Puaker Chemical
India Limited
CONCENTRATION DETERMINATION OF METALWORKING
FLUID EMULSIONS BY INDICATOR BASED TITRIMETRIC
METHOD
Qusk India Test Method Number: QLTM PI 0044.(03/08)
“1. Scope
1.1 The concentration ofa metalworking Audis one ofthe most important parameter
wich needs fo be maintanod for realizing the optimum product performance,
‘This metho describes a simple way to determine the concentration of an
‘emulsion of produets containing alkaline constituents,
2. Summary
2.4 The emulsion sample is tiated with Soltion-A using Solution indicator (end
point givos prmanest rose red coloration which doesnot change with an
‘ditions! drop of Solution-A) The conceatratin is calculated by dividing the
volume of Solution-A by a known factor (specific fora particular product)
3. Apparatus.
3.1 2m Syringes ~7 nos, (accurate up to 0.1 ml subdivision)
32 Som| Beaker
4. Chemi
4.1 Solution-A : (0.2 N HCI solution)
442 Solution : (0.1 gm Methyl red & 0.02 gm Bromocresol green in 100 mi
‘hano,)
5. Proce
5.1 ‘Take 2mi. of emulsion sample (using a syringe ; ensure the liquide fee fom ‘
any bubbles) nto a $0'ml beaker, Addl four 4 drops of Solution 1 into it. The