DATA HASIL PENGAMATAN

TOTAL REFLUX
m piknometer (g)
m larutan (g)
volume larutan (ml)
rho awal
fraksi awal

19.45
27.37
10
0.792
0.082700022

waktu (menit) T Celcius

10
66
20
72
30
77

REFLUX 50 %
m piknometer (g)
m larutan (g)
volume larutan (ml)
rho awal
fraksi awal

19.45
27.46
10
0.801
0.059767168

waktu (menit) T Celcius

10
68
20
75
30
78

REFLUX 40%
m piknometer (g)
m larutan (g)
volume larutan (ml)
rho awal
fraksi awal

19.45
27.46
10
0.801
0.059767168

waktu (menit) T Celcius

10
70
20
76
30
79

REFLUX 33%
m piknometer (g)
m larutan (g)
volume larutan (ml)
rho awal
fraksi awal

19.45
27.51
10
0.806
0.047651652

waktu (menit) T Celcius

10
70
20
76
30
79

diameter tabung (mm)

jari-jari
luas alas
1 mm3=0.001ml
1ml=1000mm3

155
77.5
18859.625

vd (mm)

Vd (mm3)
Vd(ml)
m top
rho top
13 245175.125 245.175125
25.99
0.654
16
301754
301.754
25.97
0.652
16
301754
301.754
26.1
0.665

xd
m bottom
0.86206621
27.42
0.88260192
27.47
0.75529159
27.48

vd (mm)

Vd (mm3)
13 245175.125
19 358332.875
37 697806.125

vd (mm)

Vd (mm3)
Vd(ml)
m top
rho top
xd
m bottom
13 245175.125 245.175125
26.75
0.73 0.30674034
27.43
20
377192.5
377.1925
26.67
0.722 0.3475907
27.45
37 697806.125 697.806125
26.71
0.726 0.32673986
27.52

vd (mm)

Vd (mm3)
Vd(ml)
m top
rho top
10 188596.25 188.59625
26.63
0.718
20
377192.5
377.1925
26.61
0.716
35 660086.875 660.086875
26.66
0.721

Vd(ml)
m top
rho top
xd
m bottom
245.175125
26.41
0.696 0.50599299
27.43
358.332875
26.41
0.696 0.50599299
27.48
697.806125
26.54
0.709 0.4216065
27.5

xd
m bottom
0.36932356
27.5
0.38053035
27.48
0.35294003
27.51

0
0
rho bottom
0.797
0.802
0.803

xb
tray teori
efisiensi
0.06976659
0.05731155
0.05487267
2 22.2222222

rho bottom xb
tray teori
efisiensi
0.798 0.06723923
0.803 0.05487267
0.805 0.0500432
1 11.1111111

rho bottom xb
tray teori
efisiensi
0.798 0.06723923
0.8
0.06224
0.807 0.04527492
1 11.1111111

rho bottom xb
tray teori
efisiensi
0.805 0.0500432
0.803 0.05487267
0.806 0.04765165
1 11.1111111

1
1

0.64
0.65
0.66
0.67
0.68
0.69
0.7
0.71
0.72
0.73
0.74
0.75
0.76
0.77
0.78
0.79
0.8
0.81
0.82

y
1.01340288
0.9034925
0.80254992
0.71009526
0.62564864
0.54873018
0.47886
0.41555822
0.35834496
0.30674034
0.26026448
0.2184375
0.18077952
0.14681066
0.11605104
0.08802078
0.06224
0.03822882
0.01550736

1
0.9
0.8
0.7
Fraksi Mol Aseton

0.6
0.5
0.4
0.3
0.2
0.1
0
0.64

0.66

0.68

0.7

0.72
Densitas (g/ml)

y = -79.98x3 + 200.8x2 - 170.2x + 48.66

Series1
Poly. (Series1)

0.72

0.74
Densitas (g/ml)

0.76

0.78

0.8

0.82

0.84

waktu (menit)T Celcius

Vd (ml)
10
66
20
72
30
77

m top

waktu (menit)T Celcius

Vd (ml)
10
68
20
75
30
78

m top

waktu (menit)T Celcius

Vd (ml)
10
70
20
76
30
79

m top

waktu (menit)T Celcius

Vd (ml)
10
70
20
76
30
79

m top

25.99
25.97
26.46

rho top
0.654
0.652
0.701

xd
m bottom
0.86206621
27.42
0.88260192
27.47
0.47224216
27.48

rho top
xd
m bottom
26.41
0.696 0.50599299
27.43
26.41
0.696 0.50599299
27.48
26.54
0.709 0.4216065
27.5

rho top
26.75
26.67
26.71

xd
m bottom
0.73 0.30674034
27.43
0.722 0.3475907
27.45
0.726 0.32673986
27.52

rho top
26.63
0.718
26.61
0.716
26.66
0.721

xd
m bottom
0.36932357
27.5
0.38053035
27.48
0.35294003
27.51

rho bottom
0.797
0.802
0.803

xb
0.06976659
0.05731155
0.05487267

rho bottom xb
0.798 0.06723923
0.803 0.05487267
0.805 0.0500432

Fraksi Mol Aseton Distilat

0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0

rho bottom xb
0.798 0.06723923
0.8
0.06224
0.807 0.04527492

10

15

20

25

30

35

Waktu (menit)

0.08

Fraksi Mol Aseton Bottom

0.07

rho bottom xb
0.805 0.0500432
0.803 0.05487267
0.806 0.04765165

0.06
0.05
0.04
0.03
0.02
0.01
0
5

10

15

20
Waktu (menit)

25

30

35

Total Reflux
Reflux 50%
Reflux 40%
Reflux 33%

Total Reflux
Reflux 50%
Reflux 40%
Reflux 33%

0.00

100.00

0.00

0.00

91.15

0.01

0.28

1.00
0.90

Total Reflux

1.00

Total Reflux
85.09

0.02

0.44

80.78

0.03

0.53

77.60

0.04

0.59

75.18

0.05

0.63

73.30

0.06

0.66

71.80

0.07

0.68

70.58

0.08

0.70

69.58

0.09

0.71

68.74

0.10

0.73

68.03

0.11

0.74

67.42

0.12

0.74

66.89

0.13

0.75

66.43

0.14

0.76

66.03

0.15

0.76

65.66

0.16

0.77

65.34

0.17

0.77

65.05

0.18

0.77

64.78

0.19

0.78

64.54

0.20

0.78

64.32

0.21

0.78

64.11

0.22

0.78

63.92

0.23

0.79

63.74

0.24

0.79

63.57

0.25

0.79

63.41

0.26

0.79

63.26

0.27

0.80

63.11

0.28

0.80

62.98

0.29

0.80

0.90
0.80
0.70
0.60

VLE ACETONE-WATER
0.50

GARIS LINIER
GARIS OPERASI

0.40

FRAKSI DISTILAT
FRAKSI BOTTOM

0.30
0.20

0.10
0.00
0.00

1.00
0.90
0.80

0.20

0.40

0.60

0.80

Reflux 50%

1.00

0.80

62.84

0.30

0.80

62.72

0.31

0.80

62.59

0.32

0.80

62.47

0.33

0.81

62.36

0.34

0.81

62.25

0.35

0.81

62.14

0.36

0.81

62.03

0.37

0.81

61.92

0.38

0.81

61.82

0.39

0.81

61.72

0.40

0.82

61.61

0.41

0.82

61.51

0.42

0.82

61.42

0.43

0.82

61.32

0.44

0.82

61.22

0.45

0.82

61.12

0.46

0.82

61.03

0.47

0.83

60.93

0.48

0.83

60.84

0.49

0.83

60.74

0.50

0.83

60.65

0.51

0.83

60.55

0.52

0.83

60.46

0.53

0.84

60.37

0.54

0.84

60.27

0.55

0.84

60.18

0.56

0.84

60.09

0.57

0.84

0.70
0.60
0.50

Series1
Series2

0.40

Series3
Series4

0.30

Series5
0.20
0.10
0.00
0.00

0.20

0.40

0.60

0.80

1.00

59.99

0.58

0.84

59.90

0.59

0.85

59.80

0.60

0.85

59.71

0.61

0.85

59.62

0.62

0.85

59.52

0.63

0.85

59.43

0.64

0.86

59.33

0.65

0.86

59.24

0.66

0.86

59.14

0.67

0.86

59.05

0.68

0.86

58.95

0.69

0.87

58.86

0.70

0.87

58.76

0.71

0.87

58.67

0.72

0.87

58.57

0.73

0.88

58.48

0.74

0.88

58.38

0.75

0.88

58.28

0.76

0.88

58.19

0.77

0.89

58.09

0.78

0.89

58.00

0.79

0.89

57.90

0.80

0.90

57.81

0.81

0.90

57.72

0.82

0.90

57.62

0.83

0.91

57.53

0.84

0.91

57.44

0.85

0.91

57.35

0.86

0.92

57.26

0.87

0.92

57.17

0.88

0.93

57.08

0.89

0.93

57.00

0.90

0.94

56.91

0.91

0.94

56.83

0.92

0.95

56.75

0.93

0.95

56.68

0.94

0.96

56.60

0.95

0.96

56.53

0.96

0.97

56.47

0.97

0.98

56.41

0.98

0.98

56.35

0.99

0.99

56.30

1.00

1.00

y=(1/3)x+(0.422/1.5)
x
y
0
0.373
0.746
0.746

0.00 xd

xb
1.00 0.86206621 0.06976659
0.88260192 0.05731155

y=0.5x+0.236
x
y
0 0.3776458
0.75529159 0.75529159

0.75529159 0.75529159
0.75529159
0

0.75529159 0.05487267

xd
xb
0.50599299 0.06723923
0.50599299 0.05487267
0.4216065 0.0500432

xd
xb
0.30674034 0.06723923
0.3475907
0.06224
0.32673986 0.04527492

xd
xb
0.36932357 0.0500432
0.38053035 0.05487267
0.35294003 0.04765165
1.00
0.90
0.80
0.70

y=(1/3)x+(0.422/1.5)
x
y
0
0.281071
0.4216065 0.4216065

0.4216065
0.4216065

0.4216065
0

y=(0.4/1.4)x+0.326/1.4
x
y
0 0.23338562
0.32673986 0.32673986

0.32673986 0.32673986
0.32673986
0

y=(0.33/1.33)x+(0.353/1.33)
x
y
0 0.26536844
0.35294003 0.35294003

0.35294003 0.35294003
0.35294003
0

Reflux 40%

1.00
0.90
0.80
0.70

0.70

0.70

0.60

0.60
Series1

0.50
0.40

Series2

0.40

Series3

0.30

0.30

Series4

0.20

Series5

0.10

0.50

0.20
0.10
0.00

0.00

0.00
0.00

0.20

0.40

0.60

0.80

1.00

1.00

Total Reflux (contoh pake data di modul)

0.90
0.80

0.70
0.60
0.50

Series1
Series2

0.40

Series3
0.30
0.20

0.10
0.00
0.00

0.20

0.05487267 0.05487267
0.05487267
0

0.40

0.60

0.80

1.00

0.0500432
0.0500432

0.0500432
0

0.04527492 0.04527492
0.04527492
0

0.04765165 0.04765165
0.04765165
0

reflux 33%

Series1
Series2
Series3
Series4
Series5

0.20

0.40

0.60

0.80

1.00

DATA HASIL PENGAMATAN

TOTAL REFLUX
m piknometer (g)
19.45 waktu (menit)xb
m larutan (g)
27.37
10 0.06976659
volume larutan (ml)
10
20 0.05731155
rho awal
0.792
30 0.05487267
fraksi awal
0.08270002

Laju alir molar uap

0.00258669
0.00249101
0.00048778

REFLUX 50 %
m piknometer (g)
19.45 waktu (menit)xb
m larutan (g)
27.46
10 0.06723923 -0.0011208
volume larutan (ml)
10
20 0.05487267 0.00185498
rho awal
0.801
30 0.0500432 0.00072442
fraksi awal
0.05976717
REFLUX 40%
m piknometer (g)
19.45 waktu (menit)xb
m larutan (g)
27.46
10 0.06723923
volume larutan (ml)
10
20
0.06224
rho awal
0.801
30 0.04527492
fraksi awal
0.05976717

Laju alir molar uap

-0.0010461
0.00069989
0.00237511

REFLUX 33%
m piknometer (g)
19.45 waktu (menit)xb
Laju alir molar uap
m larutan (g)
27.51
10 0.0500432 -0.0003181
volume larutan (ml)
10
20 0.05487267 -0.0006423
rho awal
0.806
30 0.04765165 0.0009604
fraksi awal
0.04765165

0.003
0.0025
0.002
0.0015

Series1

0.001

Series2

0.0005

Series3
Series4

0
-0.0005
-0.001
-0.0015

10

15

20

25

30

35

waktu (menit)Vd(ml)
10 245.175125
20
301.754
30
301.754
40
245.18

800
y = -0.2829x2 + 14.145x + 132.02
R = 1

700

y = 1.1316x2 - 22.632x + 358.33

R = 1
600

waktu (menit)Vd(ml)
10 245.175125
20 358.332875
30 697.806125
40
1263.61

y = 0.943x2 - 15.088x + 301.75

R = 1

500

y = 0.4715x2 + 4.7149x + 94.298

R = 1

400

300

waktu (menit)Vd(ml)
10 245.175125
20
377.1925
30 697.806125
40
1207.03

waktu (menit)Vd(ml)
10 188.59625
20
377.1925
30 660.086875
40
1037.294

200

100

0
10

15

+ 14.145x + 132.02
R = 1
22.632x + 358.33
R = 1
15.088x + 301.75

Total Reflux
Reflux 50%
Reflux 40%

+ 4.7149x + 94.298
R = 1

Reflux 33%
Poly. (Total Reflux)
Poly. (Reflux 50%)
Poly. (Reflux 40%)
Poly. (Reflux 33%)

20

25

30

t
329.4
331.4
333.4
335.4
337.4
339.4
341.4
343.4
345.4
347.4
349.4
351.4
353.4
355.4
357.4
359.4
361.4
363.4
365.4
367.4
369.4
371.4
373.4

pa
758.750333
811.995178
868.184322
927.432466
989.856509
1055.57551
1124.71065
1197.38518
1273.72441
1353.85563
1437.90809
1526.01296
1618.30324
1714.91376
1815.98111
1921.64359
2032.04113
2147.31531
2267.60923
2393.06748
2523.8361
2660.06251
2801.89545

pb
125.311194
137.724688
151.168926
165.711981
181.425138
198.382975
216.663433
236.347894
257.521254
280.271989
304.692228
330.877819
358.928389
388.947413
421.042268
455.324295
491.908851
530.915363
572.467376
616.692605
663.722975
713.694663
766.74814

x
1
0.92288677
0.84911855
0.78019173
0.71567592
0.65518189
0.59835718
0.5448822
0.49446682
0.44684736
0.4017838
0.35905745
0.31846881
0.2798356
0.24299111
0.20778265
0.17407021
0.14172522
0.11062946
0.08067407
0.05175869
0.02379064
0

y
1
0.98602579
0.9699887
0.95207255
0.93212693
0.90999205
0.88549827
0.85846561
0.82870324
0.79600896
0.76016865
0.7209557
0.67813041
0.63143937
0.58061481
0.52537394
0.46541819
0.40043254
0.33008471
0.25402434
0.17188218
0.0832692
0

alfa
6.05492859
5.89578522
5.74314011
5.59665307
5.45600526
5.32089767
5.19104969
5.06619779
4.9460943
4.83050637
4.71921486
4.61201347
4.50870783
4.40911472
4.3130613
4.22038447
4.13093021
4.04455298
3.9611152
3.88048674
3.80254442
3.72717164
3.65425791

komp
acetone
water
p

1
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
0

16.6513

2940.46

-35.93

18.3036

3816.44

-46.13

329.4
373.2

760

1
0.9
0.8
0.7
0.6
0.5

Series1

0.4
0.3
0.2
0.1
0
0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

Series1