0

5.14204579
6.64606009
8.15007439
9.65408869
11.15810299
12.66211729
14.16613159
15.67014589
17.17416019
18.67817449
20.18218879
21.68620309
23.19021739
24.69423169
26.19824599
27.70226029
29.20627459
30.71028889
32.21430319
33.71831749
35.22233179
36.72634609
38.23036039
39.73437469
41.23838899
42.74240329
44.24641759
45.75043189
47.25444619
48.75846049
50.26247479
51.76648909
53.27050339
54.77451769
56.27853199
57.78254629
59.28656059
60.79057489
62.29458919
63.79860349
65.30261779
66.80663209
68.31064639
69.81466069
71.31867499
72.82268929
74.32670359
75.83071789
77.33473219
78.83874649

Spettri XRD

2500

2000

1500

1000

500

unweathered
weathered
weathered2
weathered3

5.00835563
5.02506690
5.04177817
5.05848944
5.07520071
5.09191198
5.10862325
5.12533452
5.14204579
5.15875706
5.17546833
5.19217960
5.20889087
5.22560214
5.24231341
5.25902468
5.27573595
5.29244722
5.30915849
5.32586976
5.34258103
5.35929230
5.37600357
5.39271484
5.40942611
5.42613738
5.44284865
5.45955992
5.47627119
5.49298246
5.50969373
5.52640500
5.54311627
5.55982754
5.57653881
5.59325008
5.60996135
5.62667262
5.64338389
5.66009516
5.67680643
5.69351770
5.71022897
5.72694024
5.74365151
5.76036278
5.77707405
5.79378532
5.81049659
5.82720786
5.84391913
5.86063040
5.87734167

unweathered weathered weathered2 weathered3

1096
1061
962
1002
1102
1100
982
1037
1095
1144
1031
1001
1012
1105
997
1009
1037
1092
1067
998
1029
1076
949
1050
1017
1140
984
1041
992
1133
926
954
1038
1039
1022
1070
1073
1068
979
1062
1081
1079
992
1025
1039
1081
1015
1023
1068
1068
980
970
1105
1078
993
1014
1024
1111
991
1047
1017
1133
989
1064
1100
1080
957
1017
1022
1054
1029
1012
1050
1061
976
1035
1042
1066
941
1001
1030
1079
1008
1036
986
1109
974
1057
1025
1101
1004
991
1041
1061
1012
1045
1053
1064
919
915
1068
1051
992
1050
1029
1125
999
988
986
1143
1028
1005
1002
1090
957
1021
1000
1021
1032
1005
996
983
985
1062
1019
1008
926
933
1022
1066
962
959
1028
1063
1002
1012
1013
998
886
1022
1035
1107
938
988
1004
1008
923
984
1018
1044
1001
974
992
1021
1013
1040
1037
1078
983
986
999
1016
918
977
1008
973
971
965
1010
1049
913
971
997
1068
1001
954
1022
1030
967
1003
954
1010
945
1009
1000
1008
962
1024
956
967
956
952
1026
988
915
944
1016
1084
859
950
1061
1015
924
959
992
1087
992
967
1040
1016
906
962

5.89405294
5.91076421
5.92747548
5.94418675
5.96089802
5.97760929
5.99432056
6.01103183
6.02774310
6.04445437
6.06116564
6.07787691
6.09458818
6.11129945
6.12801072
6.14472199
6.16143326
6.17814453
6.19485580
6.21156707
6.22827834
6.24498961
6.26170088
6.27841215
6.29512342
6.31183469
6.32854596
6.34525723
6.36196850
6.37867977
6.39539104
6.41210231
6.42881358
6.44552485
6.46223612
6.47894739
6.49565866
6.51236993
6.52908120
6.54579247
6.56250374
6.57921501
6.59592628
6.61263755
6.62934882
6.64606009
6.66277136
6.67948263
6.69619390
6.71290517
6.72961644
6.74632771
6.76303898
6.77975025

1043
1025
971
1004
1006
1008
1021
940
1010
954
970
959
991
1008
949
971
978
1022
1002
983
978
979
952
960
1015
962
936
912
967
901
931
951
926
924
940
902
824
884
952
923
941
924
970
924
914
944
850
911
938
977
879
892
921
920

1026
1022
1018
1016
1038
982
942
972
967
1029
1036
985
967
961
986
974
986
1001
983
940
993
972
990
992
1001
1002
921
1011
949
947
948
985
987
950
973
979
1009
992
1000
925
969
948
1010
895
960
954
926
932
947
940
949
916
971
927

957
977
946
903
910
922
983
879
931
872
944
916
1023
924
950
900
867
949
932
927
871
885
882
875
898
829
867
919
890
892
841
858
880
897
906
895
868
893
874
875
819
899
855
853
919
892
842
843
896
922
860
863
895
848

918
906
902
925
954
971
992
954
967
967
960
980
985
921
1005
880
916
925
940
924
967
923
915
964
912
921
941
977
899
983
864
978
990
913
979
933
921
949
921
938
889
907
896
906
894
840
929
934
890
877
877
928
893
894

6.79646152
6.81317279
6.82988406
6.84659533
6.86330660
6.88001787
6.89672914
6.91344041
6.93015168
6.94686295
6.96357422
6.98028549
6.99699676
7.01370803
7.03041930
7.04713057
7.06384184
7.08055311
7.09726438
7.11397565
7.13068692
7.14739819
7.16410946
7.18082073
7.19753200
7.21424327
7.23095454
7.24766581
7.26437708
7.28108835
7.29779962
7.31451089
7.33122216
7.34793343
7.36464470
7.38135597
7.39806724
7.41477851
7.43148978
7.44820105
7.46491232
7.48162359
7.49833486
7.51504613
7.53175740
7.54846867
7.56517994
7.58189121
7.59860248
7.61531375
7.63202502
7.64873629
7.66544756
7.68215883

900
833
885
819
889
908
845
915
881
913
895
874
903
901
900
850
898
912
888
862
825
896
900
870
838
861
874
893
892
842
846
840
871
823
838
866
830
843
842
884
844
822
859
854
802
789
864
860
829
847
827
856
804
798

841
864
909
874
906
902
919
889
910
890
897
902
912
906
967
945
902
896
887
862
885
835
948
815
854
901
870
890
926
890
820
849
825
849
870
876
855
880
857
887
803
794
860
876
872
847
907
888
836
803
877
889
870
834

899
845
871
914
869
876
874
806
848
802
816
899
798
856
884
868
833
884
844
812
850
890
856
849
869
828
844
816
841
863
854
866
867
810
778
797
797
832
787
820
803
831
819
811
846
842
790
804
824
820
792
779
745
750

939
922
861
876
951
934
941
881
926
853
876
875
903
909
918
876
793
893
846
872
811
879
864
864
876
915
916
821
860
841
867
907
861
892
872
915
834
869
830
887
856
821
875
897
843
868
833
819
916
879
795
862
791
828

7.69887010
7.71558137
7.73229264
7.74900391
7.76571518
7.78242645
7.79913772
7.81584899
7.83256026
7.84927153
7.86598280
7.88269407
7.89940534
7.91611661
7.93282788
7.94953915
7.96625042
7.98296169
7.99967296
8.01638423
8.03309550
8.04980677
8.06651804
8.08322931
8.09994058
8.11665185
8.13336312
8.15007439
8.16678566
8.18349693
8.20020820
8.21691947
8.23363074
8.25034201
8.26705328
8.28376455
8.30047582
8.31718709
8.33389836
8.35060963
8.36732090
8.38403217
8.40074344
8.41745471
8.43416598
8.45087725
8.46758852
8.48429979
8.50101106
8.51772233
8.53443360
8.55114487
8.56785614
8.58456741

833
759
796
828
771
862
820
845
790
806
808
844
819
829
812
785
814
771
820
805
831
843
782
755
812
823
853
804
817
776
752
774
848
798
769
815
802
789
817
779
778
803
770
810
789
741
774
796
837
821
785
733
801
781

861
861
819
876
831
823
861
774
836
811
819
790
789
844
803
764
834
786
832
881
803
842
758
882
850
843
840
831
834
815
828
838
837
854
743
799
796
734
769
793
842
754
819
790
843
799
841
799
785
911
781
822
804
820

764
766
805
845
837
776
777
845
811
771
829
770
789
761
847
809
780
765
801
784
814
818
810
809
776
743
849
799
725
794
793
793
735
767
796
827
787
794
780
818
746
783
763
785
721
733
740
787
733
789
714
745
747
768

862
889
901
833
874
801
806
868
874
877
854
781
838
836
802
858
896
815
805
792
754
816
818
866
820
861
833
818
793
802
816
847
767
831
808
785
816
824
828
764
801
803
781
881
756
816
808
838
794
840
837
822
831
799

8.60127868
8.61798995
8.63470122
8.65141249
8.66812376
8.68483503
8.70154630
8.71825757
8.73496884
8.75168011
8.76839138
8.78510265
8.80181392
8.81852519
8.83523646
8.85194773
8.86865900
8.88537027
8.90208154
8.91879281
8.93550408
8.95221535
8.96892662
8.98563789
9.00234916
9.01906043
9.03577170
9.05248297
9.06919424
9.08590551
9.10261678
9.11932805
9.13603932
9.15275059
9.16946186
9.18617313
9.20288440
9.21959567
9.23630694
9.25301821
9.26972948
9.28644075
9.30315202
9.31986329
9.33657456
9.35328583
9.36999710
9.38670837
9.40341964
9.42013091
9.43684218
9.45355345
9.47026472
9.48697599

781
770
815
802
757
776
802
747
779
819
760
828
769
809
805
757
802
812
789
768
793
784
780
769
753
819
771
793
761
767
765
766
770
774
805
811
776
776
789
802
824
799
747
769
751
756
712
764
761
760
795
738
737
750

778
782
804
780
845
791
806
764
809
746
782
807
765
754
719
782
747
801
776
747
769
767
792
805
725
744
779
765
704
728
760
794
787
746
753
728
770
771
760
754
712
823
759
733
770
742
758
753
720
753
729
771
787
706

731
711
734
767
760
785
768
753
760
704
791
677
681
730
778
716
753
713
740
778
744
776
778
754
748
765
714
706
769
715
729
756
719
748
718
727
675
705
741
719
672
716
690
688
722
748
718
721
748
667
680
726
712
702

752
808
797
804
795
756
787
808
720
795
835
787
774
766
776
784
823
796
811
787
751
738
782
780
765
780
764
743
781
741
821
776
759
766
808
752
742
785
741
765
750
790
748
739
797
786
751
751
754
806
773
681
771
729

9.50368726
9.52039853
9.53710980
9.55382107
9.57053234
9.58724361
9.60395488
9.62066615
9.63737742
9.65408869
9.67079996
9.68751123
9.70422250
9.72093377
9.73764504
9.75435631
9.77106758
9.78777885
9.80449012
9.82120139
9.83791266
9.85462393
9.87133520
9.88804647
9.90475774
9.92146901
9.93818028
9.95489155
9.97160282
9.98831409
10.00502536
10.02173663
10.03844790
10.05515917
10.07187044
10.08858171
10.10529298
10.12200425
10.13871552
10.15542679
10.17213806
10.18884933
10.20556060
10.22227187
10.23898314
10.25569441
10.27240568
10.28911695
10.30582822
10.32253949
10.33925076
10.35596203
10.37267330
10.38938457

734
810
760
745
730
729
756
744
737
741
774
772
757
738
774
803
737
715
760
765
744
721
748
815
741
773
771
701
735
716
748
755
756
677
722
729
745
706
767
759
760
742
758
746
747
735
714
756
755
750
721
726
786
709

732
759
766
726
758
740
739
763
727
742
759
706
744
717
730
759
715
709
715
746
758
709
738
712
724
789
744
708
716
691
727
673
722
694
747
734
703
738
717
696
705
708
730
765
693
673
713
745
718
758
721
722
704
669

685
746
731
816
715
730
694
685
688
741
704
731
706
750
724
668
753
747
718
674
734
661
686
680
727
680
681
743
680
703
691
717
679
683
679
666
694
675
688
641
728
708
701
628
666
729
646
655
699
680
663
668
653
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783
772
769
742
766
727
768
694
728
772
798
714
751
741
726
750
750
765
709
682
722
700
694
801
768
726
730
718
773
746
753
679
688
718
776
734
739
693
752
774
743
732
720
714
718
720
693
758
772
713
664
708
772
755

10.40609584
10.42280711
10.43951838
10.45622965
10.47294092
10.48965219
10.50636346
10.52307473
10.53978600
10.55649727
10.57320854
10.58991981
10.60663108
10.62334235
10.64005362
10.65676489
10.67347616
10.69018743
10.70689870
10.72360997
10.74032124
10.75703251
10.77374378
10.79045505
10.80716632
10.82387759
10.84058886
10.85730013
10.87401140
10.89072267
10.90743394
10.92414521
10.94085648
10.95756775
10.97427902
10.99099029
11.00770156
11.02441283
11.04112410
11.05783537
11.07454664
11.09125791
11.10796918
11.12468045
11.14139172
11.15810299
11.17481426
11.19152553
11.20823680
11.22494807
11.24165934
11.25837061
11.27508188
11.29179315

765
732
734
691
733
727
767
730
729
708
725
700
716
711
714
742
756
755
753
714
728
772
757
760
734
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722
783
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719
763
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660
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675
675
685
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719
652
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732
657
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727
694
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647
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711
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662
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698
724
731
652
660
740
718
683
717
760
708
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657
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679
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726
720
646
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693
704
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731
666
738
701
676
693
704
691
772
741
796
704

664
729
683
692
636
686
670
663
692
663
682
691
674
754
664
567
679
644
676
669
652
680
682
689
640
669
660
667
706
628
668
685
687
630
673
696
681
655
681
700
663
699
630
701
655
686
663
649
694
664
647
674
675
674

713
685
733
757
734
713
737
725
694
729
715
692
694
660
692
720
665
679
714
700
669
712
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25.74704170
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900
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26.64945028
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27.55185886
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999
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28.45426744
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29.35667602
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30.25908460
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763
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31.16149318
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32.96631034
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33.86871892
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34.77112750
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35.67353608
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36.57594466
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