to the inclusion of actuated, fire safe, isolation valves on bottom outlets from large fuel storage tanks. Provision will be required to separate spilt fuel from rain water, both on the dolphin jetty and in the common systems bund. To this end, separate covered and contained collection of fuel from drainage or pressure relief will be required so that separation is only required from surface run-off. The extent of hazardous zone surrounding open sumps which may contain fuel should be reconsidered. This will be aided by the segregation of potentially very warm fuel from pressure relief and drainage.

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ANNEX 1

HAZOP AGENDA

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AGENDA

Date:

19th & 20th March 2012

Time:

09.00

Venue:

La Cour Hotel, 3, Cooper Road, Lagos

Personnel Present:

See separate Attendance Schedule

Introduction:

This is a 2 day Hazard Study meeting to identify any residual safety and operability issues within the process design for the Portside Industrial Park, Calabar.

Item 1. 2. 3. 4.

Description Attendee Introductions Introduction to HAZOP Procedure Introduction and Overview of Project HAZOP

Responsibility All PJD WSP Nigeria PJD

Time 09.00

Unloading line flush to Intermediate Tank Fuel unloading to tenant site Drains, platform sump and sump transfer Drains, bund area sump and sump transfer Tanker loading Intermix tank transfers / dosing Flow proving

5. 6.

Conclusions and next steps Project Meeting

All All

M:\PROJECTS\WSP\E5178\1 SAFETY\3 HAZARD STUDY\CALABAR - PORTSIDE - HAZOP MEETING AGENDA.DOC

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ANNEX 2

HAZOP TEAM MEMBERS LIST

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ANNEX 3

HAZOP COPY OF P&ID

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ANNEX 4

HAZOP GUIDE WORD KEY SHEET

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ANNEX 5

HAZOP RECORD

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Fuel Reticulation System - PID

Section Section 1

First Action Number Section Title 1 Unloading Line Flush

Section 2 Section 3 Section 4

39 66 74

Unloading Fuel to Tenant Site Loading Fuel to Ship from Tenant Site Fuel Dosing and Intermix Loading

Description To flush each unloading pump in turn for 1 minute each to the Inter-mix Tank. Expected total flush quantity is 12 tonnes. Adequate flushing confirmed by manual sampling. To unload fuel from a ship to a tenant site storage tank at a rate of 700 tonnes per hour. To load fuel from a tenant site to a ship using tenant's pumps and flow meters at a maximum flow rate of 700 tonnes / hour Dosing of fuel at low rate from the Intermix Tank into the unloading line during transfer to tenant storage, ensuring that overall fuel transfer remains within fuel specification. Also loading of an excess of Intermix to a road tanker. Proprietary flow proving unit used to verify the calibration of each product flow meter. Drains and pressure relief to the dolphin jetty sump. Transfer to the common services bund sump. Drains and pressure relief to the common services sump. Transfer to the Intermix Tank.

Section 5 Section 6&7

78 83

Flow Proving Unit Drains, Sumps and Transfer

Calabar HAZOP Record - Edited

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Line Flush

Section name: Section 1 Leader / Scribe: PD/PD Date: 19/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES Manual valve closed

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Include low current monitoring of pumps to detect no flow Consider position switches on key manual valves and include feedback information into control logic Detailed maintenance procedures required to ensure correct realignment of manual valves following maintenance operations Sequence must shut down in the event of a discrepancy See action 1 Consider whether any manual valves should be locked open

ACTION BY

ANSWERS AND COMMENTS

Flow

No Flow

Unloading pump runs dead headed

WSP

Manual valve closed

Unloading pump runs dead headed

WSP

Manual valve closed

Unloading pump runs dead headed

ARL

Automatic valve closed No prime on unloading pumps Flow Less Flow Manual valve not fully open

Unloading pump runs dead headed Pump cavitation

Incomplete line flush Unloading header and ship contaminated by mixed fuel from Intermix Tank Ship's pump running against substantially closed head Extemely flammable liquid discharged into open sump

Flow

Route open Reverse Flow but pump not running Air and fuel bleed to platform sump Air and fuel bleed to platform sump

Limit switches to be provided on both open and closed positions Low pressure on pump suction. Low current to pump Manual valves to have facility to be locked open or closed 3 NRVs in line to intermix tank. Discrepancy detected in control system will close actuated valves

WSP

WSP

No further action

Flow

Where Else

Confirm suitability of ship's pump to run in this way Clear operator procedure required to limit flammable release to a minimum

WSP

Zone 1 hazardous area covers ship and entire dolphin platform

ARL

Calabar HAZOP Record - Edited

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Line Flush

Section name: Section 1 Leader / Scribe: PD/PD Date: 19/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Unloading operation to be continuously manned. Procedures required to achieve prompt shutdown from both terminal and from ship. Confirm that unloading hose system is fully specified within the piping spec. No further action Consider extending dolphin platform bund to capture leakage from intermediate hose connections Investigate standard practices for confirming absence of leaks before unloading commences No further action

ACTION BY

ANSWERS AND COMMENTS

10

Flow

Where Else

Unloading hose failure

Significant environmental damage to river

ARL

11

Unloading hose failure

Significant environmental damage to river Procedures to determine number of hose sections required for type and size of ship

WSP

12

Tidal movement

Hose overextended

13

Intermediate hose joint leakage Intermediate hose joint leakage

Fuel spill outside of planned contained area

10

WSP

14

Fuel spill outside of planned contained area

11

ARL

15

Flow

Where Else

16

Flow

Where Else

17

Flow

Where Else

18

Drain valve High level switch on sump left open or and automatic pump out Loss of fuel to sump relief valve to Intermix Tank leakage Flow into Two actuated isolation header to valves and ability to tenant site monitor flow in header Leakage into Fire fuelled by entire Intermix Tank contents of Intermix Tank bund and (due to bottom entry) possible fire Flow into 2nd Only one inlet valve to the Cross contamination of unloading Intermix Tank should be headers and possible spill manifold open at any one time

No further action Actuated isolation valve to be close to tank, to close in event of fire and be firesafe design Add a NRV in each inlet line to Intermix Tank

12

WSP

13

WSP

Calabar HAZOP Record - Edited

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Line Flush

Section name: Section 1 Leader / Scribe: PD/PD Date: 19/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES Ship's pumps also running during unloading

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Procedures required to ensure ship's pumps not run at same time as unloading pump Consider whether dual flame arresters with changeover valve required

ACTION BY

ANSWERS AND COMMENTS

19

Pressure

More Pressure

Unloading is too fast or line velocity too high

14

ARL

20

Pressure

More Pressure

Blocked flame Overpressure and rupture arrester on of tank Intermix Tank Unloading hose air leak Unloading pumps cavitate causes loss of suction High vapour pressure of gasolene in warm ambient Unloading pumps cavitate temperature causes loss of suction Procedures to maintain hoses. Spare hoses.

15

WSP

21

Pressure

Less Pressure

No further action

22

Pressure

Less Pressure

16

Confirm expected temperature of fuel in ship and vapour fraction at unloading pumps. Consider whether ship's pumps can be used to provide backing pressure Review all possible causes of loss of prime of unloading pumps. Check pump minimum NPSH No further action Provide secondary high level monitoring to provide adequate safeguard against tank overfill. Consider SIL assessment

WSP

23

Pressure

Less Pressure

Power fluctuation High ambient temperature or solar gain

Unloading pumps lose prime

17

WSP

24

Temperature

More Temperature

Pipe expansion

Pipework stress design and expansion loops

25

Level

Failure of Intermix tank Overfilling and overflow of Greater Level level intermix tank transmitter

18

WSP

Calabar HAZOP Record - Edited

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Line Flush

Section name: Section 1 Leader / Scribe: PD/PD Date: 19/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED System required to separate rain water from fuel drainage or spillage. Fuel sumps to be protected from rain water Clear procedures / check lists required to ensure that transfer not started without line flush and sample check Consider providing on site lab / office facility to ensure rapid turnround of sample test results Speed of system shutdown to be determined during commissioning Consider feasibility of unloading fuel using ship's pumps. Would require unloading pump bypass. No further action Confirm whether a Zone 2 area is required surrounding the Zone 1 sump in the corner of the bund. Investigate back-up water supply to supplement municipal supply

ACTION BY

ANSWERS AND COMMENTS

26

Composition

Accumulation Extra of rainwater in Component sumps Line flush omitted before transfer to tenant Sample testing takes too long

Cannot pump out to Intermix Tank

19

WSP

27

Sequence

Step Omitted

Out of spec transfer

20

ARL

28

Sequence

Step Longer

Cannot achieve target unloading time of 24 hrs

21

ARL

29

Other

Shut down

Rapid closure of valves or Pressure surge damages stopping of pipework or pipe supports pumps

22

ARL

30

Other

Power/Servic e Failure

Local power failure

Unable to unload ship

23

WSP

31

Other

Maintenance/ Lack of pump Spares spares Extent of flammable zone

Delayed unloading

Pump spares requirements listed in pump specification

32

Other

Fire

Ignition of vapours from common area sump

24

WSP

33

Ignition of fuel spill

Fire damage to facility

Fire water storage to supply up to 3 foam monitors for 1 hour

25

WSP

Calabar HAZOP Record - Edited

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Line Flush

Section name: Section 1 Leader / Scribe: PD/PD Date: 19/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES Static generation during fuel transfer

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED

ACTION BY

ANSWERS AND COMMENTS

34

Other

Static/Earthin g

Potential vapour explosion

Earth bonding and lightning protection specified

No further action Consider additional measures to prevent or separate fuel spills before they enter the storm water drain / river Consider options to contain, mitigate or recover spill from river Stroke times and trip delays to be set during commissioning Alarms and trips required from all process parameters to be set during commissioning Check applicable advice from "National Oil Spill Protection and Mitigation Agency" Consider provision for tanker bunkering. Consider provision of domestic fresh water supply to tanker Confirm civils provision to protect pipeline Ensure that valve VBA 184 is suitable for future addition of an actuator

35

Other

Fuel spills on roads and Environment common areas Uncontained fuel spill

Fuel run-off into stormwater channel

26

WSP

36

Spill finds its way to the river Valve failure trip occurs before valve has reached end of stroke Process deviations go undetected

27

ARL

37

Other

Commisionin Stroke times g of valves Alarm and trip settings

28

ARL

38

29

ARL

39

Other

Regs

30

WSP

40 41

What Else What Else

Bunkering Domestic fresh water Damage to existing NNPC oil pipeline Interaction with future 2nd tanker berth Storm water hits low level pipe Need to flush unloading line from 2nd berth

31 32

ARL ARL

42

What Else

Pipe fracture and oil spill

33

WSP

43

What Else

Cross contamination between systems

NRVs shown in each unloading line

34

WSP

Calabar HAZOP Record - Edited

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Line Flush

Section name: Section 1 Leader / Scribe: PD/PD Date: 19/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED

ACTION BY

ANSWERS AND COMMENTS

44

What Else

45

What Else

46

What Else

Cannot flush branches for P&ID doesn't future work as products 4, 5 shown and 6 Cannot simultaneousl P&ID doesn't y unload work as products 4 to shown 7 from each berth Cannot simultaneousl P&ID doesn't y unload work as products 4 to shown 7 from each berth

Contamination

35

Unloading header must pass each product take-off branch in turn Unloading header from future 2nd berth must pass each product take-off branch in turn with separate connections to each For two unloading systems, VBA 185 and 186 need to be actuated and located downstream of the last product take-off Procedures required to prove a working radio channel (at agreed frequency) between ship and shore (common systems and tenant) before operations commence. Communication to be confirmed on regular (e.g. hourly) basis.

WSP

Loss of flexibiltiy

36

WSP

Loss of flexibiltiy

37

WSP

47

What Else

Loss of radio communicatio n between ship and shore

Radio fault

Inadequate monitoring of unloading operations

38

WSP

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Fuel to Tenant Site

Section name: Section 2 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER 1 2 3 4 Flow Flow Flow Flow

DEVIATION No Flow No Flow Less Flow Less Flow

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED See actions 1 to 4 Sequence to abort if flow rate not achieved or high pressure detected See action 5 No further action Consider control of transfer rate using flow meter and pump VSD. Ensure that max line velocity to prevent static generation is not exceeded Check regulations regarding whether top or bottom entry to tenant tank is preferred A transfer permissive signal is required from the tenant for each of 3 products. Transfer can only proceed on receipt of this signal. Permissive signal to be via fibre optic cable (preferred for reliability) or ethernet radio See actions 8 to 11

ACTION BY WSP WSP WSP

ANSWERS AND COMMENTS

Valve closed on tenant site Furthest tenant site at highest elevation Pumps sized for furthest tenant site at highest elevation

Pump dead headed

Flow meter will detect lack of flow. High pressure detection. Pumps specified to achieve 700 tonnes/hr to highest destination

39

Protracted unloading

Flow

More Flow

Excessive flow rate to nearest sites at lower elevation.

40

WSP

Flow

Tenant tanks at higher Potential for reverse flow elevation than when transfer route Reverse Flow ship, possibly opened with bottom entry Tenant site not ready for transfer

3 NRVs in line to tenant site. Discrepancy detected in control system will close actuated valves

41

WSP

Flow

Sooner Flow

Potential spill or flow to wrong destination

42

WSP

43

WSP

Flow

Where Else

WSP/ARL

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Fuel to Tenant Site

Section name: Section 2 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES Another routing valve is open or passing

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Interlocks required to allow only one routing valve to be open at any time Transfer to be stopped if fuel flow detected on another product flow meter Consider additional physical safeguard or cover by procedures if transfer discrepancy detected Procedures required to prove a working radio channel (at agreed frequency) between ship, tenant site and common systems control room before operations commence. Communication to be confirmed on regular (e.g. hourly) basis. Provide increased separation between pipe rack and roadway Install physical barriers to protect pipework from road vehicles No further action See actions 16 and 17

ACTION BY

ANSWERS AND COMMENTS

10

Flow

Where Else

Flow of fuel to incorrect destination

44

WSP

11 Loss of fuel to Intermix Inlet valve to Tank during transfer. Intermix Tank Discrepancy between fuel is passing unloaded and fuel received

45

WSP

12

46

WSP

13

Loss of radio Confusion between tenant Transfer permissive signal communicatio site and common system has ultimate control of n operators transfer

47

ARL

14

Flow

Where Else

Pipe damage due to Fuel spill due to pipe proximity of fracture caused by vehicle impact pipe rack to roadway

48

WSP

15 More Pressure Less Pressure Closed valve or ship's pump running Transfer line pressure higher than normal Transfer will be stopped if high discharge pressure detected

49

WSP

16 17

Pressure Pressure

WSP/ARL

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Fuel to Tenant Site

Section name: Section 2 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES High ambient temperature or solar gain

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Pipework stress design and expansion loops to be included in tranfer pipe design Tenant should be required to issue a "Notice of Readiness" to confirm that they have sufficient ullage capacity in their receiving tank. Failure to comply should incur penalties. Tenant design guidelines to require multiple level monitoring and sufficient control system integrity to ensure that transfer permissive signal is withdrawn when high level is reached Consider requirement for secondary safety system (independent of process PLC) to ensure that transfer is stopped if permissive signal is withdrawn No further action Procedure required to sample from the ship before unloading and from the unloading line after line flush

ACTION BY

ANSWERS AND COMMENTS

18

Temperature

More Temperature

50

WSP

19

Level

Greater Level

Insufficient ullage in receiving tank

Transfer has to be aborted before completion, resulting in delays to unloading

51

ARL

20

Receiving tank reaches high level

Tank overflow

52

WSP

21

53

WSP

22

Level

Less Level

Ship empty

Loss of pressure on the Unloading pumps cavitate pump discharge will stop transfer pumps

23

Composition

Different Stream

54

ARL

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Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Fuel to Tenant Site

Section name: Section 2 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Include procedure to flush unloading line, even if there is no change of grade. No further action

ACTION BY

ANSWERS AND COMMENTS

24 Loss of power to control PLC control system failure UPS for control system room. SCADA system failure. Fail Safe emergency stop Unloading continues, but provided in control room operator loses sight of to stop transfer what is happening Voltage spikes in incoming power supply Unloading hose uncoupled before draining complete Pumping continues after fire detected

55

ARL

25

Other

Power/Servic e Failure

26

56

Consider providing backup SCADA system Consider provision of under and over voltage detection on incoming power supply to initiate switch to generator supply Consider key interlock system on double block and bleed to guard against maloperation Consider interlock to stop transfer operations if fire protection system is operated Confirm whether fire protection from hydrants is required over entire length of transfer pipelines Provide suitable level access for routine inspection of transfer pipelines

WSP

27

Damage to PLC or SCADA system

57

WSP

28

Other

Shut down

Fuel spill to dolphin platform or to river

Procedure to close block valve and drain hoses to dolphin platform sump before uncoupling hoses

58

WSP

29

Other

Fire

Continued fuel flow to fire

59

WSP

30

60

WSP

31

Other

Access

Tranfer pipeline traverses rough ground

Cannot inspect entire length of transfer lines

61

WSP

Calabar HAZOP Record - Edited

Page 11 of 17

Printed on: 27/03/2012

Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Unloading Fuel to Tenant Site

Section name: Section 2 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED

ACTION BY

ANSWERS AND COMMENTS

32

What Else

62

33

What Else

Low points in transfer lines

Transfer lines cannot be fully drained for maintenance

63

34 No high point Transfer lines cannot be fully drained or draining is vents on slow transfer lines Future expansion of facility to more than 7 tenant sites Each product header can be extended to create 2nd tier header above the initial 7 take-offs. Remote I/O cabinets are expandable

64

35

65

Review other Section 1 actions applicable fuel WSP/ARL transfer to tenant storage Ensure that transfer lines rise continuously to tenant WSP sites to permit gravity draining to common area sump Consider drainability of WSP expansion loops Consider requirement for venting of transfer lines WSP within the tenant site to permit draining

36

What Else

Layout issues

No further action

Calabar HAZOP Record - Edited

Page 12 of 17

Printed on: 27/03/2012

Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Loading Fuel to Ship from Tenant Site

Section name: Section 3 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Consider measures required to ensure that transfer rates do not exceed permitted maximum Consider including design criteria for back-loading within tenant design guidelines A transfer permissive signal is required to be sent to the tenant for each of 3 products. Transfer can only proceed on receipt of this signal. Permissive signal to be via fibre optic cable (preferred for reliability) or ethernet radio Common site operator must obtain confirmation from the ship that they are ready to receive transfer before issuing the permission signal Established and rigorous procedures are required to prevent overfill of ship's tanks Tenant should provide sample to confirm that fuel grade is suitable for the selected loading line

ACTION BY

ANSWERS AND COMMENTS

Flow

More Flow

Pumping down hill

Static electricity hazard (and high reaction forces on pipework)

66

WSP

Flow

Less Flow

Tenant pumps too small for duty

Ship delayed at berth, incurring cost

67

WSP

Flow

Sooner Flow

Common site not ready for transfer

Potential spill or flow to wrong destination

68

WSP

69

WSP

70

ARL

Level

Greater Level

Ship's tank overfilled

Fuel spill to river

Confirm that sufficient space is available in ship's tank and that spare tank(s) is available to provide excess capacity

71

ARL

Composition

Different Stream

Wrong fuel grade for selected line

Cross contamination

72

ARL

Calabar HAZOP Record - Edited

Page 13 of 17

Printed on: 27/03/2012

Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Loading Fuel to Ship from Tenant Site

Section name: Section 3 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED Confirm ability to close electrically actuated valves in the event of power failure.

ACTION BY

ANSWERS AND COMMENTS

Other

Power/Servic e Failure

Unable to close actuated valves and stop flow of fuel downhill to ship

Stand-by generators available

73

WSP

Calabar HAZOP Record - Edited

Page 14 of 17

Printed on: 27/03/2012

Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Fuel Dosing / Intermix Loading

Section name: Section 4 Leader / Scribe: PD/PD Date: 26/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED

ACTION BY

ANSWERS AND COMMENTS

These operations were discussed during the HAZOP study of Sections 1 to 3 and then reviewed at the end of the meeting. There was insufficient time available to complete a full HAZOP procedure. A further review should be considered at the end of detail design. Flow Where Else Spillage during road tanker loading Too much dosing Dosing of gasoline into kerosene Loss of fuel to river 74 A contained tanker loading bay is required, draining to suitable sump Procedures required to ensure that dosing does not exceed acceptable amount Procedures required to ensure that only appropriate dosing is done Procedures required to ensure that any Intermix sent off site is appropriately used or redistilled to original specifications HAC to be extended to include tanker loading bay. Remote I/O panels may need to be relocated WSP

Composition

Extra Component

Only about 12 tonnes of Fuel transferred goes out Intermix are expected per of specification flush Kerosene becomes hazardous in use. (Gasoline dosing not considered acceptable.)

75

ARL

76

ARL

Composition

Different Stream

Intermix sold as domestic fuel Road tanker loading not covered by current Hazardous Area Classification

Fire or explosion if used as a domestic fuel

77

ARL

Other

Fire

Fire during loading

Normal safeguards such as tanker earthing to be provided

78

WSP

Calabar HAZOP Record - Edited

Page 15 of 17

Printed on: 27/03/2012

Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Flow Proving Unit

Section name: Section 5 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED

ACTION BY

ANSWERS AND COMMENTS

This operation was briefly discussed during the HAZOP study of Sections 1 to 3 and then reviewed at the end of the meeting. There was insufficient time available to complete a full HAZOP procedure of the detailed operation of the proving unit. A further review should be considered at the end of detail design. Spill during Flow prover to be located Flow Where Else operation of Loss of fuel to river within the common flow prover systems bunded area Flow prover Unable to check shown on flowmeters or unload from Berth 1 Flow Later Flow future Berth 2 if Berth 1 unloading line not available only Different Stream Only one transfer tank shown with flow prover Need to drain flow prover to road tanker or sump / Intermix Tank before use on different product

No further action

79

Flow prover must usable with either unloading line Consider providing a transfer tank for each product to enable prover to be drained and refilled with compatible product Ensure sufficient access and mechanical handling aids to assist removal of ball Ensure operators are adequately trained for use of the flow prover

WSP

Composition

80

WSP

Other

Flow prover Maintenance/ ball needs to Mechanical handling injury Spares be removed Incorrect operation of flow prover Inexperience of operators Flow meter calibration errors

81

WSP

What Else

82

ARL

Calabar HAZOP Record - Edited

Page 16 of 17

Printed on: 27/03/2012

Company: Aikenbeck Resources Facility: Portside Industrial Park Dwg No: No. W702-M-830 Rev 6 Dwg Title: Reticulation System - PID

Drains, Sumps and Transfer

Section name: Section 6 / 7 Leader / Scribe: PD/PD Date: 20/03/2012 Team: See Report

HAZOP ITEM PARAMETER NUMBER

DEVIATION

POSSIBLE CAUSES

CONSEQUENCES

SAFEGUARDS

ACTION NUMBER

ACTION REQUIRED

ACTION BY

ANSWERS AND COMMENTS

These operations were briefly discussed during the HAZOP study of Sections 1 to 3 and then reviewed at the end of the meeting. There was insufficient time available to complete a full HAZOP procedure for the detailed operation of the sumps. A further review should be considered at the end of detail design. Discharge Flow No Flow pumps not Cannot empty sumps primed Accumulation Extra Cannot pump out to of rainwater in Composition Component Intermix Tank sumps Fuel spill elsewhere on Contaminatio Fuel washed to river with site, outside n rain water of proposed bunds Extent of flammable zone Ignition of vapours from common area sump

83

Ensure that sump transfer pumps are self priming See action 19 Design a containment system for all rainwater run-off from site roads to a single collection / holding point to allow separation or treatment before discharge to river See action 24

WSP

WSP

Composition

84

WSP

Other

Fire

WSP

Calabar HAZOP Record - Edited

Page 17 of 17

Printed on: 27/03/2012

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