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Reprint NOVEMBER
(Third
1998 )
iReafiimlad 1997)
Indian Standard
METHODS
FOR CHEMICAL
PART 1 DETERMINATION
OF CARBON
( FOR CARBON
BY VOLUMETRIC
METHOD
OF STEELS
Third ReviCon )
..
ANALYSIS
of
carbon in the
of Carbon
be tested
for satisfactory
working
against
standard
steel of
5.2 For Plain Carbon SteelTake one gram of an accurately weighed and clean sample free from
extraneous carbon in the form of small drillings or shavings in a porcelain boat which can withstand
a temperature of 1 150C without breaking or cracking.
5.2.1
1 100C.
Introduce
the
boat
into
the
hot combustion
tube
in the
furnace
kept
at 1000
ta
@ June
1988, BIS
I
I
BUREAU
MANAK
OF
BHAVAN.
INDIAN
STANDARDS
9 EAHADURSHAH ZAFAR
NEW DELHI 110002
MARG
Gr 2
on the same
fusion
quantity
of the sample,
of accelerators
if not thoroughly
fused,
used, without
any sample
potash with
one gram of
5.7 Calculation
Carbon,
percent
= (A -
8 ) x F
where
A = burette reading after absorption
sample,
B = burette
F = Correction
5.8
Reproducibility-
of carbon dioxide
&OOl
percent
in caustic
and
and pressure
( see Table I ).
and
APPENDIX
INDIAN
IS : 228
STANDARDS
Methods
ON METHODS
for chemical
FOR CHEMICAL
ANALYSIS
OF STEELS
analysis of steels:
(Part
Determination
of manganese
2 )-I987
arsenite method ( third revision )
( Part
3 )-I 987
by alkalimetric
( Part
4)-1987
Determination
of carbon
percent ) ( third revision )
( Part
5 )-I 987
Determination
of nickel by dimethylglyoxime
( for nickel Z 01 percent ) ( third revision)
( Part
6 )-I 987
Determination
of chromium
by persulphate
chromium > 01 percent ) (third revision )
( Part
7)-1974
Determination
of molybdenum
by a-benzoinoxime
molybdenum
> 1 percent ) ( second revision)
( Part
8)-1975
Determination
of silicon
by
> 01 percent) (second revision)
( Part
9)-1975
Determination
(second revision )
Determination
of phosphorus
of sulphur
by gravimetric
the
( Part lo)-1976
Determination
of molybdenum
(for molybdenum
up to 1 percent)
revision )
method
method
gravimetric
in plain carbon
(for
revision )
carbon
( gravimetric
oxidation
3 0.1,
) method
method
method
method
(for
steels by dvolution
( for
(for
silicon
method
by thiocyanate (photometric
) method
in low and high alloy steels (second
( Part 11 )-I976
Determination
of silicon by photometric
method in carbon steels and
low alloy steels ( for silicon 001 to 005 percent ) ( second revision )
( Part 12 )-1988
Determination
of manganese
by periodate
method in low and high alloy steels (for manganese
cent ) (second revision )
( Part 13)-l
982
Determination
(spectrophotometric
)
up to 001 to 200 per-
of arsenic
(Part 14 )-I987
Determination
of carbon by thermal
0005 to 2000 percent )
conductivity
method
(for carbon
TABLE
CORhECTlON
( Clause
FACTORS
5.7 )
Pressure,
738
740
742
744
(5)
(6)
(7)
(8)
(9)
0.970
0.965
0961
0,966
0962
0,972
0.968
0.963
0959
0.954
0.975
0.970
0966
0.961
0.957
0.978
0.973
0969
0.964
0.959
0.960
0.976
0.971
0967
0962
0.944
0.940
0.935
0930
0.925
0,947
0.942
0.937
0.933
0.928
0950
0945
0.940
0.936
0.930
0.952
0947
0.943
0.938
0.933
0.955
0.950
0.945
0.940
0.936
0.918
0913
0.908
0.903
0.897
0.920
0915
0.910
0905
0*900
0.923
0,918
0.913
0.908
0.903
0.925
0.928
0920
0.923
0.931
0.926
0.921
0.892
0.887
0.882
0.876
0.870
0.895
0.889
0.884
0.878
0.873
33:
0.865
0.859
0.853
0.847
0.841
Z?
42
43
44
45
730
732
734
(1)
(2)
(3)
(4)
15
16
17
18
19
0.964
0.960
0955
0951
0.946
0.967
0.962
0958
0.953
0949
20
21
22
23
24
0942
0.937
0.932
0.927
0.922
25
26
27
mm Hg
736
746
748
750
752
754
(13)
(14)
758
760
762
764
766
768
770
(15)
(16)
(17)
(18)
(19)
(20)
(21)
(22)
756
Temperature, C
-_.-_
29
30
31
:f
34
35
3376
(10)
(11)
(12)
0.983
0978
0.974
0969
0.965
0.986
0.981
0.977
0.972
0.967
0.988
0,984
0.979
0.975
0.970
0.991
0.987
0.982
0.977
0.973
0.994
0.989
0.985
0.980
0.975
0.996
0,992
0.987
0.983
0.978
0.999
0.995
0.990
0.985
0.981
I.002
0.997
0.993
0.988
0.983
1.005
I.000
0.996
0.991
0986
I.007
I.003
0.998
0993
0989
1010
1.005
I.001
0.996
0.991
1013
1008
l-003
0.999
0.994
1015
1.011
1.006
I.001
0.996
1018
1013
1009
1004
0999
0.957
0.953
0.948
0.943
0.938
0960
0.955
0950
0.946
0.941
0963
0.958
0.953
0.948
0.943
0,965
0.961
0.956
0.951
0.946
0.968
0.963
0.958
0.954
0949
0.971
0.966
0.961
0,956
0.951
0.973
0.968
0.964
0.959
0.954
0976
0.971
0.966
0.961
0.956
0.978
0974
0.969
0.964
0.959
0981
0.976
0.972
0.967
0.962
0.984
0.979
0.974
0969
0964
0.986
0982
0977
0972
0.967
0.989
0.984
0.979
0.974
0967
0.992
0.987
0.982
0977
0.972
0.994
0990
0.985
0.980
0.975
0.933
0.928
0923
0.918
0936
0.931
0.926
0938
0.944
0.939
0,949
0.957
0.952
0946
0.962
0957
0952
0964
0.967
0.954
0.949
0.931
0.926
0954
0949
0944
0939
0.959
0.934
0.928
0923
0.944
0946
0949
0.962
0957
0952
O-928
0.951
0.946
0.941
0.936
0.931
0959
0.941
0.936
0.944
0.921
0,915
0.941
0936
0.931
0.926
0.920
0.946
0.933
0.928
0,923
0.918
0.938
0941
0944
0946
0970
0.964
0959
0954
0.949
0.913
0 907
0.902
0.896
0.891
0915
0,,910
0.904
0.899
0.893
0.918
0.912
0907
0901
0.896
0.920
0.915
0*909
0.904
0.898
0.923
0.917
0912
0.906
0.901
0925
0 920
0.914
0*909
0.903
0.933
0.928
0938
0922
0916
0941
0.935
0930
0924
0'918
0943
0938
0.932
0.927
0.921
0915
0.910
0.905
0.913
0.908
0.916
0.910
0.897
0892
0.886
0.881
0.875
0.900
0894
0889
0.884
0.878
0,902
0897
O-892
0.886
0.880
0.905
0.900
0.894
0889
0.883
0.886
0.910
0.905
0.899
0.894
0.888
0.867
0.861
0.856
0.850
0,843
0.870
0.864
0.858
0.852
0846
0.872
0.866
0.860
0.854
0.848
0.875
0.869
0.863
0.857
0.851
0.877
0871
0,866
9,859
0.853
0.880
0.874
0.868
0.862
0.856
0.882
0876
0.870
0.864
0.858
0.885
0879
0.873
0.867
0.861
0.887
0.682
0.876
0.869
0.863
0890
0,884
0878
0.872
0.866
0.892
0.886
0880
0.874
0,868
0.895
0.889
0.883
0871
0.871
0.835
0828
0.822
0.815
0.808
0,837
0.831
0824
0818
0.811
0.840
0.833
0.827
0.820
0813
0.842
0.836
0.829
0822
0816
0.844
0.838
0832
0.825
0.818
0.847
0.841
0834
0827
0.820
0.850
0.843
0.836
0.830
0.823
0,852
0.846
0.839
0832
0.825
0.854
0.848
0.841
0.835
0.828
0857
0.850
0,844
0.837
0.830
0.859
0.853
0.846
0.840
0.833
0862
0.855
0849
0.342
0.835
0.801
0.804
0.806
0,809
0.811
0.814
O-81 6
0.818
0.821
0.823
0,826
0.828
0.918
0.913
0.908
0.902
0.897
0.891
0.939
0934
0.933
0941
0936
0954
0917
0.911
0.906
0.930
0.926
0.920
0914
0.908
0916
0.911
0936
0930
0925
0.919
0.913
0.897
0.892
0886
0,879
0.873
0.900
0894
0.888
0.882
0876
0,902
0.896
0.890
0.884
0878
0.905
0899
0.893
0.887
0.881
0.907
0.902
0.896
0.889
0.883
0.910
0.904
0898
0892
0,886
0912
0906
0.900
0894
0888
0915
0.909
0903
0.897
0.890
0864
0.858
0851
0.844
0.838
0867
0.860
0.854
0847
0.840
0869
0.863
0.856
0.849
0.842
0.872
0.865
0.859
0.852
0.845
0,874
0,868
0.861
0.854
0847
0.877
0870
0.864
0.857
0.850
0,879
0.873
0866
0.869
0.852
0882
0875
0.868
0.862
0855
0.884
0878
0870
0.864
0857
0.830
0.833
0835
0.838
0840
0.843
0.845
0.848
0850
0928
0,922
0922
0.933
0927
NOTE
IS : 228 was issued as a tentative standard in 1952 and revised in 1959 covering the chemical
analysis of pig iron, cast iron and plain carton end low alloy steels. For the convenience, it was
decided to publish ccrrprehersive
series on chemical analysis of steels including high alloy steels
and another series on ct.emical analysis of pig iron and czst iron. Acccrdingly, chemical analysis of
steels was published in various parts. This standard is series of parts on chemical analysis of steels.
The other parts published are given in Appendix A. The chemical analysis of pig iron and cast iron
is being published in separate standard.
In this revision the major modifications
are as follows:
have been
factors
incorporated
from
Reprography
Unit, BE, New Delhi, India
TO
IS 228 (PART 1): 1987 METHODS FOR CHEMICAL ANALYSIS OF
STEEI~S
700
702
704
706
708
710
712
714
716
718
720
722
724
728
726
Tempera-
ture,OC
(I)
(2)
(3)
(4)
(5)
(6)
(7)
(8)
(9)
(10)
(II)
(12)
(13)
(14)
(1S)
(16)
IS
0.924
0.927
0.929
0.932
0.935
0.937
0.940
0.943
0.945
0.948
0.951
0.954
0.956
0.959
0.962
16
0.920
0.922
0.925
0.928
0.930
0.930
0.936
0.938
0.941
0.944
0.946
0.949
0.952
0.9S4
0.957
0.934
0.937
0.939
0.942
0.945
0.947
0.929
0.932
0.935
0.937
0.940
0.943
0.9S0
0.945
0.953
0.927
0.922
0.918
0.925
0.930
0.933
0.936
0.938
0.941
0.944
0.926
0.928
0.931
0.934
0.936
0.939
0.918
0.921
0.923
0.926
0.929
0.931
0.911
0.914
0.916
0.919
0.922
0.924
19
0.906
0.909
0.912
0.914
0.917
0.920
20
0.902
0.904
0.915
0.893
23
0.888
24
0.8&3
2S
0.879
0.881
0.884
0.920
0.923
0.901
0.896
0.899
0.906 0.909
0.902 0.904
0.907
0.910
0.912
0.915
0.917
0.920
0.892
0.194
0.897
0.900
0.902
0.905
0.907
0.910
0.912
0.915
0.881
0.889
0.892
0.894
0.897
0.900
0.902
0.882
0.884
0.881
0.890
0.892
0.895
0.897
26
0.87~
0.816
0.819
27
0.869
0.872
0.874
28
0.864
0.867
0.869
0.910 0.912
0.905 0.908
0.901 0.903
0.896 0.899
0.891 0.894
0.886 0.889
0.882 0.884
0.871 0.879
0.872 0.874
0.879
0.882
0.885
0.881
0.890
0.892
29
0.859
0.862
0.864
0.867
0.869
0.872
O.H74
0.877
0.880
0.882
0.885
0.887
30
0.854
O.8S~_
0.859
0.862
0.864
0.867
0.869
0.872
0.874
0.877
0.879
0.882
0.90S
0.900
0.895
0.890
0.884
31
0.849
0.854
O.8S6
0.859
0.861
0.864
0.866
0.869
0.864
0.858
0.853
0.847
0.872
0.874
0.877
O.87Q
0.866
0.869
0.871
0.861
0.863
0.866
0.860
0.850
0.8S5
0.841 0.844 0.846 0.849
0.836 0.838 0.840 0.843
0.830 0.832 0.834 0.837
0.824 0.826 0.828 0.831
0.817 0.820 0.822 0.825
0.811 0.813 0.816 0.818
0.804 0.807 0.809 0.812
0.798 0.800 0.803 0.805
0.791 0.794 0.796 0.798
0.784 0.787 0.789 0.792
0.910
0.913
0.916
0.918
0.921
0.924
0.926
0.929
0.932
0.934
0.908
0.911
0.914
0.916
0.919
0.922
0.927
0.930
0.904
0.912
0.914
0.917
0.924
0.912
0.922
0.925
0.877
32
0.843
0.846
0.848
0.851
0.854
0.856
0.859
0.861
33
0.838
0.840
0.843
0.846
0.848
0.851
0.853
0.856
34
0.833
0.835
0.838
0.840
0.843
0.845
0.848
35
0.827
0.832
0.834
0.837
0.840
0.842
0.850
0.845
0.839
0.851
43
0.778
44
0.772
0.830
0.824
0.818
0.812
0.806
0.800
0.794
0.787
0.781
0.774
45
0.765
0.761
36
0.821
37
0.816
38
0.810
39
0.804
40
0.798
41
0.791
42
0.785
0.826
0.829
0.831
0.834
0.836
0.820
0.81S
0.809
0.823
0.826
0.828
0.817
0.820
0.822
0.811
0.814
0.816
0.830 0.833
0.82S 0.827
0.818 0.821
0.802
0.805
0.807
0.796
0.799
0.801
0.790
0.792
0.795
0.783
0.786
0.788
0.776
0.779
0.781
0.770
0.772
0.77S
0.948
0.906
for
0.897
0.928
No
t
21
22
0.907
0.900 0.903
0.89S 0.898
0.891 0.893
0.886 0.889
le
0.915
sa
17
18
0.855
0.858
0.852
0.908
0.910
0.902
0.905
0.898
0.900
0.892
0.887
0.895
0.882
0.884
0.874
0.876
0.879
0.868
0.871
0.873
0.863
0.865
0.868
0.857
0.860
0.862
0.890
0.8S1
O.8S4
0.856
0.846
0.848
0.8S0
0.840
0.842
0.844
0.833
0.814
0.836 0.838
0.830 0.832
0.823 0.826
0.817 0.819
0.808
0.827
0.821
0.810
0.8]3
0.801 .......0.803
0.806
0.796
0.199
--
0.794
(MTD4)
Reprography Unit, Bls. New oeihi. indll