Shealy Environmental Services, Inc.

Document Number: F-IN-016

Revision Number: 0

Page 1 of 2
Replaces Date: NA
Effective Date: 01/15/02

CHLORIDE

EPA Method 325.3

Date: __________________

Start Time: _________

Mixed Indicator ID: ____________________

End Time: _________ Analyst: ____________

0.3% HNO3 ID: ____________________

0.25N NaOH ID: ______________________

Spike information: 50 mL of sample plus 5.0 mL of 500 mg/L Chloride stock (ID _____________________________) = 45.4 mg/L spike.
Normality of Mercuric Nitrate Titrant (ID ____________________________) = ______________ N

Sample / Standard
ID

Standard
Conc.
(mg/L)

Sample
Volume
(mL)

Final
Volume
(mL)

Dilution
Factor

Start
Titrant
Reading
(mL)

Finish
Titrant
Reading
(mL)

CHLORIDE

EPA Method 325.3

Total
Titrant
Volume
(mL)

Chloride
(mg/L)

QC

Comments

Shealy Environmental Services, Inc.

Document Number: F-IN-016
Revision Number: 0

Page 2 of 2
Replaces Date: NA
Effective Date: 01/15/02

Date: _________________________

Sample / Standard
ID

Standard
Conc.
(mg/L)

Analyst: __________
Sample
Volume
(mL)

Final
Volume
(mL)

Dilution
Factor

Start
Titrant
Reading
(mL)

Finish
Titrant
Reading
(mL)

Total
Titrant
Volume
(mL)

Chloride
(mg/L)

QC

Comments