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02
Unit 1 (2720)
Serial # 112
Summary Report
Experiment 1: TPR Ce Zr Support Tarun
Analysis Type: Temperature Programmed Reduction
Calibration: (CHM_0005) sushil new caliberation file
Measured Flow Rate: 30.00 mL STP/min
Signal Offset: -0.58381
Signal Inverted: No
Temperature
Volume
at Maximum (mL/g STP)
(C)
Peak
Number
1
2
3
4
360.7
519.1
626.7
640.0
0.55870
1.34454
0.00601
0.00277
Peak Height
0.03254
0.05457
0.00221
0.00152
Page 1
Unit 1 (2720)
Serial # 112
Tabular Report
Experiment 1: TPR Ce Zr Support Tarun
Sampling Interval: 1.0 s
Analysis Type: Temperature Programmed Reduction
Time
(minutes)
0.00
0.02
0.03
0.05
0.07
0.08
0.10
0.12
0.13
0.15
0.17
0.18
0.20
0.22
0.23
0.25
0.27
0.28
0.30
0.32
0.33
0.35
0.37
0.38
0.40
0.42
0.43
0.45
0.47
0.48
0.50
0.52
0.53
0.55
0.57
0.58
0.60
0.62
0.63
0.65
0.67
0.68
0.70
0.72
0.73
0.75
0.77
0.78
Temperature
(C)
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.8
31.7
31.7
31.7
31.8
31.8
31.8
31.8
31.8
31.8
31.9
31.9
31.9
31.8
31.9
31.9
32.0
32.0
32.0
32.1
32.1
32.2
32.2
32.2
32.2
32.3
TCD Signal
0.00000
-0.00003
-0.00001
-0.00002
-0.00003
-0.00002
-0.00001
0.00000
-0.00003
-0.00002
-0.00001
-0.00001
-0.00001
0.00001
-0.00001
0.00001
-0.00001
-0.00002
-0.00001
0.00001
0.00002
0.00000
-0.00002
-0.00002
-0.00001
0.00001
0.00001
-0.00001
0.00000
0.00002
-0.00001
-0.00001
-0.00001
-0.00004
-0.00004
-0.00002
-0.00002
-0.00003
-0.00001
-0.00002
-0.00002
-0.00002
-0.00002
-0.00002
-0.00001
-0.00004
-0.00002
-0.00002
Furnace
Temp. (C)
33.07
32.95
32.82
32.44
32.39
32.50
32.42
32.45
32.38
32.59
32.65
32.56
32.58
32.61
32.57
32.50
32.58
32.52
32.55
32.62
32.62
32.61
32.66
32.71
32.66
32.71
32.77
32.89
32.87
32.88
32.96
33.01
33.08
33.08
33.13
33.17
33.25
33.39
33.50
33.60
33.71
33.81
33.90
33.94
34.06
34.16
34.31
34.40
Auxiliary 2
Page 2
Unit 1 (2720)
Serial # 112
Time
(minutes)
0.80
0.82
0.83
0.85
0.87
0.88
0.90
0.92
0.93
0.95
0.97
0.98
1.00
1.02
1.03
1.05
1.07
1.08
1.10
1.12
1.13
1.15
1.17
1.18
1.20
1.22
1.23
1.25
1.27
1.28
1.30
1.32
1.33
1.35
1.37
1.38
1.40
1.42
1.43
1.45
1.47
1.48
1.50
1.52
1.53
1.55
1.57
1.58
1.60
1.62
1.63
1.65
1.67
1.68
Temperature
(C)
32.3
32.4
32.4
32.5
32.6
32.6
32.7
32.7
32.8
32.9
32.9
32.9
33.1
33.1
33.1
33.2
33.3
33.4
33.4
33.5
33.6
33.7
33.8
33.9
34.0
34.0
34.1
34.2
34.3
34.4
34.5
34.5
34.5
34.6
34.6
34.7
34.7
34.8
34.9
35.0
35.1
35.2
35.3
35.4
35.5
35.6
35.7
35.7
35.8
35.9
36.0
36.2
36.3
36.4
TCD Signal
-0.00001
-0.00003
-0.00004
-0.00002
0.00000
-0.00004
-0.00002
-0.00002
-0.00001
-0.00001
-0.00004
-0.00002
-0.00003
-0.00004
-0.00002
-0.00005
-0.00002
-0.00003
-0.00004
-0.00005
-0.00006
-0.00004
-0.00004
-0.00005
-0.00004
-0.00003
-0.00005
-0.00003
-0.00004
-0.00005
-0.00004
-0.00004
-0.00008
-0.00007
-0.00007
-0.00009
-0.00009
-0.00004
-0.00008
-0.00008
-0.00007
-0.00007
-0.00008
-0.00009
-0.00009
-0.00006
-0.00007
-0.00008
-0.00011
-0.00009
-0.00010
-0.00009
-0.00011
-0.00012
Furnace
Temp. (C)
34.47
34.66
34.86
35.04
35.17
35.39
35.57
35.70
35.93
36.09
36.29
36.43
36.63
36.63
36.95
37.20
37.44
37.71
38.09
38.26
38.48
38.74
39.00
39.11
39.38
39.70
39.85
40.02
40.32
40.61
40.78
40.67
40.92
41.11
41.21
41.42
42.06
42.23
42.53
42.73
43.06
43.32
43.50
43.79
43.89
44.01
44.21
44.48
44.75
44.99
45.24
45.61
45.87
46.13
Auxiliary 2
Page 3
Unit 1 (2720)
Serial # 112
Time
(minutes)
1.70
1.72
1.73
1.75
1.77
1.78
1.80
1.82
1.83
1.85
1.87
1.88
1.90
1.92
1.93
1.95
1.97
1.98
2.00
2.02
2.03
2.05
2.07
2.08
2.10
2.12
2.13
2.15
2.17
2.18
2.20
2.22
2.23
2.25
2.27
2.28
2.30
2.32
2.33
2.35
2.37
2.38
2.40
2.42
2.43
2.45
2.47
2.48
2.50
2.52
2.53
2.55
2.57
2.58
Temperature
(C)
36.5
36.5
36.6
36.8
36.9
37.0
37.1
37.1
37.2
37.2
37.3
37.5
37.6
37.7
37.9
37.9
38.1
38.2
38.3
38.5
38.6
38.7
38.8
38.9
39.1
39.1
39.3
39.4
39.5
39.6
39.7
39.7
39.8
39.8
40.0
40.1
40.2
40.3
40.4
40.6
40.7
40.9
40.9
41.0
41.2
41.2
41.4
41.5
41.6
41.7
41.8
41.9
42.0
42.1
TCD Signal
-0.00009
-0.00013
-0.00011
-0.00011
-0.00012
-0.00013
-0.00014
-0.00013
-0.00013
-0.00016
-0.00015
-0.00015
-0.00015
-0.00016
-0.00017
-0.00017
-0.00016
-0.00017
-0.00016
-0.00018
-0.00019
-0.00016
-0.00017
-0.00021
-0.00019
-0.00018
-0.00020
-0.00018
-0.00018
-0.00020
-0.00021
-0.00020
-0.00019
-0.00020
-0.00021
-0.00022
-0.00021
-0.00020
-0.00021
-0.00020
-0.00022
-0.00021
-0.00023
-0.00023
-0.00023
-0.00024
-0.00023
-0.00021
-0.00023
-0.00021
-0.00022
-0.00023
-0.00021
-0.00022
Furnace
Temp. (C)
46.38
46.54
46.66
46.69
46.97
47.17
47.35
47.57
47.60
48.10
48.21
48.43
48.70
48.79
49.09
48.99
49.23
49.63
49.64
49.93
50.27
50.48
50.54
50.74
50.93
51.03
50.99
51.35
51.36
51.64
51.75
51.85
52.00
52.13
52.22
52.13
52.38
52.60
52.64
52.87
53.05
53.20
53.28
53.41
53.56
53.58
53.92
54.03
54.16
54.20
54.41
54.59
54.72
54.79
Auxiliary 2
Page 4
Unit 1 (2720)
Serial # 112
Time
(minutes)
2.60
2.62
2.63
2.65
2.67
2.68
2.70
2.72
2.73
2.75
2.77
2.78
2.80
2.82
2.83
2.85
2.87
2.88
2.90
2.92
2.93
2.95
2.97
2.98
3.00
3.02
3.03
3.05
3.07
3.08
3.10
3.12
3.13
3.15
3.17
3.18
3.20
3.22
3.23
3.25
3.27
3.28
3.30
3.32
3.33
3.35
3.37
3.38
3.40
3.42
3.43
3.45
3.47
3.48
Temperature
(C)
42.3
42.4
42.4
42.5
42.6
42.7
42.7
42.9
42.9
43.0
43.1
43.2
43.2
43.4
43.5
43.6
43.7
43.9
44.0
44.2
44.3
44.4
44.5
44.7
44.8
44.9
45.0
45.2
45.3
45.4
45.6
45.7
45.8
45.9
46.1
46.2
46.4
46.5
46.6
46.7
46.8
47.0
47.1
47.2
47.3
47.5
47.5
47.6
47.6
47.6
47.6
47.7
47.8
48.0
TCD Signal
-0.00021
-0.00022
-0.00023
-0.00023
-0.00023
-0.00021
-0.00025
-0.00025
-0.00021
-0.00023
-0.00025
-0.00020
-0.00021
-0.00023
-0.00021
-0.00025
-0.00023
-0.00022
-0.00020
-0.00021
-0.00021
-0.00023
-0.00022
-0.00018
-0.00020
-0.00022
-0.00021
-0.00021
-0.00021
-0.00018
-0.00020
-0.00020
-0.00017
-0.00020
-0.00021
-0.00022
-0.00019
-0.00020
-0.00020
-0.00019
-0.00021
-0.00021
-0.00022
-0.00020
-0.00020
-0.00019
-0.00020
-0.00021
-0.00019
-0.00020
-0.00020
-0.00018
-0.00016
-0.00018
Furnace
Temp. (C)
54.98
54.95
55.17
55.22
55.10
55.33
55.32
55.60
55.66
55.83
55.89
55.96
56.07
56.23
56.38
56.60
56.73
56.92
56.96
57.10
57.33
57.36
57.54
57.86
58.03
58.21
58.39
58.65
58.76
58.97
59.14
59.34
59.52
59.65
59.87
60.10
60.31
60.49
60.66
60.75
60.86
60.85
61.12
61.28
61.46
61.64
61.88
62.02
62.13
62.14
62.23
62.36
62.51
62.84
Auxiliary 2
Page 5
Unit 1 (2720)
Serial # 112
Time
(minutes)
3.50
3.52
3.53
3.55
3.57
3.58
3.60
3.62
3.63
3.65
3.67
3.68
3.70
3.72
3.73
3.75
3.77
3.78
3.80
3.82
3.83
3.85
3.87
3.88
3.90
3.92
3.93
3.95
3.97
3.98
4.00
4.02
4.03
4.05
4.07
4.08
4.10
4.12
4.13
4.15
4.17
4.18
4.20
4.22
4.23
4.25
4.27
4.28
4.30
4.32
4.33
4.35
4.37
4.38
Temperature
(C)
48.1
48.3
48.5
48.6
48.8
49.0
49.1
49.3
49.4
49.6
49.8
49.9
50.0
50.2
50.3
50.5
50.6
50.8
50.9
50.9
50.8
50.9
51.0
51.1
51.3
51.5
51.6
51.8
51.9
52.0
52.1
52.2
52.3
52.4
52.6
52.8
52.9
53.1
53.3
53.4
53.6
53.8
53.9
54.1
54.2
54.4
54.4
54.6
54.6
54.7
54.8
54.9
55.1
55.3
TCD Signal
-0.00019
-0.00016
-0.00018
-0.00015
-0.00015
-0.00016
-0.00015
-0.00016
-0.00016
-0.00016
-0.00015
-0.00015
-0.00015
-0.00015
-0.00017
-0.00016
-0.00016
-0.00017
-0.00017
-0.00015
-0.00016
-0.00018
-0.00019
-0.00019
-0.00016
-0.00017
-0.00017
-0.00016
-0.00015
-0.00016
-0.00016
-0.00018
-0.00018
-0.00015
-0.00014
-0.00016
-0.00014
-0.00015
-0.00017
-0.00015
-0.00015
-0.00016
-0.00015
-0.00013
-0.00016
-0.00014
-0.00015
-0.00012
-0.00013
-0.00014
-0.00012
-0.00012
-0.00014
-0.00013
Furnace
Temp. (C)
63.00
63.26
63.46
63.63
63.87
64.03
64.22
64.42
64.64
64.93
65.21
65.41
65.56
65.81
65.96
66.17
66.37
66.62
66.55
66.49
66.34
66.48
66.61
66.85
67.03
67.26
67.44
67.53
67.85
68.09
68.27
68.41
68.62
68.75
69.00
69.23
69.51
69.70
69.77
69.90
70.12
70.35
70.53
70.50
70.65
70.75
70.84
71.08
71.04
71.16
71.21
71.68
71.93
72.17
Auxiliary 2
Page 6
Unit 1 (2720)
Serial # 112
Time
(minutes)
4.40
4.42
4.43
4.45
4.47
4.48
4.50
4.52
4.53
4.55
4.57
4.58
4.60
4.62
4.63
4.65
4.67
4.68
4.70
4.72
4.73
4.75
4.77
4.78
4.80
4.82
4.83
4.85
4.87
4.88
4.90
4.92
4.93
4.95
4.97
4.98
5.00
5.02
5.03
5.05
5.07
5.08
5.10
5.12
5.13
5.15
5.17
5.18
5.20
5.22
5.23
5.25
5.27
5.28
Temperature
(C)
55.4
55.6
55.8
55.9
56.1
56.3
56.4
56.6
56.8
57.0
57.2
57.4
57.5
57.7
57.9
58.2
58.3
58.5
58.7
58.9
59.1
59.2
59.4
59.5
59.6
59.7
59.8
60.0
60.1
60.3
60.5
60.6
60.8
60.9
61.1
61.3
61.4
61.5
61.7
61.9
62.0
62.2
62.4
62.6
62.6
62.6
62.6
62.6
62.8
63.0
63.1
63.3
63.4
63.6
TCD Signal
-0.00016
-0.00017
-0.00015
-0.00017
-0.00016
-0.00017
-0.00018
-0.00017
-0.00020
-0.00016
-0.00016
-0.00016
-0.00017
-0.00017
-0.00014
-0.00015
-0.00012
-0.00013
-0.00012
-0.00012
-0.00011
-0.00011
-0.00009
-0.00013
-0.00013
-0.00012
-0.00011
-0.00010
-0.00010
-0.00011
-0.00010
-0.00010
-0.00012
-0.00013
-0.00013
-0.00012
-0.00013
-0.00012
-0.00013
-0.00012
-0.00013
-0.00015
-0.00014
-0.00008
-0.00010
-0.00010
-0.00009
-0.00012
-0.00011
-0.00010
-0.00010
-0.00007
-0.00007
-0.00009
Furnace
Temp. (C)
72.37
72.51
72.76
72.97
73.23
73.44
73.63
73.68
73.83
73.92
74.19
74.43
74.71
74.92
75.14
75.56
75.87
76.06
76.22
76.48
76.60
76.54
76.70
76.85
77.05
77.21
77.30
77.62
77.95
78.15
78.27
78.44
78.52
78.65
78.69
78.90
78.99
79.20
79.37
79.61
79.76
80.06
80.19
80.34
80.30
80.21
80.33
80.29
80.46
80.58
80.78
80.76
80.94
81.16
Auxiliary 2
Page 7
Unit 1 (2720)
Serial # 112
Time
(minutes)
5.30
5.32
5.33
5.35
5.37
5.38
5.40
5.42
5.43
5.45
5.47
5.48
5.50
5.52
5.53
5.55
5.57
5.58
5.60
5.62
5.63
5.65
5.67
5.68
5.70
5.72
5.73
5.75
5.77
5.78
5.80
5.82
5.83
5.85
5.87
5.88
5.90
5.92
5.93
5.95
5.97
5.98
6.00
6.02
6.03
6.05
6.07
6.08
6.10
6.12
6.13
6.15
6.17
6.18
Temperature
(C)
63.8
63.9
64.1
64.3
64.4
64.5
64.7
64.8
64.9
65.0
65.1
65.3
65.4
65.6
65.8
65.9
66.1
66.3
66.5
66.7
66.9
67.0
67.2
67.4
67.5
67.6
67.8
67.9
68.1
68.2
68.4
68.5
68.7
68.9
69.1
69.2
69.4
69.6
69.8
70.0
70.2
70.3
70.5
70.7
70.9
71.1
71.2
71.4
71.6
71.7
71.9
72.1
72.2
72.4
TCD Signal
-0.00009
-0.00007
-0.00008
-0.00009
-0.00008
-0.00009
-0.00009
-0.00009
-0.00009
-0.00010
-0.00009
-0.00013
-0.00011
-0.00013
-0.00012
-0.00013
-0.00013
-0.00010
-0.00011
-0.00010
-0.00011
-0.00009
-0.00009
-0.00010
-0.00009
-0.00009
-0.00010
-0.00008
-0.00010
-0.00007
-0.00005
-0.00005
-0.00007
-0.00007
-0.00007
-0.00007
-0.00007
-0.00007
-0.00003
-0.00006
-0.00004
-0.00005
-0.00004
-0.00004
-0.00001
-0.00002
0.00000
-0.00001
0.00001
0.00001
0.00000
0.00001
-0.00001
-0.00001
Furnace
Temp. (C)
81.29
81.50
81.58
81.95
82.03
82.15
82.32
82.41
82.55
82.60
82.74
82.87
83.01
83.22
83.45
83.54
83.78
83.95
84.07
84.30
84.50
84.72
84.92
85.08
85.25
85.42
85.57
85.77
85.99
86.17
86.34
86.53
86.66
86.90
87.03
87.22
87.41
87.62
87.82
88.02
88.22
88.37
88.65
88.82
89.03
89.21
89.38
89.57
89.74
89.87
90.05
90.23
90.46
90.65
Auxiliary 2
Page 8
Unit 1 (2720)
Serial # 112
Time
(minutes)
6.20
6.22
6.23
6.25
6.27
6.28
6.30
6.32
6.33
6.35
6.37
6.38
6.40
6.42
6.43
6.45
6.47
6.48
6.50
6.52
6.53
6.55
6.57
6.58
6.60
6.62
6.63
6.65
6.67
6.68
6.70
6.72
6.73
6.75
6.77
6.78
6.80
6.82
6.83
6.85
6.87
6.88
6.90
6.92
6.93
6.95
6.97
6.98
7.00
7.02
7.03
7.05
7.07
7.08
Temperature
(C)
72.6
72.8
73.0
73.2
73.3
73.5
73.7
73.9
74.1
74.2
74.5
74.6
74.7
74.8
75.0
75.2
75.4
75.5
75.7
75.9
76.1
76.2
76.4
76.6
76.8
76.9
77.1
77.2
77.4
77.6
77.8
77.9
78.0
78.2
78.4
78.5
78.6
78.7
78.9
79.1
79.2
79.4
79.6
79.8
79.9
80.1
80.3
80.4
80.6
80.8
81.0
81.1
81.3
81.5
TCD Signal
0.00000
0.00001
0.00001
-0.00001
0.00000
0.00001
-0.00001
0.00003
0.00002
0.00003
0.00002
0.00002
0.00002
0.00001
0.00001
0.00001
0.00002
0.00001
0.00002
0.00004
0.00004
0.00003
0.00005
0.00004
0.00005
0.00005
0.00005
0.00005
0.00004
0.00004
0.00007
0.00005
0.00003
0.00005
0.00005
0.00005
0.00002
0.00003
0.00004
0.00003
0.00005
0.00003
0.00004
0.00004
0.00004
0.00005
0.00005
0.00004
0.00005
0.00007
0.00007
0.00004
0.00005
0.00005
Furnace
Temp. (C)
90.77
90.95
91.12
91.28
91.46
91.67
91.97
92.16
92.36
92.51
92.75
92.82
93.03
93.13
93.26
93.45
93.66
93.81
93.96
94.12
94.24
94.41
94.54
94.77
94.99
95.18
95.37
95.57
95.68
95.84
95.99
96.11
96.30
96.43
96.58
96.60
96.73
96.79
96.97
97.12
97.33
97.47
97.63
97.82
97.98
98.19
98.32
98.49
98.67
98.83
99.01
99.13
99.30
99.43
Auxiliary 2
Page 9
Unit 1 (2720)
Serial # 112
Time
(minutes)
7.10
7.12
7.13
7.15
7.17
7.18
7.20
7.22
7.23
7.25
7.27
7.28
7.30
7.32
7.33
7.35
7.37
7.38
7.40
7.42
7.43
7.45
7.47
7.48
7.50
7.52
7.53
7.55
7.57
7.58
7.60
7.62
7.63
7.65
7.67
7.68
7.70
7.72
7.73
7.75
7.77
7.78
7.80
7.82
7.83
7.85
7.87
7.88
7.90
7.92
7.93
7.95
7.97
7.98
Temperature
(C)
81.6
81.8
81.9
82.1
82.3
82.4
82.6
82.7
82.9
83.1
83.2
83.5
83.6
83.8
83.9
84.1
84.2
84.4
84.5
84.7
84.9
85.0
85.2
85.4
85.6
85.7
85.8
86.0
86.0
86.2
86.2
86.3
86.5
86.7
86.8
87.0
87.3
87.4
87.6
87.7
87.9
88.1
88.3
88.5
88.7
88.9
89.0
89.2
89.4
89.6
89.9
90.0
90.2
90.4
TCD Signal
0.00002
0.00002
0.00002
0.00002
0.00002
0.00002
0.00003
0.00005
0.00007
0.00006
0.00005
0.00007
0.00009
0.00009
0.00008
0.00005
0.00009
0.00007
0.00007
0.00006
0.00007
0.00005
0.00006
0.00005
0.00006
0.00007
0.00005
0.00007
0.00008
0.00008
0.00009
0.00010
0.00011
0.00013
0.00011
0.00013
0.00013
0.00012
0.00014
0.00012
0.00012
0.00011
0.00010
0.00010
0.00011
0.00011
0.00012
0.00013
0.00012
0.00013
0.00015
0.00012
0.00012
0.00015
Furnace
Temp. (C)
99.54
99.65
99.93
100.01
100.18
100.33
100.44
100.68
100.84
100.94
101.07
101.28
101.46
101.60
101.76
102.00
102.14
102.26
102.40
102.60
102.70
102.90
103.00
103.16
103.38
103.39
103.61
103.76
103.83
104.05
104.15
104.24
104.41
104.61
104.80
105.05
105.18
105.31
105.45
105.60
105.75
105.88
106.14
106.33
106.51
106.70
106.90
107.06
107.37
107.55
107.75
107.94
108.14
108.33
Auxiliary 2
Page 10
Unit 1 (2720)
Serial # 112
Time
(minutes)
8.00
8.02
8.03
8.05
8.07
8.08
8.10
8.12
8.13
8.15
8.17
8.18
8.20
8.22
8.23
8.25
8.27
8.28
8.30
8.32
Temperature
(C)
90.5
90.7
90.9
91.1
91.3
91.4
91.6
91.8
92.0
92.2
92.4
92.6
92.8
92.9
93.1
93.3
93.5
93.6
93.8
94.0
TCD Signal
0.00015
0.00016
0.00016
0.00017
0.00018
0.00018
0.00016
0.00018
0.00019
0.00017
0.00020
0.00020
0.00017
0.00018
0.00019
0.00020
0.00019
0.00020
0.00019
0.00020
Furnace
Temp. (C)
108.44
108.67
108.82
109.06
108.94
109.21
109.39
109.62
109.91
110.08
110.32
110.52
110.83
110.99
111.22
111.40
111.15
111.71
111.83
111.96
The table has been truncated to 500 entries. Consider using a larger sampling interval.
Auxiliary 2
Page 11
Unit 1 (2720)
Serial # 112
Page 12
0.05
0.04
0.03
0.02
0.01
0.00
50
100
150
200
250
300
350
400
Temperature (C)
450
500
550
600
650
700
Unit 1 (2720)
Serial # 112
Page 13