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  • Lampiran B Asetan

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    Ryan Wahyudi
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    The document contains calculations for the synthesis of acetanilide. It first calculates the moles and masses of the reactants: aniline (0.0463 mol), acetic acid (0.0299 mol), and acetic anhydride (3.564 g). It then shows the balanced chemical reaction and calculates that 0.0299 mol of acetanilide is produced with a molar mass of 135.16 g/mol, giving a theoretical yield of 4.041284 g. The actual yield from synthesis was 4.138 g and after recrystallization was 1.213 g, giving a percent yield of 70.68% and efficiency of 69.98%.

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    Lampiran b Asetan

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    The document contains calculations for the synthesis of acetanilide. It first calculates the moles and masses of the reactants: aniline (0.0463 mol), acetic acid (0.0299 mol), and acetic anhydride (3.564 g). It then shows the balanced chemical reaction and calculates that 0.0299 mol of acetanilide is produced with a molar mass of 135.16 g/mol, giving a theoretical yield of 4.041284 g. The actual yield from synthesis was 4.138 g and after recrystallization was 1.213 g, giving a percent yield of 70.68% and efficiency of 69.98%.

    Copyright:

    © All Rights Reserved
    Scarica in formato DOCX, PDF, TXT o leggi online su Scribd
    Segnala contenuti inappropriati
    10 visualizzazioni3 pagine

    Lampiran B Asetan

    Caricato da

    Ryan Wahyudi
    The document contains calculations for the synthesis of acetanilide. It first calculates the moles and masses of the reactants: aniline (0.0463 mol), acetic acid (0.0299 mol), and acetic anhydride (3.564 g). It then shows the balanced chemical reaction and calculates that 0.0299 mol of acetanilide is produced with a molar mass of 135.16 g/mol, giving a theoretical yield of 4.041284 g. The actual yield from synthesis was 4.138 g and after recrystallization was 1.213 g, giving a percent yield of 70.68% and efficiency of 69.98%.

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    di 3

    LAMPIRAN B

    HASIL PERHITUNGAN

    1. Perhitungan Bahan Baku


    a) Anilin
    i.

    Volume

    = 2,73 ml

    ii.

    Mr

    = 93,13 gr/mol

    iii.

    = 1,02 gr/ml

    iv.

    Massa (m)

    = Vx
    = 2,73 x 93,13

    v.

    Mol (n)

    = 4,3134 gr
    = -m
    Mr
    = 4,3134
    93,13
    = 0,0463 mol

    b) Asam asetat glasial


    i.

    Volume

    = 1,73 ml

    ii.

    Mr

    = 60,05 gr/mol

    iii.

    = 1,049 gr,ml

    iv.

    Massa (m)

    = Vx
    = 1,73 x 1,049

    v.

    Mol (n)

    = 1, 81477 gr
    = m
    Mr
    = 21,84177
    60,05
    = 0,0299 mol

    c) Asetat anhidrat
    i. Volume

    = 3,3 ml

    ii.

    Mr

    = 102 gr/mol

    iii.

    = 1,08 gr/ml

    iv.

    Massa (m)

    = Vx
    = 3,3 x 1,08
    = 3,564 gram

    2. Perhitungan Mol dan Massa Asetanilida


    C6H5NH2 + CH3COOH
    M
    B
    S

    0,0463
    0,0299
    0,0164

    CH3COC6H5NH + H2O

    0,0299
    0,0299

    n Asetanila
    Mr Asetanilida

    0,0299
    0,0299

    = 0,0299 mol
    = 135,16 gr/mol

    Massa (m) = n x Mr
    = 0,0299 x 135,16
    = 4,041284 gram
    3. Perhitungan Rendemen
    Berat sintesis
    = 4,138 gr
    Berat rekristalisasi = 1,213 gr

    100

    Percent yield = sintesis rekristalisasi


    sintesis
    =

    4,138 1,213
    4,138
    = 70,68%
    Efisiensi

    100

    teoritis percobaan
    teoritis

    100

    0,0299
    0,0299

    4,041284 1,213
    4,041284

    = 69,98%

    100

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