KARANATAKA STATE OPEN UNIVERSITY

M Tech in CHEMICAL

SEMESTER SYSTEM

SYLLABUS

M Tech in Chemical Subject Code Subject Title Semester-I CM1001 Advanced Numerical Methods CM1002 Advanced Thermodynamics CM1003 Advanced Reaction Engineering CM1004 Petrochemicals Engineering Elective-I CMP001 Petro Products Testing Lab Semester -II Subject Code Subject Title Max Marks 100 100 100 100 100 100 Max Credits 6 6 6 6 6 3 100 100 100 100 100 100 6 6 6 6 6 3 Max Marks Max Credits

CM2001 Advanced Separation Process CM2002 Solvent Extraction CM2003 Advanced Transport Concepts Elective-II Elective-III CMP002 Instrumental Methods of Analysis Lab

III Semester Subject Code CM3001 CM3002 CM3003 Subject Title Advanced Process Control Process Modelling and Simulation Chemical Process Design Elective-IV Elective-V CMP003 Project Phase-I Max Marks 100 100 100 100 100 100 Max Credits 6 6 6 6 6 3

IV Semester Subject Code CM4001 Subject Title Catalyst Design and Application Elective-VI CMP004 Project Phase-II Max Marks 100 100 400 Max Credits 6 6 12

Total Marks = 2400 Total Credits = 123

List of Electives Subject Code Subject Title CME001 CME002 CME003 CME004 CME005 CME006 CME007 CME008 CME009 CME010 CME011 CME012 Petroleum Refinery Engineering Environmental Engineering Energy Management Natural Gas Engineering Multiphase Flow Risk Analysis and Management Computational Fluid Dynamics Project Engineering and Process Plant Fluidization Engineering Total Quality Management Safety and Hazard Control Polymer Technology

SEMESTER :I Subject Code : CM1001 Subject Title : Advanced Numerical Methods Structure of the Course Content BLOCK 1 Algebraic Equation
Unit 1: Systems of linear equations Jacobi, Gauss Seidel, SOR methods Unit 2: Thomas algorithm for tridiagonal systems; Systems of nonlinear equations Unit 3: Successive approximation method, methods for improved convergence Unit 4: Successive approximation method, methods for improved convergence

BLOCK 2 ordinary Differential Equations-IVPS

Unit 1: Runge Kutta Methods Unit 2: Step size control and estimates of error Unit 3: Numerical stability, solution of stiff ODEs Unit 4: ODE-IVPs coupled with algebraic equations

BLOCK 3 ordinary Differential Equations-BVPS

Unit 1: Finite difference method Unit 2: Orthogonal collocation method Unit 3: Orthogonal collocation with finite element method Unit 4: Galerkin finite element method, shooting technique

BLOCK 4 Partial Differential Equations-FDM

Unit 1: Parabolic equations Different explicit and implicit methods Unit 2: Alternating direction explicit and implicit methods; Elliptic equations Unit 3: Point iterative methods, line iterative methods, ADI methods Unit 4: First order hyperbolic equations method of characteristics

BLOCK 5 Partial Differential Equations-FEM

Unit 1: Partial differential equations Unit 2: Finite element method Unit 3: Orthogonal collocation method Unit 4: Orthogonal collocation with finite element method

Books:
1.Jain, M. K., S. R. Iyengar, M. B. Kanchi, R. K. Jain, Computational Methods for Partial Differential Equations, New Age Publishers 2. Gupta, S.K., Numerical Methods for Engineers, New Age Publishers

SEMESTER :I Subject Code : CM1002 Subject Title : Advanced Thermodynamics Structure of the Course Content BLOCK 1 Basic Concept
Unit 1: Energy and first Law Unit 2: Reversibility and second Law Unit 3: Review of Basic Postulates, equilibrium criteria Unit 4: Legendre Transformation and Maxwells relations

BLOCK 2

Stability and Phase Transition

Unit 1: Stability of thermodynamic systems Unit 2: First order phase transitions and critical phenomenon Unit 3: Phase rule, single component phase diagrams Unit 4: Thermodynamic properties from volumetric and thermal data

BLOCK 3

Multicomponent Mixtures

Unit 1: Partial molar properties, fugacities in gas and liquid mixtures Unit 2: Activity coefficients, Ideal and Non-ideal solutions Unit 3: Gibbs-Duhem equation, Wilson, NRTL Unit 4: UNIQUAC equations, UNIFAC method

BLOCK 4

Phase Equilibrium

Unit 1: VLE - Equations of state, corresponding states Unit 2: Henrys Law, lattice theory Unit 3: Criticality, high pressure VLE Unit 4: Other phase equilibriums- SLE/LLE/VLLE

BLOCK 5 Chemical Equilibrium

Unit 1: Introduction to Chemical Equilibrium Unit 2: Homogeneous gas and liquid phase reactions Unit 3: Heterogeneous reactions Unit 4: Phase and chemical equilibrium

Books:
1.Tester, J. W. and M. Model, Thermodynamics and Its Applications. 3rd Edn. Prentice Hall, New Jersey 2. Rao., Y.V.C., Chemical Engineering Thermodynamics, University Press, Hyderabad 3.Prausnitz, J.M., Lichtenthaler R.M. and Azevedo, E.G., Molecular thermodynamics of fluid-phase Equilibria, 3rd Edn, Prentice Hall Inc., New Jersey

SEMESTER :I Subject Code : CM1003 Subject Title : Advanced Reaction Engineering Structure of the Course Content BLOCK 1 Kinetics of Heterogeneous Reactions
Unit 1: Catalytic reactions, rate controlling steps Unit 2: Langmuir-Hinshelwood model, Rideal-Eiley mechanism Unit 3: Steady state approximation, noncatalytic fluid-solid reactions Unit 4: Shrinking and unreacted core model

BLOCK 2 External Diffusion Effects in Heterogeneous Reactions

Unit 1: Introduction to heterogeneous Unit 2: Mass and heat transfer coefficients in packed beds Unit 3: Quantitative treatment of external transport effects Unit 4: Modelling diffusion with and without reaction

BLOCK 3

Internal Transport Process in Porous Catalysts

Unit 1: Interpellet mass Unit 2: Heat transfer Unit 3: Evaluation of effectiveness factor Unit 4: Mass and heat transfer with reaction.

BLOCK 4 Analysis and Design of Heterogeneous Reactors

Unit 1: Introduction to Reactors Unit 2: Isothermal and adiabatic fixed bed reactors Unit 3: Non-isothermal and non-adiabatic fixed bed reactors Unit 4: Determination, evaluation of reaction kinetics for heterogeneous systems

BLOCK 5

Reactor Models

Unit 1: Two-phase fluidized bed model Unit 2: Slurry reactor model Unit 3: Trickle bed reactor model Unit 4: Case studies

Books:
1. Carberry, J. J., Chemical and Catalytic Reaction Engineering, Dover Publications 2.Froment, G. F. and Bischoff, K. B., Chemical Reactor Design and Analysis, 2nd Edition, John Wiley & Sons, New York

SEMESTER :I Subject Code : CM1004 Subject Title : Petrochemicals Engineering Structure of the Course Content BLOCK 1 Introduction to Petrochemicals
Unit 1: Overview of petrochemical Unit 2: Overview of petrochemical industrial Growth in India Unit 3: Economics in Petrochemicals Unit 4: Feedstock Selection for Petrochemicals

BLOCK 2 Accessories in Petrochemicals-I

Unit 1: Steam reforming, Hydrogen Unit 2: Synthesis gas, cracking of gaseous and liquid for stocks Unit 3: Olefins, Diolifins Unit 4: Acetylene and Aromatics and their separation

BLOCK 3 Accessories in Petrochemicals-II

Unit 1: Alkylation, Oxidation Unit 2: Dehydrogenation, Nitration Unit 3: Chlorination Unit 4: Sulphonation and Isomerization

BLOCK 4

Chemicals

Unit 1: Chemicals from synthesis gas Unit 2: Olefins Unit 3: Diolefins Unit 4: Acetylene and Aromatics

BLOCK 5

Production Techniques

Unit 1: Modes and techniques Unit 2: Production of Polyethylene, PVC Unit 3: Polypropylene, SAN, ABS, SBR, Polyacrylonitrile Unit 4: Polycarbonates, Polyurethane, Nylon, PET

Books:
1.Sitting M., Aromatics Hydrocarbons, Manufacture and Technology, Noyes Data Corporation 2. Brownstein A.M. Trends in PetroChemical , Petroleum Publishing Company 3. Stevens P.M. Polymer Chemistry, Addison Wesley Publishing Company

SEMESTER :I Subject Code : CMP001 Subject Title : Petro Products Testing Lab Structure of the Course Content List of Experiments
1. Determination of flash point 2. Viscosity Determination 3. Aniline point determination 4. API gravity determination 5. Determination of aromatic content 6. Hydrogen sulphide content determination 7. Sulphur content determination 8. Determination of calorific value 9. Bitumen testing 10. Carbon residue determination (Conradson apparatus) 11. Cloud point and pour point estimation 12. Cgealing point of wax 13. Foaming characteristics of lube oil 14. Smoke point estimation 15. Corrosion testing of petroleum oil 16. API distillation apparatus 17. Moisture determination other than Karl-Fischer method

SEMESTER : II Subject Code : CM2001 Subject Title : Advanced Separation Process Structure of the Course Content BLOCK 1 General Concept in Separation Process
Unit 1: Recent advances in separation techniques based on size Unit 2: Surface properties, ionic properties and characteristics of substances Unit 3: Process concept, theory and equipment used in cross flow filtration Unit 4: Cross flow electrofiltration, dual functional filter

BLOCK 2

Membrane Separations

Unit 1: Types and choice of membranes, plate and frame, tubular Unit 2: Spiral wound and hollow fibre membrane reactors and their relative merits Unit 3: Pilot plant and laboratory membrane pemeators involving dialysis Unit 4: Microfiltration and Donnan dialysis, economics of membrane operations

BLOCK 3 Separations by Adsorption Techniques

Unit 1: Mechanism, types and choice of adsorbents Unit 2: Normal adsorption techniques, affinity chromatography Unit 3: Types of equipment and commercial processes Unit 4: Recent advances and process economics

BLOCK 4

Ionic Separations

Unit 1: Controlling factors, Applications Unit 2: Types of equipment employed for electrophoresis Unit 3: Dielectrophoresis, Ion Exchange chromatography and electrodialysis Unit 4: Commercial processes

BLOCK 5

Special Techniques

Unit 1: Separations involving lyophilization, pervaporation techniques for solids Unit 2: Liquids and gases, industrial viability and examples Unit 3: Zone melting, addiuctive crystallization, other separation processes Unit 4: Industrial effluent treatment by modern techniques

Books:
1.Nakagawal, O. V., Membrane Science and Technology, Marcel Dekker 2.Rousseau, R. W., Handbook of Separation Process Technology, John Wiley, New York 3.King, C. J., Separation Processes, Tata McGraw Hill Co., Ltd

SEMESTER : II Subject Code : CM2002 Subject Title : Solvent Extraction Structure of the Course Content BLOCK 1 Equilibrium in Liquid-Liquid System
Unit 1: Binary and ternary liquid equilibria, Tie-lines, Critical solution temperature Unit 2: Tie line correlations, Contour/prism diagrams Unit 3: Binary / Ternary prediction methods of activity coefficient Unit 4: Theory and Prediction of diffusivity in liquids

BLOCK 2

Differential/Stage-Wise Equilibrium Contact Operations

Unit 1: Equilibrium stage-wise contact, Single and multiple contacts Unit 2: Calculation methods, Fractional extraction with reflux of raffinate Unit 3: Contact, HETS, NETS, HTU, NTU concepts Unit 4: Mass transfer efficiency, Axial mixing

BLOCK 3

Dispersion and Coalescence in Extractors

Unit 1: Characteristics of dispersion in single and multiple nozzle distributors Unit 2: Drop size and formation and coalescence Unit 3: Effect of drop oscillation, wobbling and Internal circulation Unit 4: Prediction of drop size and characteristics velocity in spray

BLOCK 4

Design of Liquid Extraction Columns-I

Unit 1: Design of extractor height and diameter Unit 2: Prediction of flow capacities in terms of flooding rates, Unit 3: Regime of operating envelops Unit 4: Hydrodynamic design variables such as hold up

BLOCK 5

Design of Liquid Extraction Columns-II

Unit 1: Characteristic velocities, pressure drop Unit 2: Correction of mass transfer data Unit 3: Axial mixing correction for column height Unit 4: Interfacial area estimations

Books:
1.Hanson, C., Baird, M. H. I. and Lo, T. C., Hand Book of Solvent Extraction, Wiley International, New York 2. Laddha, G. S. and Degaleesan, T. E., Transport Phenomena in Liquid Extraction, Tata McGraw Hill, New Delhi 3. Hanson, C., Recent Advances in Liquid Extraction, Pergamon Press, London

SEMESTER : II Subject Code : CM2003 Subject Title : Advanced Transport Concepts Structure of the Course Content BLOCK 1 Basic Concept of Transport Properties
Unit 1: Phenomenological Equations and Transport properties Unit 2: Rheological behaviour of fluids Unit 3: Balance Equations Unit 4: Differential and Integral equations

BLOCK 2 Applications of Differential Equations of Change

Unit 1: Applications in laminar transport in compressible fluids Unit 2: Applications in Turbulent transport in compressible fluids Unit 3: Applications in laminar and turbulent transport in incompressible fluids Unit 4: Boundary layer theory

BLOCK 3 Applications of Integral Equations of Change

Unit 1: Macroscopic balance for isothemal and nonisothermal systems Unit 2: Macroscopic balance for isothemal systems and their applications Unit 3: Macroscopic balance for nonisothemal systems and their applications Unit 4: Heat and Mass transport problems

BLOCK 4

Interphase and Multiphase momentum Transfer

Unit 1: Friction factor, Fluid Fluid systems Unit 2: Flow patterns in vertical and horizontal pipes Unit 3: Formulation of bubbles and drops and their size distribution Unit 4: Solid fluid systems, Forces acting on stagnant and moving solids,

BLOCK 5 Interphase Transport in Non-isothermal

Unit 1: Heat Transfer coefficient, Forced convection in tubes Unit 2: Around submerged objects, Heat Transfer by free convection Unit 3: Film type and dropwise condensation and equations for heat transfer Unit 4: Heat transfer in boiling liquids

Books:
1. Brodkey, R. S. and Hershey, H. C., Transport Phenomena A Unified Approach, Brodkey Publishing 2.Welty, J.R., Wicks, C. E. and Wilson, R. E., Fundamentals of Momentum, Heat Mass Transfer, 5th Edn., John Wiley and Sons 3.Bird R.B., Stewart, W. E. and Lightfoot, E. N., Transport Phenomena, 2nd Edn., John Wiley and Sons

SEMESTER : II Subject Code : CMP002 Subject Title : Instrumental Methods of Analysis Lab Structure of the Course Content List of Experiments
1. UV-Visible spectrophotometer 2. Infrared spectrophotometer 3. Gas chromatograph. 4. High performance liquid chromatograph 5. Atomic absorption spectrophotometer. 6. Flame photometer 7. Thermo gravimetric analyzer 8. Differential scanning calorimeter 9. Differential thermal analyzer

SEMESTER : III Subject Code : CM3001 Subject Title : Advanced Process Control Structure of the Course Content BLOCK 1 Advanced Control Strategies
Unit 1: Feed forward, cascade Unit 2: Dead time compensation Unit 3: Split range, selective and override control Unit 4: Automatic tuning and gain scheduling

BLOCK 2

Internal Model Control

Unit 1: Model based control Unit 2: IMC structure Unit 3: Development and design Unit 4: IMC based PID control

BLOCK 3 Multivariable Controls

Unit 1: Control loop interaction general pairing problem Unit 2: Relative gain array and application Unit 3: Sensitivity. Multivariable control zeros and performance limitations Unit 4: Directional sensitivity and operability, decoupling

BLOCK 4

Discrete Systems

Unit 1: Z Transform and inverse Z Unit 2: Transform properties, Discrete Time Response of dynamic system Unit 3: Pulse Transfer Function Unit 4: Closed Loop System Stability

BLOCK 5 Digital Feedback Controllers

Unit 1: Design of digital feedback controllers Unit 2: Digital approximation of classical Unit 3: Effect of sampling, Dahlins algorithms, Dead beat algorithm Unit 4: Ringing, IMC algorithm, simplified model predictive algorithm

Books:
1.Stephanopolous, G., Chemical Process Control, Prentice Hall of India, New Delhi 2.Bequette, B. W., Process Control: Modelling, Design, and Simulation, Prentice Hall

SEMESTER : III Subject Code : CM3002 Subject Title : Process Modelling and Simulation Structure of the Course Content BLOCK 1 Introduction to Modelling and Simulation
Unit 1: Introduction to Modelling and Simulation Unit 2: Classification of mathematical models Unit 3: Conservation equations and auxiliary relations Unit 4: Population balance and stochastic modelling

BLOCK 2

Steady State Lumped Systems

Unit 1: Degree of freedom analysis, single and network of process units Unit 2: Systems yielding linear and non-linear algebraic equations, flowsheeting Unit 3: Sequential modular and equation oriented approach Unit 4: Solution of linear and non-linear algebraic equations

BLOCK 3

Unsteady State Lumped Systems

Unit 1: Analysis of liquid level tank, gravity flow tank Unit 2: Jacketed stirred tank heater, reactors, flash and distillation column Unit 3: Solution of ODE initial value problems Unit 4: Matrix differential equations, simulation of closed loop systems

BLOCK 4 Steady State Distributed Systems

Unit 1: Analysis of compressible flow, heat exchanger Unit 2: Packed columns Unit 3: Plug flow reactor Unit 4: Solution of ODE boundary value problems

BLOCK 5 Unsteady State Distributed Systems

Unit 1: Analysis laminar flow in pipe, sedimentation, boundary layer flow Unit 2: Conduction, heat exchanger, heat transfer in packed bed, diffusion Unit 3: Packed bed adsorption, plug flow reactor, hierarchy in model development Unit 4: Classification and solution of partial differential equations

Books:
1.Luyben, W.L., "Process Modelling Simulation and Control", McGraw-Hill Book Co 2..Ramirez, W., "Computational Methods in Process Simulation", 2nd Edn., Butterworths, New York 3.Franks, R. G. E., Mathematical Modelling in Chemical Engineering, John Wiley

SEMESTER : III Subject Code : CM3003 Subject Title : Chemical Process Design Structure of the Course Content BLOCK 1 Introduction to Chemical Process Design
Unit 1: Introduction to Chemical Process Design Unit 2: The Hierarchy of Chemical process Design Unit 3: Overall process Design Unit 4: Approaches to design

BLOCK 2 Choices of Reactors and Separator

Unit 1: Reaction path, reactor performance Unit 2: Practical reactors Unit 3: Separation of Heterogeneous mixtures Unit 4: Homogeneous fluid mixtures

BLOCK 3

Synthesis of Reaction-Separation Systems

Unit 1: Introduction to Synthesis of Reaction Unit 2: Process recycles Unit 3: Batch processes Unit 4: Process yield

BLOCK 4

Distillation Sequencing

Unit 1: Introduction to Distillation Sequencing Unit 2: Using simple columns Unit 3: Using columns with more than two products Unit 4: Distillation Sequencing Using thermal coupling

BLOCK 5

Heat Exchanger Network &Utilities

Unit 1: Heat recovery pinch Unit 2: The Problem table Algorithm Unit 3: Utilities Selection Unit 4: Energy targets capital & total Cost targets

Books:
1.Douglas, J.M., Conceptual Design of Chemical Process, McGraw Hill, New York 2. Smith, R., Chemical Process Design, McGraw Hill, New York

SEMESTER : III Subject Code : CMP003 Subject Title : Project Phase-I Structure of the Course Content

SEMESTER : IV Subject Code : CM4001 Subject Title : Catalyst Design and Application Structure of the Course Content BLOCK 1 Catalysis and Catalytic Kinetics
Unit 1: General definition of catalysts, illustration of a catalytic a process Unit 2: Design for catalysts Primary constituents, secondary constituents Unit 3: Catalyst supports-choice of support material Unit 4: Chemical interaction, Deactivation steps involved in global catalytic rate

BLOCK 2 Adsorption- Diffusion and Heterogeneous Catalysis

Unit 1: Adsorption and Heterogeneous Catalysis Unit 2: Electron structure of catalysts; Chemical properties of surfaces Unit 3: Theories and Adsorption; Semi conduction and catalysts Unit 4: Defect structure in crystal lattices, Thermodynamics basics of catalysis

BLOCK 3 Productions of Some Catalysts

Unit 1: Precipitation method Alumino silicate catalyst Unit 2: Production of tabletted chromium catalysts for the conversion of CO Unit 3: Platinum network catalysts of Ammonia oxidation Unit 4: Catalysts of natural clays, zeolites and ion exchange resins

BLOCK 4

Methods of Studying Catalysts

Unit 1: Methods of determining catalysts static methods, dynamic method Unit 2: Adsorption for determining catalyst surface and pore radii Unit 3: Determination of true and apparent densities of catalysts Unit 4: Structural study of electron microscopy

BLOCK 5 Analysis and Design of Heterogeneous Catalytic Reactors

Unit 1: Fixed bed reaction, continuity equations, reactor parameters Unit 2: Reaction significance of dimensionless parameters Unit 3: Physical dimensionless parameters Unit 4: Selectivity in slurry reactors; catalytic gaue reactor, trickle bed reactors

Books:
1. Trimm D.L., Design of Industrial catalsysts, Elsevier Scientific Publishing Company, Amsterdam Oxford New York 2.Muchlyonor I, Dobkina E.,.Deryozhkina V,.and Sorco V., Catalyst Technology Catalyst Technology MIR Publication, Moscow 3. Carbery J.J. Chemical and Catalytic, Reaction Engineering, McGraw Hill Book Co

SEMESTER : IV Subject Code : CMP004 Subject Title : Project Phase-II Structure of the Course Content

ELECTIVE Subject Code : CME001 Subject Title : Petroleum Refinery Engineering Structure of the Course Content BLOCK 1 Introduction to Petroleum
Unit 1: Origin, Exploration and production of petroleum Unit 2: Types of crudes, Composition, characteristics Unit 3: Products pattern and characteristics, indigenous and imported crudes Unit 4: Availability Vs Demands, Future outlook

BLOCK 2

Refining

Unit 1: Engineering aspects of refining, Reaction stoichiometry Unit 2: Chemical kinetics; Thermo chemistry and chemical equilibrium Unit 3: Mixuing in flow systems; Reactor design. Crude heating, Unit 4: Energy input and recovery, Vacuum distillation, Types of trays

BLOCK 3 Solvent Extractions

Unit 1: Lube oil and wax processing, Solvent extraction, Dewaxing, Deciling, Unit 2: Clay contacting, principles, technologies, operating parameters Unit 3: Product qualities, Air blowing technology Unit 4: Storage and handling of crude products

BLOCK 4

Catalysts

Unit 1: Fluid catalytic cracking, principles, recent developments Unit 2: Feedstocks and product yields and qualities, Unit 3: Catalysts and operating parameters Unit 4: Hydrocracking, principles, process requirements

BLOCK 5

Catalytic Reforming

Unit 1: Catalytic reforming and Isomerisation, Reforming, Principles Unit 2: Developments in technology, Catalyst types and their performance Unit 3: Effects of operating parameters, Feed quality, Product improvement Unit 4: Sulphur removal, Aromatics removal, Hydrofinishing

Books:
1. Nelson, W.L Petroleum Refinery Engineering McGraw Hill Publishing Company Limited 2. Smalheer, C.V and R.Kennedy Smith Lubricant Additives. The Lezius Hill Company, Cleveland, Ohio. USA 3. Hobson, G.D. Modern petroleum Refining Technology, 4th Edition, Institute of Petroleum U.K

ELECTIVE Subject Code : CME002 Subject Title : Environmental Engineering Structure of the Course Content BLOCK 1 Environmental Awareness
Unit 1: Environment Unit 2: Friendly chemical Process Unit 3: Hazard and risk analysis Unit 4: Environmental Audit

BLOCK 2

Chemical Engineering Process

Unit 1: Unit Operations Unit 2: Application of - Abatement of water pollution Unit 3: Current strategies to control air pollution Unit 4: Disposal of solid wastes

BLOCK 3 Recycling Methodologies

Unit 1: Introduction to Recycling Techniques Unit 2: Economic recovery and recycling of waste Unit 3: Transport fuel Unit 4: Bio-diesel for a cleaner environment

BLOCK 4 Clean Technologies

Unit 1: Towards Eco- friendly products of chemical industry Unit 2: Pesticides Their transfer and Transformation in the environment Unit 3: Biological technology for effluent treatments Unit 4: ElectroChemical for effluent treatments

BLOCK 5

Pollution Prevention

Unit 1: Mass exchange network synthesis for pollution control and minimization Unit 2: Policies for regulation of environmental impacts Unit 3: Concept of common effluent treatment Unit 4: Environmental legislations, Role of Government and Industries

Books:
1. Rao M.N and H.V.N. Rao. Air pollution ,Tata McGraw Hill Publishing Co. Ltd 2.Peavy H.S. Rowe D.R., and George Technologious, Environmental Engineering, Mc Graw Hill Book Company, Ny 3.Rao, C.S Environmental Pollution control Engineering, Wiley- Eastern Ltd

ELECTIVE Subject Code : CME003 Subject Title : Energy Management Structure of the Course Content BLOCK 1 Introduction to Energy Resources
Unit 1: Energy Resources Unit 2: Conventional Non conventional Unit 3: Energy Reserves and Depletion Unit 4: Non renewable energy sources

BLOCK 2

Power Generation Process

Unit 1: Power generation by steam, Hydroelectric, Diesel oil Unit 2: Nuclear fission and Natural gas, Co-generation of power Unit 3: Selection of power generation process Unit 4: Economical and technical efficiency of power generation ,

BLOCK 3

Renewable Energy

Unit 1: Renewable sources of energy Unit 2: Thermal and power generation using water Unit 3: Wind, seawave, Solar energy Unit 4: Geothermal and biomass utilization

BLOCK 4

Energy Consumption

Unit 1: Energy consumption, Demand pattern Unit 2: Energy planning Short term and long term, Energy conservation Unit 3: Need for Energy recovery Unit 4: Various types of Energy audit advantages

BLOCK 5

Recovering Energy Techniques

Unit 1: Recovery of waste heat Unit 2: Optimum shell and tube heat exchanger Unit 3: Heat exchanger network, evaporator systems Unit 4: Boiler, turbo generator system

Books:
1. Loftiness, R.L. Energy Hand Book, Van Nostrand Reinhold Company, New York 2. Francis, W. and M.C. Peter Fuels and fuel technology, Pergamon Press 3. Nagpal, G.R Power Plant Engineering, Khanna Publishers

ELECTIVE Subject Code : CME004 Subject Title : Natural Gas Engineering Structure of the Course Content BLOCK 1 Introduction to Natural Gas
Unit 1: Availability of natural gas Unit 2: Properties and composition Unit 3: Exploration and control of gas Unit 4: Estimation of availability quantity

BLOCK 2 Applications of Natural Gas

Unit 1: Natural gas application in Chemical Process Unit 2: Natural gas application in transportation industry LNG technology, Unit 3: Natural gas storage and transport Unit 4: Economics of natural gas utilization

BLOCK 3 Flows of Fluids

Unit 1: General Hydrodynamic equations for flow of fluids through porous media Unit 2: Two dimensional flow problems and potential theory methods Unit 3: Gravity flow systems, systems of non uniform permeability Unit 4: Multiple well systems using computerized streamline tracking methods

BLOCK 4

Design of gas System

Unit 1: Use of multiphase flow correlations to determine flow ratio Unit 2: Pressure traverse in flowing oil wells, gas condensate wells Unit 3: Gathering systems and pipe lines Unit 4: Application of correlations to the design of gas system

BLOCK 5

Reservoir Properties

Unit 1: Reservoir fluid properties Unit 2: PVT properties for oil gas systems Unit 3: Phase Behavior of complex hydrocarbon mixtures at high temperature Unit 4: Thermodynamic property evaluation, packages used in petroleum industry

Books:
1.Donald L.Katz and Robert L.Lee, Natural Gas Engineering, Mc Graw Hill Publishing Company, NY 2.Speight, J.G Fuel Science and Technology Handbook, Marcel Decker Inc 3.Guide to Natural Gas Utilization Technologies, Fairmount Press Inc

ELECTIVE Subject Code : CME005 Subject Title : Multiphase Flow Structure of the Course Content BLOCK 1 Characteristics of Multiphase Flow
Unit 1: Significance of multiphase flows, important non-dimensional numbers Unit 2: Parameters of characterization, calculation of particle size Unit 3: Size distributions and moments Unit 4: Size distribution models

BLOCK 2 Particle Fluid Interactions

Unit 1: Equation of motion for a single particle, calculation of drag Unit 2: Motion of a particle in two-dimensions, Unit 3: Effects of acceleration, effects of coupling; Interaction between particles Unit 4: Sphere model, soft sphere model, discrete element modeling

BLOCK 3 Modelling of Multiphase Flows

Unit 1: Flow patterns - identification and classification Unit 2: Flow pattern maps and transition - momentum and energy balance Unit 3: Homogeneous and separated flow models Unit 4: Correlations for use with homogeneous and separated flow models

BLOCK 4 Conservation Techniques

Unit 1: Averaging procedures - time, volume Unit 2: Ensemble averaging, quasi-one-dimensional flow Unit 3: Two-fluid volume-averaged equations of motion Unit 4: Turbulence and two-way coupling

BLOCK 5

Multiphase Systems

Unit 1: Flow regime and hydrodynamic characteristics of packed bed Unit 2: Fluidized bed, pneumatic conveying, bubble column, trickle beds Unit 3: Conventional and novel measurement techniques for multiphase systems Unit 4: Laser Doppler anemometry, Particle Image Velocimetry

Books:
1. Crowe, C. T., Sommerfeld, M. and Tsuji, Y., Multiphase Flows with Droplets and Particles, CRC Press 2.Clift, R., Weber, M.E. and Grace, J.R., Bubbles, Drops, and Particles, Academic Press, New York 3.Fan, L. S. and Zhu, C., Principles of Gas-solid Flows, Cambridge University Press

ELECTIVE Subject Code : CME006 Subject Title : Risk Analysis and Management Structure of the Course Content BLOCK 1 Introduction to Risk Analysis
Unit 1: General: Risk types, Completion Unit 2: Permitting, Resource, Operating Unit 3: Environmental, Manageable, and Insurable Unit 4: Risk Causes, Risk Analysis types and causes

BLOCK 2

Risk Analysis Methods

Unit 1: Risk adjusted discounted rate method Unit 2: Certainty Equivalent Coefficient method, Quantitative Sensitivity analysis Unit 3: Probability distribution, Coefficient of variation method, Unit 4: Crude Procedures, Payback period, expected monetary value method

BLOCK 3

Risk Management

Unit 1: Emergency relief Systems, Diers program, Bench scale experiments Unit 2: Design of emergency relief systems, Internal emergency planning Unit 3: Risk management plan, mandatory technology option analysis Unit 4: Risk management alternatives, risk management tools

BLOCK 4 Risk Assurances and Assessment

Unit 1: Property Insurance, Transport insurance Unit 2: Liability insurance, Pecunious insurance, Risk Assessment Unit 3: Scope Canvey study, Rijimond pilot study Unit 4: Fault tree analysis, Event tree analysis, Zero Infinity dilemma

BLOCK 5

Risk Analysis in Chemical Industries

Unit 1: Handling and storage of Chemicals, Process plants Unit 2: Personnel protection equipments. Environmental risk analysis Unit 3: International environmental management system Unit 4: Corporate management system, Environmental risk assessment

Books:
1. Srivastav, S., Industrial Maintenance Management, Sultan Chand & Co 2. Rao, P. C. K., Project Management and Control, Sultan Chand & Co., Ltd 3. Sincero, A. P. and Sincero, G. A., Environmental Engineering A Design Approach, Prentice Hall of India

ELECTIVE Subject Code : CME007 Subject Title : Computational Fluid Dynamics Structure of the Course Content BLOCK 1 Conservation Laws
Unit 1: Governing equations of fluid flow and heat transfer Unit 2: Mass conservation, momentum and energy equation Unit 3: Differential and integral forms Unit 4: Conservation and non-conservation form

BLOCK 2

Turbulence

Unit 1: Characteristics of turbulent flows Unit 2: Time averaged Navier Stokes equations Unit 3: Turbulence models one and two equation Unit 4: Reynolds stress, LES and DNS

BLOCK 3

Finite Volume Method

Unit 1: Diffusion problems explicit and implicit time integration Unit 2: Convection-diffusion problems properties of discretisation schemes Unit 3: Central, upwind, hybrid, QUICK schemes Unit 4: Solution of discretised equations

BLOCK 4 Flow Field Computations

Unit 1: Pressure velocity coupling Unit 2: Staggered grid Unit 3: Simple Algorithms Unit 4: PISO algorithm for steady and unsteady flows

BLOCK 5

Grid Generation

Unit 1: Physical aspects Unit 2: Simple and multiple connected regions Unit 3: Grid generation by PDE solution Unit 4: Grid generation by algebraic mapping

Books:
1. Anderson, J. D., Computational Fluid Dynamics: The Basics with Applications, McGraw-Hill 2.Fletcher, C. A. J., Computational Techniques for Fluid Dynamics, Springer Verlag 3.Versteeg, H.K. and Malalasekera, W., An Introduction to Computational Fluid Dynamics: .The Finite Volume Method, Pearson Education Ltd

ELECTIVE Subject Code : CME008 Subject Title : Project Engineering and Process Plant Structure of the Course Content BLOCK 1 Introduction to Project Engineering
Unit 1: Project definition, Project Profile and standards Unit 2: Feedback information (MIS) Unit 3: Evaluation and Modification Unit 4: Selection, Criteria

BLOCK 2

Process Planning

Unit 1: Planning the process, Strategic and Managerial Planning Unit 2: Organising the process planning, cost and costing, Cost Control systems Unit 3: Methods (PERT/CPM), Engineering Flow Diagrams, Cost requirements Unit 4: Analysis and Estimation of Process Feasibilities

BLOCK 3

Plant Engineering Management

Unit 1: Objectives, Programme, Control, Plant Location and Site Selection Unit 2: Layout diagrams, Selection and procurement of equipments Unit 3: Installation, Recommission, Commissioning and performance appraisal Unit 4: Strategies choice and Influence, Product planning and development

BLOCK 4

Safety Standards

Unit 1: Process safety, Materials safety and Handling regulations Unit 2: Safety in equipment and machinery operations Unit 3: Design considerations of safety organization and control Unit 4: Pollution, Pollution control and Abatement, Industrial Safety Standard

BLOCK 5

Pollution Control

Unit 1: Government regulations on procurement of raw materials Unit 2: Export Import regulations, Pricing policy, Industrial licensing procedure Unit 3: Excise and commercial taxes, Policies on depreciation and corporate tax Unit 4: Factory act, Regulations of Pollution Control Board .

Books:
1. Cheremisinoff, N. P., Practical Guide to Industrial Safety: Methods for Process Safety Professionals, CRC Press 2. Couper, J. R., Process Engineering Economics, CRC Press 3. Perry, J. H. Chemical Engineers Hand Book, 8th Ed., McGraw Hill, New York

ELECTIVE Subject Code : CME009 Subject Title : Fluidization Engineering Structure of the Course Content BLOCK 1 Introduction to Fluidization
Unit 1: The Fluidized state, Nature of hydrodynamic suspension Unit 2: Particle forces, species of Fluidization, Regimization of the fluidized state Unit 3: Operating models for fluidization systems Unit 4: Applications of fluidization systems

BLOCK 2

Hydrodynamics of Fluidization Systems

Unit 1: General bed behaviour, pressure drop, Flow regimes, Incipient Fluidization Unit 2: Pressure fluctuations, Phase Holdups, Measurements Techniques Unit 3: Empirical Correlations for Solids holdup, liquid holdup and gas holdup Unit 4: Flow models generalized wake model, structural wake model

BLOCK 3

Solids Mixing and Segregation

Unit 1: Phase juxtapositions operation shifts, Reversal points Unit 2: Degree of segregation, Mixing Segregation equilibrium Unit 3: Generalised fluidization of poly disperse systems Unit 4: Liquid phase Mixing and gas phase mixing

BLOCK 4 Heats and Mass Transfer in Fluidization System

Unit 1: Mass transfer Gas Liquid mass transfer Unit 2: Liquid Solid mass transfer and wall to bed mass transfer, Heat transfer Unit 3: Bed heat transfer, Immersed vertical cylinder to bed heat transfer Unit 4: Immersed horizontal cylinder to bed heat transfer

BLOCK 5

Special Systems

Unit 1: Conical Fluidized bed, Moving bed, Slurry bubble columns Unit 2: Turbulent bed contactor, Two phase and Three phase inverse fluidized bed Unit 3: Semi fluidized bed systems, Annular systems, Typical applications Unit 4: Powder characterization and modeling by bed collapsing

Books:
1. Kunii, D. and Levenspiel, O., Fluidization Engineering, 2nd Edn., Butterworth-Heinemann, London 2. Kwauk, M., Fluidization - Idealized and Bubbleless, with applications, Science Press 3. Fan, L. S., Gas- liquid Solid Fluidization Engineering, Butterworths

ELECTIVE Subject Code : CME010 Subject Title : Total Quality Management Structure of the Course Content BLOCK 1 Concepts of TQM
Unit 1: Philosophy of TQM, Customer focus Unit 2: Organization, top management commitment Unit 3: Team work Unit 4: Quality philosophies of Deming, Crosby and Muller

BLOCK 2

TQM Process

Unit 1: QC Tools, Problem solving methodologies Unit 2: New management tools Unit 3: Work habits, quality circles Unit 4: Bench marking, strategic quality planning

BLOCK 3

TQM Systems

Unit 1: Quality policy deployment Unit 2: Quality function deployment Unit 3: Standardization Unit 4: Designing for quality, manufacturing for quality

BLOCK 4 Quality Systems

Unit 1: Need for ISO 9000 system Unit 2: Advantages, clauses of ISO 9000 Unit 3: Implementation of ISO 9000 Unit 4: Quality costs, quality, auditing, case studies

BLOCK 5

Implementation of TQM

Unit 1: Steps, KAIZEN Unit 2: 5s, JIT Unit 3: POKAYOKE, Taguchi methods Unit 4: Case studies

Books:
1. Rose J. E., Total quality Management, Kogan Page Ltd 2. Bank, J., The essence of Total Quality Management, Prentice Hall of India 3. Bonds, G., Beyond Total Quality Management, McGraw Hill

ELECTIVE Subject Code : CME011 Subject Title : Safety and Hazard Control Structure of the Course Content BLOCK 1 Basic Concept of Safety
Unit 1: Conventional and modern concepts of safety Unit 2: Basic Principles and concepts in hazard identification, Chemical hazards Unit 3: Process and operation hazard, Hazards from utilities like air, water, steam Unit 4: Occupational health hazards, Hazard and operability Studies, Safety Audits

BLOCK 2 Accident Analysis

Unit 1: Past Accident Analysis Unit 2: Consequence Analysis of fire, gas/vapour Unit 3: Dispersions and explosion, Vulnerability models Unit 4: Fault and Event Tree Analysis

BLOCK 3 Risk Assessments

Unit 1: Introduction to Risk Assessment Unit 2: Safety in plant design and layout Unit 3: Risk Assessment Unit 4: Case Studies

BLOCK 4

Safety Measures

Unit 1: Safety measures in handling and storage of chemicals Unit 2: Process plant Unit 3: Personnel Protection Unit 4: First Aid

BLOCK 5

Emergency Plans

Unit 1: Need of Emergency Plans Unit 2: Disaster mitigation Unit 3: Emergency Preparedness plans Unit 4: Case Studies

Books:
1.Well, G.S Safety Process Plants Design, George Godwin Ltd., London, John Wilelys and Sons, New York 2. Safety in Chemical and Petrochemical Industries, Report of the Inter Ministry Group, Dept. of Chemicals and Petrochemicals, Govt.of India, ICMA Publications. 3. Major Hazard Control, Manual by International Labour Organization, Geneva

ELECTIVE Subject Code : CME012 Subject Title : Polymer Technology Structure of the Course Content BLOCK 1 Introduction to Polymer Processing Methods
Unit 1: Introduction to Polymer Technology Unit 2: Introduction to various Polymer Processing methods Unit 3: Machinery Morphology Unit 4: Structure of Polymers

BLOCK 2

Channel Models

Unit 1: Screw Extrusion Geometry of screw Simplified Flat plate Model Unit 2: Rectangular channel model; cylindrical Channel Model Unit 3: Helical Channel Model; Newtonian and Non-Newtonian flows Unit 4: Isothermal, non-isothermal and adiabatic Models

BLOCK 3

Moulding Process

Unit 1: Injection Moulding Unit 2: Various parts of the moulds Unit 3: Analysis of flow through mould Cavity Unit 4: Various Models; Balancing of runners

BLOCK 4

Mixing Operations

Unit 1: Newtonian and non-Newtonian models Unit 2: Calendar fed with finite sheet Unit 3: Normal stress and viscosity effects Unit 4: oating Mixing operations

BLOCK 5

Expert Systems

Unit 1: Modelling of Polymer Process Unit 2: Advanced Process in Polymer Technology Unit 3: Knowledge based expert systems for modeling of polymer processing Unit 4: Case Studies

Books:
1. Agassant, J.F. Avenas, P, Sergant, J,Ph., and Correon, P.J. Polymer Porcessing Carl Hamsen Verlag Munich 2.Tucker C.L, Fundamentals of Computer Modelling for Polymer Processing, Carl Hamsen Verlag, Munich